CN108130731A - A kind of polyester filament spinning oil and preparation method thereof - Google Patents

A kind of polyester filament spinning oil and preparation method thereof Download PDF

Info

Publication number
CN108130731A
CN108130731A CN201711344595.2A CN201711344595A CN108130731A CN 108130731 A CN108130731 A CN 108130731A CN 201711344595 A CN201711344595 A CN 201711344595A CN 108130731 A CN108130731 A CN 108130731A
Authority
CN
China
Prior art keywords
parts
polyester filament
spinning oil
filament spinning
minutes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711344595.2A
Other languages
Chinese (zh)
Inventor
储平
徐有琦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu New Lucky Polytron Technologies Inc
Original Assignee
Jiangsu New Lucky Polytron Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu New Lucky Polytron Technologies Inc filed Critical Jiangsu New Lucky Polytron Technologies Inc
Priority to CN201711344595.2A priority Critical patent/CN108130731A/en
Publication of CN108130731A publication Critical patent/CN108130731A/en
Pending legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402Amides imides, sulfamic acids
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • D06M13/148Polyalcohols, e.g. glycerol or glucose
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/256Sulfonated compounds esters thereof, e.g. sultones
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/282Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
    • D06M13/292Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of polyester filament spinning oil and preparation method thereof, the polyester filament is made of with spinning oil the raw material of following parts by weight:57 parts of lauric acid diethyl amide, 35 parts of neopelex, 5 10 parts of glycerine, 13 parts of octyl phosphate, 57 parts of nano-powder, 13 parts of dispersant, 10 20 parts of ethyl alcohol, 13 parts of sodium secondary alkyl sulfonate, 24 parts of dimethyl silicone polymer, 35 parts of sorbitan fatty acid ester, 10 20 parts of deionized water.The polyester filament of the present invention is stablized with spinning oil property, safe and harmless, and preparation process is energy saving, at low cost.

