CN108275652A - A kind of syngas for synthetic ammonia fine de-sulfur purifier - Google Patents
A kind of syngas for synthetic ammonia fine de-sulfur purifier Download PDFInfo
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- CN108275652A CN108275652A CN201810079162.7A CN201810079162A CN108275652A CN 108275652 A CN108275652 A CN 108275652A CN 201810079162 A CN201810079162 A CN 201810079162A CN 108275652 A CN108275652 A CN 108275652A
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- tank body
- separator tank
- water
- solenoid valve
- syngas
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Gas Separation By Absorption (AREA)
Abstract
Syngas for synthetic ammonia fine de-sulfur purifier, including rinsing separation device main body, recirculated water water inlet system and recirculated water outlet system, separator tank body lower part is provided with gas feed, separator tank body lower part is provided with water level monitor device, separator tank body top is provided with wire mesh demister, separator tank body top is provided with gas vent, water washing spray head is arranged in silk stocking demister lower end, it is arranged in separator tank interior, recirculated water outlet system is arranged in separator tank body bottom end, support leg is welded on separator tank body bottom outer surface, structure of the invention is reasonable, it is easy to operate, the dust in unstripped gas can effectively be removed, greatly increase the service life of compressor.
Description
Technical field
The present invention relates to process gas processing technology field, more particularly to a kind of syngas for synthetic ammonia fine de-sulfur purifier.
Background technology
Ammonia is important one of inorganic chemical product, and ammonia synthesizing industry occupies an important position in national economy, removes liquid
Ammonia can be directly as fertilizer outside, the nitrogenous fertilizer and various nitrogenous composite fertilizers that agriculturally use are the synthesis using ammonia as raw material
Ammonia is one of large chemical products, plays the part of very important role in the industrial production, improves and safeguards that the production of synthesis ammonia is set
It is standby also to have far-reaching significance.
General chemical enterprise has an ammonia synthesis unit mostly, syngas for synthetic ammonia after pressure swing adsorption decarbonization, need by
To remove the sulfide in unstripped gas completely, the desulfurizing agent because using after desulfurization, contains fine de-sulfur for activated carbon in unstripped gas
There is a large amount of dust, after unstripped gas is using compressor, because containing dust, to cause compresser cylinder to wear, part dust meeting
It is attached on air valve, greatly reduces the service life of compresser cylinder and air valve, increase operation and maintenance cost.
Invention content
In view of the above-mentioned problems, having carried out Improvement, it is de- that the purpose of the present invention is to provide a kind of syngas for synthetic ammonia essences
Sulphur purifier.
The technical solution adopted in the present invention is as follows：
A kind of syngas for synthetic ammonia fine de-sulfur purifier, including rinsing separation device main body, recirculated water water inlet system with
And recirculated water outlet system；Wherein rinsing separation device main body includes：Separator tank body, support leg；Under the separator tank body
Portion is provided with gas feed；The separator tank body lower part is provided with water level monitor device；Separator tank body top is arranged
There is wire mesh demister；Separator tank body top is provided with gas vent；The recirculated water water inlet system includes：Water washing spray
Head, circulating water inlet, entering water electromagnetic valve, unstripped gas blowing pipe, blowing pipe solenoid valve；The water washing spray head setting is removed in silk stocking
Foam device lower end is arranged in separator tank interior；The recirculated water outlet system includes：Circulating water outlet pipe, outlet pipe electromagnetism
Valve, unstripped gas anti-blowpipe, anti-blowpipe solenoid valve；The recirculated water outlet system is arranged in separator tank body bottom end；The support
Foot is welded on separator tank body bottom outer surface.
It is further improved as said program：The water washing spray head is connect with circulating water inlet.
It is further improved as said program：The entering water electromagnetic valve is connect with circulating water inlet, control loop water inlet
Pipe.
It is further improved as said program：Unstripped gas blowing pipe setting water washing spray head and entering water electromagnetic valve it
Between, it is external to be located at separator pot.
It is further improved as said program：The unstripped gas blowing pipe other end connects blowing pipe solenoid valve.
It is further improved as said program：Circulating water outlet pipe one end connection separator tank body bottom end, the other end
It is provided with outlet pipe solenoid valve.
It is further improved as said program：The unstripped gas anti-blowpipe connects circulating water outlet pipe, is arranged in separator
Between tank body and outlet pipe solenoid valve, the unstripped gas anti-blowpipe other end is provided with anti-blowpipe solenoid valve.
It is further improved as said program：Water level monitor device, water inlet pipe solenoid valve, blowing pipe solenoid valve, outlet pipe
Solenoid valve and anti-blowpipe solenoid valve are controlled by external computer.
Compared with the technology of the existing same industry, usefulness of the present invention is：The configuration of the present invention is simple is easily installed behaviour
Make, the dust of unstripped gas in ammonia production process is washed by cleaning dust device, removes the dust contained in unstripped gas, significantly
Improve compresser cylinder and air valve service life, at the same unstripped gas washed by recirculated water after temperature decrease, compressor
The amount of inflating also is increased and is also improved the utilization rate of raw material, has saved cost, improves the economic benefit of enterprise.
