CN108017722A - One kind utilizes mulberry branch separation cladding and bar material, Preparation method and use - Google Patents
One kind utilizes mulberry branch separation cladding and bar material, Preparation method and use Download PDFInfo
- Publication number
- CN108017722A CN108017722A CN201810095380.XA CN201810095380A CN108017722A CN 108017722 A CN108017722 A CN 108017722A CN 201810095380 A CN201810095380 A CN 201810095380A CN 108017722 A CN108017722 A CN 108017722A
- Authority
- CN
- China
- Prior art keywords
- sent
- bast
- cladding
- ramulus mori
- bar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000463 material Substances 0.000 title claims abstract description 194
- 238000005253 cladding Methods 0.000 title claims abstract description 109
- 240000000249 Morus alba Species 0.000 title claims abstract description 78
- 235000008708 Morus alba Nutrition 0.000 title claims abstract description 78
- 238000000926 separation method Methods 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 93
- 239000000835 fiber Substances 0.000 claims abstract description 64
- 238000000034 method Methods 0.000 claims abstract description 59
- 239000001814 pectin Substances 0.000 claims abstract description 54
- 229920001277 pectin Polymers 0.000 claims abstract description 54
- 235000010987 pectin Nutrition 0.000 claims abstract description 54
- 210000003491 skin Anatomy 0.000 claims abstract description 31
- 239000000284 extract Substances 0.000 claims abstract description 26
- 210000002615 epidermis Anatomy 0.000 claims abstract description 25
- 239000012043 crude product Substances 0.000 claims abstract description 16
- 238000012545 processing Methods 0.000 claims description 101
- 239000007788 liquid Substances 0.000 claims description 68
- 238000001035 drying Methods 0.000 claims description 63
- 108010029541 Laccase Proteins 0.000 claims description 46
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 41
- 238000002386 leaching Methods 0.000 claims description 32
- 239000002994 raw material Substances 0.000 claims description 27
- 108090000790 Enzymes Proteins 0.000 claims description 26
- 102000004190 Enzymes Human genes 0.000 claims description 26
- 229940088598 enzyme Drugs 0.000 claims description 26
- 239000004382 Amylase Substances 0.000 claims description 24
- 108010065511 Amylases Proteins 0.000 claims description 24
- 102000013142 Amylases Human genes 0.000 claims description 24
- 235000019418 amylase Nutrition 0.000 claims description 24
- 239000011362 coarse particle Substances 0.000 claims description 24
- 239000002002 slurry Substances 0.000 claims description 23
- 108010059892 Cellulase Proteins 0.000 claims description 21
- 239000007864 aqueous solution Substances 0.000 claims description 21
- 229940106157 cellulase Drugs 0.000 claims description 21
- 239000002253 acid Substances 0.000 claims description 20
- 230000002378 acidificating effect Effects 0.000 claims description 20
- 238000004519 manufacturing process Methods 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 20
- 238000012216 screening Methods 0.000 claims description 18
- 238000010790 dilution Methods 0.000 claims description 17
- 239000012895 dilution Substances 0.000 claims description 17
- 239000000243 solution Substances 0.000 claims description 17
- 230000018044 dehydration Effects 0.000 claims description 16
- 238000006297 dehydration reaction Methods 0.000 claims description 16
- 239000012535 impurity Substances 0.000 claims description 16
- 238000002791 soaking Methods 0.000 claims description 16
- 239000002562 thickening agent Substances 0.000 claims description 16
- 238000010792 warming Methods 0.000 claims description 16
- 230000007062 hydrolysis Effects 0.000 claims description 15
- 238000006460 hydrolysis reaction Methods 0.000 claims description 15
- 238000005406 washing Methods 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 238000002803 maceration Methods 0.000 claims description 10
- 239000004753 textile Substances 0.000 claims description 10
- 239000002023 wood Substances 0.000 claims description 10
- 238000005520 cutting process Methods 0.000 claims description 9
- 239000000047 product Substances 0.000 claims description 9
- 238000000967 suction filtration Methods 0.000 claims description 9
- 206010013786 Dry skin Diseases 0.000 claims description 8
- 239000000428 dust Substances 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- -1 finally Substances 0.000 claims description 8
- 238000000227 grinding Methods 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 8
- 238000001556 precipitation Methods 0.000 claims description 8
- 239000013049 sediment Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 239000006228 supernatant Substances 0.000 claims description 8
- 238000003828 vacuum filtration Methods 0.000 claims description 8
- 230000036541 health Effects 0.000 claims description 5
- 239000000287 crude extract Substances 0.000 claims description 2
- 239000003973 paint Substances 0.000 claims 2
- 108010089934 carbohydrase Proteins 0.000 claims 1
- 229940126678 chinese medicines Drugs 0.000 claims 1
- 239000002699 waste material Substances 0.000 abstract description 6
- 239000000123 paper Substances 0.000 description 8
- 238000001914 filtration Methods 0.000 description 7
- 230000008569 process Effects 0.000 description 7
- 238000009835 boiling Methods 0.000 description 6
- 238000000605 extraction Methods 0.000 description 6
- 241000255789 Bombyx mori Species 0.000 description 5
- 241000209094 Oryza Species 0.000 description 5
- 235000007164 Oryza sativa Nutrition 0.000 description 5
- 239000003814 drug Substances 0.000 description 5
- 238000002789 length control Methods 0.000 description 5
- 235000009566 rice Nutrition 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 239000000686 essence Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 229920005610 lignin Polymers 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- 238000009366 sericulture Methods 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- 238000004065 wastewater treatment Methods 0.000 description 3
- 239000003513 alkali Substances 0.000 description 2
- 238000009395 breeding Methods 0.000 description 2
- 230000001488 breeding effect Effects 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000003317 industrial substance Substances 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- 239000000077 insect repellent Substances 0.000 description 2
- 239000003895 organic fertilizer Substances 0.000 description 2
- 238000010129 solution processing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011953 bioanalysis Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000011094 fiberboard Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 239000012633 leachable Substances 0.000 description 1
- 238000010297 mechanical methods and process Methods 0.000 description 1
- 238000000874 microwave-assisted extraction Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 238000011112 process operation Methods 0.000 description 1
- 238000013138 pruning Methods 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
- C08B37/0048—Processes of extraction from organic materials
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21B—FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
- D21B1/00—Fibrous raw materials or their mechanical treatment
- D21B1/04—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
- D21B1/06—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by dry methods
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C5/00—Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Mechanical Engineering (AREA)
- Paper (AREA)
- Fodder In General (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
It is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step the invention discloses one kind：A, stock up, b, decoct twice, c, decoction liquor concentration, dry, d, decoction material skin, bar separating treatment, and e, cladding carry out epidermis, green peel and bast separating treatment, and f, produce pectin crude product, bast fiber using bast, and g, using bar material produce stem's fiber.The present invention can have not only been realized by decoction liquor extract of mulberry twig, but also can be kept completely separate the skin bar of ramulus mori and be separated, and epidermis, green peel are kept completely separate with bast and separate, and the bast after separating produces pectin crude product and bast fiber, and the bar after separating produces stem's fiber；It is truly realized the generalizations such as the pectin to mulberry branch, bast fiber, stem's fiber, flowing water line drawing; it make use of every value of mulberry branch comprehensively, improve the utilization rate and utility value of mulberry branch, the present invention improves mulberry branch utilization rate; comprehensive utilization of waste materials is realized, protects environment.
Description
Technical field
The present invention relates to extract of mulberry twig, pectin, bast fiber, stem's fiber preparation technique field, more particularly to one
Kind utilizes mulberry branch separation cladding and bar material, Preparation method and use.
Background technology
Ramulus mori is the branch for obtaining good mulberry leaf for sericulture and getting off from mulberry tree beta pruning, and ramulus mori is widely used, and whole body is
Treasured, is both a kind of good fibrous raw material and a kind of traditional Chinese medicine.Ramulus Mori can be divided into epidermis, green peel, bast, tough
Skin is pure white, flexible, fiber is elongated, intensity is big, and ramulus mori rod color is white, medulla is few.
Ramulus mori is the accessory substance of sericulture industry, and in China, planting mulberry and breeding silkworm are with a long history, and kind mulberry scope is extremely wide, ramulus mori resource pole
It is abundant.Last year, statistics is done according to national silk, and China mulberry field area is up to 1189.51 ten thousand mu, in addition to mulberry leaf are used to breed silkworms, every year
The mulberry branch yield that winter, two season of summer mulberry tree are trimmed is up to more than 30,000,000 tons, however, the utilization rate of ramulus mori is extremely low, about
10% or so.More than 2000 ten thousand tons of mulberry branch is burnt up as discarded object by common people (silkworm and mulberry practitioner) as domestic fuel, or
Abandon and rot in field under natural conditions effect on the spot, or on-site incineration, cause significant wastage and the pollution of resource
Environment.The utilization of mulberry branch has become planting mulberry and breeding silkworm industry problem anxious to be resolved.Research and development utilize ramulus mori, will can not only give up
The mulberry branch utilization of resources abandoned, moreover, it is also possible to increase income for local common people (silkworm and mulberry practitioner), poverty-stricken area takes off
It is poor to get rich, improve the ecological environment, there is larger society, economy, environmental benefit.
