CN108125882A - Strong root strengthen the hair phytoremediation element and preparation method thereof - Google Patents
Strong root strengthen the hair phytoremediation element and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to a kind of strong root strengthen the hair phytoremediation element and preparation method thereof, the strong root strengthen the hair phytoremediation element is prepared from the following materials：Glycerine, cetostearyl alcohol, hydrolyzed wheat protein, panthenol, Cacumen Platycladi extract, ginger-root extract, EDETATE SODIUM, essence, methylisothiazolinone, conditioner for hair, water.Strong root strengthen the hair phytoremediation element of the invention and preparation method thereof, using practical value and functional component as index, it studies under Different Preparation parameter, the variation of strong root strengthen the hair phytoremediation element practical value and functional component index, so as to work out the optimum process condition of strong root strengthen the hair phytoremediation element；Ingredient in formula complements each other, and can nourish moisturizing hair comprehensively, repairs damaged hair, supplements nutrition needed for hair follicle, strong root strengthen the hair makes hair comprehensively be improved, smooth soft bright, high resilience.
Description
Technical field
The present invention relates to a kind of hairs to repair element, specifically, being related to a kind of strong root strengthen the hair phytoremediation element and its preparing
Method.
Background technology
In today of 21st century, beautiful and maintenance is as the mainstream of society, and the simple dust for dispelling hair is
It is not basic demand of the people to hair, possesses the pursuit that a pitch-black, beautiful hair is many people that like to be beautiful, therefore clear
The reparation to the hair for moistening, protecting and being damaged of hair can be reached while clean, hair is made to lock moisture, keep elasticity
And nutrition is the target that people pursue jointly.
Contain about 15% moisture in our hair, but if less than 10%, hair will be dried, is easily broken, present
The phenomenon that going out electrostatic.The most important composition of hair is protein, fiber, has some gaps between fiber and fibre bundle, in gap
The natural moisturizing factor of moisture can be absorbed by being covered with.Moisturizing factor in hair is more, and hair moisture is more sufficient, and hair is just more soft
It is soft, it is more flexible.Instead if lacking moisture between the fiber of hair, hair just will appear withered, water shortage, it is short-tempered, harden, easily
The disconnected, symptoms such as scalp is fuel-displaced, this is also increasingly severe to annoying people.
The hair generally existing problems with of people：By air environment influenced and hair-waving, hair dyeing increased popularity, people
Hair there are different degrees of damages and very universal；Chemical composition in hair-waving liquid medicine can suffer the scale on hair surface layer
To destroying, coming off, hair internal structure is made to be in unprotect state, moisture and nutrient loss, keratoprotein occur denaturation,
It loses, hair is made easily to turn to be yellow, embrittlement, lackluster, no elasticity, the influence of coarse overhauling, in addition air environment, hair
It damages serious and universal.Due to root of hair and hair malnutrition, root of hair forms embolism, influences the nutrition of hair follicle, make hair follicle gradual
Atrophy damages, and then hair is tapered, dry even become fragile comes off.As hair lengths increase, hair scale piece cellular portions
It comes off, hair compliance is deteriorated, and is easy to distort, and causes combing and hair knotting and fracture easily occurs in washing process.
Hair conditioner is also known as Rinsing, is generally used in pairs with shampoo, is uniformly applied to appropriate hair conditioner on hair after hair washing,
It gently rubs one minute or so, then with clear water rinsed clean, therefore also someone is known as rinsing conditioner, belongs to hair cosmetic.
We are mainly made of common hair conditioner cationic surfactant, conditioner and chelating agent, this kind of chemistry
Formulation products are more smooth often at that time with rear pretty good, but hair do after be still crude, lackluster, and cleaning-free hair conditioner
Only possess anti-static function, can only be formed and protected in hair surface, root of hair can not be goed deep at all, conserve damaged hair.And this
Class hair conditioner is only used for the submissive effect of the hair tip, and the fat secretion balance of hair follicle can be influenced in the use of root of hair, causes hair
Capsule secretion grease is vigorous, makes the fuel-displaced serious even hair of hair and influences the normal life of people, it is impossible to really play reparation
The effect of hair
Invention content
The technical problem to be solved in the present invention is to provide a kind of phytoremediation elements for having strong root strengthen the hair.The present invention is to pass through
Following technical scheme is realized：The strong root strengthen the hair phytoremediation element of the present invention, is prepared from the following materials：Glycerine, spermaceti
Stearyl alcohol, hydrolyzed wheat protein, panthenol, Cacumen Platycladi extract, ginger-root extract, EDETATE SODIUM, essence, methylisothiozoline
Ketone, conditioner for hair, water.
