CN108160709A - A kind of titanium alloy hot seamless tube production system and its production technology - Google Patents
A kind of titanium alloy hot seamless tube production system and its production technology Download PDFInfo
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- CN108160709A CN108160709A CN201810075684.XA CN201810075684A CN108160709A CN 108160709 A CN108160709 A CN 108160709A CN 201810075684 A CN201810075684 A CN 201810075684A CN 108160709 A CN108160709 A CN 108160709A
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- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 95
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 75
- 238000005516 engineering process Methods 0.000 title claims abstract description 21
- 238000005096 rolling process Methods 0.000 claims abstract description 81
- 238000010438 heat treatment Methods 0.000 claims abstract description 47
- 238000003303 reheating Methods 0.000 claims abstract description 33
- 238000000034 method Methods 0.000 claims abstract description 24
- 238000012360 testing method Methods 0.000 claims abstract description 19
- 238000012545 processing Methods 0.000 claims abstract description 13
- 230000007704 transition Effects 0.000 claims abstract description 13
- 238000005553 drilling Methods 0.000 claims abstract description 9
- 238000009785 tube rolling Methods 0.000 claims abstract description 5
- 238000005242 forging Methods 0.000 claims description 36
- 238000001816 cooling Methods 0.000 claims description 19
- 230000008569 process Effects 0.000 claims description 16
- 230000032683 aging Effects 0.000 claims description 12
- 239000007789 gas Substances 0.000 claims description 12
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical group [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 8
- 230000008901 benefit Effects 0.000 claims description 8
- 239000000498 cooling water Substances 0.000 claims description 8
- 238000002791 soaking Methods 0.000 claims description 8
- 238000003860 storage Methods 0.000 claims description 8
- 238000007689 inspection Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 229910052786 argon Inorganic materials 0.000 claims description 4
- 239000003595 mist Substances 0.000 claims description 4
- 238000004513 sizing Methods 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 208000002193 Pain Diseases 0.000 claims description 3
- 239000003638 chemical reducing agent Substances 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 238000001514 detection method Methods 0.000 claims description 3
- 239000002699 waste material Substances 0.000 claims description 3
- 230000005611 electricity Effects 0.000 claims 2
- 238000004321 preservation Methods 0.000 claims 1
- 229910000831 Steel Inorganic materials 0.000 abstract description 14
- 239000010959 steel Substances 0.000 abstract description 14
- 238000011084 recovery Methods 0.000 abstract description 8
- 230000001680 brushing effect Effects 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 5
- 239000011248 coating agent Substances 0.000 abstract description 2
- 238000000576 coating method Methods 0.000 abstract description 2
- 230000001681 protective effect Effects 0.000 abstract description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 20
- 239000010936 titanium Substances 0.000 description 20
- 229910052719 titanium Inorganic materials 0.000 description 18
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- 238000003801 milling Methods 0.000 description 4
- 239000011253 protective coating Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 239000002344 surface layer Substances 0.000 description 4
- 238000005097 cold rolling Methods 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 241001074085 Scophthalmus aquosus Species 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 238000005098 hot rolling Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B19/00—Tube-rolling by rollers arranged outside the work and having their axes not perpendicular to the axis of the work
- B21B19/02—Tube-rolling by rollers arranged outside the work and having their axes not perpendicular to the axis of the work the axes of the rollers being arranged essentially diagonally to the axis of the work, e.g. "cross" tube-rolling ; Diescher mills, Stiefel disc piercers or Stiefel rotary piercers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B19/00—Tube-rolling by rollers arranged outside the work and having their axes not perpendicular to the axis of the work
- B21B19/02—Tube-rolling by rollers arranged outside the work and having their axes not perpendicular to the axis of the work the axes of the rollers being arranged essentially diagonally to the axis of the work, e.g. "cross" tube-rolling ; Diescher mills, Stiefel disc piercers or Stiefel rotary piercers
- B21B19/04—Rolling basic material of solid, i.e. non-hollow, structure; Piercing, e.g. rotary piercing mills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B37/00—Control devices or methods specially adapted for metal-rolling mills or the work produced thereby
- B21B37/74—Temperature control, e.g. by cooling or heating the rolls or the product
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B39/00—Arrangements for moving, supporting, or positioning work, or controlling its movement, combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B39/14—Guiding, positioning or aligning work
- B21B39/16—Guiding, positioning or aligning work immediately before entering or after leaving the pass
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Metal Rolling (AREA)
- Forging (AREA)
- Heat Treatment Of Steel (AREA)
Abstract
The present invention relates to a kind of titanium alloy hot seamless tube production system and its production technologies, belong to titanium alloy seamless pipe processing technique field, it solves to need the technical issues of applying coating, production difficulty are big, lumber recovery is low in the titanium alloy seamless pipe operation of rolling, this system includes what is set gradually by production process route:Heating of pipe blank stove, punch, transition reheating furnace, three-roll pipe mill, test instrument on line area, Pierced billet reheating furnace, stretch reducing machine group, temperature adjustment tunnel, straightener and cold bed; it is cooled down after pipe blanking through drilling/rolling, tube rolling rolling, stretch reducing, online thermal straightening and cold bed; finished product titanium alloy hot seamless tube; electric furnace is set respectively in different phase in the operation of rolling, ensures to provide pipe reasonable rolling temperature for subsequent processing while quality of tube blank steel;Brushing protective materials is not required in the operation of rolling, reduces by a procedure;Stringent rolling temperature control reduces resistance of deformation, reduces unit power consumption, cost-effective, improves the lumber recovery of titanium alloy tube.