Existing method using mulberry branch exist production product it is single, low production efficiency, production cost, pollution control into
This height, the problems such as utilization rate is low, ramulus mori conversion ratio, output capacity are low.China Patent No. 201310588118.1 discloses a kind of skin
The step of bar separating process, this method, is as follows：A, raw material is cut into section with stock-cutter, forms coarse fodder；B, coarse fodder is screened, washed
Wash composition fine fodder；C, fine fodder is divided into two class of wet feed and siccative：Fine fodder of the moisture more than 50% is known as wet feed, and moisture exists
50% and less than 50% fine fodder is known as siccative；D, siccative is sent into boiling vessel heating boosting boiling, then carries out material water separation, point
Separate out the material come and form boiling material；E, enzymolysis processing process：Boiling material is digested with zytase dilution, and wet feed pectase is dilute
Release liquid and zytase dilution is digested, wet feed is digested with pectase dilution and zytase dilution, enzymolysis
The wet feed after boiling material or enzymolysis afterwards is known as material for making clothes, and material for making clothes send to peeling machine and carries out peeling processing, drives off skin and bar.Should
It is unclean that embodiment of the method 1,4 solves peeling existing for ramulus mori dry method peeling machine, and surface thing handles unclean and Manual moist
Method peeling labor intensity is big, the problems such as labor productivity is low, but later in practice process, it is found that this method still remains mulberry
The water isolated after limb material boiling does not efficiently use, and wastewater treatment is difficult.Enzymolysis process operating procedure step process ramulus mori steams
Boil material and wet feed time length, high energy consumption；Bast and bar slurrying stain are more, it is of poor quality the problems such as, be not suitable for industrialized production.
China Patent No. 201410235988.x discloses a kind of method for extracting medicine and slurrying comprehensive utilization ramulus mori.Should
Method includes the following steps：A, raw material is cut into section with stock-cutter, forms coarse fodder；B, coarse fodder is screened, washing forms fine fodder；C, essence
Material is sent into extractor heating and is decocted, and feed liquid separates after decoction, and the material separated forms decoction material, and liquid forms decoction liquor；D、
Decoction liquor is sent into the semi-finished product cream liquid that evaporator produces one ramulus mori cream of medicine etc.；E, decoction material is sent to peeling machine and is carried out at peeling
Reason, isolates skin and bar；F, separated bast and stalk slurrying.In the skin bar separating process that this method solve my invention
Ramulus mori using there are the problem of, i.e.,：The decoction liquor for decocting ramulus mori has been made to the raw material for producing medicine, has reduced and decocts at waste liquid
Reason.Meanwhile the processing step of enzymolysis process operation is eliminated, realize ramulus mori extraction medicine and slurrying comprehensive utilization ramulus mori.But
Later, separated although production practices find that the technology decoction material skin (bast) and bar in skin bar separation process are kept completely separate, point
Epidermis, bast and bar have been separated out, but has still remained the drawbacks of degumming is excessive, has destroyed bast fiber structure, it is epidermis, green peel, tough
Skin, which is not properly separated, to be separated, and is interweaved together, is exactly with small part bast, bast in separated epidermis, green peel
In be difficult to remove with part epidermis, green peel, using bioanalysis, APMP or mechanical method for making pulp by extruding, the product black of production
Tiny epidermis, green peel is more, does not reach quality requirement, and market does not receive the product.Meanwhile bast slurrying, also contain in bast
A large amount of pectin be extracted into waste water, add wastewater treatment difficulty and cost.Therefore, its industrialization is limited.
The content of the invention
Part in view of the shortcomings of the prior art, it is an object of the invention to provide one kind to utilize mulberry branch separation cladding
With bar material, Preparation method and use, can not only realize by decoction liquor extract of mulberry twig, but also can be by skin (bast) bar of ramulus mori
It is kept completely separate and separates, epidermis, green peel are kept completely separate with bast and separate, and the bast after separating produces pectin crude product and bast fiber,
Bar after separating produces stem's fiber, and the epidermis, green peel after separating contain substantial amounts of lignin, and recycling is made production mosquito-repellent incense raw material or carried
Take lignin or make organic fertilizer etc.；It is truly realized generalization, the flowing water such as the pectin to mulberry branch, bast fiber, stem's fiber
Line drawing, make use of every value of mulberry branch comprehensively, improve the utilization rate and utility value of mulberry branch.
The purpose of the present invention is achieved through the following technical solutions：
A kind of preparation method that cladding and bar material are separated using mulberry branch, its method and step are as follows：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, the length for often saving ramulus mori section is controlled 10~80
Millimeter, is then screened by screening machine, screens and retain 10~80 millimeters of ramulus mori section, washed after screening with material washing machine
Wash, remove silt particle, dust and other impurity on ramulus mori section, form ramulus mori section fine fodder；
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：4~15 ratio is sent into extractor, by extractor
In ramulus mori section fine fodder be uniformly mixed with water, first time decoction is carried out to extractor heat temperature raising, specific method is as follows：To extraction
When tank is warming up to 70~90 DEG C, and when soaking time 1~3 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature
Decoct, when decocting time is 2~6 small, decocts terminate simultaneously to carry out feed liquid separation for the first time；
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：4~8 ratio is sent into extractor, by the ramulus mori section essence in extractor
Material is uniformly mixed with water, and carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To heating up in the tank of extractor
To 100 DEG C, and 100 DEG C of temperature are kept to decoct, when decocting time is 2~4 small；Then proceed to be heated to the tank of extractor
Interior pressure is kept the temperature when reaching 0.01~0.09Mpa, when soaking time is 0.5~3 small；
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor；
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent in spray dryer
It is dry, up to extract of mulberry twig after drying；
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
A kind of mulberry branch cladding and bar material, are by using obtained by mulberry branch separation cladding and bar preparation method for material
's.
A kind of purposes of mulberry branch cladding, is used to prepare pectin crude extract, its method is as follows：
E, mulberry branch separation cladding and the obtained cladding of bar preparation method for material will be utilized to be converted into over dry, by every
1000 kilograms take 40~double centner water acid adding to adjust pH value to 3~5, and composition acidic aqueous solution is then uniform by acidic aqueous solution
Be sprayed onto on the cladding after exhausted bar, by the cladding after sprinkling send to bast seperator carry out separating treatment, by the epidermis in cladding,
Green peel is completely isolated with bast；
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：8~18 ratio acid adding
And maceration extract pH value is adjusted to 1~4, it is then fed into microwave treater and carries out microwave treatment, that is sent into microwave treater is tough
Skin how much time with microwave treatment, the proportional relation of microwave power, i.e., the bast being sent into microwave treater is more, in microwave
During processing, the time of microwave treatment is relatively longer, the selected power of microwave treater just relatively it is bigger (such as bast be sent into
250g, then the microwave power of microwave treater is 400~1500 watts, and the microwave time is 5~20 minutes)；Microwave treatment terminates, will
Material, liquid carry out being separated by filtration processing, and the material separated forms tough cladding, and the liquid separated forms leaching liquor；
G, the leaching liquor in step F is sent into rotary evaporator, it is dense that vacuum is carried out under 50~65 DEG C of temperature conditionss
Contracting, after concentration, is slowly added to 95% ethanol of equivalent, stirring makes the pectin in leaching liquor fully be reacted with ethanol；Reaction is completed
Afterwards, 20-32 minutes are stood, makes pectin Precipitation, then handled using vacuum filtration machine suction filtration, what much filtrate was measured with one times
75% ethanol wash, removes other impurity, finally, pectin sediment is put into 50~70 DEG C of drying machine dryings, crushes to obtain pectin
Crude product.
A kind of purposes of pectin crude product, for the raw material as production pectin.
