CN108142776A - A kind of fig skin antioxidant and preparation method thereof - Google Patents

A kind of fig skin antioxidant and preparation method thereof Download PDF

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Publication number
CN108142776A
CN108142776A CN201611096151.7A CN201611096151A CN108142776A CN 108142776 A CN108142776 A CN 108142776A CN 201611096151 A CN201611096151 A CN 201611096151A CN 108142776 A CN108142776 A CN 108142776A
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weight
parts
mentioned
vitamin
skin
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CN201611096151.7A
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Inventor
黄升谋
林淦
余海忠
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Hubei University of Arts and Science
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Hubei University of Arts and Science
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Priority to CN201611096151.7A priority Critical patent/CN108142776A/en
Publication of CN108142776A publication Critical patent/CN108142776A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3472Compounds of undetermined constitution obtained from animals or plants
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of fig skin antioxidants and preparation method thereof.The fig skin antioxidant of the present invention includes following component:Fig bark extract, ginseng pulverate, licorice powder, sodium citrate, vitamin A, vitamin E, vitamin C, vitamin D.Present invention materials are natural, and nutritive value is high, has no toxic side effect, can anticoagulation and reducing blood lipid, enhancing immunocyte, antitumor, there is good antioxidation, have a wide range of application.

Description

A kind of fig skin antioxidant and preparation method thereof
Technical field
The invention belongs to technical field of food additives, and in particular to a kind of anti-oxidant addition of fig skin and its preparation side Method.
Background technology
Existing food oxydating resistance additive mainly has chemical food antioxidant and the anti-oxidant addition of wholefood Two major class of agent, wherein, chemical food antioxidant works well, but there are the shortcomings of different degrees of toxic side effect, It is used for a long time or excessive amount causes to damage to body.Artificial chemistry food oxydating resistance additive refers to manually chemical synthesis Obtained by method.At the same time, a large amount of research report is pointed out, almost all of chemical food antioxidant all cannot Nutriment is provided to human body, certain chemical food antioxidants can even be detrimental to health.
Invention content
It is an object of the invention to overcome prior art defect, a kind of fig skin antioxidant is provided.
Another object of the present invention is to provide the preparation method of the fig skin antioxidant.
Technical scheme is as follows:
A kind of fig skin antioxidant includes the component of following parts by weight:
Fig bark extract 90-100 parts by weight
Ginseng pulverate's 0.3-0.5 parts by weight
Licorice powder 0.01-0.02 parts by weight
Sodium citrate 0.01-0.02 parts by weight
Vitamin A 0.4-0.6 parts by weight
Vitamin E 0.1-0.3 parts by weight
Vitamin C 1-3 parts by weight
Vitamin D 0.1-0.2 parts by weight
Another technical solution of the present invention is as follows:
A kind of preparation method of above-mentioned fig skin antioxidant, includes the following steps:
(1)By fig skin successively through ethanol water heat reflux extraction, ether extraction, PEG 20000 chromatography column chromatography, After Silon chromatography, eluant ethanol recrystallization and drying, the fig bark extract is made;
(2)By above-mentioned fig bark extract 90-100 parts by weight, ginseng pulverate's 0.3-0.5 parts by weight, licorice powder 0.01-0.02 weights Measure part, sodium citrate 0.01-0.02 parts by weight, vitamin A 0.4-0.6 parts by weight, vitamin E 0.1-0.3 parts by weight, vitamin C1-3 parts by weight, vitamin D 0.1-0.2 parts by weight are mixed evenly, up to the anti-oxidant addition of fig skin after drying Agent.
In a preferred embodiment of the invention, the step(1)Include the following steps:
A, ethanol water will be added in after above-mentioned fig skin drying and crushing to extract 20-30 minutes, and mistake in 50-60 DEG C of heat reflux Filter, obtains leaching liquor;
B, above-mentioned leaching liquor with ether is extracted, obtains extract liquor;
C, above-mentioned extract liquor is subjected to column chromatography, then the ethanol aqueous wash with a concentration of 10-20% with PEG 20000 column It is de-, obtain first order eluent;
D, above-mentioned first order eluent by the use of Silon as adsorbent is chromatographed, then is washed with the mixed liquor of aqueous acetic acid It is de-, obtain second level eluent;
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the fig bark extract after drying.