Preferably, the strong root strengthen the hair phytoremediation element, is prepared by the raw material of following mass percent：5-15%
Glycerine, 2-7% cetostearyl alcohols, 0.5-3% hydrolyzed wheat proteins, 0.2-0.6% panthenols, 0.5-3% Cacumen Platycladi extracts,
0.5-3% ginger-root extracts, 0.05-0.25%EDTA disodiums, 0.5-2% essence, 0.0005-0.0015% methylisothiozolines
Ketone, 0.5-1.5% conditioner for hair, surplus are water.
The essence is citrus type essence, mint type essence, beans flavor essence, milk flavoured type essence, lemon type essence, vegetables
It is one or more in type essence.
The conditioner for hair is guar hydroxypropyltrimonium chloride and/or chitosan quaternary ammonium salt.In the present invention one
In a embodiment, the conditioner for hair is gathered by 70-80wt% guar hydroxypropyltrimonium chlorides and 20-30wt% shells
Sugared quaternary ammonium salt composition.
The preparation method of the hydrolyzed wheat protein is：By wheat crushing to 30-80 mesh, wheat flour is obtained；By wheat flour
It is 1 to press solid-liquid ratio with water：(5-15) is mixed, and pH to 8-12,35-55 are adjusted with the sodium hydrate aqueous solution of 0.05-0.15mol/L
Water-bath stirs 40-80min by 100-300r/min of rotating speed at DEG C, centrifuges, abandons precipitation, obtain supernatant；Use 0.05-
The salt acid for adjusting pH of 0.15mol/L adds in supernatant quality 0.1-0.4% glucose oxidases, supernatant to 5-6 to supernatant
Quality 0.2-0.6% ficins are 30-50 DEG C in temperature and enzymolysis 50- are carried out by 100-300r/min of rotating speed
Then temperature is risen to 85-95 DEG C and 5-15min enzyme deactivations is kept to live, obtains hydrolyzate by 120min；It is dry that hydrolyzate is subjected to spraying
It is dry to get hydrolyzed wheat protein.
Further, the preparation method of the hydrolyzed wheat protein is：By wheat crushing to 30-80 mesh, wheat flour is obtained；
It is 1 that wheat flour and water are pressed solid-liquid ratio：(5-15) is mixed, and pH to 8- is adjusted with the sodium hydrate aqueous solution of 0.05-0.15mol/L
Water-bath stirs 40-80min by 100-300r/min of rotating speed at 12,35-55 DEG C, centrifuges, abandons precipitation, obtain supernatant；
With the salt acid for adjusting pH of 0.05-0.15mol/L to 5-6, it is glycoxidative to add in supernatant quality 0.1-0.4% grapes to supernatant
Enzyme, supernatant quality 0.2-0.6% ficins, being 30-50 DEG C in temperature, progress is red by 100-300r/min of rotating speed
Then temperature is risen to 85-95 DEG C and 5-15min enzyme deactivations is kept to live, obtains hydrolyzate by outer assistance enzymolysis 50-120min；It will hydrolysis
Liquid is spray-dried to get hydrolyzed wheat protein.
The infrared power of the infrared assistance enzymolysis is 150-250W, infrared radiation distance is 2-5cm, radiation modality is photograph
It penetrates 2-4min stopping 2-4min and then irradiates 2-4min again and stop 2-4min successively alternately.
The condition of the spray drying is that inlet air temperature is 175-185 DEG C, intake velocity 25-35m3/ h, charging rate
For 5-7mL/min, temperature of outgoing air is 75-85 DEG C.
The rotating speed of the centrifugation is 5000-8000r/min, time 15-25min.
The preparation method of above-mentioned strong root strengthen the hair phytoremediation element, includes the following steps：
(1) it adds water in water phase pot, adds in conditioner for hair, be uniformly mixed, sequentially add EDETATE SODIUM, water
Solution wheat gluten, panthenol, Cacumen Platycladi extract, ginger-root extract are uniformly mixed, and are warming up to 80-90 DEG C, are obtained water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 80-90 DEG C, be uniformly mixed, obtained
Oil phase material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, homogeneous 3-13 minutes at 60-90 DEG C,
Then 15-25 minutes are kept the temperature, be eventually adding essence, methylisothiazolinone is uniformly mixed to obtain the final product.