A kind of purposes of mulberry branch cladding, is used to prepare bast fiber extract, its method is as follows：
E, mulberry branch separation cladding and the obtained cladding of bar preparation method for material will be utilized to be converted into over dry, by every
1000 kilograms take 40~double centner water acid adding to adjust pH value to 3~5, and composition acidic aqueous solution is then uniform by acidic aqueous solution
Be sprayed onto on the cladding after exhausted bar, by the cladding after sprinkling send to bast seperator carry out separating treatment, by the epidermis in cladding,
Green peel is completely isolated with bast；
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：8~18 ratio acid adding
And maceration extract pH value is adjusted to 1~4, it is then fed into microwave treater and carries out microwave treatment, that is sent into microwave treater is tough
Skin how much time with microwave treatment, the proportional relation of microwave power, i.e., the bast being sent into microwave treater is more, in microwave
During processing, the time of microwave treatment is relatively longer, the selected power of microwave treater just relatively it is bigger (such as bast be sent into
250g, then the microwave power of microwave treater is 400~1500 watts, and the microwave time is 5~20 minutes), microwave treatment terminates, will
Material, liquid carry out being separated by filtration processing, and the material separated forms tough cladding；
H, the tough cladding in step F is converted into over dry material, 2~5 kilograms of laccase, zytase is weighed by every 1000 kilograms
1~3 kilogram, 40~50 kilograms of water mix and be heated up to 40~70 DEG C form laccase, zytase dilutions, then by laccase,
Zytase dilution is uniformly sprayed on tough cladding, is sent after sprinkling to enzymolysis storehouse and is carried out enzymolysis processing, and enzymolysis time is 3~10
Hour, hydrolysis temperature is 40~80 DEG C, and the tough cladding after enzymolysis is sent to fiberizer processing；To handle obtained bast slurry send to
Eliminating potential pool, which disappears to dive, to be handled, and the latent processing time that disappears, the bast slurry after the latent processing that disappears was sent to thickener dehydration for 20~40 minutes
Reason, dewatered bast slurry is sent into drying machine processing, up to bast fiber after the completion of drying.
A kind of purposes of bast fiber, makees the raw material of production speciality paper etc. for paper industry or is given birth to for textile industry
Produce the raw material of textile etc..
A kind of purposes of ramulus mori bar material, is used to prepare stem's fiber extract, its method is as follows：
I, Gan Liaozhi stems fiber：Bar material in claim 2 is sent to fiberizer and is roughly ground, by bar material grinding into filament shape
Coarse fodder, by filament shape coarse fodder be converted into over dry and according to material water weight proportion be 1:2~4 ratio is sent to microwave treater and is carried out
Filament shape coarse fodder (is converted into over dry first, is 1 according to filament shape coarse fodder over dry and water weight proportion by microwave treatment:2~4
Ratio send to microwave treater carry out microwave treatment), the filament shape coarse fodder being sent into microwave treater how much with microwave
The time of reason, the proportional relation of microwave power, i.e., the filament shape coarse fodder being sent into microwave treater is more, in microwave treatment,
The time of microwave treatment is relatively longer, the selected power of microwave treater just relatively it is bigger (such as filament shape coarse fodder be sent into
250g, then the microwave power of microwave treater is 400~1500 watts, and the microwave time is 5~20 minutes)；After microwave treatment
Coarse fodder, be converted into over dry material, 2~8 kilograms of cellulase, 2~8 kilograms of laccase weighed by every 1000 kilograms, amylase 0.5~
3 kilograms, 200~300 kilograms of water mix and be heated up to 50~70 DEG C form cellulase, laccase, amylase mixed enzyme solutions；Then
Cellulase, laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder, the filament shape coarse fodder after sprinkling is sent to enzyme
Xie Cang carries out enzymolysis processing, and when enzymolysis time is 4~16 small, hydrolysis temperature is 50~70 DEG C；Filament shape coarse fodder after enzymolysis is sent
To high concentration plate mill processing, obtained coarse particles will be handled and sent to eliminating potential pool disappear latent processing, the latent time that disappears for 20~40 minutes, disappears
Coarse particles after latent processing are sent to thickener dehydration, and dewatered coarse particles are sent to drying machine processing, are after the completion of dry
Obtain stem's fiber.
A kind of purposes of stem's fiber, makees the original of production newsprint, cultural paper, package paper etc. for paper industry
Material, or the raw material for textile industry work production textile etc..
A kind of purposes according to using mulberry branch separation cladding and the obtained decoction liquor of bar preparation method for material, is used for
The raw material of Chinese medicinal material, health products, drink, raw-food material or feedstuff is produced, its specific method is as follows：
Produced after the decoction liquor produced using mulberry branch separation cladding and bar preparation method for material is concentrated and dried
Extract of mulberry twig, the extract of mulberry twig are used for the raw material for producing Chinese medicinal material, health products, drink, raw-food material or feedstuff.
Wood material cutting machine, screening machine, material washing machine, extractor, evaporator, drier, peeling machine employed in the present invention,
The equipment such as bast seperator, microwave treater, rotary evaporator, suction filtration machine, enzymolysis storehouse, fiberizer, high concentration plate mill can use
Existing mature equipment, can also be separately manufactured, the water employed in the present invention by the specific design requirement for implementing the present invention, its
Water quality is selected by Industry code requirements.
The present invention compared with the prior art, has the following advantages and beneficial effect：
(1) for the present invention in ramulus mori decoction process, first low temperature immersion, makes fine fodder be impregnated with uniformly, infiltration is abundant, then slowly rises
Pressure, low-voltage temperature-keeping decoct；It is fully dissolved out in this way, both having reached the leachable thing of ramulus mori, turn avoid high temperature, high pressure decocts, bast
Excessive degumming, causes fibre structure to change, after peeling machine is handled, and together with being interweaved with epidermis, green peel.Present invention warp
Peracidity aqueous solution and bast separator for processing, which solve epidermis, green peel is difficult to 100% with bast and separates the technology separated hardly possible
Topic.
(2) the separated bast of the present invention produces bast fiber using microwave extraction method extraction pectin, has both extracted bast
In pectin recycling make the utilization of resources, and reached and produced bast fiber and remove the effect that can be only achieved of pectin with chemical method；This
Tough cladding after invention extraction pectin is not added with the industrial chemicals such as alkali, bast fiber can be made after enzymolysis processing, that produces is tough
Tiny epidermis, green peel of the hide fiber without black, improve bast fiber quality, can produce extraordinary paper material, can also spin
Woven garment industry production textile raw material, its pectin crude product produced make production pectin starting material.
(3) the separated Gan Liaozhi stems fiber of the present invention would not also produce noxious material without using industrial chemicals such as alkali,
Screening, washing, decoction are have passed through, the soluble matter for influencing quality and increase enzyme amount is eliminated, after microwave treatment, easy to enzyme
Absorption and infiltration, obtained stem's fiber quality is good after enzymolysis processing, and yield rate is high, it can be used as newsprint, culture
Paper, package paper raw material etc., separated bar material can also make fiber board raw material.
(4) extracting method of the invention has significant society, and economy and environmental benefit, mulberry branch of the present invention first produce mulberry
Branch extract, produces the bar material after extract of mulberry twig and carries out skin bar separation, the cladding after separation carries out epidermis, green peel, bast again
Separation, separated bast produce pectin crude product and bast fiber, and the bar material after separating produces stem's fiber, will so produce ramulus mori
Extract, pectin crude product, bast fiber, stem's fiber are used in combination with ramulus mori, and the conversion ratio of its raw material, output capacity improve,
Industrial production cost is reduced, improves product quality, overcomes the deficiency in current art.
(5) present invention takes inter-trade utilization and makes full use of simultaneously converting wastes resource, its extracting method is real
Show comprehensive extraction of mulberry branch, therefore without any waste material, it is specific using as follows：1) waste residue that stock produces can produce
Edible fungi raw materials；2) separated epidermis, green peel are cuticula, not containing cellulose, and containing substantial amounts of lignin, ash content, recycling is given birth to
Production mosquito-repellent incense raw material extracts lignin or makees organic fertilizer etc..Meanwhile the present invention is as follows without any discharge of wastewater, concrete reason：
1) Chinese medicinal material can be made by decocting the extract of mulberry twig produced after the decoction liquor concentrate drying of ramulus mori, can also make health products, drink, food
Product raw material, also raw material capable of using as feed；2) returned after the wastewater treatment that the waste water of stock generation, bast fiber processed, stem's fiber produce
Receive and utilize.No bled steam discharge：The exhaust steam produced during concentrate drying recycles, and has both saved the energy, can also return
Effective medicinal ingredient in exhaust steam is received, the present invention improves mulberry branch utilization rate, realizes comprehensive utilization of waste materials, protects
Environment.
(6) present invention takes full advantage of mulberry branch and produces scrap feed material in the extracts such as pectin, bast fiber, stem's fiber
Resource is pulping and paper-making industry, pharmaceutical industry, textile industry, food service industry service, is increased income for sericulture there, avoids raw material quilt
Open incineration pollutes air and causes haze weather serious.
Embodiment
The present invention is described in further detail with reference to embodiment：
Embodiment one
One kind is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, the length for often saving ramulus mori section is controlled 10~80
Millimeter, is then screened by screening machine, screens and retain 10~80 millimeters of ramulus mori section, washed after screening with material washing machine
Wash, remove silt particle, dust and other impurity on ramulus mori section, form ramulus mori section fine fodder.
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：4~15 ratio is sent into extractor, by extractor
In ramulus mori section fine fodder be uniformly mixed with water, first time decoction is carried out to extractor heat temperature raising, specific method is as follows：To extraction
When tank is warming up to 70~90 DEG C, and when soaking time 1~3 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature
Decoct, when decocting time is 2~6 small, decocts terminate simultaneously to carry out feed liquid separation for the first time.
