CN108070426A - A kind of nano combined lubricating oil and preparation method thereof - Google Patents
A kind of nano combined lubricating oil and preparation method thereof Download PDFInfo
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- CN108070426A CN108070426A CN201610986738.9A CN201610986738A CN108070426A CN 108070426 A CN108070426 A CN 108070426A CN 201610986738 A CN201610986738 A CN 201610986738A CN 108070426 A CN108070426 A CN 108070426A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/05—Metals; Alloys
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/08—Inorganic acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/283—Esters of polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/72—Extended drain
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention discloses a kind of nano combined lubricating oil and preparation method thereof, the nano combined lubricating oil includes base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index improver, detergent-dispersant additive, antioxidant and antirust agent；Each ingredient is respectively according to mass percent：Tin nanoparticles 0.8 1.2%, copper nano particles 2.8 3.2%, CaCO3Nano-particle 0.1 0.3%, viscosity index improver 8 32%, detergent-dispersant additive are 4 8.5%, antioxidant 0.1 0.8%, antirust agent 0.2 1%, oil based on surplus.Each ingredient is uniformly mixed, is dehydrated；It heats and temperature is controlled to be stirred 60 360 minutes in 60 80 DEG C, uniformly mixed lube product is sent into manufactured goods tank to obtain the final product.Energy saving wear-resistant of the present invention can effectively save consumption of lubricating oil；Fuel oil more than 5% can be saved；It is environmentally protective, emissions figure 50% or so can be reduced, can effectively realize low-carbon environment-friendly.
Description
Technical field
The present invention relates to technical field of lubricating oil, are specifically a kind of nano combined lubricating oil and preparation method thereof.
Background technology
The lubricating action of lubricating oil mainly slows down component of machine fretting wear, reduces energy loss.By lubricating oil plus
Enter in body, be transported to the cylinder of machine, bent axle, the fortune such as piston rod and intake valve, air bleeding valve by pipeline, oil circuit by oil pump
In dynamic component, body recycling is then flowed back to again.It is made of base oil and additive, and nano lubricating oil complex technique is
Effectively improve the important technical of gasoline and diesel engine lubrication performance.
The preparation and application technology of today's society nano metal material has huge progress to have reached modern industrialization
The level of batch production, nanometer technology are widely used in various fields.Lubricating oil addition nano-metal particle can be with
The antiwear and friction reduction property of lubricating oil is significantly improved, this also opens new approach for the tremendous development in lubricating oil field.
The content of the invention
It is an object of the invention to provide a kind of nano combined lubricating oil and preparation method thereof, to solve to receive in the prior art
The technical barrier that presence of the rice ultrafine metal particle in lubricating oil is dispersed, stability is low and oxidizable, easily precipitates.
To achieve the above object, the present invention provides following technical solution：
A kind of nano combined lubricating oil, including base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity refer to
Number modifier, detergent-dispersant additive, antioxidant and antirust agent；Each ingredient is respectively according to mass percent：Tin nanoparticles
0.8-1.2%, copper nano particles 2.8-3.2%, CaCO3Nano-particle 0.1-0.3%, viscosity index improver 8-32%, peace and quiet point
Powder is 4-8.5%, antioxidant 0.1-0.8%, antirust agent 0.2-1%, oil based on surplus.
As further embodiment of the present invention：The nano combined lubricating oil, each ingredient are respectively according to mass percent：
Tin nanoparticles 1%, copper nano particles 3%, CaCO3Nano-particle 0.2%, viscosity index improver 10-30%, detergent-dispersant additive are
4.2-8%, antioxidant 0.2-0.5%, antirust agent 0.4-0.8%, oil based on surplus.
As further embodiment of the present invention：The base oil is gasoline engine oil, diesel engine oil, gear oil.
As further embodiment of the present invention：Further include synthetic ester or poly alpha olefine synthetic oil, tackifier, and component content
For：Synthetic ester or poly alpha olefine synthetic oil 50%, tackifier 4%.
As further embodiment of the present invention：Synthetic ester is polyol ester.
As further embodiment of the present invention：Further include anti-foaming agent.
As further embodiment of the present invention：Further include electrical isolation agent.
As further embodiment of the present invention：The electrical isolation agent is dimethyl silicone polymer.
A kind of production method of nano combined lubricating oil, comprises the following steps：
Step 1, uniformly mixed dehydrator of being sent into is dehydrated after each ingredient is weighed according to mass percent；
Step 2 is respectively stirred mixing into being distributed into batch blending system by dewatered, heats and controls temperature in 60-80
DEG C stirring 60-360 minute, to obtain the final product by uniformly mixed lube product feeding manufactured goods tank.