Compared with prior art, the present invention has the advantages that following prominent and effect：
Strong root strengthen the hair phytoremediation element of the invention and preparation method thereof, using practical value and functional component as index, research
Under Different Preparation parameter, the variation of strong root strengthen the hair phytoremediation element practical value and functional component index, so as to work out
The optimum process condition of strong root strengthen the hair phytoremediation element；Ingredient in formula complements each other, and can nourish moisturizing hair comprehensively, repairs
Damaged hair supplements nutrition needed for hair follicle, and strong root strengthen the hair makes hair comprehensively be improved, smooth soft bright, high resilience.
Specific embodiment
Below by specific embodiment, the present invention is further described.
Glycerine in embodiment, CAS：56-81-5.
Cetostearyl alcohol in embodiment is provided, model 1670 by 100,000 Chemical Co., Ltd. of Shandong.
Panthenol in embodiment, CAS：81-13-0.
Cacumen Platycladi extract in embodiment is provided, withdrawal ratio 10 by Shaanxi Teng Mai biotechnologies Co., Ltd：
1 (extracting to obtain 1g Cacumen Platycladi extracts per 10g cacumen biotaes).
Ginger-root extract in embodiment is provided, withdrawal ratio 10 by Shaanxi Hui Ke plants development corporation, Ltd.：1 is (i.e. every
10g cacumen biotaes extract to obtain 1g Cacumen Platycladi extracts).
EDETATE SODIUM in embodiment, CAS：139-33-3.
Lemon extract in embodiment is provided by Hangzhou Berry essence and flavoring agent Co., Ltd, and appearance is powder.
Methylisothiazolinone in embodiment, CAS：2682-20-4.
Guar hydroxypropyltrimonium chloride is provided by Hubei Yuancheng Saichuang Technology Co., Ltd. in embodiment.
Chitosan quaternary ammonium salt in embodiment, also known as hydroxypropyltrimethylammonium chloride chitosan, by the macro bright chemical reagent in Jining
Co., Ltd provides.
Wheat is the small wheat kernel that Anhui Yanzhifang Food Co., Ltd provides in embodiment, and kind is barley.
Glucose oxidase is glycoxidative for the food-grade grape that one hundred emerging bio tech ltd of Wuhan provides in embodiment
Enzyme, enzyme activity are 100,000 U/g.
Ficin is the food-grade fig that Bei Nuoke bio tech ltd of Jining City provides in embodiment
Protease, enzyme activity are 100,000 U/g.
The infrared radiation source of infrared assistance enzymolysis is infrared ray bulb in embodiment, by Haining City Qiyi Illumination Appliances Co., Ltd
It provides, wave-length coverage：1.72-16.66μm.
Embodiment 1
Strong root strengthen the hair phytoremediation element, is prepared by the raw material of following mass percent：10% glycerine, 5% spermaceti are hard
Lipidol, 2.5% hydrolyzed wheat protein, 0.4% panthenol, 2.5% Cacumen Platycladi extract, 2% ginger-root extract, 0.15%EDTA bis-
Sodium, 0.8% lemon extract, 0.001% methylisothiazolinone, 1% guar hydroxypropyltrimonium chloride, surplus for go from
Sub- water.
The preparation method of the hydrolyzed wheat protein is：By wheat crushing to 60 mesh, wheat flour is obtained；By 100g wheat flours
Be stirred 5min by 300r/min of rotating speed with 1000g deionizations, with the sodium hydrate aqueous solution of 0.1mol/L adjust pH to
Water-bath stirs 60min by 150r/min of rotating speed at 9.5,45 DEG C, centrifuges 20min by 6000r/min of rotating speed, it is heavy to abandon
It forms sediment, obtains supernatant；With the salt acid for adjusting pH of 0.1mol/L to 5.5,0.25% glucose of supernatant quality is added in supernatant
Oxidizing ferment, 0.4% ficin of supernatant quality be 35 DEG C in temperature and enzymolysis 60min carried out by 150r/min of rotating speed,
Then temperature is risen to 93 DEG C keeps 10min enzyme deactivations to live, and obtains hydrolyzate；Hydrolyzate is spray-dried small to get hydrolyzing
Aleuronat.Wherein, it is 180 DEG C that the condition of the spray drying, which is inlet air temperature, intake velocity 30m3/ h, charging rate are
6mL/min, temperature of outgoing air are 80 DEG C.