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：4~8 ratio is sent into extractor, by the ramulus mori section essence in extractor
Material is uniformly mixed with water, and carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To heating up in the tank of extractor
To 100 DEG C, and 100 DEG C of temperature are kept to decoct, when decocting time is 2~4 small；Then proceed to be heated to the tank of extractor
Interior pressure is kept the temperature when reaching 0.01~0.09Mpa, when soaking time is 0.5~3 small.
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor.
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent to drying in drier,
Up to extract of mulberry twig after drying.
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
E, the cladding separated in step D is converted into over dry, 40~double centner water acid adding tune is taken by every 1000 kilograms
PH value is saved to 3~5, acidic aqueous solution is formed, is then uniformly sprayed onto acidic aqueous solution on the cladding after exhausted bar, after sprinkling
Cladding send to bast seperator carry out separating treatment, the epidermis in cladding, green peel and bast is completely isolated.
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：8~18 ratio acid adding
And maceration extract pH value is adjusted to 1~4, it is then fed into microwave treater and carries out microwave treatment, that is sent into microwave treater is tough
Skin how much time with microwave treatment, the proportional relation of microwave power, i.e., the bast being sent into microwave treater is more, in microwave
During processing, the time of microwave treatment is relatively longer, the selected power of microwave treater just relatively it is bigger (such as bast be sent into
250g, then the microwave power of microwave treater is 400~1500 watts, and the microwave time is 5~20 minutes), material, liquid are filtered
Separating treatment, the material separated form tough cladding, and the liquid separated forms leaching liquor.
G, the leaching liquor in step F is sent into rotary evaporator, it is dense that vacuum is carried out under 50~65 DEG C of temperature conditionss
Contracting, after concentration, is slowly added to 95% ethanol of equivalent, stirring makes the pectin in leaching liquor fully be reacted with ethanol；Reaction is completed
Afterwards, 20-32 minutes are stood, makes pectin Precipitation, then handled using vacuum filtration machine suction filtration, what much filtrate was measured with one times
75% ethanol wash, removes other impurity, finally, pectin sediment is put into 50~70 DEG C of drying machine dryings, crushes to obtain pectin
Crude product.
H, the tough cladding in step F is converted into over dry material, 2~5 kilograms of laccase, zytase is weighed by every 1000 kilograms
1~3 kilogram, 40~50 kilograms of water mix and be heated up to 40~70 DEG C form laccase, zytase dilutions, then by laccase,
Zytase dilution is uniformly sprayed on tough cladding, is sent after sprinkling to enzymolysis storehouse and is carried out enzymolysis processing, and enzymolysis time is 3~10
Hour, hydrolysis temperature is 40~80 DEG C, and the tough cladding after enzymolysis is sent to fiberizer processing；To handle obtained bast slurry send to
Eliminating potential pool, which disappears to dive, to be handled, and the latent processing time that disappears, the bast slurry after the latent processing that disappears was sent to thickener dehydration for 20~40 minutes
Reason, dewatered bast slurry is sent into drying machine processing, up to bast fiber after the completion of drying.
I, Gan Liaozhi stems fiber：By step D through the separated bar material of peeling machine send to fiberizer roughly grind, by bar material grinding into
Filament shape coarse fodder, by filament shape coarse fodder be converted into over dry and according to material water weight proportion be 1:2 ratio is sent to microwave treater
Microwave treatment is carried out (filament shape coarse fodder to be converted into over dry first, is 1 according to filament shape coarse fodder over dry and water weight proportion:2
Ratio send to microwave treater carry out microwave treatment), the filament shape coarse fodder being sent into microwave treater how much with microwave
The time of reason, the proportional relation of microwave power, i.e., the filament shape coarse fodder being sent into microwave treater is more, in microwave treatment,
The time of microwave treatment is relatively longer, the selected power of microwave treater just relatively it is bigger (such as filament shape coarse fodder be sent into
250g, then the microwave power of microwave treater is 400~1500 watts, and the microwave time is 5~20 minutes)；After microwave treatment
Coarse fodder, be converted into over dry material, 2~8 kilograms of cellulase, 2~8 kilograms of laccase, amylase 0.5 weighed by every 1000 kilograms
~3 kilograms, 200~300 kilograms of water mix and be heated up to 50~70 DEG C form cellulase, laccase, amylase mixed enzyme solutions；So
Cellulase, laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder afterwards, the filament shape coarse fodder after sprinkling send to
Digest storehouse and carry out enzymolysis processing, when enzymolysis time is 4~16 small, hydrolysis temperature is 50~70 DEG C；Filament shape coarse fodder after enzymolysis
Send to high concentration plate mill processing, obtained coarse particles will be handled and sent to eliminating potential pool disappear latent processing, the latent time that disappears for 20~40 minutes,
The coarse particles after latent processing that disappear are sent to thickener dehydration, and dewatered coarse particles are sent to drying machine processing, after the completion of dry
Up to stem's fiber.
Embodiment two
One kind is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, often saves the length control of ramulus mori section in 30 millis
Rice, is then screened by screening machine, screens and retain 30 millimeters of ramulus mori section, washed, removed with material washing machine after screening
Silt particle, dust and the other impurity on ramulus mori section are removed, forms ramulus mori section fine fodder.
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：6 ratio is sent into extractor, by extractor
Ramulus mori section fine fodder is uniformly mixed with water, carries out first time decoction to extractor heat temperature raising, specific method is as follows：To extractor liter
When temperature is to 70 DEG C, and when soaking time 2 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature to decoct, decocts
When time is 3 small, decocts terminate simultaneously to carry out feed liquid separation for the first time.
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：8 ratio is sent into extractor, by the ramulus mori section fine fodder in extractor
It is uniformly mixed with water, carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To being warming up in the tank of extractor
100 DEG C, and keep 100 DEG C of temperature to decoct, when decocting time is 3 small；Then proceed to be heated to the tank internal pressure of extractor
Power is kept the temperature when reaching 0.08Mpa, when soaking time is 0.5 small.
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor.
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent to drying in drier,
Up to extract of mulberry twig after drying.
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
E, the cladding separated in step D is converted into over dry, takes 50 kilograms of water acid addings to adjust PH by every 1000 kilograms
Value forms acidic aqueous solution, is then uniformly sprayed onto acidic aqueous solution on the cladding after exhausted bar, by the cladding after sprinkling to 3
Send to bast seperator and carry out separating treatment, the epidermis in cladding, green peel and bast is completely isolated.
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：10 ratio acid adding is simultaneously adjusted
Maceration extract pH value is saved to 1, microwave treater is then fed into and carries out microwave treatment, the bast being sent into microwave treater how much with
The time of microwave treatment, the proportional relation of microwave power, i.e., the bast being sent into microwave treater is more, in microwave treatment,
The time of microwave treatment is relatively longer, the selected power of microwave treater just relatively it is bigger (such as bast be sent into 250g, then
The microwave power of microwave treater is 400~1500 watts, and the microwave time is 5~20 minutes), microwave treatment terminates, by material, liquid
Carry out being separated by filtration processing, the material separated forms tough cladding, and the liquid separated forms leaching liquor.
G, the leaching liquor in step F is sent into rotary evaporator, is concentrated in vacuo under 55 DEG C of temperature conditionss, it is dense
After contracting, 95% ethanol of equivalent is slowly added to, stirring makes the pectin in leaching liquor fully be reacted with ethanol；It is quiet after the completion of reaction
Put 22 minutes, make pectin Precipitation, then handled using vacuum filtration machine suction filtration, much filtrate is washed with 75% alcohol of one times of amount
Wash, remove other impurity, finally, pectin sediment is put into 55 DEG C of drying machine dryings, crushes to obtain pectin crude product.
H, the tough cladding in step F is converted into over dry material, 4 kilograms of laccase, zytase 1,000 is weighed by every 1000 kilograms
Gram, 40 kilograms of water mix and be heated up to 45 DEG C form laccase, zytase dilutions, then by laccase, zytase dilution
Uniformly it is sprayed on tough cladding, is sent after sprinkling to enzymolysis storehouse and carry out enzymolysis processing, when enzymolysis time is 4 small, hydrolysis temperature 50
DEG C, the tough cladding after enzymolysis is sent to fiberizer processing；The bast slurry that processing obtains is sent to eliminating potential pool to disappear to dive and is handled, disappear latent place
It is 20 minutes to manage the time, and the bast slurry after the latent processing that disappears is sent to be sent into dry to thickener dehydration, dewatered bast slurry
Dry machine processing, up to bast fiber after the completion of drying.