Description
Technical field
The invention belongs to titanium alloy seamless pipe processing technique field, more particularly to a kind of titanium alloy hot seamless tube production system
System and its production technology.
Background technology
Titanium or titanium alloy seamless pipe light weight, intensity are high, mechanical performance is superior, corrosion resistance and good, are mainly used for making
Aircraft engine compressor part and rocket, the structural member of guided missile and high-speed aircraft, electrolytic industry electrode, the condensation in power station
Device, petroleum refining and the industry manufacture fields such as the heater of sea water desalination and environment pollution control device.Titanium or titanium alloy without
The main of slit-tube bores bore hole by extrusion forming, pipe or tiltedly pierces through the three classes production system of hole cold rolling cold-drawn.Extrusion forming
Lumber recovery is low, poor dimensional precision, and production cost is high;Pipe brill bore size precision is preferable, but high processing costs, production efficiency
It is low with lumber recovery;Although cold rolling cold-drawn lumber recovery is higher after roll piercing, intensity height, plasticity are poor under such titanium alloy room temperature,
Cold-rolling deformation drag is big, needs repeatedly to anneal repeatedly, low production efficiency, and production cost is high.Therefore titanium and titanium are directed in modern production
Alloy seamless pipe needs a kind of energy saving, efficient production system.
Titanium chemism is larger, with O, N, H, CO, CO in air2, vapor and ammonia chemically react, can generate
The hard such as TiC, TiN surface layer;Titanium absorbs the very high hardened layer of oxygen formation hardness at 600 DEG C or more, is generated due to absorbing gas
Hard crisp skin depth up to 0.1-0.15mm, hardenability increases 20%-30%.Titanium chemical affinity is big, and easily rub table with tool
Face generates sticking phenomenon.Titanium heats in nitrogen to burn, and protected in heating process with argon gas.Titanium thermal conductivity factor is Fe
1/5, Ni 1/4, Al 1/14, and the thermal conductivity factor low about 50% of the thermal conductivity ratio titanium of various titanium alloys.The bullet of titanium alloy
Property modulus is about the 1/2 of steel, poor rigidity.
The physics and chemical characteristic of above-mentioned titanium determine that titanium alloy seamless pipe rolls difficulty than general steel pipe, aluminum pipe, magnesium
The rolling difficulty of the tubing such as compo pipe is much greater, and the rolling of titanium alloy seamless pipe is difficult to be obtained from the rolling mill practice of other tubing
Valuable reference.But also it is no lack of the technology of titanium alloy seamless pipe rolling in the prior art, such as patent name is " a kind of
The production technology of titanium or titanium alloy seamless pipe and material feeding structure in milling train foreground used "(Application No. is:201611093871.8)
And patent name is " a kind of preparation method of titanium alloy oil well pipe "(Application No. is:201611051807.3)It is although all public
A kind of production technology of titanium or titanium alloy seamless pipe has been opened, but in order to inhibit the activity on pipe surface in hot procedure, institute
With need " in titanium or titanium alloy blank surface brushing protective coating ", there are the defects of be:1st, it is needed in protective coating a variety of
Different substances, 2, the technics comparing of brushing protective coating it is time-consuming, extend the production cycle of pipe fitting, increase the production of pipe fitting
Cost;Such as patent name is " a kind of hot rolling large-diameter thin-wall titanium alloy seamless pipe production technology "(Application No. is:
201611065459.5)Although add maintenance tunnel, the work of maintenance tunnel between finish rolling hollow billet process and aligning process
With the function of being only heating heating, it is impossible to according to the temperature of tube surface in actual production process, heated up to pipe fitting or
Cooling is handled, and pipe fitting is made really to meet the needs of pipe fitting surface temperature in aligning process in next step.In addition, existing mainstream titanium closes
Still titanium alloy tube is rolled using duo mill in the processing technology of golden seamless pipe, not only wall thickness reducing amount is small, lumber recovery is low, prolongs
It stretches that coefficient is small, also results in the titanium alloy tube surfaces externally and internally that production obtains and generate screw thread, the fixation of two rolling process centering guides is set
It puts so that titanium alloy tube operation of rolling outer surface, which scratches, even to be cracked, and roll spacing, which cannot be adjusted, to be caused easily to roll during rolling
Card.
Invention content
The defects of it is an object of the invention to overcome the prior art, solves the titanium alloy seamless pipe operation of rolling in the prior art
In need the technical issues of applying coating, production difficulty are big, lumber recovery is low, a kind of titanium alloy hot seamless tube production system is provided
And its production technology.
