CN108208907A - A kind of atomization reconstituted tobacco processing method and its application - Google Patents
A kind of atomization reconstituted tobacco processing method and its application Download PDFInfo
- Publication number
- CN108208907A CN108208907A CN201810264780.9A CN201810264780A CN108208907A CN 108208907 A CN108208907 A CN 108208907A CN 201810264780 A CN201810264780 A CN 201810264780A CN 108208907 A CN108208907 A CN 108208907A
- Authority
- CN
- China
- Prior art keywords
- atomization
- reconstituted tobacco
- tobacco
- acid
- cigarette
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 119
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 119
- 238000000889 atomisation Methods 0.000 title claims abstract description 60
- 238000003672 processing method Methods 0.000 title claims abstract description 18
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 57
- MDYZKJNTKZIUSK-UHFFFAOYSA-N tyloxapol Chemical compound O=C.C1CO1.CC(C)(C)CC(C)(C)C1=CC=C(O)C=C1 MDYZKJNTKZIUSK-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000002253 acid Substances 0.000 claims abstract description 10
- 238000005554 pickling Methods 0.000 claims abstract description 8
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 50
- 238000002156 mixing Methods 0.000 claims description 27
- 239000004088 foaming agent Substances 0.000 claims description 25
- 239000000835 fiber Substances 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000000853 adhesive Substances 0.000 claims description 18
- 230000001070 adhesive effect Effects 0.000 claims description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 18
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- QAIPRVGONGVQAS-DUXPYHPUSA-N trans-caffeic acid Chemical compound OC(=O)\C=C\C1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-DUXPYHPUSA-N 0.000 claims description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 10
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 8
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical group [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 8
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 7
- 229910052799 carbon Inorganic materials 0.000 claims description 7
- 230000005855 radiation Effects 0.000 claims description 7
- 238000005096 rolling process Methods 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- ACEAELOMUCBPJP-UHFFFAOYSA-N (E)-3,4,5-trihydroxycinnamic acid Natural products OC(=O)C=CC1=CC(O)=C(O)C(O)=C1 ACEAELOMUCBPJP-UHFFFAOYSA-N 0.000 claims description 6
- 235000004883 caffeic acid Nutrition 0.000 claims description 6
- 229940074360 caffeic acid Drugs 0.000 claims description 6
- QAIPRVGONGVQAS-UHFFFAOYSA-N cis-caffeic acid Natural products OC(=O)C=CC1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-UHFFFAOYSA-N 0.000 claims description 6
- 235000015165 citric acid Nutrition 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 claims description 5
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 claims description 5
- 206010013786 Dry skin Diseases 0.000 claims description 5
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 claims description 5
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 5
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 claims description 5
- 235000001368 chlorogenic acid Nutrition 0.000 claims description 5
- 229940074393 chlorogenic acid Drugs 0.000 claims description 5
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 claims description 5
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 5
- 235000013599 spices Nutrition 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims description 4
- 235000021314 Palmitic acid Nutrition 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- HDSBZMRLPLPFLQ-UHFFFAOYSA-N Propylene glycol alginate Chemical compound OC1C(O)C(OC)OC(C(O)=O)C1OC1C(O)C(O)C(C)C(C(=O)OCC(C)O)O1 HDSBZMRLPLPFLQ-UHFFFAOYSA-N 0.000 claims description 4
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical group [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 4
- 229920000591 gum Polymers 0.000 claims description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 4
- QWDJLDTYWNBUKE-UHFFFAOYSA-L magnesium bicarbonate Chemical compound [Mg+2].OC([O-])=O.OC([O-])=O QWDJLDTYWNBUKE-UHFFFAOYSA-L 0.000 claims description 4
- 229910000022 magnesium bicarbonate Inorganic materials 0.000 claims description 4
- 239000002370 magnesium bicarbonate Substances 0.000 claims description 4
- 235000014824 magnesium bicarbonate Nutrition 0.000 claims description 4
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims description 4