I, Gan Liaozhi stems fiber：By step D through the separated bar material of peeling machine send to fiberizer roughly grind, by bar material grinding into
Filament shape coarse fodder, by filament shape coarse fodder be converted into over dry and according to material water weight proportion be 1:2.5 ratio is sent to microwave treatment
Device carries out microwave treatment and (filament shape coarse fodder is converted into over dry first, is with water weight proportion according to filament shape coarse fodder over dry
1:2.5 ratio is sent to microwave treater and carries out microwave treatment), the present embodiment send to microwave treater and carries out the thin of microwave treatment
Filamentous coarse fodder weight about 250g, microwave treatment time are 5 minutes, and the microwave power of microwave treater is 900 watts；Microwave treatment
After coarse fodder, be converted into over dry material, 2.5 kilograms of cellulase, 4 kilograms of laccase, amylase 0.5 weighed by every 1000 kilograms
Kilogram, 200 kilograms of water mix and be heated up to 50 DEG C form cellulase, laccase, amylase mixed enzyme solutions；Then by cellulose
Enzyme, laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder, and the filament shape coarse fodder after sprinkling send to enzymolysis storehouse and carries out
Enzymolysis processing, when enzymolysis time is 6 small, hydrolysis temperature is 50 DEG C；Filament shape coarse fodder after enzymolysis is sent to high concentration plate mill processing,
Obtained coarse particles will be handled and sent to eliminating potential pool and disappeared latent processing, the latent time that disappears for 25 minutes, the coarse particles after the latent processing that disappears send to
Thickener dehydration, dewatered coarse particles are sent to drying machine processing, up to stem's fiber after the completion of drying.
Embodiment three
One kind is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, often saves the length control of ramulus mori section in 40 millis
Rice, is then screened by screening machine, screens and retain 40 millimeters of ramulus mori section, washed, removed with material washing machine after screening
Silt particle, dust and the other impurity on ramulus mori section are removed, forms ramulus mori section fine fodder.
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：8 ratio is sent into extractor, by extractor
Ramulus mori section fine fodder is uniformly mixed with water, carries out first time decoction to extractor heat temperature raising, specific method is as follows：To extractor liter
When temperature is to 75 DEG C, and when soaking time 1.5 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature to decoct, decocts
Boil the time for 3.5 it is small when, decoct terminate simultaneously to carry out feed liquid separation for the first time.
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：7 ratio is sent into extractor, by the ramulus mori section fine fodder in extractor
It is uniformly mixed with water, carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To being warming up in the tank of extractor
100 DEG C, and keep 100 DEG C of temperature to decoct, when decocting time is 2 small；Then proceed to be heated to the tank internal pressure of extractor
Power is kept the temperature when reaching 0.07Mpa, when soaking time is 0.6 small.
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor.
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent in spray dryer
It is dry, up to extract of mulberry twig after drying.
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
E, the cladding separated in step D is converted into over dry, takes 60 kilograms of water acid addings to adjust PH by every 1000 kilograms
Value forms acidic aqueous solution, is then uniformly sprayed onto acidic aqueous solution on the cladding after exhausted bar, by the cladding after sprinkling to 3
Send to bast seperator and carry out separating treatment, the epidermis in cladding, green peel and bast is completely isolated.
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：11 ratio acid adding is simultaneously adjusted
Maceration extract pH value is saved to 1, the bast of weight about 250g is then sent into microwave treater and carries out microwave treatment, microwave treater
600 watts of microwave power, 12 minutes microwave time, microwave treatment terminates, will material, liquid carry out being separated by filtration processing, separate
Material form tough cladding, the liquid separated forms leaching liquor.
G, the leaching liquor in step F is sent into rotary evaporator, is concentrated in vacuo under 56 DEG C of temperature conditionss, it is dense
After contracting, 95% ethanol of equivalent is slowly added to, stirring makes the pectin in leaching liquor fully be reacted with ethanol；It is quiet after the completion of reaction
Put 24 minutes, make pectin Precipitation, then handled using vacuum filtration machine suction filtration, much filtrate is washed with 75% alcohol of one times of amount
Wash, remove other impurity, finally, pectin sediment is put into 60 DEG C of drying machine dryings, crushes to obtain pectin crude product.
H, the tough cladding in step F is converted into over dry material, 3.6 kilograms of laccase, zytase is weighed by every 1000 kilograms
1.4 kilograms, 45 kilograms of water mix and be heated up to 50 DEG C form laccase, zytase dilutions, it is then that laccase, zytase is dilute
Release liquid to be uniformly sprayed on tough cladding, sent after sprinkling to enzymolysis storehouse and carry out enzymolysis processing, when enzymolysis time is 4.5 small, enzymolysis temperature
Spend for 55 DEG C, the tough cladding after enzymolysis is sent to fiberizer processing；The bast slurry obtained after processing is sent to eliminating potential pool to disappear to dive and is located
Reason, the latent processing time that disappears, the bast slurry after the latent processing that disappears was sent to thickener dehydration, dewatered tough latex for 25 minutes
Material is sent into drying machine processing, up to bast fiber after the completion of drying.
I, Gan Liaozhi stems fiber：By step D through the separated bar material of peeling machine send to fiberizer roughly grind, by bar material grinding into
Filament shape coarse fodder, by filament shape coarse fodder be converted into over dry and according to material water weight proportion be 1:2.5 ratio is sent to microwave treatment
Device carries out microwave treatment and (filament shape coarse fodder is converted into over dry first, is with water weight proportion according to filament shape coarse fodder over dry
1:2.5 ratio is sent to microwave treater and carries out microwave treatment), the present embodiment send to microwave treater and carries out the thin of microwave treatment
Filamentous coarse fodder weight about 250g, microwave treatment time are 6 minutes, and the microwave power of microwave treater is 800 watts；Microwave treatment
After coarse fodder, be converted into over dry material, 2.8 kilograms of cellulase, 3.8 kilograms of laccase, amylase weighed by every 1000 kilograms
0.6 kilogram, 250 kilograms of water mix and be heated up to 55 DEG C form cellulase, laccase, amylase mixed enzyme solutions；Then by fiber
Plain enzyme, laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder, the filament shape coarse fodder after sprinkling send to enzymolysis storehouse into
Row enzymolysis processing, when enzymolysis time is 7 small, hydrolysis temperature is 55 DEG C；Filament shape coarse fodder after enzymolysis is sent to high concentration plate mill
Reason, the coarse particles obtained after processing are sent to eliminating potential pool and are disappeared latent processing, the latent time that disappears for 30 minutes, the coarse particles after the latent processing that disappears
Send to thickener dehydration, dewatered coarse particles are sent to drying machine processing, up to stem's fiber after the completion of drying.
Example IV
One kind is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, often saves the length control of ramulus mori section in 50 millis
Rice, is then screened by screening machine, screens and retain 50 millimeters of ramulus mori section, washed, removed with material washing machine after screening
Silt particle, dust and the other impurity on ramulus mori section are removed, forms ramulus mori section fine fodder.
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：10 ratio is sent into extractor, by extractor
Ramulus mori section fine fodder is uniformly mixed with water, carries out first time decoction to extractor heat temperature raising, specific method is as follows：To extractor liter
When temperature is to 80 DEG C, and when soaking time 1.5 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature to decoct, decocts
Boil the time for 3.5 it is small when, decoct terminate simultaneously to carry out feed liquid separation for the first time.
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：6 ratio is sent into extractor, by the ramulus mori section fine fodder in extractor
It is uniformly mixed with water, carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To being warming up in the tank of extractor
100 DEG C, and keep 100 DEG C of temperature to decoct, when decocting time is 2 small；Then proceed to be heated to the tank internal pressure of extractor
Power is kept the temperature when reaching 0.06Mpa, when soaking time is 0.7 small.
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor.
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent in spray dryer
It is dry, up to extract of mulberry twig after drying.
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
E, the cladding separated in step D is converted into over dry, takes 70 kilograms of water acid addings to adjust PH by every 1000 kilograms
Value forms acidic aqueous solution, is then uniformly sprayed onto acidic aqueous solution on the cladding after exhausted bar, by the cladding after sprinkling to 4
Send to bast seperator and carry out separating treatment, the epidermis in cladding, green peel and bast is completely isolated.
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：12 ratio acid adding is simultaneously adjusted
Maceration extract pH value is saved to 2, the bast of weight about 250g is then sent into microwave treater and carries out microwave treatment, microwave treater
700 watts of microwave power, 10 minutes microwave time, microwave treatment terminates, will material, liquid carry out being separated by filtration processing, separate
Material form tough cladding, the liquid separated forms leaching liquor.
G, the leaching liquor in step F is sent into rotary evaporator, is concentrated in vacuo under 57 DEG C of temperature conditionss, it is dense
After contracting, 95% ethanol of equivalent is slowly added to, stirring makes the pectin in leaching liquor fully be reacted with ethanol；It is quiet after the completion of reaction
Put 26 minutes, make pectin Precipitation, then handled using vacuum filtration machine suction filtration, much filtrate is washed with 75% alcohol of one times of amount
Wash, remove other impurity, finally, pectin sediment is put into 60 DEG C of drying machine dryings, crushes to obtain pectin crude product.