The present invention is achieved by the following technical programs.
A kind of titanium alloy hot seamless tube production system, it includes the punch set gradually by production process route, three
Roll tube rolling mill, stretch reducing machine group, temperature adjustment tunnel, straightener and cold bed, further include electric furnace, and the electric furnace adds including pipe
Hot stove, transition reheating furnace and Pierced billet reheating furnace, wherein:Heating of pipe blank stove is set to the head end of production system, and pipe is through pipe
Punch middle punch rolling is transported to after base heating stove heat, the punch is two roller small-angle guide-roller type punches, with wearing
Hole machine axis direction is provided with three-roll pipe mill parallelly, is also set up between the tail end of punch and the head end of three-roll pipe mill
There is transition reheating furnace, the hollow forging after three-roll pipe mill rolling is transported to test instrument on line area, is provided in the test instrument on line area
Warm resistive heater is mended, hollow forging test instrument on line is transported to Pierced billet reheating furnace in area after ageing treatment, and Pierced billet reheating furnace adds
It is transported to stretch reducing in stretch reducing machine group after hot hollow forging to stretch reducing temperature, the production tube after stretch reducing machine group sizing is through temperature adjustment tunnel
Road is transported in straightener and aligns, and the production tube after aligning is transported to cold bed cooling, and production tube after cooling is transported to production tube
Storage area stores;Resistive heater is provided in the temperature adjustment tunnel, several fans, temperature adjustment tunnel are equidistantly provided in temperature adjustment tunnel
Road adjustment production tube temperature is 600-700 DEG C.
A kind of production technology of titanium alloy hot seamless tube production system, includes the following steps:
A, pipe blanking;
B, pipe inspection and reconditioning;
C, pipe heats in heating of pipe blank stove:
It is reducibility gas atmosphere in heating of pipe blank stove, heating of pipe blank stove heat stepwise pipe, the heat stepwise includes preheating
Section, bringing-up section and soaking zone, preheating section blank temperature are 500-650 DEG C, and preheating time is generally 30-90min;Bringing-up section pipe
Temperature is 650-1100 DEG C, heating time 60-90min;Soaking zone blank temperature is 1100-1150 DEG C, soaking time 60-
150min, drop temperature are 950-1120 DEG C;
D, two roller small-angle guide-roller type punch drilling/rolling:Wherein, 8-12 ° of feed angle is adjustable, 5 ° of fixations of rolling angle, and roll turns
Fast 40-80r/min is adjustable, roll rotational speed 40-60r/min when stinging pipe, and the seamless hollow billet of titanium alloy, hollow billet temperature after perforation is made
It is 900-1000 DEG C;
E, hollow billet reheats in transition reheating furnace:
Outer diameter and wall-thickness ratio are D/S after drilling/rolling, and as 10≤D/S < 20, thick-wall titanium alloy is seamless, and hollow billet directly passes through
Pipe device immigration subsequent processing is moved to be rolled;As 20≤D/S≤40, thin-wall titanium alloy is seamless hollow billet is in transition reheating furnace
In be reheated to 950-1050 DEG C, then move into subsequent processing by moving pipe device and rolled;
F, three-roll pipe mill rolls:Wherein, three-roll pipe mill roll off angle is adjustable for 0-6 °, and 8-10 ° of feed angle is adjustable, roll revolution
For 60-120r/min, rolling titanium alloy tube speed is 0.22m/s~0.50m/s, and the seamless hollow forging of titanium alloy is made;
G, hollow forging test instrument on line is handled:
Whether need ageing treatment that test instrument on line is handled point two lines according to hollow forging:When hollow forging needs to carry out ageing treatment
When, hollow forging is as cold as 480-560 DEG C into test instrument on line area is hollow first, then, to 950 DEG C, mends temperature into benefit temperature in Pierced billet reheating furnace
When being not more than ± 10 DEG C to waste tube outer surface and the inner surface temperature difference, hollow forging passes through Pierced billet reheating furnace into follow-up rolling process;When
When hollow forging does not need to carry out ageing treatment, hollow forging is directly through Pierced billet reheating furnace into follow-up rolling process;
H, stretch reducing machine group rolls:Roll cooling water is closed in the stretch reducing machine group operation of rolling, after the completion of the rolling of stretch reducing machine group successively
The cooling water per rack is opened to cool down stretch reducing machine roll;
I, temperature adjustment tunnel temperature adjustment:Hot finished product seamless titanium alloy pipe blank temperature after being rolled according to stretch reducing machine group, the heating of temperature adjustment tunnel
Or cool down, pipe is made to meet the temperature of pipe needs in follow-up aligning process, pipe aligns process into follow-up;
J, hot production tube on-line straightening
Straightener straightening temperature section is 600-700 DEG C, and the maximum speed of aligning of straightener is 0.5-0.8m/s, straightening roll angle
30 ° ± 3 ° of adjusting range is subject to and meets more than 3/4 more than barrel length of titanium alloy tube and straightening roll contact line length, rectifys
Titanium alloy tube temperature is 550-600 DEG C after straight;The straightener is the online thermal straightening machine of six rollers or the online thermal straightening machine of seven rollers
Or nine online thermal straightening machine of roller;
K, the titanium alloy tube after aligning is cooled to room temperature on cold bed;
L, it by after cold bed titanium alloy tube sawing after cooling, flaw detection, hand inspection, is packaged into production tube storage area.