The preparation method of above-mentioned strong root strengthen the hair phytoremediation element, includes the following steps：
(1) deionized water is added in into the homogeneous emulsifying machine (type provided using Guangzhou Ju Tao mechanical equipments Co., Ltd
Number be JT-B-150 vacuum homogeneous emulsifying machine) water phase pot in, add in guar hydroxypropyltrimonium chloride, using rotating speed as
60r/min stirrings 5min is uniformly mixed, and sequentially adds EDETATE SODIUM, hydrolyzed wheat protein, panthenol, Cacumen Platycladi extract, ginger
Root extract stirs 15min as 60r/min using rotating speed and is uniformly mixed, and is warming up to 85 DEG C, obtains water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 85 DEG C, stirred by 60r/min of rotating speed
15min is uniformly mixed, and obtains oil phase material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, using rotating speed as 3000r/ at 85 DEG C
Then min homogeneous 5 minutes keeps the temperature 10 minutes, be eventually adding essence, methylisothiazolinone is stirred by 60r/min of rotating speed
15min is uniformly mixed to obtain the final product.
Embodiment 2
Strong root strengthen the hair phytoremediation element, is prepared by the raw material of following mass percent：10% glycerine, 5% spermaceti are hard
Lipidol, 2.5% hydrolyzed wheat protein, 0.4% panthenol, 2.5% Cacumen Platycladi extract, 2% ginger-root extract, 0.15%EDTA bis-
Sodium, 0.8% lemon extract, 0.001% methylisothiazolinone, 1% guar hydroxypropyltrimonium chloride, surplus for go from
Sub- water.
The preparation method of the hydrolyzed wheat protein is：By wheat crushing to 60 mesh, wheat flour is obtained；By 100g wheat flours
Be stirred 5min by 300r/min of rotating speed with 1000g deionizations, with the sodium hydrate aqueous solution of 0.1mol/L adjust pH to
Water-bath stirs 60min by 150r/min of rotating speed at 9.5,45 DEG C, centrifuges 20min by 6000r/min of rotating speed, it is heavy to abandon
It forms sediment, obtains supernatant；With the salt acid for adjusting pH of 0.1mol/L to 5.5,0.25% glucose of supernatant quality is added in supernatant
Oxidizing ferment, 0.4% ficin of supernatant quality are 35 DEG C in temperature and infrared auxiliary enzymes are carried out by 150r/min of rotating speed
60min is solved, temperature then is risen to 93 DEG C keeps 10min enzyme deactivations to live, and obtains hydrolyzate；Hydrolyzate is spray-dried, i.e.,
Obtain hydrolyzed wheat protein.Wherein, the infrared power of the infrared assistance enzymolysis is 200W, and infrared radiation distance is 3.5cm, is irradiated
Mode stops 3min and then irradiates 3min again to stop 3min successively alternately for irradiation 3min；The condition of the spray drying
Be inlet air temperature it is 180 DEG C, intake velocity 30m3/ h, charging rate 6mL/min, temperature of outgoing air are 80 DEG C.
The preparation method of above-mentioned strong root strengthen the hair phytoremediation element, includes the following steps：
(1) deionized water is added in into the homogeneous emulsifying machine (type provided using Guangzhou Ju Tao mechanical equipments Co., Ltd
Number be JT-B-150 vacuum homogeneous emulsifying machine) water phase pot in, add in guar hydroxypropyltrimonium chloride, using rotating speed as
60r/min stirrings 5min is uniformly mixed, and sequentially adds EDETATE SODIUM, hydrolyzed wheat protein, panthenol, Cacumen Platycladi extract, ginger
Root extract stirs 15min as 60r/min using rotating speed and is uniformly mixed, and is warming up to 85 DEG C, obtains water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 85 DEG C, stirred by 60r/min of rotating speed
15min is uniformly mixed, and obtains oil phase material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, using rotating speed as 3000r/ at 85 DEG C
Then min homogeneous 5 minutes keeps the temperature 10 minutes, be eventually adding essence, methylisothiazolinone is stirred by 60r/min of rotating speed
15min is uniformly mixed to obtain the final product.