H, the tough cladding in step F is converted into over dry material, 3.4 kilograms of laccase, zytase is weighed by every 1000 kilograms
1.6 kilograms, 45 kilograms of water mix and be heated up to 55 DEG C form laccase, zytase dilutions, it is then that laccase, zytase is dilute
Release liquid to be uniformly sprayed on tough cladding, sent after sprinkling to enzymolysis storehouse and carry out enzymolysis processing, when enzymolysis time is 5 small, hydrolysis temperature
For 60 DEG C, the tough cladding after enzymolysis is sent to fiberizer processing；The bast slurry obtained after processing is sent to eliminating potential pool to disappear to dive and is handled,
Latent processing time disappeared as 30 minutes, the bast slurry after the latent processing that disappears is sent to thickener dehydration, dewatered bast slurry
Drying machine processing is sent into, up to bast fiber after the completion of drying.
I, Gan Liaozhi stems fiber：By step D through the separated bar material of peeling machine send to fiberizer roughly grind, by bar material grinding into
Filament shape coarse fodder, by filament shape coarse fodder be converted into over dry and according to material water weight proportion be 1:3 ratio is sent to microwave treater
Microwave treatment is carried out (filament shape coarse fodder to be converted into over dry first, is 1 according to filament shape coarse fodder over dry and water weight proportion:3
Ratio send to microwave treater carry out microwave treatment), the present embodiment send to microwave treater carry out microwave treatment filament shape
Coarse fodder weight about 250g, microwave treatment time are 7 minutes, and the microwave power of microwave treater is 700 watts；Microwave treatment terminates
Coarse fodder afterwards, is converted into over dry material, and 3 kilograms of cellulase, 3.6 kilograms of laccase, amylase 0.7 thousand are weighed by every 1000 kilograms
Gram, 250 kilograms of water mix and be heated up to 60 DEG C form cellulase, laccase, amylase mixed enzyme solutions；Then by cellulase,
Laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder, and the filament shape coarse fodder after sprinkling send to enzymolysis storehouse and carries out enzyme
Solution processing, when enzymolysis time is 8 small, hydrolysis temperature is 60 DEG C；Filament shape coarse fodder after enzymolysis is sent to high concentration plate mill processing, will
The coarse particles obtained after processing, which are sent to eliminating potential pool, to disappear latent processing, the latent time that disappears for 35 minutes, the coarse particles after the latent processing that disappears send to
Thickener dehydration, dewatered coarse particles are sent to air drier processing, up to stem's fiber after the completion of drying.
Embodiment five
One kind is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, often saves the length control of ramulus mori section in 60 millis
Rice, is then screened by screening machine, screens and retain 60 millimeters of ramulus mori section, washed, removed with material washing machine after screening
Silt particle, dust and the other impurity on ramulus mori section are removed, forms ramulus mori section fine fodder.
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：12 ratio is sent into extractor, by extractor
Ramulus mori section fine fodder is uniformly mixed with water, carries out first time decoction to extractor heat temperature raising, specific method is as follows：To extractor liter
When temperature is to 85 DEG C, and when soaking time 1 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature to decoct, decocts
When time is 3.5 small, decocts terminate simultaneously to carry out feed liquid separation for the first time.
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：5 ratio is sent into extractor, by the ramulus mori section fine fodder in extractor
It is uniformly mixed with water, carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To being warming up in the tank of extractor
100 DEG C, and keep 100 DEG C of temperature to decoct, when decocting time is 3 small；Then proceed to be heated to the tank internal pressure of extractor
Power is kept the temperature when reaching 0.05Mpa, when soaking time is 0.8 small.
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor.
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent in spray dryer
It is dry, up to extract of mulberry twig after drying.
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
E, the cladding separated in step D is converted into over dry, takes 80 kilograms of water acid addings to adjust PH by every 1000 kilograms
Value forms acidic aqueous solution, is then uniformly sprayed onto acidic aqueous solution on the cladding after exhausted bar, by the cladding after sprinkling to 4
Send to bast seperator and carry out separating treatment, the epidermis in cladding, green peel and bast is completely isolated.
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：13 ratio acid adding is simultaneously adjusted
Maceration extract pH value is saved to 2, the bast of weight about 250g is then sent into microwave treater and carries out microwave treatment, microwave treater
800 watts of microwave power, 8 minutes microwave time, microwave treatment terminates, will material, liquid carry out being separated by filtration processing, separate
Material forms tough cladding, and the liquid separated forms leaching liquor.
G, the leaching liquor in step F is sent into rotary evaporator, is concentrated in vacuo under 58 DEG C of temperature conditionss, it is dense
After contracting, 95% ethanol of equivalent is slowly added to, stirring makes the pectin in leaching liquor fully be reacted with ethanol；It is quiet after the completion of reaction
Put 28 minutes, make pectin Precipitation, then handled using vacuum filtration machine suction filtration, much filtrate is washed with 75% alcohol of one times of amount
Wash, remove other impurity, finally, pectin sediment is put into 65 DEG C of drying machine dryings, crushes to obtain pectin crude product.
H, the tough cladding in step F is converted into over dry material, 3.2 kilograms of laccase, zytase is weighed by every 1000 kilograms
1.8 kilograms, 50 kilograms of water mix and be heated up to 60 DEG C form laccase, zytase dilutions, it is then that laccase, zytase is dilute
Release liquid to be uniformly sprayed on tough cladding, sent after sprinkling to enzymolysis storehouse and carry out enzymolysis processing, when enzymolysis time is 5 small, hydrolysis temperature
For 65 DEG C, the tough cladding after enzymolysis is sent to fiberizer processing；The bast slurry obtained after processing is sent to eliminating potential pool to disappear to dive and is handled,
Latent processing time disappeared as 35 minutes, the bast slurry after the latent processing that disappears is sent to thickener dehydration, dewatered bast slurry
Drying machine processing is sent into, up to bast fiber after the completion of drying.
I, Gan Liaozhi stems fiber：By step D through the separated bar material of peeling machine send to fiberizer roughly grind, by bar material grinding into
Filament shape coarse fodder is converted into over dry and is 1 according to material water weight proportion by filament shape coarse fodder:4 ratio send to microwave treater into
Filament shape coarse fodder (is converted into over dry first, is 1 according to filament shape coarse fodder over dry and water weight proportion by row microwave treatment:4
Ratio is sent to microwave treater and carries out microwave treatment), the present embodiment send to microwave treater the filament shape for carrying out microwave treatment thick
Expect weight about 250g, microwave treatment time is 8 minutes, and the microwave power of microwave treater is 600 watts；After microwave treatment
Coarse fodder, be converted into over dry material, 3.2 kilograms of cellulase, 3.4 kilograms of laccase, amylase 0.8 thousand weighed by every 1000 kilograms
Gram, 300 kilograms of water mix and be heated up to 65 DEG C form cellulase, laccase, amylase mixed enzyme solutions；Then by cellulase,
Laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder, and the filament shape coarse fodder after sprinkling send to enzymolysis storehouse and carries out enzyme
Solution processing, when enzymolysis time is 9 small, hydrolysis temperature is 65 DEG C；Filament shape coarse fodder after enzymolysis is sent to high concentration plate mill processing, will
The coarse particles obtained after processing, which are sent to eliminating potential pool, to disappear latent processing, the latent time that disappears for 35 minutes, the coarse particles after the latent processing that disappears send to
Thickener dehydration, dewatered coarse particles are sent to drying machine processing, up to stem's fiber after the completion of drying.
Embodiment six
One kind is as follows using mulberry branch separation cladding and bar material, Preparation method and use, its method and step：
A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, often saves the length control of ramulus mori section in 70 millis
Rice, is then screened by screening machine, screens and retain 70 millimeters of ramulus mori section, washed, removed with material washing machine after screening
Silt particle, dust and the other impurity on ramulus mori section are removed, forms ramulus mori section fine fodder.
B, by ramulus mori section fine fodder and water according to material water weight proportion 1：14 ratio is sent into extractor, by extractor
Ramulus mori section fine fodder is uniformly mixed with water, carries out first time decoction to extractor heat temperature raising, specific method is as follows：To extractor liter
When temperature is to 90 DEG C, and when soaking time 1 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature to decoct, decocts
When time is 4 small, decocts terminate simultaneously to carry out feed liquid separation for the first time.
Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, will be separated
Ramulus mori section fine fodder and water according to material water weight proportion 1：4 ratio is sent into extractor, by the ramulus mori section fine fodder in extractor
It is uniformly mixed with water, carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To being warming up in the tank of extractor
100 DEG C, and keep 100 DEG C of temperature to decoct, when decocting time is 2 small；Then proceed to be heated to the tank internal pressure of extractor
Power is kept the temperature when reaching 0.04Mpa, when soaking time is 0.9 small.
Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts isolate twice
The liquid come, which merges, to be stood, and leaching supernatant, forms decoction liquor.
C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent in spray dryer
It is dry, up to extract of mulberry twig after drying.
D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding
With bar material.