- 239000008108 microcrystalline cellulose Substances 0.000 claims description 4
- 229940016286 microcrystalline cellulose Drugs 0.000 claims description 4
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 4
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 4
- 235000010409 propane-1,2-diol alginate Nutrition 0.000 claims description 4
- 239000000770 propane-1,2-diol alginate Substances 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 claims description 3
- 229910000020 calcium bicarbonate Inorganic materials 0.000 claims description 3
- 239000001508 potassium citrate Substances 0.000 claims description 3
- 229960002635 potassium citrate Drugs 0.000 claims description 3
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 3
- 235000011082 potassium citrates Nutrition 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000002699 waste material Substances 0.000 claims description 3
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 2
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- 239000001828 Gelatine Substances 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
- 239000003929 acidic solution Substances 0.000 claims description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- 235000010407 ammonium alginate Nutrition 0.000 claims description 2
- 239000000728 ammonium alginate Substances 0.000 claims description 2
- KPGABFJTMYCRHJ-YZOKENDUSA-N ammonium alginate Chemical compound [NH4+].[NH4+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O KPGABFJTMYCRHJ-YZOKENDUSA-N 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 239000004832 casein glue Substances 0.000 claims description 2
- 238000010790 dilution Methods 0.000 claims description 2
- 239000012895 dilution Substances 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 238000009775 high-speed stirring Methods 0.000 claims description 2
- 239000004310 lactic acid Substances 0.000 claims description 2
- 235000014655 lactic acid Nutrition 0.000 claims description 2
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 claims description 2
- 239000001095 magnesium carbonate Substances 0.000 claims description 2
- 229910000021 magnesium carbonate Inorganic materials 0.000 claims description 2
- 239000001630 malic acid Substances 0.000 claims description 2
- 235000011090 malic acid Nutrition 0.000 claims description 2
- 229940098695 palmitic acid Drugs 0.000 claims description 2
- 235000011007 phosphoric acid Nutrition 0.000 claims description 2
- 229960003975 potassium Drugs 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 2
- 235000010413 sodium alginate Nutrition 0.000 claims description 2
- 239000000661 sodium alginate Substances 0.000 claims description 2
- 229940005550 sodium alginate Drugs 0.000 claims description 2
- 239000001509 sodium citrate Substances 0.000 claims description 2
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 2
- 235000011083 sodium citrates Nutrition 0.000 claims description 2
- 239000011975 tartaric acid Substances 0.000 claims description 2
- 235000002906 tartaric acid Nutrition 0.000 claims description 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 2
- 239000004836 Glue Stick Substances 0.000 claims 1
- 235000011054 acetic acid Nutrition 0.000 claims 1
- 239000003925 fat Substances 0.000 claims 1
- 235000019197 fats Nutrition 0.000 claims 1
- GBCAVSYHPPARHX-UHFFFAOYSA-M n'-cyclohexyl-n-[2-(4-methylmorpholin-4-ium-4-yl)ethyl]methanediimine;4-methylbenzenesulfonate Chemical compound CC1=CC=C(S([O-])(=O)=O)C=C1.C1CCCCC1N=C=NCC[N+]1(C)CCOCC1 GBCAVSYHPPARHX-UHFFFAOYSA-M 0.000 claims 1
- 229960004838 phosphoric acid Drugs 0.000 claims 1
- 235000010408 potassium alginate Nutrition 0.000 claims 1
- 239000000737 potassium alginate Substances 0.000 claims 1
- MZYRDLHIWXQJCQ-YZOKENDUSA-L potassium alginate Chemical compound [K+].[K+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O MZYRDLHIWXQJCQ-YZOKENDUSA-L 0.000 claims 1
- 229940083542 sodium Drugs 0.000 claims 1
- 235000015424 sodium Nutrition 0.000 claims 1
- 230000001953 sensory effect Effects 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 239000002304 perfume Substances 0.000 abstract description 7
- 238000010924 continuous production Methods 0.000 abstract description 2
- 235000007983 food acid Nutrition 0.000 abstract 1
- 235000013373 food additive Nutrition 0.000 abstract 1
- 239000002778 food additive Substances 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 description 10
- 239000003205 fragrance Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 239000003610 charcoal Substances 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