Further, in the step c, heating of pipe blank stove is step-by-step movement electric furnace or is annular electric furnace,
Reducibility gas in heating of pipe blank stove is argon gas.
Further, in the step c, each section of the heating time difference during heating of pipe blank stove heat stepwise
It is accordingly adjusted according to pipe outer diameter size.
Further, in the step c, the titanium alloy pipe to discharge after heat stepwise is in β phase regions, titanium alloy pipe
Resistance of deformation K is 65-120MPa.
Further, in the step d, the upper bottom guide in two roller small-angle guide-roller type punches is by guide wheel generation
It replaces.
Further, in the step d, the guide wheel is rotated by motor via reducer driving screw in copper nut
It realizes pressure and rises, adapt to the pipe of different tube diameters.
Further, in the step d and step e, drilling/rolling is used with roll cooling in the tube rolling operation of rolling
High-pressure water mist cools down, and nozzle is far from rolling entrance.
Further, in the step k, cold bed is walking beam cooler or is chain-type cooling bed.
The present invention has the advantages that compared with prior art.
1st, titanium alloy rolling deformation temperature range is narrow, and stringent rolling temperature control reduces resistance of deformation, substantially reduces unit
Power consumption, it is cost-effective, while improve the lumber recovery of titanium alloy tube;
2nd, blank is not required to brushing protective materials, reduces by a procedure;
3rd, guide-roller type punch substitutes the upper bottom guide that conventional through-hole machine uses using upper and lower guide wheel, efficiently solve titanium alloy by
Friction between rolling tool and the metal sticking phenomenon generated, rolling tool consumption are reduced;
4th, further the hollow billet after perforation is carried out using three roller roller mills subtracting the rolling work such as wall extension, rolling angle, feed angle
Skill parameter adjustment flexibility and reliability, units consumption is low compared with two roller roller mills, and pipe inside and outside surface quality is good.
Description of the drawings
Fig. 1 is production system overall structure diagram of the present invention, the arrow expression technological process direction in figure.
Fig. 2 is two roller small-angle guide-roller type perforating roller of perforating machine system schematic diagrames in Fig. 1.
Fig. 3 is production technological process of the present invention.
In figure, 1 is heating of pipe blank stove, and 2 be punch, and 3 be transition reheating furnace, and 4 be three-roll pipe mill, and 5 be online normal
Change area, 6 be Pierced billet reheating furnace, and 7 be stretch reducing machine group, and 8 be temperature adjustment tunnel, and 9 be straightener, and 10 be cold bed, and 21 be left roll, 22
It is hollow billet for upper block, 23,24 be lower tumbler, and 25 be right roll, and 26 be high-pressure water mist cooling nozzles.
Specific embodiment
It elaborates with reference to embodiment to the present invention:The present embodiment is to carry out based on the technical solution of the present invention
Implement, give detailed embodiment and specific operating process, but protection scope of the present invention is not limited to following implementation
Example.
As depicted in figs. 1 and 2, a kind of titanium alloy hot seamless tube production system in the present embodiment, it is included by production
Punch 2, three-roll pipe mill 4, stretch reducing machine group 7, temperature adjustment tunnel 8, straightener 9 and the cold bed 10 that process route is set gradually, also
Including electric furnace, the electric furnace includes heating of pipe blank stove 1, transition reheating furnace 3 and Pierced billet reheating furnace 6, wherein:Pipe
Base heating furnace 1 is set to the head end of production system, and pipe is transported to 2 middle punch of punch rolling after the heating of heating of pipe blank stove 1,
The punch 2 is two roller small-angle guide-roller type punches, is provided with three-roll pipe mill parallelly with 2 axis direction of punch
4, transition reheating furnace 3 is additionally provided between the tail end of punch 2 and the head end of three-roll pipe mill 4, after three-roll pipe mill 4 rolls
Hollow forging be transported to test instrument on line area 5, the warm resistive heater of benefit, hollow forging test instrument on line area 5 are provided in the test instrument on line area 5
Middle that Pierced billet reheating furnace 6 is transported to after ageing treatment, Pierced billet reheating furnace 6 is transported to after heating hollow forging to stretch reducing temperature
Stretch reducing in stretch reducing machine group 7, the production tube after 7 sizing of stretch reducing machine group, which is transported to through temperature adjustment tunnel 8 in straightener 9, to be aligned, and is rectified
Production tube after straight is transported to cold bed 10 and cools down, and production tube after cooling is transported to the storage of production tube storage area;The temperature adjustment tunnel
Resistive heater is provided in road 8, several fans are equidistantly provided in temperature adjustment tunnel 8, temperature adjustment tunnel 8 adjusts production tube temperature and is
600-700℃。
It is shown in Fig. 3 just like kind of a production technology for titanium alloy hot seamless tube production system, include the following steps:
A, pipe blanking.