E, the cladding separated in step D is converted into over dry, takes 90 kilograms of water acid addings to adjust PH by every 1000 kilograms
Value forms acidic aqueous solution, is then uniformly sprayed onto acidic aqueous solution on the cladding after exhausted bar, by the cladding after sprinkling to 5
Send to bast seperator and carry out separating treatment, the epidermis in cladding, green peel and bast is completely isolated.
F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：14 ratio acid adding is simultaneously adjusted
Maceration extract pH value is saved to 1, the bast of weight about 250g is then sent into microwave treater and carries out microwave treatment, microwave treater
900 watts of microwave power, 6 minutes microwave time, microwave treatment terminates, will material, liquid carry out being separated by filtration processing, separate
Material forms tough cladding, and the liquid separated forms leaching liquor.
G, the leaching liquor in step F is sent into rotary evaporator, is concentrated in vacuo under 59 DEG C of temperature conditionss, it is dense
After contracting, 95% ethanol of equivalent is slowly added to, stirring makes the pectin in leaching liquor fully be reacted with ethanol；It is quiet after the completion of reaction
Put 30 minutes, make pectin Precipitation, then handled using vacuum filtration machine suction filtration, much filtrate is washed with 75% alcohol of one times of amount
Wash, remove other impurity, finally, pectin sediment is put into 70 DEG C of drying machine dryings, crushes to obtain pectin crude product.
H, the tough cladding in step F is converted into over dry material, 3 kilograms of laccase, zytase 2,000 is weighed by every 1000 kilograms
Gram, 50 kilograms of water mix and be heated up to 65 DEG C form laccase, zytase dilutions, then by laccase, zytase dilution
Uniformly it is sprayed on tough cladding, is sent after sprinkling to enzymolysis storehouse and carry out enzymolysis processing, when enzymolysis time is 6 small, hydrolysis temperature 70
DEG C, the tough cladding after enzymolysis is sent to fiberizer processing；The bast slurry obtained after processing is sent to eliminating potential pool to disappear to dive and is handled, is disappeared latent
Processing time is 40 minutes, and the bast slurry after the latent processing that disappears, which is sent to thickener dehydration, dewatered bast slurry, to be sent into
Drying machine processing, up to bast fiber after the completion of drying.
I, Gan Liaozhi stems fiber：By step D through the separated bar material of peeling machine send to fiberizer roughly grind, by bar material grinding into
Filament shape coarse fodder, the filament shape coarse fodder of about 250g is sent to microwave treater and carries out microwave treatment, and microwave treatment time is 9 points
Clock, the microwave power of microwave treater is 500 watts；Coarse fodder after microwave treatment, is converted into over dry material, by every 1000 kilograms
3.5 kilograms of cellulase, 3 kilograms of laccase are weighed, 0.9 kilogram, 300 kilograms water of amylase mix and are heated up to 70 DEG C of composition fibers
Plain enzyme, laccase, amylase mixed enzyme solution；Then by cellulase, laccase, that amylase mixed enzyme solution is uniformly sprayed onto filament shape is thick
On material, the filament shape coarse fodder after sprinkling send to enzymolysis storehouse and carries out enzymolysis processing, when enzymolysis time is 10 small, hydrolysis temperature 70
℃；Filament shape coarse fodder after enzymolysis is sent to high concentration plate mill processing, and the coarse particles obtained after processing are sent to eliminating potential pool to disappear to dive and are located
Reason, the latent time that disappears, the coarse particles after the latent processing that disappears were sent to thickener dehydration, and dewatered coarse particles are sent to dry for 40 minutes
Dry machine processing, up to stem's fiber after the completion of drying.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should all be included in the protection scope of the present invention.
Claims (9)
- A kind of 1. preparation method that cladding and bar material are separated using mulberry branch, it is characterised in that：Its method and step is as follows：A, stock up：Mulberry branch is cut into ramulus mori section by wood material cutting machine, the length for often saving ramulus mori section is controlled at 10~80 millimeters, Then screened by screening machine, screen and retain 10~80 millimeters of ramulus mori section, washed, removed with material washing machine after screening Silt particle, dust and the other impurity on ramulus mori section are removed, forms ramulus mori section fine fodder；B, by ramulus mori section fine fodder and water according to material water weight proportion 1：4~15 ratio is sent into extractor, by extractor Ramulus mori section fine fodder is uniformly mixed with water, carries out first time decoction to extractor heat temperature raising, specific method is as follows：To extractor liter When temperature is to 70~90 DEG C, and when soaking time 1~3 is small；It is then followed by being warming up to 100 DEG C, and keeps 100 DEG C of temperature to decoct Boil, when decocting time is 2~6 small, decocts terminate simultaneously to carry out feed liquid separation for the first time；Feed liquid separates；Ramulus mori section fine fodder feed separation in extractor is out carried out decocting for second, the mulberry that will be separated Minor matters fine fodder is with water according to material water weight proportion 1：4~8 ratio is sent into extractor, by the ramulus mori section fine fodder in extractor with Water is uniformly mixed, and carrying out second to extractor heat temperature raising decocts, and specific method is as follows：To being warming up in the tank of extractor 100 DEG C, and keep 100 DEG C of temperature to decoct, when decocting time is 2~4 small；Then proceed to be heated in the tank of extractor Pressure is kept the temperature when reaching 0.01~0.09Mpa, when soaking time is 0.5~3 small；Then feed liquid separation is carried out, the ramulus mori section fine fodder residue separated forms decoction material, decocts what is separated twice Liquid, which merges, to be stood, and leaching supernatant, forms decoction liquor；C, decoction liquor concentration, drying：The decoction liquor of step B is sent into evaporator concentration, is then sent in drier dry, drying Afterwards up to extract of mulberry twig；D, decoction material skin, bar separation：The decoction material of step B is sent into peeling machine and carries out skin, bar separation, isolated cladding and bar Material.
- 2. a kind of mulberry branch cladding and bar material, it is characterised in that be prepared by claim 1 the method.
- A kind of 3. purposes of mulberry branch cladding, it is characterised in that：Pectin crude extract is used to prepare, its method is as follows：E, cladding in claim 2 is converted into over dry, takes 40~double centner water acid adding to adjust pH value to 3 by every 1000 kilograms ~5, acidic aqueous solution is formed, then acidic aqueous solution is uniformly sprayed onto on the cladding after exhausted bar, the cladding after sprinkling is sent Separating treatment is carried out to bast seperator, the epidermis in cladding, green peel and bast is completely isolated；F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：8~18 ratio acid adding is simultaneously adjusted Maceration extract pH value is saved to 1~4, microwave treater is then fed into and carries out microwave treatment, microwave treatment terminates, and material, liquid were carried out Separating treatment is filtered, the material separated forms tough cladding, and the liquid separated forms leaching liquor；G, the leaching liquor in step F is sent into rotary evaporator, is concentrated in vacuo under 50~65 DEG C of temperature conditionss, it is dense After contracting, 95% ethanol of equivalent is slowly added to, stirring makes the pectin in leaching liquor fully be reacted with ethanol；It is quiet after the completion of reaction Put 20-32 minutes, make pectin Precipitation, then handled using vacuum filtration machine suction filtration, one times of 75% wine measured of much filtrate Fine purifiation is washed, and removes other impurity, finally, pectin sediment is put into 50~70 DEG C of drying machine dryings, crushes to obtain pectin crude product.
- A kind of 4. purposes for the pectin crude product produced in accordance with the method for claim 3, it is characterised in that：For as production The raw material of pectin.
- A kind of 5. purposes of mulberry branch cladding, it is characterised in that：Bast fiber extract is used to prepare, its method is as follows：E, cladding in claim 2 is converted into over dry, takes 40~double centner water acid adding to adjust pH value to 3 by every 1000 kilograms ~5, acidic aqueous solution is formed, then acidic aqueous solution is uniformly sprayed onto on the cladding after exhausted bar, the cladding after sprinkling is sent Separating treatment is carried out to bast seperator, the epidermis in cladding, green peel and bast is completely isolated；F, the bast separated in step E is converted into over dry, by material, liquid weight proportion 1：8~18 ratio acid adding is simultaneously adjusted Maceration extract pH value is saved to 1~4, microwave treater is then fed into and carries out microwave treatment, microwave treatment terminates, and material, liquid were carried out Separating treatment is filtered, the material separated forms tough cladding；H, the tough cladding in step F is converted into over dry material, 2~5 kilograms of laccase, zytase 1~3 is weighed by every 1000 kilograms Kilogram, 40~50 kilograms of water mix and be heated up to 40~70 DEG C and form laccase, zytase dilutions, it is then that laccase, wood is poly- Carbohydrase dilution is uniformly sprayed on tough cladding, is sent after sprinkling to enzymolysis storehouse and is carried out enzymolysis processing, and enzymolysis time is small for 3~10 When, hydrolysis temperature is 40~80 DEG C, and the tough cladding after enzymolysis is sent to fiberizer processing；By the bast slurry obtained after processing send to Eliminating potential pool, which disappears to dive, to be handled, and the latent processing time that disappears, the bast slurry after the latent processing that disappears was sent to thickener dehydration for 20~40 minutes Reason, dewatered bast slurry is sent into drying machine processing, up to bast fiber after the completion of drying.