- 239000003595 mist Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 235000006679 Mentha X verticillata Nutrition 0.000 description 2
- 244000246386 Mentha pulegium Species 0.000 description 2
- 235000016257 Mentha pulegium Nutrition 0.000 description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 description 2
- 235000004357 Mentha x piperita Nutrition 0.000 description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 244000299461 Theobroma cacao Species 0.000 description 2
- 235000009470 Theobroma cacao Nutrition 0.000 description 2
- 229960004106 citric acid Drugs 0.000 description 2
- 229940119429 cocoa extract Drugs 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000001050 hortel pimenta Nutrition 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 235000019505 tobacco product Nutrition 0.000 description 2
- 241001474374 Blennius Species 0.000 description 1
- 240000008564 Boehmeria nivea Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 229960000583 acetic acid Drugs 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000004026 adhesive bonding Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000010216 calcium carbonate Nutrition 0.000 description 1
- FYHXNYLLNIKZMR-UHFFFAOYSA-N calcium;carbonic acid Chemical compound [Ca].OC(O)=O FYHXNYLLNIKZMR-UHFFFAOYSA-N 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 235000010980 cellulose Nutrition 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- YPSNMKHPDJVGEX-UHFFFAOYSA-L potassium;sodium;3-carboxy-3-hydroxypentanedioate Chemical compound [Na+].[K+].OC(=O)CC(O)(C([O-])=O)CC([O-])=O YPSNMKHPDJVGEX-UHFFFAOYSA-L 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention provides a kind of atomization reconstituted tobacco processing method and its application, on roll-in method Process ba- sis, in low temperature reconstituted tobacco in process of production, using containing carbonate, the food additives and acid pickling step of bicarbonate radical, it chemically reacts, it is porous in producing bubbles inside, increase internal surface area, the Alevaire of high-content is made to be more evenly distributed, surface adhesion, reconstituted tobacco intensity is good, improve machine cigarette adaptability on atomization reconstituted tobacco, enable the normal cigarette of existing cigarette making and tipping machine, continuous production is good, production efficiency is high, and aspirate atomizing effect improvement, cigarette perfume is enriched, sensory effects are good.
Description
Technical field
The present invention relates to heating not to burn novel tobacco field, and in particular to a kind of atomization reconstituted tobacco processing method and its
Using.
Background technology
Novel tobacco heating tobacco product form of not burning is rich and varied in the world now, such as luxuriant and rich with fragrance iQos not, British-American Tobacco
The Glo of grass, the charcoal heating cigarette Core that RJ Reynolds Tobacco Holdings ,Inc. releases, heating incombustible material is all to use reconstituted tobacco as carrier, only
It is that technology is not quite similar.It is a kind of based on tobacco component to heat the reconstituted tobacco that do not burn, loads large dosage of Alevaire,
Alevaire is discharged by high-temperature heating during use, forms the functional form reconstituted tobacco of haze effect, there is mist in processing technology
Change amount is little, is unevenly distributed, and is easily adhered in processing, easily skids, is difficult to the defects of normal cigarette and deficiency.
Invention content
According to above-mentioned insufficient and defect, the object of the present invention is to provide a kind of atomization reconstituted tobacco processing method and its answer
With on roll-in method Process ba- sis, in low temperature reconstituted tobacco in process of production, using the food containing carbonate or bicarbonate radical
Product additive and acid pickling step, chemically react, porous in producing bubbles inside, increase internal surface area, make the mist of high-content
Agent is more evenly distributed, and surface adhesion, reconstituted tobacco intensity is good, improves machine cigarette adaptability on atomization reconstituted tobacco, makes
The normal cigarette of existing cigarette making and tipping machine energy, continuous production is good, production efficiency is high, and aspirates atomizing effect improvement, and cigarette perfume is enriched,
Sensory effects are good.