Description

A kind of polyester filament spinning oil and preparation method thereof
Technical field
The invention belongs to field of fabric producing technology, specifically relate to a kind of polyester filament spinning oil and its preparation side Method.
Background technology
Natural fiber is the basic material of textile industry by the chemical fibre that extrusion obtains.Strand and fiber add rear Different mechanical force and thermal stress are subjected to during work.In order to ensure fiber is injury-free in this process, squeezed out in fiber It should oil immediately after forming.
After dacron product is by monomer polymerization in spinning process, spinning oil can be adjusted between fiber and fiber, fiber Frictional property between metal, reduce friction coefficient, reduce because friction generate electrostatic, make fiber have good convergence, Flatness and fiber separation meet the relevant needs of fiber post-processing.
At present, some conventional spinning oils in the market use process can occur seriously to smolder, coking, lousiness, broken end, The problems such as polluting workshop condition.So it is urgent problem to need to find a kind of spinning oil efficiently, environmentally friendly.
Invention content
The purpose of the present invention is to provide a kind of polyester filament spinning oil and preparation method thereof, to solve above-mentioned background The problem of being proposed in technology.
To achieve the above object, the present invention provides following technical solution:
A kind of polyester filament spinning oil, according to parts by weight, including following components:Lauric acid diethyl amide 5-7 Part, 3-5 parts of neopelex, 5-10 parts of glycerine, 1-3 parts of octyl phosphate, 5-7 parts of nano-powder, dispersant 1-3 Part, 10-20 parts of ethyl alcohol, 1-3 parts of sodium secondary alkyl sulfonate, 2-4 parts of dimethyl silicone polymer, 3-5 parts of sorbitan fatty acid ester, 10-20 parts of deionized water.
Preferably, the nano-powder is one or more than one kinds of in kaolin, diatomite, sepiolite powder.
Preferably, the ethyl alcohol is absolute ethyl alcohol, rank is that analysis is pure.
Preferably, the grain size of the nano-powder is 5-50nm.
Preferably, the dispersant is one in triethanolamine, calgon, polyethylene glycol, sodium cellulose xanghate Kind or more than one.
Preferably, the preparation method of the polyester filament spinning oil, specific steps include:
Step 1,10-20 parts of deionized water, 50-60 DEG C of oil bath heating are added in a kettle;
Step 2,5-7 parts of lauric acid diethyl amide, 3-5 parts of neopelex, 5-10 parts of glycerine, octyl group are added in 1-3 parts of phosphate, stirs 20-30 minutes by 500-1000 revs/min;
Step 3, first by 10-20 parts of 5-7 parts of nano-powder, 1-3 parts of dispersant, ethyl alcohol progress ultrasonic disperses, ultrasonic power For 500-800W, ultrasonic time is 10-20 minutes;
Step 4, temperature is reduced to 20-30 DEG C, the solution of step 3 is poured into the solution of step 2,500-1000 revs/min Clock stirs 20-30 minutes;
Step 5,1-3 parts of sodium secondary alkyl sulfonate of addition, 3-5 parts of sorbitan fatty acid ester, 500-1000 revs/min, Stirring 30-40 minutes;
Step 6,2-4 parts of dimethyl silicone polymer is added in, 500-1000 revs/min, is stirred 10-20 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, polyester filament of the invention is stablized with spinning oil property, safe and harmless, and preparation process is energy saving, cost It is low.
2nd, it is equal with good spinnability, flatness, coherent after polyester filament of the invention is applied with spinning oil Well, no lousiness, end breakage rate is low, and waste silk rate is low.
3rd, after polyester filament of the invention is applied with spinning oil in spinning process, smoke is few, noncoking carbonization, nothing Pollution.
4th, mutual compatibility, synergistic effect between various raw materials used in polyester filament spinning oil of the invention, common group Into the product haveing excellent performance.
5th, simplify technique, safe operation is simple, is easy to industrialized production.
6th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of polyester filament spinning oil, according to parts by weight, including following components:Lauric acid two 5-7 parts of glycollic amide, 3-5 parts of neopelex, 5-10 parts of glycerine, 1-3 parts of octyl phosphate, 5-7 parts of nano-powder, 1-3 parts of dispersant, 10-20 parts of ethyl alcohol, 1-3 parts of sodium secondary alkyl sulfonate, 2-4 parts of dimethyl silicone polymer, sorbitan fatty 3-5 parts of acid esters, 10-20 parts of deionized water.
The present invention also provides a kind of preparation method of polyester filament spinning oil, specific steps include:
Step 1,10-20 parts of deionized water, 50-60 DEG C of oil bath heating are added in a kettle;
