CN108339296A - 一种自分散性有机硅消泡剂制备方法及相应的自分散性有机硅消泡剂 - Google Patents
一种自分散性有机硅消泡剂制备方法及相应的自分散性有机硅消泡剂 Download PDFInfo
- Publication number
- CN108339296A CN108339296A CN201810125818.4A CN201810125818A CN108339296A CN 108339296 A CN108339296 A CN 108339296A CN 201810125818 A CN201810125818 A CN 201810125818A CN 108339296 A CN108339296 A CN 108339296A
- Authority
- CN
- China
- Prior art keywords
- organic silicon
- self
- silicon defoamer
- preparation
- dispersing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 31
- 239000010703 silicon Substances 0.000 title claims abstract description 31
- 239000013530 defoamer Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- -1 dimethyl siloxane Chemical class 0.000 claims abstract description 18
- 229920002545 silicone oil Polymers 0.000 claims abstract description 13
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims abstract description 12
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 12
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 11
- 229920000570 polyether Polymers 0.000 claims abstract description 11
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims abstract description 11
- 229920001577 copolymer Polymers 0.000 claims abstract description 10
- JHUFGBSGINLPOW-UHFFFAOYSA-N 3-chloro-4-(trifluoromethoxy)benzoyl cyanide Chemical compound FC(F)(F)OC1=CC=C(C(=O)C#N)C=C1Cl JHUFGBSGINLPOW-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000126 substance Substances 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 2
- 239000002518 antifoaming agent Substances 0.000 abstract description 15
- 230000000694 effects Effects 0.000 abstract description 9
- 239000006210 lotion Substances 0.000 abstract description 6
- 239000000839 emulsion Substances 0.000 abstract description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 239000004215 Carbon black (E152) Substances 0.000 description 5
- 229930195733 hydrocarbon Natural products 0.000 description 5
- 150000002430 hydrocarbons Chemical class 0.000 description 5
- 229910052782 aluminium Inorganic materials 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000003995 emulsifying agent Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 239000004411 aluminium Substances 0.000 description 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 3
- 238000007334 copolymerization reaction Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 description 2
- 238000004945 emulsification Methods 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 125000000963 oxybis(methylene) group Chemical group [H]C([H])(*)OC([H])([H])* 0.000 description 2
- JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 description 2
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 1
- RKJPSNVUYDHRAL-UHFFFAOYSA-M P.[Br-].C(C1=CC=CC=C1)[P+](C1=CC=CC=C1)(C1=CC=CC=C1)C1=CC=CC=C1 Chemical compound P.[Br-].C(C1=CC=CC=C1)[P+](C1=CC=CC=C1)(C1=CC=CC=C1)C1=CC=CC=C1 RKJPSNVUYDHRAL-UHFFFAOYSA-M 0.000 description 1
- LRCPOJGBEQAERD-UHFFFAOYSA-M [P].[Br-].C(CCC)[P+](CCCC)(CCCC)CCCC Chemical compound [P].[Br-].C(CCC)[P+](CCCC)(CCCC)CCCC LRCPOJGBEQAERD-UHFFFAOYSA-M 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 1
- 235000013539 calcium stearate Nutrition 0.000 description 1
- 239000008116 calcium stearate Substances 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229940008099 dimethicone Drugs 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 1
- 125000005702 oxyalkylene group Chemical group 0.000 description 1
- 229920000233 poly(alkylene oxides) Polymers 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000056 polyoxyethylene ether Polymers 0.000 description 1
- 229940051841 polyoxyethylene ether Drugs 0.000 description 1
- ASUAYTHWZCLXAN-UHFFFAOYSA-N prenol Chemical compound CC(C)=CCO ASUAYTHWZCLXAN-UHFFFAOYSA-N 0.000 description 1
- UIIIBRHUICCMAI-UHFFFAOYSA-N prop-2-ene-1-sulfonic acid Chemical compound OS(=O)(=O)CC=C UIIIBRHUICCMAI-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- BWYYYTVSBPRQCN-UHFFFAOYSA-M sodium;ethenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C=C BWYYYTVSBPRQCN-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/02—Foam dispersion or prevention
- B01D19/04—Foam dispersion or prevention by addition of chemical substances