The invention is realized by the following technical scheme：
A kind of atomization reconstituted tobacco processing method and its application, specifically comprise the following steps：
(1) raw material prepares：Matter prepares various raw materials by mass percentage：Tobacco material 40~63%, Alevaire 10~
35%th, adhesive 2~10%, essence spice for cigarette 0.1~5%, foaming agent 0.1-5%, fiber 1~5%, water 10~43%,
The one kind or its mixing of the foaming agent for carbonate or in bicarbonate；
(2) dry material co-grinding：Tobacco material, solid adhesive are put into Lowtemperaturepulverizer high speed in proportion to crush
Uniformly, dry material powder is obtained, mesh number is the mesh of 40 mesh~200；
(3) wet stock mixing is uniformly dispersed：The fiber that above-mentioned steps (1) prepare pours into material barrel in proportion with water
In, be stirring evenly and then adding into above-mentioned steps 1) Alevaire, the tobacco aromaticss of quality proportioning, then using microwave radiation technology mixing obtained by
Mixed material, and mixed material is added in the dry material powder that above-mentioned steps (2) obtain, high-speed stirred is uniform together,
Make fiber, Alevaire, adhesive, foaming agent, tobacco aromaticss dispersion evenly；
The foaming agent is added according to the ratio of step (1) in step (2) and/or in step (3)；
(4) roll-in：The mixed material that above-mentioned steps are obtained, then through 1~6 rolling process, obtain thickness 0.15mm-
The atomization reconstituted tobacco of 0.3mm；
(5) pickling：The atomization reconstituted tobacco that above-mentioned steps (4) are obtained impregnates 3~300S in an acidic solution, more excellent
Available pH value impregnated in the acid solution of 3-6, then dry；
(6) it is dry：The atomization reconstituted tobacco that above-mentioned steps (5) are obtained, through 80~150 DEG C of baking oven heat dryings to aqueous
Amount 1~7% obtains the atomization reconstituted tobacco of the present invention.
Further, following methods addition can be used in the foaming agent：
A) foaming agent is milled in step (2) together with tobacco material, solid adhesive or in tobacco material, solid
It adds in and is uniformly mixed after the completion of body adhesive milling, form dry material powder；
B) property foaming agent is first dissolved in water, then by step (3) with fiber and the Alevaire of step 1) quality proportioning, cigarette
It is mixed with fragrance high-speed stirred；Or after pouring into the fiber prepared by step (1), water in material barrel in step (3), uniformly
The foaming agent of step (1) quality proportioning is added in, while is stirred to dissolving or be uniformly dispersed.Foaming agent uses step again after adding in
(3) the obtained mixed material of mode microwave radiation technology mixing, and by mixed material be added to that above-mentioned steps (2) obtain it is dry
In material powders, high-speed stirred is uniform together, makes fiber, Alevaire, foaming agent, tobacco aromaticss dispersion evenly；
C) foaming agent in the way of a) and b) is combined and added, make fiber, Alevaire, adhesive, foaming agent, tobacco aromaticss
It is uniformly dispersed.
Further, the tobacco material is tobacco leaf, offal, tobacco waste one or more therein mix.
Further, the Alevaire for propylene glycol, glycerine one or two therein, food-grade, quality proportioning
It is 1:1~50.
Further, the adhesive is rosin resin, gelatine, casein glue, sodium alginate, ammonium alginate, seaweed
The one or more of mixing therein of sour potassium, CMC, bassora gum, polyethylene oxide, microcrystalline cellulose, propylene glycol alginate.
Further, the tobacco aromaticss for mint flavouring, tobacco extract, cocoa extract, coffee-extract or
The mixing of one or more of other essence spice for cigarette.
Further, the carbonate be calcium carbonate, sodium carbonate, potassium carbonate, the mixing of one or more of magnesium carbonate, institute
Bicarbonate is stated as the mixing of one or more of sodium bicarbonate, magnesium bicarbonate, saleratus, calcium bicarbonate.
Further, the fiber is wood pulp cellulose, ramie pulp fiber or its mixture.
Further, the water prepared in the step (1) is 30~80 DEG C of warm water.
Further, the rate of step (3) the high speed stirring is 100~800r/min.
Further, in the step (3) microwave frequency be 2450MHz, microwave power be 200~1000W, the time 10
~30min.
Further, the acid solution described in the step (5) is by hydrochloric acid, sulfuric acid, lactic acid, tartaric acid, malic acid, vinegar
Acid, citric acid, sodium citrate, potassium citrate, potassium citrate sodium, phosphoric acid, palmitic acid, chlorogenic acid, one kind in caffeic acid or several
Kind dilution dissolving obtains.