Step 2,5-7 parts of lauric acid diethyl amide, 3-5 parts of neopelex, 5-10 parts of glycerine, octyl group are added in 1-3 parts of phosphate, stirs 20-30 minutes by 500-1000 revs/min;
Step 3, first by 10-20 parts of 5-7 parts of nano-powder, 1-3 parts of dispersant, ethyl alcohol progress ultrasonic disperses, ultrasonic power For 500-800W, ultrasonic time is 10-20 minutes;
Step 4, temperature is reduced to 20-30 DEG C, the solution of step 3 is poured into the solution of step 2,500-1000 revs/min Clock stirs 20-30 minutes;
Step 5,1-3 parts of sodium secondary alkyl sulfonate of addition, 3-5 parts of sorbitan fatty acid ester, 500-1000 revs/min, Stirring 30-40 minutes;
Step 6,2-4 parts of dimethyl silicone polymer is added in, 500-1000 revs/min, is stirred 10-20 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 1
The invention discloses a kind of polyester filament spinning oil, according to parts by weight, including following components:Lauric acid two 5 parts of glycollic amide, 3 parts of neopelex, 5 parts of glycerine, 1 part of octyl phosphate, 5 parts of nano-powder, 1 part of dispersant, 10 parts of ethyl alcohol, 1 part of sodium secondary alkyl sulfonate, 2 parts of dimethyl silicone polymer, 3 parts of sorbitan fatty acid ester, deionized water 10 Part.
The present invention also provides a kind of preparation method of polyester filament spinning oil, specific steps include:
Step 1,10 parts of deionized water, 50 DEG C of oil bath heating are added in a kettle;
Step 2,5 parts of lauric acid diethyl amide, 3 parts of neopelex, 5 parts of glycerine, octyl phosphate 1 are added in Part, it 500 revs/min, stirs 20 minutes;
Step 3, first by 5 parts of nano-powder, 1 part of dispersant, 10 parts of ethyl alcohol progress ultrasonic disperses, ultrasonic power 500W, Ultrasonic time is 10 minutes;
Step 4, temperature is reduced to 20 DEG C, the solution of step 3 is poured into the solution of step 2,500 revs/min, stirring 20 Minute;
Step 5,1 part of sodium secondary alkyl sulfonate, 3 parts of sorbitan fatty acid ester are added in, 500 revs/min, stirs 30 points Clock;
Step 6,2 parts of dimethyl silicone polymer is added in, 500 revs/min, is stirred 10 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 2
The invention discloses a kind of polyester filament spinning oil, according to parts by weight, including following components:Lauric acid two 6 parts of glycollic amide, 4 parts of neopelex, 8 parts of glycerine, 2 parts of octyl phosphate, 6 parts of nano-powder, 2 parts of dispersant, 15 parts of ethyl alcohol, 2 parts of sodium secondary alkyl sulfonate, 3 parts of dimethyl silicone polymer, 4 parts of sorbitan fatty acid ester, deionized water 15 Part.
The present invention also provides a kind of preparation method of polyester filament spinning oil, specific steps include:
Step 1,15 parts of deionized water, 55 DEG C of oil bath heating are added in a kettle;
Step 2,6 parts of lauric acid diethyl amide, 4 parts of neopelex, 8 parts of glycerine, octyl phosphate 2 are added in Part, it 800 revs/min, stirs 25 minutes;
Step 3, first by 6 parts of nano-powder, 2 parts of dispersant, 15 parts of ethyl alcohol progress ultrasonic disperses, ultrasonic power 700W, Ultrasonic time is 15 minutes;
Step 4, temperature is reduced to 25 DEG C, the solution of step 3 is poured into the solution of step 2,800 revs/min, stirring 25 Minute;
Step 5,2 parts of sodium secondary alkyl sulfonate, 4 parts of sorbitan fatty acid ester are added in, 800 revs/min, stirs 35 points Clock;
Step 6,3 parts of dimethyl silicone polymer is added in, 800 revs/min, is stirred 15 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 3
The invention discloses a kind of polyester filament spinning oil, according to parts by weight, including following components:Lauric acid two 7 parts of glycollic amide, 5 parts of neopelex, 10 parts of glycerine, 3 parts of octyl phosphate, 7 parts of nano-powder, 3 parts of dispersant, 20 parts of ethyl alcohol, 3 parts of sodium secondary alkyl sulfonate, 4 parts of dimethyl silicone polymer, 5 parts of sorbitan fatty acid ester, deionized water 20 Part.
The present invention also provides a kind of preparation method of polyester filament spinning oil, specific steps include:
Step 1,20 parts of deionized water, 60 DEG C of oil bath heating are added in a kettle;
Step 2,7 parts of lauric acid diethyl amide, 5 parts of neopelex, 10 parts of glycerine, octyl phosphate are added in It 3 parts, 1000 revs/min, stirs 30 minutes;
Step 3, first by 7 parts of nano-powder, 3 parts of dispersant, 20 parts of ethyl alcohol progress ultrasonic disperses, ultrasonic power 800W, Ultrasonic time is 10 minutes;
Step 4, temperature is reduced to 20 DEG C, the solution of step 3 is poured into the solution of step 2,800 revs/min, stirring 25 Minute;
Step 5,3 parts of sodium secondary alkyl sulfonate, 5 parts of sorbitan fatty acid ester are added in, 900 revs/min, stirs 30 points Clock;
Step 6,4 parts of dimethyl silicone polymer is added in, 1000 revs/min, is stirred 10 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Embodiment 4