- B01D19/0404—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance
- B01D19/0409—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance compounds containing Si-atoms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/02—Foam dispersion or prevention
- B01D19/04—Foam dispersion or prevention by addition of chemical substances
- B01D19/0404—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance
- B01D19/0422—Foam dispersion or prevention by addition of chemical substances characterised by the nature of the chemical substance compounds containing S-atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Degasification And Air Bubble Elimination (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201810125818.4A CN108339296B (zh) | 2018-02-07 | 2018-02-07 | 一种自分散性有机硅消泡剂制备方法及相应的自分散性有机硅消泡剂 |
Applications Claiming Priority (1)
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CN201810125818.4A CN108339296B (zh) | 2018-02-07 | 2018-02-07 | 一种自分散性有机硅消泡剂制备方法及相应的自分散性有机硅消泡剂 |
Publications (2)
Publication Number | Publication Date |
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CN108339296A true CN108339296A (zh) | 2018-07-31 |
CN108339296B CN108339296B (zh) | 2021-02-05 |
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Family Applications (1)
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CN201810125818.4A Active CN108339296B (zh) | 2018-02-07 | 2018-02-07 | 一种自分散性有机硅消泡剂制备方法及相应的自分散性有机硅消泡剂 |
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CN (1) | CN108339296B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112048607A (zh) * | 2020-09-03 | 2020-12-08 | 山东大众机械制造股份有限公司 | 一种阀体热处理工艺 |
CN113730964A (zh) * | 2021-09-14 | 2021-12-03 | 浙江传化华洋化工有限公司 | 消泡剂及其制备方法和应用 |
CN115142298A (zh) * | 2022-07-13 | 2022-10-04 | 慈溪基中纸业有限公司 | 一种包装纸生产工艺 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101003946A (zh) * | 2006-12-25 | 2007-07-25 | 山东东岳高分子材料有限公司 | 氟硅改性聚氨酯防水防油处理剂及其制备方法 |
CN102343165A (zh) * | 2011-10-20 | 2012-02-08 | 山东大易化工有限公司 | 一种高效有机硅消泡剂 |
CN103819630A (zh) * | 2014-03-05 | 2014-05-28 | 威尔(福建)生物有限公司 | 一种聚醚改性有机硅消泡剂及其制备方法和用途 |
CN104707365A (zh) * | 2013-12-11 | 2015-06-17 | 江南大学 | 一种制备氨基聚醚有机硅复配型消泡剂的方法 |
CN106731034A (zh) * | 2016-12-22 | 2017-05-31 | 新疆水处理工程技术研究中心有限公司 | 一种复合型消泡剂 |
-
2018
- 2018-02-07 CN CN201810125818.4A patent/CN108339296B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101003946A (zh) * | 2006-12-25 | 2007-07-25 | 山东东岳高分子材料有限公司 | 氟硅改性聚氨酯防水防油处理剂及其制备方法 |
CN102343165A (zh) * | 2011-10-20 | 2012-02-08 | 山东大易化工有限公司 | 一种高效有机硅消泡剂 |
CN104707365A (zh) * | 2013-12-11 | 2015-06-17 | 江南大学 | 一种制备氨基聚醚有机硅复配型消泡剂的方法 |
CN103819630A (zh) * | 2014-03-05 | 2014-05-28 | 威尔(福建)生物有限公司 | 一种聚醚改性有机硅消泡剂及其制备方法和用途 |
CN106731034A (zh) * | 2016-12-22 | 2017-05-31 | 新疆水处理工程技术研究中心有限公司 | 一种复合型消泡剂 |
Non-Patent Citations (1)
Title |
---|
商春燕: "聚醚接枝硅油的合成研究及交联物对其性能的影响", 《中国优秀硕士学位论文全文数据库工程科技Ⅰ辑》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112048607A (zh) * | 2020-09-03 | 2020-12-08 | 山东大众机械制造股份有限公司 | 一种阀体热处理工艺 |
CN113730964A (zh) * | 2021-09-14 | 2021-12-03 | 浙江传化华洋化工有限公司 | 消泡剂及其制备方法和应用 |
CN113730964B (zh) * | 2021-09-14 | 2023-01-10 | 浙江传化华洋化工有限公司 | 消泡剂及其制备方法和应用 |
CN115142298A (zh) * | 2022-07-13 | 2022-10-04 | 慈溪基中纸业有限公司 | 一种包装纸生产工艺 |
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CN108339296B (zh) | 2021-02-05 |
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Address after: 510000 Room 202, 560 Changgengxi Street, Jitang, Huangpu District, Guangzhou City, Guangdong Province Applicant after: GUANGZHOU CAIRUN NEW MATERIALS Co.,Ltd. Address before: 510000 Room 202, 560 Changgengxi Street, Jitang, Huangpu District, Guangzhou City, Guangdong Province Applicant before: GUANGZHOU CAIRUN CHEMICAL Co.,Ltd. |
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TR01 | Transfer of patent right |
Effective date of registration: 20240218 Address after: 510000 Building C, No. 5, Gongye 1st Road, Shangshao Industrial Zone, Xintang Town, Zengcheng District, Guangzhou, Guangdong Patentee after: Guangzhou Shengju Paint Co.,Ltd. Country or region after: China Address before: 510000 Room 202, 560 Changgengxi Street, Jitang, Huangpu District, Guangzhou City, Guangdong Province Patentee before: GUANGZHOU CAIRUN NEW MATERIALS Co.,Ltd. Country or region before: China |