A kind of atomization reconstituted tobacco prepared such as the above method, cigarette is processed after chopping or corrugation, in electrical heating or carbon
It is applied in heating low temperature cigarette.Due on roll-in method Process ba- sis, using chemical method, low temperature reconstituted tobacco being made to add in production
It during heated drying, chemically reacts, generation bubble is porous, increases internal surface area, and the Alevaire distribution for making high-content is more equal
Even, surface adhesion improves machine cigarette adaptability on atomization reconstituted tobacco, enables the normal cigarette of existing cigarette making and tipping machine, and
Aspirating atomizing effect improves, and sensory effects are good.
The beneficial effects of the invention are as follows：
(1) atomization reconstituted tobacco is prepared using present invention process method, by the mistake of tobacco material and adhesive co-grinding
Make their mixed distributions uniform in journey, warm water stir and evenly mix and microwave radiation technology under the action of, not only high-content Alevaire, gluing
Agent, tobacco material, fragrance etc. are uniformly distributed, good bonding, and reconstituted tobacco is made to have certain intensity, reduce powder rate, enhancing
Resist processing；
(2) after roll process, atomization reconstituted tobacco is subjected to pickling, then during heated drying steps, reconstituted tobacco is heated
Under the conditions of soda acid chemical reaction generate great amount of carbon dioxide minute bubbles, make reconstituted tobacco internal surface area increase, atomization agent content into
One step improves, and atomizing effect is good, and reconstituted tobacco surface adhesion, flexibility (adaptability) of operation improve, low applied to electrical heating, charcoal heating etc.
In warm rolling cigarette, suction smog is uniform and reaches traditional cigarette suction amount of smoke level；
(3) in addition through under acid, warm water stirring and microwave radiation technology synergistic effect, aroma component is more precipitated and releases in tobacco leaf
It puts, cigarette perfume is enriched full during heated atomization, and consumer is made to generate satisfaction and novel sense.
The simple mild easily realization of present invention process condition, can realize high fog agent being uniformly distributed in reconstituted tobacco, and
Normal volume, which is connected into, heats the cigarette that do not burn, and production efficiency is high, applies, has in electrical heating, charcoal heating novel tobacco product
Good prospects for commercial application.
Specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A kind of atomization reconstituted tobacco processing method, specifically comprises the following steps：
(1) raw material prepares：Tobacco leaf 45%, Alevaire 25.9%, adhesive (bassora gum, polyethylene oxide, microcrystalline cellulose
Element, food-grade, mass ratio 1:0.5:0.8) 2%, 1%, 35 DEG C of essence spice for cigarette 5%, foaming agent 0.1%, wood-fibred temperature
Water 21%, above-mentioned raw materials prepare according to mass percent；
The Alevaire is propylene glycol, glycerine, food-grade, mass ratio 1：18；
The tobacco aromaticss for mint flavouring, tobacco extract, between quality proportioning be 1:0.6；The foaming
Agent is bicarbonate, specially sodium bicarbonate, saleratus, and the two quality proportioning is 1:0.5；
(2) dry material co-grinding：Tobacco material, solid adhesive are put into Lowtemperaturepulverizer high speed in proportion to crush
Uniformly, mesh number is 50 mesh；
(3) wet stock mixing is uniformly dispersed：Above-mentioned steps 1) described in fiber and warm water pour into material barrel in proportion,
150r/min stir while, add in above-mentioned steps 1) quality proportioning Alevaire, tobacco aromaticss and foaming agent, it is auxiliary using microwave
(microwave frequency 2450MHz, microwave power 300W, 30min) is helped to make obtained mixing thing liquid uniform, and by the mixture
Liquid is slowly added into above-mentioned steps 2) in the dry material powder, 150r/min is stirred evenly together, makes fiber, Alevaire, cigarette
With dispersions such as fragrance evenly；
(4) roll-in：By above-mentioned steps 4) dried mixed material, then through 1~6 rolling process, obtain thickness 0.2mm
Atomization reconstituted tobacco；
(5) pickling：By above-mentioned steps 4) obtained atomization reconstituted tobacco, it is impregnated in certain density organic acid soln
60S, taking-up drain；
The organic acid is citric acid, palmitic acid, food-grade, and quality proportioning between any two is 1:0.8, described has
Aqueous solution of the machine acid solution for organic acid, pH value 3；
(6) it is dry：By above-mentioned steps 5) the atomization reconstituted tobacco of drying, through 80 DEG C of baking oven heat dryings to water content 5%,
Obtain the atomization reconstituted tobacco of the present invention.