Description of the drawings
Attached drawing is used for providing further understanding technical solution of the present invention, and a part for constitution instruction, with this
The embodiment of application technical solution for explaining the present invention together, does not constitute the limitation to technical solution of the present invention.
Fig. 1 is a kind of syngas for synthetic ammonia fine de-sulfur purifier structural schematic diagram provided by the invention.
Wherein, 1, separator tank body；2, gas feed；3, gas feed；4, wire mesh demister；5, water washing spray head；6, it follows
Ring water water inlet pipe；7, water inlet pipe solenoid valve；8, unstripped gas blowing pipe；9, blowing pipe solenoid valve；10, circulating water outlet pipe；11, go out
Water solenoid valve；12, unstripped gas anti-blowpipe；13, anti-blowpipe solenoid valve；14, water level monitor device；15, support leg.
Specific implementation mode
To make the purpose of the present invention, process program and advantage be more clear, below in conjunction with attached drawing to the reality of the present invention
Example is applied to be described in detail.It should be noted that in the absence of conflict, the spy in embodiment and embodiment in the application
Sign mutually can be combined arbitrarily.
As shown in Figure 1, a kind of syngas for synthetic ammonia fine de-sulfur purifier of the embodiment of the present invention, including washing separation dress
Set main body, recirculated water water inlet system and recirculated water outlet system；Wherein rinsing separation device main body includes：Separator tank body 1,
Support leg 15；1 lower part of separator tank body is provided with gas feed 2；1 lower part of separator tank body is provided with monitoring water level
14 devices；1 top of separator tank body is provided with wire mesh demister 4；1 top of separator tank body is provided with gas and goes out
Mouth 3；The recirculated water water inlet system includes：Water washing spray head 5, circulating water inlet 6, entering water electromagnetic valve 7, unstripped gas blowing pipe 8,
Blowing pipe solenoid valve 9；The setting of the water washing spray head 5 is arranged in 4 lower end of silk stocking demister inside separator tank body 1；It is described to follow
Ring water outlet system includes：Circulating water outlet pipe 10, outlet pipe solenoid valve 11, unstripped gas anti-blowpipe 12, anti-blowpipe solenoid valve 13；
The recirculated water outlet system is arranged in 1 bottom end of separator tank body；The support leg 15 is welded on 1 bottom outer of separator tank body
Face.
Water washing spray head 5 is connect with circulating water inlet 6；The entering water electromagnetic valve 7 is connect with circulating water inlet 6, control
Circulation water inlet pipe 6；The unstripped gas blowing pipe 8 is arranged between water washing spray head 5 and entering water electromagnetic valve 7, is located at separator tank body 1
Outside；8 other end of the unstripped gas blowing pipe connection blowing pipe solenoid valve 9；10 one end of the circulating water outlet pipe connects separator
1 bottom end of tank body, the other end are provided with outlet pipe solenoid valve 11；The unstripped gas anti-blowpipe 12 connects circulating water outlet pipe 10, if
It sets between separator tank body 1 and outlet pipe solenoid valve 11,12 other end of unstripped gas anti-blowpipe is provided with anti-blowpipe solenoid valve 13；
Water inlet pipe solenoid valve 7, blowing pipe solenoid valve 9, outlet pipe solenoid valve 11 and anti-blowpipe solenoid valve 13 are controlled by external computer.
The syngas for synthetic ammonia fine de-sulfur purifier is in use, computer control water inlet pipe solenoid valve 7 starts, with cycle
The water washing spray head 5 that water water inlet pipe 6 connects starts to spray water, and the ammonia unstripped gas after fine de-sulfur passes through separator after being come out by fine de-sulfur tower
The gas feed 2 of 1 bottom end of tank body enters in separator tank body 1, a large amount of dust is contained in ammonia unstripped gas, ammonia unstripped gas is from bottom to top
The misty water area sprayed by water washing spray head 5, subsequently into wire mesh demister 4, the foam and water droplet isolated；It is purified
Ammonia unstripped gas is gone out by the gas vent 3 on 1 top of separator tank body, into three sections of imports of compressor；The water of water washing spray head 5 flows to
1 bottom of separator tank body, launch computer outlet pipe solenoid valve 11 make recirculated water return to sedimentation basin precipitation, the water cycle profit after precipitation
With water level monitor device 14 is according on computers automatically according to Liquid level valve aperture；After purification, computer control is blown
Pipe solenoid valve 9 and anti-blowpipe solenoid valve 13 start, and understand the dust stratification on effluent pipe mouth and water washing spray head 5.
Embodiment described above is only the explanation of the present invention, is not imposed any restrictions to the present invention, every according to the present invention
Operation principle still falls within the present invention's to any simple modification, change and equivalence change made by above example structure
In protection domain.