In a preferred embodiment of the invention, the step(1)Step a in, ethanol water it is a concentration of 20-30%, the ethanol water total weight are 2-3 times of fig tare weight amount after drying and crushing.
In a preferred embodiment of the invention, the step(1)Step d in, the Silon be 200 Mesh, a concentration of 1-2% of the aqueous acetic acid.
The beneficial effects of the invention are as follows:
1st, containing fig skin in antioxidant of the invention, materials are natural, and nutritive value is high, has no toxic side effect, can Anticoagulation and reducing blood lipid enhance immunocyte, are antitumor, have good antioxidation, have a wide range of application;
2nd, the vitamin E in antioxidant of the invention is polyphenoils and membrane stabilizer important in cell membrane, is maintained The normal mechanism of musculature and metabolism, energy supply and calcium ion intake and release particularly during contraction of muscle have Important role;
3rd, the vitamin C in antioxidant of the invention can obviously reduce exercise induced oxidative stress.
Specific embodiment
Technical scheme of the present invention is further detailed and described below by way of specific embodiment.
Embodiment 1
(1)Prepare fig bark extract:
A, 2kg20% ethanol waters will be added in after 1kg fig skin drying and crushings, will be extracted 20 minutes, and mistake in 50 DEG C of heat reflux Filter concentration, obtains leaching liquor;
B, above-mentioned leaching liquor with ether is extracted, obtains extract liquor;
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is eluted with a concentration of 10% ethanol water, Obtain first order eluent;
D, above-mentioned first order eluent is chromatographed by the use of the Silon of 200 mesh as adsorbent, then with 1% aqueous acetic acid Elution, obtains second level eluent;
E, above-mentioned second level eluent is recrystallized twice with ethyl alcohol, to get the fig bark extract after drying;
(2)By above-mentioned 90 parts by weight of fig bark extract, 0.3 parts by weight of ginseng pulverate, 0.01 parts by weight of licorice powder, sodium citrate 0.01 parts by weight, 0.4 parts by weight of vitamin A, 0.1 parts by weight of vitamin E, 1 parts by weight of vitamin C, 0.1 parts by weight of vitamin D It is mixed evenly, up to the fig skin antioxidant after drying.
Embodiment 2
(1)Prepare fig bark extract:
A, 2.5kg25% ethanol waters will be added in after 1kg fig skin drying and crushings, will be extracted 25 minutes in 55 DEG C of heat reflux, and Filtering and concentrating obtains leaching liquor;
B, above-mentioned leaching liquor with ether is extracted, obtains extract liquor;
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is eluted with a concentration of 15% ethanol water, Obtain first order eluent;
D, above-mentioned first order eluent is chromatographed by the use of the Silon of 200 mesh as adsorbent, then water-soluble with 1.5% acetic acid Liquid elutes, and obtains second level eluent;
E, above-mentioned second level eluent is recrystallized twice with ethyl alcohol, to get the fig bark extract after drying;
(2)By above-mentioned 95 parts by weight of fig bark extract, 0.4 parts by weight of ginseng pulverate, 0.015 parts by weight of licorice powder, citric acid 0.015 parts by weight of sodium, 0.5 parts by weight of vitamin A, 0.2 parts by weight of vitamin E, Catergen parts by weight, 0.15 weight of vitamin D Amount part is mixed evenly, up to the fig skin antioxidant after drying.
Embodiment 3
(1)Prepare fig bark extract:
A, 3kg30% ethanol waters will be added in after 1kg fig skin drying and crushings, will be extracted 30 minutes, and mistake in 60 DEG C of heat reflux Filter concentration, obtains leaching liquor;
B, above-mentioned leaching liquor with ether is extracted, obtains extract liquor;
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is eluted with a concentration of 20% ethanol water, Obtain first order eluent;
D, above-mentioned first order eluent is chromatographed by the use of the Silon of 200 mesh as adsorbent, then with 2% aqueous acetic acid Elution, obtains second level eluent;
E, above-mentioned second level eluent is recrystallized twice with ethyl alcohol, to get the fig bark extract after drying;
(2)By above-mentioned 100 parts by weight of fig bark extract, 0.5 parts by weight of ginseng pulverate, 0.02 parts by weight of licorice powder, citric acid 0.02 parts by weight of sodium, 0.6 parts by weight of vitamin A, 0.3 parts by weight of vitamin E, 3 parts by weight of vitamin C, 0.2 weight of vitamin D Part is mixed evenly, up to the fig skin antioxidant after drying.
The foregoing is only a preferred embodiment of the present invention, therefore cannot limit the range that the present invention is implemented according to this, i.e., According to the equivalent changes and modifications that the scope of the claims of the present invention and description are made, all should still belong in the range of the present invention covers.