A kind of atomization reconstituted tobacco prepared such as the above method, inside have bubble porous, increase internal surface area, contain height
The Alevaire of amount is more evenly distributed, and surface adhesion, reconstituted tobacco intensity is good, improves machine cigarette on atomization reconstituted tobacco and adapts to
Property, enable the normal cigarette of existing cigarette making and tipping machine, processed through cigarette, applied in electrical heating or carbon heating low temperature cigarette, aspirate mist
Change effect improved, amount of smoke is big and uniformly release, cigarette perfume are enriched, and has peppermint refrigerant sense, sensory effects are good.
Embodiment 2
A kind of atomization reconstituted tobacco processing method, specifically comprises the following steps：
(1) raw material prepares：Tobacco material 58.5%, Alevaire 15%, adhesive 5%, foaming agent 2.5%, flavouring essence for tobacco
Fragrance 2%, 2%, 40 DEG C of warm water 15% of flaxen fiber, above-mentioned raw materials prepare according to mass percent；
The tobacco material is the mixing of tobacco leaf, offal, and it is 10 to match:1；
The Alevaire is the mixing of propylene glycol, glycerine, and food-grade, it is 1 to match:10；
Mixing of the adhesive for bassora gum, polyethylene oxide, propylene glycol alginate, quality proportioning 1:0.6:
1.2；
The tobacco aromaticss include tobacco extract, cocoa extract, between quality proportioning be 1：0.5；Described
Organic acid include citric acid, chlorogenic acid, caffeic acid, between quality proportioning be 1:0.8；1.5；The foaming agent includes carbonic acid
Calcium, calcium bicarbonate, quality proportioning 1:0.3；；
(2) dry material co-grinding：Tobacco material, solid adhesive, foaming agent are put into Lowtemperaturepulverizer in proportion
It crushes at a high speed uniformly, mesh number is 110 mesh；
(3) wet stock mixing is uniformly dispersed：Above-mentioned steps 1) described in fiber and warm water pour into material barrel in proportion,
While 300r/min is stirred, above-mentioned steps 1 are added in) Alevaire, the tobacco aromaticss of quality proportioning, it is then (micro- using microwave radiation technology
Wave frequency rate is 2450MHz, microwave power 600W, 21min) make obtained mixing thing liquid uniform, and the mixing thing liquid is delayed
Slowly above-mentioned steps 2 are added to) in the dry material powder, 300r/min is stirred evenly together, makes fiber, Alevaire, cigarette fragrant
The dispersions such as material are evenly；
(4) roll-in：By above-mentioned steps 4) dried mixed material, then through 4 rolling process, obtain thickness 0.28mm's
It is atomized reconstituted tobacco；
(5) pickling：By above-mentioned steps 4) obtained atomization reconstituted tobacco, it is impregnated in certain density organic acid soln
300S, taking-up drain；
The organic acid is citric acid, caffeic acid, food-grade, quality proportioning 1:0.5, the organic acid soln pH
Be worth is 6；
(6) it is dry：By above-mentioned steps 5) atomization reconstituted tobacco, through 115 DEG C of baking oven heat dryings to water content 3%, obtain
To the atomization reconstituted tobacco of the present invention.
A kind of atomization reconstituted tobacco prepared such as the above method, it is porous in producing bubbles inside, increase internal surface area, make height
The Alevaire of content is more evenly distributed, surface adhesion, improves machine cigarette adaptability on atomization reconstituted tobacco, makes existing cigarette
The normal cigarette of unit energy, is processed through cigarette, is applied in electrical heating or carbon heating low temperature cigarette, suction atomizing effect improves, cigarette
Perfume is abundant, and with cocoa aroma, sensory effects are good.