The invention discloses a kind of polyester filament spinning oil, according to parts by weight, including following components:Lauric acid two 7 parts of glycollic amide, 5 parts of neopelex, 8 parts of glycerine, 1 part of octyl phosphate, 7 parts of nano-powder, 3 parts of dispersant, 20 parts of ethyl alcohol, 1 part of sodium secondary alkyl sulfonate, 4 parts of dimethyl silicone polymer, 3 parts of sorbitan fatty acid ester, deionized water 20 Part.
The present invention also provides a kind of preparation method of polyester filament spinning oil, specific steps include:
Step 1,20 parts of deionized water, 55 DEG C of oil bath heating are added in a kettle;
Step 2,7 parts of lauric acid diethyl amide, 5 parts of neopelex, 8 parts of glycerine, octyl phosphate 1 are added in Part, it 800 revs/min, stirs 20 minutes;
Step 3, first by 7 parts of nano-powder, 3 parts of dispersant, 20 parts of ethyl alcohol progress ultrasonic disperses, ultrasonic power 800W, Ultrasonic time is 20 minutes;
Step 4, temperature is reduced to 30 DEG C, the solution of step 3 is poured into the solution of step 2,800 revs/min, stirring 25 Minute;
Step 5,1 part of sodium secondary alkyl sulfonate, 3 parts of sorbitan fatty acid ester are added in, 900 revs/min, stirs 30 points Clock;
Step 6,4 parts of dimethyl silicone polymer is added in, 800 revs/min, is stirred 10 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation is made Finished product.
Test case
Polyester filament is handled using the polyester filament spinning oil of embodiment 1,2,3,4, test result is as follows:
The above-mentioned various embodiments enumerated, under the premise of reconcilable, can be combined with each other implementation, those skilled in the art It can combine above to the explanation of embodiment, as the foundation being combined to the technical characteristic in different embodiments.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of polyester filament spinning oil, it is characterised in that:The polyester filament includes following parts by weight with spinning oil Several raw materials:5-7 parts of lauric acid diethyl amide, 3-5 parts of neopelex, 5-10 parts of glycerine, octyl phosphate 1-3 Part, 5-7 parts of nano-powder, 1-3 parts of dispersant, 10-20 parts of ethyl alcohol, 1-3 parts of sodium secondary alkyl sulfonate, dimethyl silicone polymer 2-4 Part, 3-5 parts of sorbitan fatty acid ester, 10-20 parts of deionized water.
2. polyester filament spinning oil according to claim 1, it is characterised in that:The nano-powder is kaolinite It is one or more than one kinds of in soil, diatomite, sepiolite powder.
3. polyester filament spinning oil according to claim 1, it is characterised in that:The ethyl alcohol for absolute ethyl alcohol, Rank is pure to analyze.
4. polyester filament spinning oil according to claim 1, it is characterised in that:The grain size of the nano-powder is 5-50nm。
5. polyester filament spinning oil according to claim 1, it is characterised in that:The dispersant is three ethyl alcohol It is one or more than one kinds of in amine, calgon, polyethylene glycol, sodium cellulose xanghate.
6. a kind of preparation method using any one of the claims 1-5 polyester filament spinning oils, feature It is:Specific steps include:
Step 1,10-20 parts of deionized water, 50-60 DEG C of oil bath heating are added in a kettle;
Step 2,5-7 parts of lauric acid diethyl amide, 3-5 parts of neopelex, 5-10 parts of glycerine, octylphosphonic acid are added in 1-3 parts of ester, stirs 20-30 minutes by 500-1000 revs/min;
Step 3, first by 10-20 parts of 5-7 parts of nano-powder, 1-3 parts of dispersant, ethyl alcohol progress ultrasonic disperses, ultrasonic power is 500-800W, ultrasonic time are 10-20 minutes;
Step 4, temperature is reduced to 20-30 DEG C, the solution of step 3 is poured into the solution of step 2,500-1000 revs/min, stirred It mixes 20-30 minutes;
Step 5,1-3 parts of sodium secondary alkyl sulfonate, 3-5 parts of sorbitan fatty acid ester are added in, 500-1000 revs/min, is stirred 30-40 minutes;
Step 6,2-4 parts of dimethyl silicone polymer is added in, 500-1000 revs/min, is stirred 10-20 minutes;
Step 7, stirring is shut down, obtains prepared liquid polyester filament spinning oil;
Step 8, it stands and is cooled in reaction kettle liquid polyester filament spinning oil and is less than 20 DEG C, blowing encapsulation, finished product.
CN201711344595.2A 2017-12-15 2017-12-15 A kind of polyester filament spinning oil and preparation method thereof Pending CN108130731A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711344595.2A CN108130731A (en) 2017-12-15 2017-12-15 A kind of polyester filament spinning oil and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711344595.2A CN108130731A (en) 2017-12-15 2017-12-15 A kind of polyester filament spinning oil and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108130731A true CN108130731A (en) 2018-06-08