Embodiment 3
Strong root strengthen the hair phytoremediation element, is prepared by the raw material of following mass percent：10% glycerine, 5% spermaceti are hard
Lipidol, 2.5% hydrolyzed wheat protein, 0.4% panthenol, 2.5% Cacumen Platycladi extract, 2% ginger-root extract, 0.15%EDTA bis-
Sodium, 0.8% lemon extract, 0.001% methylisothiazolinone, 1% guar hydroxypropyltrimonium chloride, surplus for go from
Sub- water.
The preparation method of the hydrolyzed wheat protein is：By wheat crushing to 60 mesh, wheat flour is obtained；By 100g wheat flours
Be stirred 5min by 300r/min of rotating speed with 1000g deionizations, with the sodium hydrate aqueous solution of 0.1mol/L adjust pH to
Water-bath stirs 60min by 150r/min of rotating speed at 9.5,45 DEG C, centrifuges 20min by 6000r/min of rotating speed, it is heavy to abandon
It forms sediment, obtains supernatant；With the salt acid for adjusting pH of 0.1mol/L to 5.5,0.4% fig egg of supernatant quality is added in supernatant
White enzyme is 35 DEG C in temperature and infrared assistance enzymolysis 60min is carried out by 150r/min of rotating speed, temperature then is risen to 93 DEG C of holdings
10min enzyme deactivations are lived, and obtain hydrolyzate；Hydrolyzate is spray-dried to get hydrolyzed wheat protein.Wherein, it is described infrared auxiliary
The infrared power for helping enzymolysis is 200W, and infrared radiation distance is 3.5cm, and radiation modality stops 3min, Ran Houzai for irradiation 3min
It irradiates 3min and stops 3min successively alternately；The condition of the spray drying is that inlet air temperature is 180 DEG C, and intake velocity is
30m3/ h, charging rate 6mL/min, temperature of outgoing air are 80 DEG C.
The preparation method of above-mentioned strong root strengthen the hair phytoremediation element, includes the following steps：
(1) deionized water is added in into the homogeneous emulsifying machine (type provided using Guangzhou Ju Tao mechanical equipments Co., Ltd
Number be JT-B-150 vacuum homogeneous emulsifying machine) water phase pot in, add in guar hydroxypropyltrimonium chloride, using rotating speed as
60r/min stirrings 5min is uniformly mixed, and sequentially adds EDETATE SODIUM, hydrolyzed wheat protein, panthenol, Cacumen Platycladi extract, ginger
Root extract stirs 15min as 60r/min using rotating speed and is uniformly mixed, and is warming up to 85 DEG C, obtains water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 85 DEG C, stirred by 60r/min of rotating speed
15min is uniformly mixed, and obtains oil phase material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, using rotating speed as 3000r/ at 85 DEG C
Then min homogeneous 5 minutes keeps the temperature 10 minutes, be eventually adding essence, methylisothiazolinone is stirred by 60r/min of rotating speed
15min is uniformly mixed to obtain the final product.
Embodiment 4
Strong root strengthen the hair phytoremediation element, is prepared by the raw material of following mass percent：10% glycerine, 5% spermaceti are hard
Lipidol, 2.5% hydrolyzed wheat protein, 0.4% panthenol, 2.5% Cacumen Platycladi extract, 2% ginger-root extract, 0.15%EDTA bis-
Sodium, 0.8% lemon extract, 0.001% methylisothiazolinone, 1% chitosan quaternary ammonium salt, surplus are deionized water.
The preparation method of the hydrolyzed wheat protein is：By wheat crushing to 60 mesh, wheat flour is obtained；By 100g wheat flours
Be stirred 5min by 300r/min of rotating speed with 1000g deionizations, with the sodium hydrate aqueous solution of 0.1mol/L adjust pH to
Water-bath stirs 60min by 150r/min of rotating speed at 9.5,45 DEG C, centrifuges 20min by 6000r/min of rotating speed, it is heavy to abandon
It forms sediment, obtains supernatant；With the salt acid for adjusting pH of 0.1mol/L to 5.5,0.25% glucose of supernatant quality is added in supernatant
Oxidizing ferment, 0.4% ficin of supernatant quality are 35 DEG C in temperature and infrared auxiliary enzymes are carried out by 150r/min of rotating speed
60min is solved, temperature then is risen to 93 DEG C keeps 10min enzyme deactivations to live, and obtains hydrolyzate；Hydrolyzate is spray-dried, i.e.,
Obtain hydrolyzed wheat protein.Wherein, the infrared power of the infrared assistance enzymolysis is 200W, and infrared radiation distance is 3.5cm, is irradiated
Mode stops 3min and then irradiates 3min again to stop 3min successively alternately for irradiation 3min；The condition of the spray drying
Be inlet air temperature it is 180 DEG C, intake velocity 30m3/ h, charging rate 6mL/min, temperature of outgoing air are 80 DEG C.