Compared with prior art, the beneficial effects of the invention are as follows：
（1）Energy saving wear-resistant, copper nano-particle make the extreme pressure of lubricating oil, abrasion resistance notable with being used while sijna rice corpuscles
It improves, enhances the lubrication and anti-wear effect of machine parts；And CaCO3Nano-particle can be produced effectively in the process in the use of neutral lubrication oil
Raw sulfuric acid prevents the formation of deposit and corrosion occurs.For this purpose, the nano combined lube drain phase reach 3 using the present invention
Ten thousand kilometers；Consumption of lubricating oil can effectively be saved；Fuel oil (gasoline, diesel oil) more than 5% can be saved；
（2）It is environmentally protective, emissions figure 50% or so can be reduced, can effectively realize low-carbon environment-friendly.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical solution in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, those of ordinary skill in the art's all other embodiments obtained without making creative work, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of nano combined lubricating oil, including base oil, tin nanoparticles, copper nano particles, CaCO3
Nano-particle, viscosity index improver, detergent-dispersant additive, antioxidant and antirust agent；Each ingredient is distinguished according to mass percent
It is：Tin nanoparticles 0.8%, copper nano particles 2.8%, CaCO3Nano-particle 0.1%, viscosity index improver 8% are peace and quiet scattered
Agent is 4%, antioxidant 0.1%, antirust agent 0.2%, oily based on surplus.The base oil is gasoline engine oil.
The production method of the nano combined lubricating oil, comprises the following steps：
Step 1, by base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index improver, peace and quiet point
Powder, antioxidant are uniformly mixed feeding dehydrator and are dehydrated after being weighed with antirust agent according to mass percent.
Step 2, by dewatered base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index (VI) change
Be sent into batch blending system into agent, detergent-dispersant additive, antioxidant and antirust agent and be stirred and mix, heat and control temperature in
60 DEG C are stirred 60 minutes, and uniformly mixed lube product is sent into manufactured goods tank to obtain the final product.
Embodiment 2
In the embodiment of the present invention, a kind of nano combined lubricating oil, including base oil, tin nanoparticles, copper nano particles, CaCO3
Nano-particle, viscosity index improver, detergent-dispersant additive, antioxidant and antirust agent；Each ingredient is distinguished according to mass percent
It is：Tin nanoparticles 1.2%, copper nano particles 3.2%, CaCO3Nano-particle 0.3%, viscosity index improver 32% are peace and quiet scattered
Agent is 8.5%, antioxidant 0.8%, antirust agent 1%, oily based on surplus.The base oil is diesel engine oil.
The production method of the nano combined lubricating oil, comprises the following steps：
Step 1, by base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index improver, peace and quiet point
Powder, antioxidant are uniformly mixed feeding dehydrator and are dehydrated after being weighed with antirust agent according to mass percent.
Step 2, by dewatered base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index (VI) change
Be sent into batch blending system into agent, detergent-dispersant additive, antioxidant and antirust agent and be stirred and mix, heat and control temperature in
80 DEG C are stirred 360 minutes, and uniformly mixed lube product is sent into manufactured goods tank to obtain the final product.
Embodiment 3
In the embodiment of the present invention, a kind of nano combined lubricating oil, including base oil, tin nanoparticles, copper nano particles, CaCO3
Nano-particle, viscosity index improver, detergent-dispersant additive, antioxidant and antirust agent；Each ingredient is distinguished according to mass percent
It is：Tin nanoparticles 1%, copper nano particles 3%, CaCO3Nano-particle 0.2%, viscosity index improver 10%, detergent-dispersant additive are
4.2%, antioxidant 0.2%, antirust agent 0.4%, oil based on surplus.The base oil is gear oil.
The production method of the nano combined lubricating oil, comprises the following steps：
Step 1, by base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index improver, peace and quiet point
Powder, antioxidant are uniformly mixed feeding dehydrator and are dehydrated after being weighed with antirust agent according to mass percent.
Step 2, by dewatered base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index (VI) change
Be sent into batch blending system into agent, detergent-dispersant additive, antioxidant and antirust agent and be stirred and mix, heat and control temperature in
65 DEG C are stirred 100 minutes, and uniformly mixed lube product is sent into manufactured goods tank to obtain the final product.
Embodiment 4
In the embodiment of the present invention, a kind of nano combined lubricating oil, including base oil, tin nanoparticles, copper nano particles, CaCO3
Nano-particle, viscosity index improver, detergent-dispersant additive, antioxidant, antirust agent, synthetic ester or poly alpha olefine synthetic oil and increasing
Stick；Each ingredient is respectively according to mass percent：Tin nanoparticles 1%, copper nano particles 3%, CaCO3Nano-particle 0.2%,
Viscosity index improver 30%, detergent-dispersant additive 8%, antioxidant 0.5%, antirust agent 0.8%, synthetic ester or poly alpha olefin synthesis
Oil 50%, tackifier 4%, oil based on surplus.Synthetic ester is polyol ester.Base oil is gasoline engine oil.
The production method of the nano combined lubricating oil, comprises the following steps：
Step 1, by base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index improver, peace and quiet point
Powder, antioxidant are uniformly mixed feeding dehydrator and are dehydrated after being weighed with antirust agent according to mass percent.