B, pipe inspection and reconditioning.
C, pipe heats in heating of pipe blank stove 1:
Since titanium chemism is larger, with the O in air2、N、H2、CO、CO2Chemically reacted with vapor, can generate TiC,
The hard such as TiN surface layer, therefore using electric furnace, electric furnace can be step-by-step movement electric furnace and annular electric furnace.Heating
Stove uses micro- reducibility gas environment, and reducibility gas is argon gas.It prevents pipe surface from generating hard surface layer, influences punch and sting
Steel also avoids hard surface layer fragment and is pressed into tube body in the operation of rolling to generate defect.Difference with existing patent is to leave out
To the process of pipe brushing protective coating;
Titanium thermal conductivity factor is the 1/14 of 1/4, the Al of 1/5, the Ni of Fe, and the thermal conductivity factor of the thermal conductivity ratio titanium of various titanium alloys
Low about 50%.Furnace power output power gradient is automatically adjusted using industry control program using electric furnace, realizes that pipe is each in stove
The temperature-controllable of a bringing-up section.It is reducibility gas atmosphere in heating of pipe blank stove 1,1 heat stepwise pipe of heating of pipe blank stove is described
Heat stepwise includes preheating section, bringing-up section and soaking zone, and preheating section blank temperature is 500-650 DEG C, and preheating time is generally 30-
90min;Bringing-up section blank temperature is 650-1100 DEG C, heating time 60-90min;Soaking zone blank temperature is 1100-1150
DEG C, soaking time 60-150min, drop temperature is 950-1120 DEG C;Heating time and pipe outer diameter are related greatly.Drop temperature is
950-1120 DEG C, at this time titanium alloy be in β phase regions, resistance of deformation K is about 65-120MPa.
D, two roller small-angle guide-roller type punches, 2 drilling/rolling, hollow billet temperature is 900-1000 DEG C after perforation.
Feature 1:Roll uses small-angle tapered roller.Roller shape influences metal flow direction when barrel roll rolls, to metal stream
It is dynamic to form reaction force, it is unfavorable for metal flow, is also easy to produce infolding phenomenon.Appearance in pipe is easily formed during barrel roll rolling simultaneously
Surface helix line.Tapered roller is five sections of roller shapes, there is rolloff band, solves the problems, such as barrel roll helix, while tapered roller body of roll edge is rolled
The component velocity in line direction processed gradually increases, and adapts to the speed of pipe and increases, does not have reaction force to pipe.Bullet based on titanium alloy
Property modulus be about the 1/2 of steel, poor rigidity, mutability should not make thin-wall tube, therefore use small-angle tapered roller, 8-12 ° of feed angle
It is adjustable, 5 ° of fixations of rolling angle.To prevent titanium alloy from generating processing hardening phenomenon in the operation of rolling, rolled, rolled using the slow-speed of revolution
Roller rotating speed 40-80r/min is adjustable, roll rotational speed 40-60r/min when stinging pipe, and the seamless hollow billet of titanium alloy is made;
Feature 2:Since titanium chemical affinity is big, easily sticking phenomenon is generated with tool friction surface.Two roller conelets of titanium alloy tube
Angle guide-roller type punch substitutes the upper bottom guide that conventional through-hole machine uses using upper and lower guide wheel, efficiently solve titanium alloy due to
Friction between rolling tool and the metal sticking phenomenon generated, upper and lower guide wheel drive screw in copper spiral shell by motor via reducer
Rotation realizes pressure and rises to adapt to different pipes in mother;
Feature 3:Titanium chemism is larger, is easily chemically reacted with water and steam, generates cementation zone, easily causes simultaneously
Hollow billet surface fine crack.Roll cooling is cooled down using high-pressure water mist in the operation of rolling, and arrangement is as shown in Fig. 2, nozzle
Far from rolling entrance, ensure that roller roll surface in rolling is dried.
E, outer diameter and wall-thickness ratio are D/S after drilling/rolling, and as 10≤D/S < 20, thick-wall titanium alloy is seamless, and hollow billet is straight
Shifting pipe device immigration subsequent processing was connected to be rolled;As 20≤D/S≤40, thin-wall titanium alloy is seamless hollow billet in transition again
950-1050 DEG C is reheated in heating furnace 3, then is rolled by moving pipe device immigration subsequent processing;
F, three-roll pipe mill 4 rolls:
Three-roll pipe mill by three belt roller shoulders the vertex being arranged in using roll line as the equilateral triangle of the centre of form, roll axis with
Roll line is into two angles of inclination.Roll axis tilts a feed angle in vertical direction and roll line, for realizing that spiral is rolled
System;Interlock a roll off angle with roll line in the horizontal direction.In the pass surrounded in three rolls and a plug, by perforating
The hollow billet sent is sleeved on long plug, is sent into pipe mill and rolled with supply bobbin device;Hollow billet is in deformed area through biting, subtracting wall(Together
When tube reducing), it is smooth and return circle and as hollow forging.During oblique milling screw rolling metal in deformed area by the period of roll and plug
Continuous action and the variation for generating shape and size.Deformation of rolled wire be actually from justifying to justifying triangle again to round process.