Family

ID=62389462

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711344595.2A Pending CN108130731A (en) 2017-12-15 2017-12-15 A kind of polyester filament spinning oil and preparation method thereof

Country Status (1)

Country Link
CN (1) CN108130731A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109957861A (en) * 2019-02-28 2019-07-02 常州凯途纺织品有限公司 A kind of heat-resisting oxidation-resistance spinning oil

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1811050A (en) * 2005-01-26 2006-08-02 上海巨人高科技新型材料有限公司 Nanometer polyester fiber FDY spinning oil prepn and its prepn process
CN101235592A (en) * 2008-03-07 2008-08-06 吴江市良燕纺织助剂厂 Terylene FDY nano spinning oil and preparation method thereof
CN104032570A (en) * 2014-06-27 2014-09-10 无锡市崇安区科技创业服务中心 Spinning oil and preparation method thereof
CN104674547A (en) * 2015-01-26 2015-06-03 海安巨丰化纤有限公司 Nano additive for spinning and oiling agent
CN104988722A (en) * 2015-07-13 2015-10-21 湖州宏鑫绸厂 Novel polyester fiber spinning oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1811050A (en) * 2005-01-26 2006-08-02 上海巨人高科技新型材料有限公司 Nanometer polyester fiber FDY spinning oil prepn and its prepn process
CN101235592A (en) * 2008-03-07 2008-08-06 吴江市良燕纺织助剂厂 Terylene FDY nano spinning oil and preparation method thereof
CN104032570A (en) * 2014-06-27 2014-09-10 无锡市崇安区科技创业服务中心 Spinning oil and preparation method thereof
CN104674547A (en) * 2015-01-26 2015-06-03 海安巨丰化纤有限公司 Nano additive for spinning and oiling agent
CN104988722A (en) * 2015-07-13 2015-10-21 湖州宏鑫绸厂 Novel polyester fiber spinning oil

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109957861A (en) * 2019-02-28 2019-07-02 常州凯途纺织品有限公司 A kind of heat-resisting oxidation-resistance spinning oil

Similar Documents

Publication Publication Date Title
CN100385061C (en) Nanometer polyester fiber FDY spinning oil prepn and its prepn process
CN103469571B (en) A kind of water soluble vinylon finish and manufacture method thereof
CN101230541A (en) Hemp softening oil, preparation method and use thereof
CN111691013A (en) Polyester spinning oil and preparation method thereof
CN105885355A (en) High-heat-resistance insulating composite and preparation method thereof
CN103757899A (en) General grade pitch-based carbon fiber spinning oil
CN108130731A (en) A kind of polyester filament spinning oil and preparation method thereof
CN108624995A (en) A kind of preparation method of polyamide spinning finisher
CN111501338B (en) Efficient preparation process of DTY elasticizing auxiliary agent composite material
CN109309186A (en) A kind of PVDF diaphragm and preparation method thereof
CN108252087A (en) A kind of ultra-fine yarn spinning oil agent and preparation method thereof
CN103061119B (en) Oiling agent used for cotton fiber
CN115746939B (en) Preparation method of biodegradable environment-friendly lubricant
CN112458570A (en) Graphene latex yarn with high mechanical property and preparation method thereof
CN105482029A (en) Energy saving and environmental protection bio-based aqueous emulsion polymer and preparation method thereof
CN105625034A (en) Dipping liquid used for preparing nanoscale semiconductive non-woven fabric
CN111764171A (en) Phosphorus-boron compound after-finishing anti-dripping polyester fabric based on polydopamine surface modification and preparation method thereof
CN108035152A (en) A kind of spinning sizing agent and preparation method thereof
CN106734269A (en) Hexagon stainless steel profile shapes production method and products thereof
CN112852387A (en) Phase change material and preparation method and application thereof
CN1035781C (en) Ramie Oil
CN101775665B (en) Low-alkali degumming process for hemp plants at room temperature
CN108252126A (en) A kind of low temperature dyeing accelerant and preparation method thereof
CN105887246B (en) A kind of cement products vinal spinning oil
CN108035149A (en) A kind of environment-friendly type polyacrylic fibre oil and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180608