The preparation method of above-mentioned strong root strengthen the hair phytoremediation element, includes the following steps：
(1) deionized water is added in into the homogeneous emulsifying machine (type provided using Guangzhou Ju Tao mechanical equipments Co., Ltd
Number be JT-B-150 vacuum homogeneous emulsifying machine) water phase pot in, add in chitosan quaternary ammonium salt, using rotating speed for 60r/min stirring
5min is uniformly mixed, and sequentially adds EDETATE SODIUM, hydrolyzed wheat protein, panthenol, Cacumen Platycladi extract, ginger-root extract to turn
Speed stirs 15min for 60r/min and is uniformly mixed, and is warming up to 85 DEG C, obtains water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 85 DEG C, stirred by 60r/min of rotating speed
15min is uniformly mixed, and obtains oil phase material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, using rotating speed as 3000r/ at 85 DEG C
Then min homogeneous 5 minutes keeps the temperature 10 minutes, be eventually adding essence, methylisothiazolinone is stirred by 60r/min of rotating speed
15min is uniformly mixed to obtain the final product.
Embodiment 5
Strong root strengthen the hair phytoremediation element, is prepared by the raw material of following mass percent：10% glycerine, 5% spermaceti are hard
Lipidol, 2.5% hydrolyzed wheat protein, 0.4% panthenol, 2.5% Cacumen Platycladi extract, 2% ginger-root extract, 0.15%EDTA bis-
Sodium, 0.8% lemon extract, 0.001% methylisothiazolinone, 0.75% guar hydroxypropyltrimonium chloride, 0.25%
Chitosan quaternary ammonium salt, surplus are deionized water.
The preparation method of the hydrolyzed wheat protein is：By wheat crushing to 60 mesh, wheat flour is obtained；By 100g wheat flours
Be stirred 5min by 300r/min of rotating speed with 1000g deionizations, with the sodium hydrate aqueous solution of 0.1mol/L adjust pH to
Water-bath stirs 60min by 150r/min of rotating speed at 9.5,45 DEG C, centrifuges 20min by 6000r/min of rotating speed, it is heavy to abandon
It forms sediment, obtains supernatant；With the salt acid for adjusting pH of 0.1mol/L to 5.5,0.25% glucose of supernatant quality is added in supernatant
Oxidizing ferment, 0.4% ficin of supernatant quality are 35 DEG C in temperature and infrared auxiliary enzymes are carried out by 150r/min of rotating speed
60min is solved, temperature then is risen to 93 DEG C keeps 10min enzyme deactivations to live, and obtains hydrolyzate；Hydrolyzate is spray-dried, i.e.,
Obtain hydrolyzed wheat protein.Wherein, the infrared power of the infrared assistance enzymolysis is 200W, and infrared radiation distance is 3.5cm, is irradiated
Mode stops 3min and then irradiates 3min again to stop 3min successively alternately for irradiation 3min；The condition of the spray drying
Be inlet air temperature it is 180 DEG C, intake velocity 30m3/ h, charging rate 6mL/min, temperature of outgoing air are 80 DEG C.
The preparation method of above-mentioned strong root strengthen the hair phytoremediation element, includes the following steps：
(1) deionized water is added in into the homogeneous emulsifying machine (type provided using Guangzhou Ju Tao mechanical equipments Co., Ltd
Number be JT-B-150 vacuum homogeneous emulsifying machine) water phase pot in, add in guar hydroxypropyltrimonium chloride, chitosan season
Ammonium salt stirs 5min as 60r/min using rotating speed and is uniformly mixed, sequentially adds EDETATE SODIUM, hydrolyzed wheat protein, panthenol, side
CedarLeaves extract, ginger-root extract stir 15min as 60r/min using rotating speed and are uniformly mixed, and are warming up to 85 DEG C, obtain water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 85 DEG C, stirred by 60r/min of rotating speed
15min is uniformly mixed, and obtains oil phase material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, using rotating speed as 3000r/ at 85 DEG C
Then min homogeneous 5 minutes keeps the temperature 10 minutes, be eventually adding essence, methylisothiazolinone is stirred by 60r/min of rotating speed
15min is uniformly mixed to obtain the final product.