Step 2, by dewatered base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index (VI) change
Be sent into batch blending system into agent, detergent-dispersant additive, antioxidant and antirust agent and be stirred and mix, heat and control temperature in
75 DEG C are stirred 250 minutes, and uniformly mixed lube product is sent into manufactured goods tank to obtain the final product.
Embodiment 5
In the embodiment of the present invention, a kind of nano combined lubricating oil, including base oil, tin nanoparticles, copper nano particles, CaCO3
Nano-particle, viscosity index improver, detergent-dispersant additive, antioxidant, antirust agent, electrical isolation agent, synthetic ester or poly alpha olefin
Synthetic oil and tackifier；Each ingredient is respectively according to mass percent：Tin nanoparticles 1%, copper nano particles 3%, CaCO3Nanometer
Particle 0.2%, viscosity index improver 20%, detergent-dispersant additive 6%, antioxidant 0.4%, antirust agent 0.6%, synthetic ester 50%,
Tackifier 4%, be electrically insulated agent 0.1%, oil based on surplus.Synthetic ester is polyol ester.Base oil is diesel engine oil.The electricity is absolutely
Edge agent is dimethyl silicone polymer.
The production method of the nano combined lubricating oil, comprises the following steps：
Step 1, by base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index improver, peace and quiet point
Powder, antioxidant are uniformly mixed feeding dehydrator and are dehydrated after being weighed with antirust agent according to mass percent.
Step 2, by dewatered base oil, tin nanoparticles, copper nano particles, CaCO3Nano-particle, viscosity index (VI) change
Be sent into batch blending system into agent, detergent-dispersant additive, antioxidant and antirust agent and be stirred and mix, heat and control temperature in
70 DEG C are stirred 150 minutes, and uniformly mixed lube product is sent into manufactured goods tank to obtain the final product.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requirement rather than above description limit, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
Moreover, it will be appreciated that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
Using specification as an entirety, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (9)
1. a kind of nano combined lubricating oil, which is characterized in that including base oil, tin nanoparticles, copper nano particles, CaCO3Nanometer
Particle, viscosity index improver, detergent-dispersant additive, antioxidant and antirust agent；Each ingredient is respectively according to mass percent：Tin
Nano particle 0.8-1.2%, copper nano particles 2.8-3.2%, CaCO3Nano-particle 0.1-0.3%, viscosity index improver 8-
32%, detergent-dispersant additive 4-8.5%, antioxidant 0.1-0.8%, antirust agent 0.2-1%, oil based on surplus.
2. nano combined lubricating oil according to claim 1, which is characterized in that each ingredient is distinguished according to mass percent
It is：Tin nanoparticles 1%, copper nano particles 3%, CaCO3Nano-particle 0.2%, viscosity index improver 10-30% are peace and quiet scattered
Agent is 4.2-8%, antioxidant 0.2-0.5%, antirust agent 0.4-0.8%, oil based on surplus.
3. nano combined lubricating oil according to claim 1 or 2, which is characterized in that the base oil is gasoline engine oil, bavin
Oil machine oil, gear oil.
4. nano combined lubricating oil according to claim 1 or 2, which is characterized in that further include synthetic ester or poly alpha olefin
Synthetic oil, tackifier, and component content is：Synthetic ester or poly alpha olefine synthetic oil 50%, tackifier 4%.
5. nano combined lubricating oil according to claim 4, which is characterized in that synthetic ester is polyol ester.
6. nano combined lubricating oil according to claim 1 or 2, which is characterized in that further include anti-foaming agent.
7. nano combined lubricating oil according to claim 1 or 2, which is characterized in that further include electrical isolation agent.
8. nano combined lubricating oil according to claim 7, which is characterized in that the electrical isolation agent is poly dimethyl silicon
Oxygen alkane.
9. the production method of a kind of nano combined lubricating oil as described in claim 1-8 is any, which is characterized in that including following
Step：
Step 1, uniformly mixed dehydrator of being sent into is dehydrated after each ingredient is weighed according to mass percent；
Step 2 is respectively stirred mixing into being distributed into batch blending system by dewatered, heats and controls temperature in 60-80
DEG C stirring 60-360 minute, to obtain the final product by uniformly mixed lube product feeding manufactured goods tank.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610986738.9A CN108070426A (en) | 2016-11-10 | 2016-11-10 | A kind of nano combined lubricating oil and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610986738.9A CN108070426A (en) | 2016-11-10 | 2016-11-10 | A kind of nano combined lubricating oil and preparation method thereof |
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| CN201610986738.9A Pending CN108070426A (en) | 2016-11-10 | 2016-11-10 | A kind of nano combined lubricating oil and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112574795A (en) * | 2019-09-30 | 2021-03-30 | 集美大学 | Preparation method of graphene loaded spherical metal |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112574795A (en) * | 2019-09-30 | 2021-03-30 | 集美大学 | Preparation method of graphene loaded spherical metal |
| CN112574795B (en) * | 2019-09-30 | 2022-11-04 | 集美大学 | Preparation method of graphene loaded spherical metal |
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