Embodiment 3
A kind of atomization reconstituted tobacco processing method, specifically comprises the following steps：
(1) raw material prepares：Tobacco material 55%, Alevaire 20%, adhesive 6%, essence spice for cigarette 1%, foaming agent
4%, 4%, 80 DEG C of warm water 10% of fiber, above-mentioned raw materials prepare according to mass percent；
The tobacco material is tobacco leaf, offal, tobacco waste, mass ratio 8:1:1；
The Alevaire is propylene glycol, glycerine, food-grade, quality proportioning 1:6；
The adhesive is bassora gum, polyethylene oxide, microcrystalline cellulose, propylene glycol alginate, mass ratio 1:
0.5：0.8：1.1；
The tobacco aromaticss for tobacco extract, coffee-extract, between quality proportioning be 1：1.2；Described has
Machine acid for citric acid, palmitic acid, chlorogenic acid, caffeic acid, between quality proportioning be 1:0.5；0.8:0.9；The bicarbonate
Salt is sodium bicarbonate, magnesium bicarbonate, calcium carbonate, quality proportioning 1:0.5：1, the fiber is the mixing of wood-fibred, flaxen fiber
Object, ratio 1:1；
(2) dry material co-grinding：By in tobacco material, solid adhesive, foaming agent calcium carbonate, magnesium bicarbonate press than
Example is put into Lowtemperaturepulverizer high speed and crushes uniformly, and mesh number is 180 mesh；
(3) wet stock mixing is uniformly dispersed：Above-mentioned steps 1) described in fiber and warm water pour into material barrel in proportion,
While 600r/min is stirred, above-mentioned steps 1 are added in) bicarbonate in the Alevaire of quality proportioning, tobacco aromaticss and foaming agent
Sodium, then microwave radiation technology (microwave frequency 2450MHz, power 900W, 12min) is used to make obtained mixing thing liquid uniform,
And the mixing thing liquid is slowly added into above-mentioned steps 2) and in the dry material powder, 600r/min is stirred evenly together, makes fibre
Dimension, Alevaire, tobacco aromaticss and bicarbonate dispersion are evenly；
(4) roll-in：By above-mentioned steps 4) dried mixed material, then through 3 rolling process, obtain thickness 0.25mm's
It is atomized reconstituted tobacco；
(5) pickling：By above-mentioned steps 4) obtained atomization reconstituted tobacco, it is impregnated in certain density organic acid soln
60S, taking-up drain；
The organic acid is chlorogenic acid, caffeic acid, food-grade, quality proportioning 1:1.2, the organic acid soln is dense
Spend is 0.15%；
(6) it is dry：By above-mentioned steps 5) atomization reconstituted tobacco, through 150 DEG C of baking oven heat dryings to water content 1%, obtain
To the atomization reconstituted tobacco of the present invention.
A kind of atomization reconstituted tobacco prepared such as the above method, producing bubbles inside is porous, increases internal surface area, contains height
The Alevaire of amount is more evenly distributed, surface adhesion, improves machine cigarette adaptability on atomization reconstituted tobacco, makes existing rolling up and connecting machine
The normal cigarette of group energy, is processed through cigarette, is applied in electrical heating or carbon heating low temperature cigarette, suction atomizing effect improves, atomization
Amount is big and uniform, good with abundant cigarette perfume and coffee aroma, sensory effects.
Test example 1：Sensory effects are evaluated
Machine cigarette is into atomization cigarette sample on atomization reconstituted tobacco prepared by embodiment 1-3, with compareing (common roll-in method
The atomization cigarette that machine cigarette forms on atomization thin slice), carry out sensory evaluating smoking contrast experiment.
The result shows that (as shown in table 1)：The atomization that machine cigarette is prepared on atomization reconstituted tobacco provided by the invention is again
Tobacco leaf is made, producing bubbles inside is porous, increases internal surface area, the Alevaire of high-content is made to be more evenly distributed, surface adhesion changes
Machine cigarette adaptability on atomization reconstituted tobacco has been apt to it, existing cigarette making and tipping machine normal volume is enable to deliver a child production, has been heated in electrical heating or carbon
It is applied in low temperature cigarette, through sensory evaluation, suction atomizing effect improves, and atomization quantity is big and uniform, clear with abundant cigarette perfume, peppermint
Icy gas, cocoa or coffee character fragrance, sensory effects are good.