Claims (8)
1. a kind of syngas for synthetic ammonia fine de-sulfur purifier, it include rinsing separation device main body, recirculated water water inlet system with
And recirculated water outlet system；Wherein rinsing separation device main body includes：Separator tank body, support leg；Under the separator tank body
Portion is provided with gas feed；The separator tank body lower part is provided with water level monitor device；Separator tank body top is arranged
There is wire mesh demister；Separator tank body top is provided with gas vent；The recirculated water water inlet system includes：Water washing spray
Head, circulating water inlet, entering water electromagnetic valve, unstripped gas blowing pipe, blowing pipe solenoid valve；The water washing spray head setting is removed in silk stocking
Foam device lower end is arranged in separator tank interior；The recirculated water outlet system includes：Circulating water outlet pipe, outlet pipe electromagnetism
Valve, unstripped gas anti-blowpipe, anti-blowpipe solenoid valve；The recirculated water outlet system is arranged in separator tank body bottom end；The support
Foot is welded on separator tank body bottom outer surface.
2. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Water washing spray head with follow
Ring water water inlet pipe connects.
3. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Entering water electromagnetic valve with
Circulating water inlet connects, control loop water inlet pipe.
4. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Unstripped gas blowing pipe
It is arranged between water washing spray head and entering water electromagnetic valve, it is external is located at separator pot.
5. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Unstripped gas blowing pipe
The other end connects blowing pipe solenoid valve.
6. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Circulating water outlet pipe
One end connects separator tank body bottom end, and the other end is provided with outlet pipe solenoid valve.
7. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Unstripped gas anti-blowpipe
Circulating water outlet pipe is connected, is arranged between separator tank body and outlet pipe solenoid valve, the unstripped gas anti-blowpipe other end is provided with
Anti-blowpipe solenoid valve.
8. a kind of syngas for synthetic ammonia fine de-sulfur purifier according to claim 1, it is characterized in that：Monitoring water level fills
It sets, water inlet pipe solenoid valve, blowing pipe solenoid valve, outlet pipe solenoid valve and anti-blowpipe solenoid valve are controlled by external computer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810079162.7A CN108275652A (en) | 2018-01-26 | 2018-01-26 | A kind of syngas for synthetic ammonia fine de-sulfur purifier |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810079162.7A CN108275652A (en) | 2018-01-26 | 2018-01-26 | A kind of syngas for synthetic ammonia fine de-sulfur purifier |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108275652A true CN108275652A (en) | 2018-07-13 |
Family
ID=62805407
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810079162.7A Pending CN108275652A (en) | 2018-01-26 | 2018-01-26 | A kind of syngas for synthetic ammonia fine de-sulfur purifier |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108275652A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114653311A (en) * | 2022-03-22 | 2022-06-24 | 武汉氢能与燃料电池产业技术研究院有限公司 | Dehydrogenation reactor for liquid organic hydrogen storage material |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000279736A (en) * | 1999-03-29 | 2000-10-10 | Toyo Eng Corp | Device for treating fluid containing urea dust and ammonia and treating method using the same and urea production facility installing the same |
| CN102397733A (en) * | 2010-09-15 | 2012-04-04 | 张步芳 | Whirlwind dedusting and desulphuration device |
| CN204447629U (en) * | 2015-02-11 | 2015-07-08 | 辽宁中维高新技术有限公司 | From clear dry fog case |
| CN105195017A (en) * | 2014-06-30 | 2015-12-30 | 董志峰 | Efficient washing-desulfuration-dust removing process equipment for exhaust gas of marine diesel engine |
| CN106582157A (en) * | 2015-10-16 | 2017-04-26 | 安徽华尔泰化工股份有限公司 | Device for removing dust after synthesis ammonia raw material gas fine desulfurization |
-
2018
- 2018-01-26 CN CN201810079162.7A patent/CN108275652A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000279736A (en) * | 1999-03-29 | 2000-10-10 | Toyo Eng Corp | Device for treating fluid containing urea dust and ammonia and treating method using the same and urea production facility installing the same |
| CN102397733A (en) * | 2010-09-15 | 2012-04-04 | 张步芳 | Whirlwind dedusting and desulphuration device |
| CN105195017A (en) * | 2014-06-30 | 2015-12-30 | 董志峰 | Efficient washing-desulfuration-dust removing process equipment for exhaust gas of marine diesel engine |
| CN204447629U (en) * | 2015-02-11 | 2015-07-08 | 辽宁中维高新技术有限公司 | From clear dry fog case |
| CN106582157A (en) * | 2015-10-16 | 2017-04-26 | 安徽华尔泰化工股份有限公司 | Device for removing dust after synthesis ammonia raw material gas fine desulfurization |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114653311A (en) * | 2022-03-22 | 2022-06-24 | 武汉氢能与燃料电池产业技术研究院有限公司 | Dehydrogenation reactor for liquid organic hydrogen storage material |
| CN114653311B (en) * | 2022-03-22 | 2023-06-09 | 武汉氢能与燃料电池产业技术研究院有限公司 | Dehydrogenation reactor for liquid organic hydrogen storage material |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180713 |