It is than three-roll pipe mill advantage with two-roller mill:Product accuracy is high, because of the oblique milling of cored bar, in a time
Multiple spreading effect, greatly improves wall thickness accuracy;Flexibility is big in production, and pass ruler just can be changed by the clutch of roll
It is very little, it has an enormous advantage to tissue production;Deposit of tools quantity is few.
When rolling titanium alloy tube, roll is in low speed rotation before starting to bite, after hollow billet enters roll with plug
Start once to bite, titanium alloy tube hollow billet is only diametrically being compressed at this moment, as steel pipe advances, is opened in the shoulder of roll
Beginning hollow billet inner surface contact mandrel surface carries out subtracting wall, realizes secondary bite.It normally bites rear roll rotational speed and is increased to setting
Mill speed carries out high-speed rolling.Roll rotational speed drops back to low speed after the end of rolling.Usual biting speed is mill speed
70% 。
In the titanium alloy tube for producing D/S > 16, to prevent hollow forging front end from generating flare, stung in hollow billet by roll
Before entering, topping roll is under the action of quick-opening device, and roll gap is more slightly larger than normal rolling roll gap, when the shoulder that hollow billet head passes through roll
Afterwards, topping roll quickly recovers to normal rolling position.It is about 0.3 second to depress actuation time.
Titanium alloy tube is 0-6 ° adjustable with 4 roll off angle of three-roll pipe mill, feed angle:0-12 ° adjustable, and feed angle increases, and rolls
Muzzle velocity processed is accelerated, and expanding value increases, but as the increase of feed angle, rolling stability reduce, wall unevenness is in increase
Trend easily generates internal thread.Therefore it is sent when producing thick-walled pipe using larger feed angle, thin-wall tube production using smaller
Into angle.But feed angle is also unsuitable too small when producing thin-wall tube, because feed angle is too small, mill speed is slow, especially thin-walled
Guan Shi, rolling time is long to be easy to cause the increasing of steel pipe head and tail temperature difference, the wall unevenness being formed on length of steel pipe direction.
Influence of the roll revolution to steel pipe is consistent with the influence of feed angle.In the case of in view of milling train force-power parameter,
When rolling titanium alloy tube, relatively low 8-10 ° of roll revolution 60-120r/min and smaller feed angle should be used, rolls titanium alloy
The seamless hollow forging of titanium alloy is made in pipe speed 0.22m/s~0.50m/s.
Three-high mill strictly controls roll cooling water, the roll type of cooling and piercer roll cooling side in the operation of rolling
Formula is identical.
G, hollow forging test instrument on line is handled:
Whether need ageing treatment that test instrument on line is handled point two lines according to hollow forging:When hollow forging needs to carry out ageing treatment
When, hollow forging is as cold as 480-560 DEG C into test instrument on line area 5 is hollow first, then, to 950 DEG C, is mended into benefit temperature in Pierced billet reheating furnace 6
When temperature to waste tube outer surface and the inner surface temperature difference is not more than ± 10 DEG C, hollow forging passes through Pierced billet reheating furnace 6 into follow-up rolling process;
When hollow forging does not need to carry out ageing treatment, hollow forging is directly through Pierced billet reheating furnace 6 into follow-up rolling process.
H, stretch reducing machine group 7 rolls:
The process that the process subtracted is a hollow body tandem rolling is opened, other than playing sizing, also requirement has larger reducing rate,
In addition to this, stretch reducing also requires to realize the purpose for subtracting wall by establishing tension between each rack.
Hollow forging is come out of the stove after reheating electric furnace and being heated to 950 DEG C, is exported in furnace delivery table and is carried out surface temperature measurement.Titanium alloy tube
Driven separately is used with stretch reducing machine group 7, because being determined the characteristics of collective's differential gearing cannot come by adjusting main Overlap electric machine
Each rack is made to reach an ideal speed, ensures that titanium alloy tube does not occur processing hardening phenomenon in the operation of rolling.So rolling
It during system, can only ensure some tension by rationally adjusting the rotating speed of each motor under the equal principle of second flow, carry out
Wall thickness is finely tuned(Generally 0.5mm is not exceeded).
Roll cooling water is strictly controlled in the operation of rolling, roll cooling water is closed in the operation of rolling, after the completion of rolling
The cooling water per rack is opened successively to cool down roll.
I, 8 temperature adjustment of temperature adjustment tunnel:
When rolling titanium alloy tube, since heat dissipation metal is efficient, and requirement of each technique to temperature range is very small, in tradition
It is transmitted on roller-way, is unable to control scattering and disappearing for its heat, also can not just meet its requirement of lower one of technique to temperature, so as to cause
Its performance requirement is not achieved in the seamless pipe rolled out.