Table 1. is atomized sensory evaluation of the reconstituted tobacco cigarette processing in electrical heating or charcoal heating low temperature cigarette
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in all should
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (10)
1. a kind of atomization reconstituted tobacco processing method, it is characterised in that：Include the following steps：
(1) raw material prepares：Matter prepares various raw materials by mass percentage：Tobacco material 40~63%, Alevaire 10~35%, glue
Stick 2~10%, essence spice for cigarette 1~5%, foaming agent 0.1-5%, fiber 1~5%, water 10~43%, the foaming agent
For one kind in carbonate or bicarbonate or its mixing；
(2) dry material co-grinding：Tobacco material, solid adhesive are put into Lowtemperaturepulverizer high speed in proportion to crush
It is even, obtain dry material powder, mesh number is the mesh of 40 mesh~200；
(3) wet stock mixing is uniformly dispersed：The fiber that above-mentioned steps (1) prepare is poured into material barrel in proportion with water,
It is stirring evenly and then adding into above-mentioned steps 1) Alevaire, the tobacco aromaticss of quality proportioning, then it is obtained using microwave radiation technology mixing
Mixed material, and mixed material is added in the dry material powder that above-mentioned steps (2) obtain, high-speed stirred is uniform together, makes
Fiber, Alevaire, foaming agent, tobacco aromaticss dispersion are evenly；
The foaming agent is added according to the ratio of step (1) in step (2) and/or in step (3)；
(4) roll-in：The mixed material that above-mentioned steps (3) are obtained, then through 1~6 rolling process, obtain thickness 0.15mm-
The atomization reconstituted tobacco of 0.3mm；
(5) pickling：The atomization reconstituted tobacco that above-mentioned steps (4) are obtained impregnates 3~600S, more preferably may be used in an acidic solution
It is impregnated in the acid solution of 3-6 with pH value, then dried；
(6) it is dry：The atomization reconstituted tobacco that above-mentioned steps (5) are obtained, through 80~150 DEG C of baking oven heat dryings to water content 1
~7%, obtain the atomization reconstituted tobacco of the present invention.
2. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：The tobacco material for tobacco leaf,
The one or more of mixing therein of offal, tobacco waste.
3. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：The Alevaire for propylene glycol,
Glycerine one or two therein, food-grade, quality proportioning 1:1~50.
4. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：The adhesive is rosin tree
Fat, gelatine, casein glue, sodium alginate, ammonium alginate, potassium alginate, CMC, bassora gum, polyethylene oxide, microcrystalline cellulose,
Propylene glycol alginate one or more of mixing therein.
5. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：The carbonate is calcium carbonate, carbon
The mixing of one or more of sour sodium, potassium carbonate, magnesium carbonate, the bicarbonate is sodium bicarbonate, magnesium bicarbonate, bicarbonate
The mixing of one or more of potassium, calcium bicarbonate.
6. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：The water prepared in the step (1)
For 30~80 DEG C of warm water.
7. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：Step (3) the high speed stirring
Rate be 100~800r/min.
8. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：Microwave frequency in the step (3)
For 2450MHz, microwave power is 200~1000W, and the time is 10~30min.
9. atomization reconstituted tobacco processing method as described in claim 1, it is characterised in that：Acid described in the step (5)
Property solution is by hydrochloric acid, sulfuric acid, lactic acid, tartaric acid, malic acid, acetic acid, citric acid, sodium citrate, potassium citrate, potassium citrate
The dilution dissolving of one or more of sodium, phosphoric acid, palmitic acid, chlorogenic acid, caffeic acid obtains.
10. a kind of atomization reconstituted tobacco prepared such as any one of claim 1-9 the methods, the cigarette after chopping or corrugation
Processing is applied in electrical heating or carbon heating low temperature cigarette.
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