Test case 1
The submissive performance of the strong root strengthen the hair phytoremediation element of embodiment 1-5 is tested：
Material prepares：The hair of same women is selected, length is about 300mm, cuts off the hair tip and root of hair, hair is divided into
The topknot of 10g/ beams.
Testing procedure is as follows：
(1) the dry comb carding force A1 of topknot is measured；
(2) topknot is massaged 1 minute with the laruyl alcohol sodium sulfovinate aqueous cleaning that 2mL mass fractions are 10%, originally
It is rinsed 1 minute in water, avoids hair knotting；The deionized water of 800mL is added in the beaker of 1000mL, by bay alcohol sulfuric ester
Topknot after sodium water solution cleaning is submerged in water, takes out, and extra water is removed from root of hair to the hair tip, measures the wet comb comb of topknot
Manage power A2；
(3) strong root strengthen the hair phytoremediation element of the present invention is configured to the strong root strengthen the hair plant that mass fraction is 10% to repair
Multiple element aqueous solution handles topknot with the strong root strengthen the hair phytoremediation element aqueous solutions of 2mL, is massaged 1 minute from root of hair to the hair tip, originally
It is rinsed 1 minute in water, avoids hair knotting；The deionized water of 800m is added in the beaker of 1000mL, by strong root strengthen the hair plant
Repairing element, treated that topknot is submerged in water, takes out, and removes extra water from root of hair to the hair tip, the wet comb for measuring topknot combs
Power A3；
(4) topknot that step (3) obtains is dried, measures the dry comb carding force A4 of topknot.
The carding force test of each topknot is repeated 9 times, and takes its average value as test result.
Calculation formula is as follows：
Wet comb carding force reduced rate, %=(A2-A3)/A2；
Dry comb carding force reduced rate, %=(A1-A4)/A1.
The tensile testing machine for the model WDS-5 that test equipment is provided using Jinan Wei Pin testing machines Co., Ltd.
Specific test result is shown in Table 1.
Table 1：Submissive performance test data table
Test case 2
The removing free radical performance of the strong root strengthen the hair phytoremediation element of embodiment 1-5 is tested：
Remove free radical experiment：
Strong root strengthen the hair phytoremediation element is made into the sample solution that mass concentration is 0.5% with water, is tested.It takes
The Tris-HCl buffer solution 4.5mL of 0.05mol/L pH=8.2,20min is preheated in 25 DEG C of water-baths.Add 1mL samples
The pyrogallol solution of solution and 0.4mL 25mmol/L after mixing, reacts 5min in 25 DEG C of water-baths, adds in 8mol/L's
HCl 1.0mL terminate reaction.Reference is made with Tris-HCl buffer solutions, absorbance value is surveyed at 299nm.Blank control 1mL water
To substitute sample.Calculate clearance rate.
Ultra-oxygen anion free radical clearance rate (%)=[1- (C2/C1)] × 100%
In formula：C1 is the absorbance value of blank control；C2 is the absorbance value of sample.
Specific test result is shown in Table 1.
Table 1：Remove free radical the performance test results table
The present invention is using submissive performance and removes free radical performance as index, using the preparation technology parameter of embodiment 2, Qiang Gen
Strengthen the hair phytoremediation element is most outstanding；Ingredient in formula complements each other, and can nourish moisturizing hair comprehensively, repairs impaired hair
Hair supplements nutrition needed for hair follicle, and strong root strengthen the hair makes hair comprehensively be improved, smooth soft bright, high resilience.
Claims (10)
1. a kind of strong root strengthen the hair phytoremediation element, which is characterized in that be prepared from the following materials：Glycerine, cetostearyl alcohol, water
Solve wheat gluten, panthenol, Cacumen Platycladi extract, ginger-root extract, EDETATE SODIUM, essence, methylisothiazolinone, hair conditioning
Agent, water.
2. a kind of strong root strengthen the hair phytoremediation element, which is characterized in that be prepared by the raw material of following mass percent：5-15%
Glycerine, 2-7% cetostearyl alcohols, 0.5-3% hydrolyzed wheat proteins, 0.2-0.6% panthenols, 0.5-3% Cacumen Platycladi extracts,
0.5-3% ginger-root extracts, 0.05-0.25%EDTA disodiums, 0.5-2% essence, 0.0005-0.0015% methylisothiozolines
Ketone, 0.5-1.5% conditioner for hair, surplus are water.
3. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 2, it is characterised in that：The essence is citrus
It is one or more in type essence, mint type essence, beans flavor essence, milk flavoured type essence, lemon type essence, Vegetable-type essence.
4. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 2, it is characterised in that：The conditioner for hair
For guar hydroxypropyltrimonium chloride and/or chitosan quaternary ammonium salt.
5. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 2, it is characterised in that：The hydrolyzed wheat egg
White preparation method is：By wheat crushing to 30-80 mesh, wheat flour is obtained；It is 1 that wheat flour and water are pressed solid-liquid ratio：(5-15)
Mixing adjusts pH to 8-12 with the sodium hydrate aqueous solution of 0.05-0.15mol/L, and water-bath is using rotating speed as 100- at 35-55 DEG C
300r/min stirs 40-80min, centrifuges, abandons precipitation, obtain supernatant；With the salt acid for adjusting pH of 0.05-0.15mol/L
To 5-6, supernatant quality 0.1-0.4% glucose oxidases, supernatant quality 0.2-0.6% fig eggs are added in supernatant
White enzyme is 30-50 DEG C in temperature and enzymolysis 50-120min is carried out by 100-300r/min of rotating speed, temperature then is risen to 85-95
DEG C 5-15min enzyme deactivations is kept to live, obtain hydrolyzate；Hydrolyzate is spray-dried to get hydrolyzed wheat protein.
6. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 2, it is characterised in that：The hydrolyzed wheat egg
White preparation method is：By wheat crushing to 30-80 mesh, wheat flour is obtained；It is 1 that wheat flour and water are pressed solid-liquid ratio：(5-15)
Mixing adjusts pH to 8-12 with the sodium hydrate aqueous solution of 0.05-0.15mol/L, and water-bath is using rotating speed as 100- at 35-55 DEG C
300r/min stirs 40-80min, centrifuges, abandons precipitation, obtain supernatant；With the salt acid for adjusting pH of 0.05-0.15mol/L
To 5-6, supernatant quality 0.1-0.4% glucose oxidases, supernatant quality 0.2-0.6% fig eggs are added in supernatant
White enzyme is 30-50 DEG C in temperature and infrared assistance enzymolysis 50-120min is carried out by 100-300r/min of rotating speed, then by temperature
Rising to 85-95 DEG C keeps 5-15min enzyme deactivations to live, and obtains hydrolyzate；Hydrolyzate is spray-dried to get hydrolyzed wheat egg
In vain.
7. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 6, it is characterised in that：The infrared auxiliary enzymes
The infrared power of solution is 150-250W, infrared radiation distance is 2-5cm, radiation modality is irradiation 2-4min stoppings 2-4min, right
It irradiates 2-4min again afterwards and stops 2-4min successively alternately.
8. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 6, it is characterised in that：The spray drying
Condition is that inlet air temperature is 175-185 DEG C, intake velocity 25-35m3/ h, charging rate 5-7mL/min, temperature of outgoing air are
75-85℃。
9. the preparation method of strong root strengthen the hair phytoremediation element as claimed in claim 6, it is characterised in that：The centrifugation
Rotating speed is 5000-8000r/min, time 15-25min.
10. the preparation method of strong root strengthen the hair phytoremediation element as described in any one of claim 1-9, it is characterised in that：Including
Following step：
(1) add water in water phase pot, add in conditioner for hair, be uniformly mixed, sequentially add EDETATE SODIUM, hydrolysis it is small
Aleuronat, panthenol, Cacumen Platycladi extract, ginger-root extract are uniformly mixed, and are warming up to 80-90 DEG C, obtain water phase material；
(2) glycerine, cetostearyl alcohol are sequentially added in oil phase pot, is heated to 80-90 DEG C, be uniformly mixed, obtain oil phase
Material；
(3) water phase material is pumped into emulsification pot, stirs and oil phase material is pumped under homogeneous, homogeneous 3-13 minutes at 60-90 DEG C, then
Heat preservation 15-25 minutes, is eventually adding essence, methylisothiazolinone is uniformly mixed to obtain the final product.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109998963A (en) * | 2019-05-24 | 2019-07-12 | 戴金花 | Hair conditioner and preparation method thereof is repaired in nutrition |
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