Titanium alloy aligning is using thermal straightening, and straightening temperature section is 600-700 DEG C, and the tube temperature after stretch reducing machine rolls
It it is 800-900 DEG C, pipe needs to regulate and control tube temperature by temperature adjustment tunnel, ensures that pipe meets in follow-up aligning process
The temperature that pipe needs, temperature adjustment tunnel use Electric heating.Temperature regulate and control system depending on titanium alloy tube material, prevent by
In the unreasonable influence titanium alloy metallographic variation of the variation of temperature.
J, hot production tube on-line straightening
Straightener main function is that supplied materials steel pipe is aligned, and eliminates steel pipe in rolling, transport, heat treatment and cooling procedure
The bending of generation makes steel pipe directly spend and meets related request, while plays and return round effect to steel pipe, ensures pipe end and steel pipe surface
Face quality.
9 straightening temperature section of straightener is 600-700 DEG C, and the maximum aligning speed of straightener 9 is 0.5-0.8m/s, is aligned
30 ° ± 3 ° of roller angle adjusting range, being more than more than the 3/4 of barrel length to meet titanium alloy tube and straightening roll contact line length is
Standard, titanium alloy tube temperature is 550-600 DEG C after aligning;The straightener 9 is warm online for the online thermal straightening machine of six rollers or seven rollers
Straightener or the online thermal straightening machine of nine rollers.
K, the titanium alloy tube after aligning is cooled to room temperature on cold bed 10;
L, it by after 10 titanium alloy tube sawing after cooling of cold bed, flaw detection, hand inspection, is packaged into production tube storage area.
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
It is familiar with those skilled in the art in the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in should all be contained
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (9)
1. a kind of titanium alloy hot seamless tube production system, it includes the punch set gradually by production process route(2), three
Roll tube rolling mill(4), stretch reducing machine group(7), temperature adjustment tunnel(8), straightener(9)And cold bed(10), further include electric furnace, the electricity
Heating furnace includes heating of pipe blank stove(1), transition reheating furnace(3)And Pierced billet reheating furnace(6), it is characterised in that:Heating of pipe blank
Stove(1)The head end of production system is set to, pipe is through heating of pipe blank stove(1)Punch is transported to after heating(2)Middle punch rolls,
The punch(2)For two roller small-angle guide-roller type punches, with punch(2)Axis direction is provided with three rollings parallelly
Pipe machine(4), punch(2)Tail end and three-roll pipe mill(4)Head end between be additionally provided with transition reheating furnace(3), three rollers
Pipe mill(4)Hollow forging after rolling is transported to test instrument on line area(5), the test instrument on line area(5)In be provided with benefit temperature heating electricity
Hinder silk, hollow forging test instrument on line area(5)It is middle that Pierced billet reheating furnace is transported to after ageing treatment(6), Pierced billet reheating furnace(6)Heating
Stretch reducing machine group is transported to after hollow forging to stretch reducing temperature(7)Middle stretch reducing, stretch reducing machine group(7)Production tube after sizing is through adjusting
Warm tunnel(8)It is transported to straightener(9)Middle aligning, the production tube after aligning are transported to cold bed(10)Cooling, finished product after cooling
Pipe is transported to the storage of production tube storage area;The temperature adjustment tunnel(8)In be provided with resistive heater, temperature adjustment tunnel(8)In it is equidistant
It is provided with several air cooling devices, temperature adjustment tunnel(8)It is 600-700 DEG C to adjust production tube temperature.