Claims (4)

1. a kind of fig skin antioxidant, it is characterised in that:Include the component of following parts by weight:
Fig bark extract 90-100 parts by weight
Ginseng pulverate's 0.3-0.5 parts by weight
Licorice powder 0.01-0.02 parts by weight
Sodium citrate 0.01-0.02 parts by weight
Vitamin A 0.4-0.6 parts by weight
Vitamin E 0.1-0.3 parts by weight
Vitamin C 1-3 parts by weight
Vitamin D 0.1-0.2 parts by weight
The extracting method of above-mentioned fig bark extract is as follows:
A, net will be sieved with 100 mesh sieve after above-mentioned fig skin drying and crushing and adds in ethanol water in 50-60 DEG C of heat reflux extraction 20- 30 minutes, and filter, obtain leaching liquor;
B, above-mentioned leaching liquor with ether is extracted, obtains extract liquor;
C, above-mentioned extract liquor is subjected to column chromatography, then the ethanol aqueous wash with a concentration of 10-20% with PEG 20000 column It is de-, obtain first order eluent;
D, above-mentioned first order eluent by the use of Silon as adsorbent is chromatographed, then is eluted with aqueous acetic acid, obtain Two level eluent;
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the fig bark extract after drying.
2. a kind of preparation method of fig skin antioxidant described in claim 1, it is characterised in that:Including walking as follows Suddenly:
(1)By fig skin successively through ethanol water heat reflux extraction, ether extraction, PEG 20000 column chromatography, polyamides After the analysis of amine bisque, eluant ethanol recrystallization and drying, the fig bark extract is made, which includes the following steps:
A, ethanol water will be added in after above-mentioned fig skin drying and crushing to extract 20-30 minutes, and mistake in 50-60 DEG C of heat reflux Filter, obtains leaching liquor;
B, above-mentioned leaching liquor with ether is extracted, obtains extract liquor;
C, above-mentioned extract liquor is subjected to column chromatography, then the ethanol aqueous wash with a concentration of 10-20% with PEG 20000 column It is de-, obtain first order eluent;
D, above-mentioned first order eluent by the use of Silon as adsorbent is chromatographed, then is washed with the mixed liquor of aqueous acetic acid It is de-, obtain second level eluent;
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the fig bark extract after drying;
(2)By above-mentioned fig bark extract 90-100 parts by weight, ginseng pulverate's 0.3-0.5 parts by weight, licorice powder 0.01-0.02 weights Measure part, sodium citrate 0.01-0.02 parts by weight, vitamin A 0.4-0.6 parts by weight, vitamin E 0.1-0.3 parts by weight, vitamin C1-3 parts by weight, vitamin D 0.1-0.2 parts by weight are mixed evenly, up to the anti-oxidant addition of fig skin after drying Agent.
3. a kind of preparation method of fig skin antioxidant as claimed in claim 2, it is characterised in that:The step (1)Step a in, a concentration of 20-30% of ethanol water, the ethanol water total weight be drying and crushing after fig 2-3 times of tare weight amount.
4. a kind of preparation method of fig skin antioxidant as claimed in claim 2, it is characterised in that:The step (1)Step d in, the Silon be 200 mesh, a concentration of 1-2% of the aqueous acetic acid.
CN201611096151.7A 2016-12-02 2016-12-02 A kind of fig skin antioxidant and preparation method thereof Pending CN108142776A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611096151.7A CN108142776A (en) 2016-12-02 2016-12-02 A kind of fig skin antioxidant and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611096151.7A CN108142776A (en) 2016-12-02 2016-12-02 A kind of fig skin antioxidant and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108142776A true CN108142776A (en) 2018-06-12

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109042841A (en) * 2018-08-06 2018-12-21 湖北文理学院 A kind of protective agent and Cryopreservation for fruits and vegetables
CN110537658A (en) * 2019-02-27 2019-12-06 湖北文理学院 preparation method of blueberry sesame powder antioxidant additive

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109042841A (en) * 2018-08-06 2018-12-21 湖北文理学院 A kind of protective agent and Cryopreservation for fruits and vegetables
CN110537658A (en) * 2019-02-27 2019-12-06 湖北文理学院 preparation method of blueberry sesame powder antioxidant additive

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Application publication date: 20180612