2. a kind of production technology of titanium alloy hot seamless tube production system as described in claim 1, it is characterised in that including
Following steps:
A, pipe blanking;
B, pipe inspection and reconditioning;
C, pipe is in heating of pipe blank stove(1)Middle heating:
Heating of pipe blank stove(1)In for reducibility gas atmosphere, heating of pipe blank stove(1)Heat stepwise pipe, the heat stepwise packet
Preheating section, bringing-up section and soaking zone are included, preheating section blank temperature is 500-650 DEG C, and preheating time is generally 30-90min;Heating
Section blank temperature is 650-1100 DEG C, heating time 60-90min;Soaking zone blank temperature is 1100-1150 DEG C, during heat preservation
Between 60-150min, drop temperature be 950-1120 DEG C;
D, two roller small-angle guide-roller type punch(2)Drilling/rolling:Wherein, 8-12 ° of feed angle is adjustable, and 5 ° of fixations of rolling angle are rolled
Roller rotating speed 40-80r/min is adjustable, roll rotational speed 40-60r/min when stinging pipe, and the seamless hollow billet of titanium alloy, hollow billet after perforation is made
Temperature is 900-1000 DEG C;
E, hollow billet is in transition reheating furnace(3)In reheat:
Outer diameter and wall-thickness ratio are D/S after drilling/rolling, and as 10≤D/S < 20, thick-wall titanium alloy is seamless, and hollow billet directly passes through
Pipe device immigration subsequent processing is moved to be rolled;As 20≤D/S≤40, thin-wall titanium alloy is seamless hollow billet is in transition reheating furnace
(3)In be reheated to 950-1050 DEG C, then move into subsequent processing by moving pipe device and rolled;
F, three-roll pipe mill(4)Rolling:Wherein, three-roll pipe mill(4)Roll off angle is adjustable for 0-6 °, and 8-10 ° of feed angle is adjustable, rolls
Roller revolution is 60-120r/min, and rolling titanium alloy tube speed is 0.22m/s~0.50m/s, and the seamless hollow forging of titanium alloy is made;
G, hollow forging test instrument on line is handled:
Whether need ageing treatment that test instrument on line is handled point two lines according to hollow forging:When hollow forging needs to carry out ageing treatment
When, hollow forging is first into test instrument on line area(5)It is hollow to be as cold as 480-560 DEG C, then into Pierced billet reheating furnace(6)Middle temperature of mending is to 950
DEG C, when benefit temperature to waste tube outer surface and the inner surface temperature difference are not more than ± 10 DEG C, hollow forging passes through Pierced billet reheating furnace(6)Into subsequently rolling
Process processed;When hollow forging does not need to carry out ageing treatment, hollow forging is directly through Pierced billet reheating furnace(6)Into follow-up rolling process;
H, stretch reducing machine group(7)Rolling:In stretch reducing machine group(7)Roll cooling water, stretch reducing machine group are closed in the operation of rolling(7)It has rolled
The cooling water per rack is opened successively after to cool down stretch reducing machine roll;
I, temperature adjustment tunnel(8)Temperature adjustment:According to stretch reducing machine group(7)Hot finished product seamless titanium alloy pipe blank temperature, temperature adjustment tunnel after rolling
Road(8)Heating cools down, and pipe is made to meet the temperature of pipe needs in follow-up aligning process, and pipe aligns process into follow-up;
J, hot production tube on-line straightening
Straightener(9)Straightening temperature section is 600-700 DEG C, straightener(9)Maximum aligning speed be 0.5-0.8m/s, aligning
30 ° ± 3 ° of roller angle adjusting range, being more than more than the 3/4 of barrel length to meet titanium alloy tube and straightening roll contact line length is
Standard, titanium alloy tube temperature is 550-600 DEG C after aligning;The straightener(9)It is online for the online thermal straightening machine of six rollers or seven rollers
Thermal straightening machine or the online thermal straightening machine of nine rollers;
K, in cold bed(10)On the titanium alloy tube after aligning is cooled to room temperature;
L, by cold bed(10)After titanium alloy tube sawing after cooling, flaw detection, hand inspection, it is packaged into production tube storage area.
3. a kind of titanium alloy hot seamless tube production technology according to claim 2, it is characterised in that:In the step c
In, heating of pipe blank stove(1)For step-by-step movement electric furnace or it is annular electric furnace, heating of pipe blank stove(1)In reproducibility gas
Body is argon gas.
4. a kind of titanium alloy hot seamless tube production technology according to claim 2, it is characterised in that:In the step c
In, heating of pipe blank stove(1)Each section of heating time during heat stepwise accordingly adjusts respectively according to pipe outer diameter size.
5. a kind of titanium alloy hot seamless tube production technology according to claim 4, it is characterised in that:In the step c
In, the titanium alloy pipe to discharge after heat stepwise is in β phase regions, and titanium alloy pipe resistance of deformation K is 65-120MPa.
6. a kind of titanium alloy hot seamless tube production technology according to claim 2, it is characterised in that:In the step d
In, two roller small-angle guide-roller type punches(2)In upper bottom guide replaced by guide wheel.
7. a kind of titanium alloy hot seamless tube production technology according to claim 6, it is characterised in that:In the step d
In, the guide wheel is rotated realization pressure by motor via reducer driving screw and is risen in copper nut, adapts to different tube diameters
Pipe.
8. a kind of titanium alloy hot seamless tube production technology according to claim 2, it is characterised in that:In the step d
With in step e, in drilling/rolling and the tube rolling operation of rolling roll cooling cooled down using high-pressure water mist, nozzle is far from rolling entrance
Section.
9. a kind of titanium alloy hot seamless tube production technology according to claim 2, it is characterised in that:In the step k
In, cold bed(10)For walking beam cooler or it is chain-type cooling bed.
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CN110369546A (en) * | 2019-08-01 | 2019-10-25 | 四川三洲特种钢管有限公司 | A method of producing large-bore titanium alloy hot seamless tube |
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CN112708737A (en) * | 2020-12-17 | 2021-04-27 | 广州众山精密科技有限公司 | Method for preventing tube wall of metal material from being scratched in tube annealing furnace |
CN113441551A (en) * | 2021-06-30 | 2021-09-28 | 北京科技大学 | Thick-walled seamless steel pipe and preparation method thereof |
CN113441551B (en) * | 2021-06-30 | 2022-07-01 | 北京科技大学 | Thick-walled seamless steel pipe and preparation method thereof |
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