- A kind of 6. purposes for the bast fiber produced in accordance with the method for claim 5, it is characterised in that：For paper industry Make the raw material of production speciality paper or make the raw material of production textile for textile industry.
- A kind of 7. purposes of ramulus mori bar material, it is characterised in that：Stem's fiber extract is used to prepare, its method is as follows：I, Gan Liaozhi stems fiber：Bar material in claim 2 is sent to fiberizer and is roughly ground, bar material grinding is thick into filament shape Material, by filament shape coarse fodder be converted into over dry and according to material water weight proportion be 1:2~4 ratio is sent micro- to microwave treater progress Ripple is handled, and the coarse fodder after microwave treatment, is converted into over dry material, and 2~8 kilograms of cellulase, paint are weighed by every 1000 kilograms 2~8 kilograms of enzyme, 0.5~3 kilogram, 200~300 kilograms water of amylase, which mix and are heated up to 50~70 DEG C, forms cellulase, paint Enzyme, amylase mixed enzyme solution；Then cellulase, laccase, amylase mixed enzyme solution are uniformly sprayed onto on filament shape coarse fodder, sprayed Filament shape coarse fodder after spilling send to enzymolysis storehouse and carries out enzymolysis processing, and when enzymolysis time is 4~16 small, hydrolysis temperature is 50~70 ℃；Filament shape coarse fodder after enzymolysis is sent to high concentration plate mill processing, and the coarse particles obtained after processing are sent to eliminating potential pool to disappear to dive and are located Reason, the latent time that disappears, the coarse particles after the latent processing that disappears, which are sent to thickener dehydration, dewatered coarse particles, to be sent for 20~40 minutes To drying machine processing, up to stem's fiber after the completion of drying.
- A kind of 8. purposes for the stem's fiber produced in accordance with the method for claim 7, it is characterised in that：For paper industry Make the raw material of production newsprint, cultural paper, package paper, or make the raw material of production textile for textile industry.
- A kind of 9. purposes for the decoction liquor produced in accordance with the method for claim 1, it is characterised in that：For producing Chinese medicines Material, health products, drink, the raw material of raw-food material or feedstuff, its specific method are as follows：The extract of mulberry twig produced after the decoction liquor produced in claim 1 step B is concentrated and dried, the extract of mulberry twig are used In the raw material of production Chinese medicinal material, health products, drink, raw-food material or feedstuff.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810095380.XA CN108017722B (en) | 2018-01-31 | 2018-01-31 | Method for separating bark material and stalk material by utilizing mulberry branches, preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810095380.XA CN108017722B (en) | 2018-01-31 | 2018-01-31 | Method for separating bark material and stalk material by utilizing mulberry branches, preparation method and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108017722A true CN108017722A (en) | 2018-05-11 |
| CN108017722B CN108017722B (en) | 2021-04-27 |
Family
ID=62075052
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810095380.XA Active CN108017722B (en) | 2018-01-31 | 2018-01-31 | Method for separating bark material and stalk material by utilizing mulberry branches, preparation method and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108017722B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108691226A (en) * | 2018-05-30 | 2018-10-23 | 张明勋 | A kind of paper mulberry branch method of comprehensive utilization detached based on cladding and bar material |
| CN109176778A (en) * | 2018-10-15 | 2019-01-11 | 张明勋 | A kind of method and daily necessity using branch bast fiber production daily necessity |
| CN115058915A (en) * | 2022-06-15 | 2022-09-16 | 江苏博汇纸业有限公司 | Production process of unbleached pulp for papermaking |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101372763A (en) * | 2008-09-26 | 2009-02-25 | 绍兴中纺院江南分院有限公司 | Method for preparing bamboo primary fibre using composite biological enzyme |
| CN101634049A (en) * | 2009-08-28 | 2010-01-27 | 广西绢麻纺织科学研究所 | Method for rapidly separating bast surface layer of ramulus mori |
| CN102532334A (en) * | 2011-10-24 | 2012-07-04 | 巴勇舸 | Method for producing flaxseed mucilage |
| CN103263514A (en) * | 2013-05-23 | 2013-08-28 | 浙江省柑桔研究所 | Method for extracting flavones, low-molecule pectin and cellulose from orange peels in combined way |
| CN103724452A (en) * | 2013-12-02 | 2014-04-16 | 东北林业大学 | Method for extracting pectin from peony fruit pods |
| CN103989747A (en) * | 2014-05-30 | 2014-08-20 | 张明勋 | Method for comprehensively utilizing mulberry twig through medicine extraction and pulping |
| CN105442059A (en) * | 2015-11-09 | 2016-03-30 | 长兴业美纺织有限公司 | Chinese alpine rush fibers having good antibacterial performance and used for weaving |
-
2018
- 2018-01-31 CN CN201810095380.XA patent/CN108017722B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101372763A (en) * | 2008-09-26 | 2009-02-25 | 绍兴中纺院江南分院有限公司 | Method for preparing bamboo primary fibre using composite biological enzyme |
| CN101634049A (en) * | 2009-08-28 | 2010-01-27 | 广西绢麻纺织科学研究所 | Method for rapidly separating bast surface layer of ramulus mori |
| CN102532334A (en) * | 2011-10-24 | 2012-07-04 | 巴勇舸 | Method for producing flaxseed mucilage |
| CN103263514A (en) * | 2013-05-23 | 2013-08-28 | 浙江省柑桔研究所 | Method for extracting flavones, low-molecule pectin and cellulose from orange peels in combined way |
| CN103724452A (en) * | 2013-12-02 | 2014-04-16 | 东北林业大学 | Method for extracting pectin from peony fruit pods |
| CN103989747A (en) * | 2014-05-30 | 2014-08-20 | 张明勋 | Method for comprehensively utilizing mulberry twig through medicine extraction and pulping |
| CN105442059A (en) * | 2015-11-09 | 2016-03-30 | 长兴业美纺织有限公司 | Chinese alpine rush fibers having good antibacterial performance and used for weaving |
Non-Patent Citations (4)
| Title |
|---|
| 刘琳等: ""桑皮纳米纤维的制备和果胶的提取及其应用研究"", 《第六届长三角科技论坛—产业用纺织品/非织造布的技术升级与产品创新纺织分论坛论文集》 * |
| 刘钟栋: "《微波技术在食品工业中的应用》", 28 February 1998, 中国轻工业出版社 * |
| 李文颖等: "《远古仓颉与中华汉字》", 31 December 2003, ***出版社 * |
| 罗猛著: "《长春花生物碱高效提取技术研究》", 31 May 2012, 黑龙江科学技术出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108691226A (en) * | 2018-05-30 | 2018-10-23 | 张明勋 | A kind of paper mulberry branch method of comprehensive utilization detached based on cladding and bar material |
| CN109176778A (en) * | 2018-10-15 | 2019-01-11 | 张明勋 | A kind of method and daily necessity using branch bast fiber production daily necessity |
| CN115058915A (en) * | 2022-06-15 | 2022-09-16 | 江苏博汇纸业有限公司 | Production process of unbleached pulp for papermaking |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108017722B (en) | 2021-04-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110978171B (en) | Preparation method and application of bamboo pulp fiber and bamboo extract from bamboo | |
| CN106283795B (en) | A method of separation hemicellulose and cellulose | |
| CN108017722A (en) | One kind utilizes mulberry branch separation cladding and bar material, Preparation method and use | |
| CN103320476B (en) | Method and technology for high-value comprehensive utilization of banana stems and leaves | |
| CN104975356A (en) | Mulberry bark degumming method | |
| CN108179646A (en) | With the method for plant fiber material production xylose, high-boiling alcohol lignin and fiber | |
| CN109112891A (en) | A method of wrapping paper is prepared with arghan and banana caulo slurry | |
| CN103387599A (en) | Technology for extracting protein of folium mori | |
| CN106676925A (en) | Immersion-free papermaking process capable of taking plant stalks as raw materials | |
| CN105862494A (en) | Method for preparing unbleached pulp from sunflower seed shells | |
| CN106632586B (en) | Method for simultaneously extracting starch and protein | |
| CN110791996B (en) | Method for preparing radix puerariae residue slurry from radix puerariae residues and making paper | |
| CN104928958A (en) | Method of producing corrugated paper with straw | |
| CN108691226A (en) | A kind of paper mulberry branch method of comprehensive utilization detached based on cladding and bar material | |
| CN110643052A (en) | Method for extracting gutta-percha by treating eucommia ulmoides shells with sodium hydroxide/urea aqueous solution | |
| CN106397611A (en) | Separation method for two-step-organic-solvent biological-refined ingredients of oil tea processing wastes | |
| CN102660778B (en) | Method for preparing cotton stalk bast spinning process fibers by biological technology and degumming reaction kettle | |
| CN104088181A (en) | Method for extracting sap and pulping from paper mulberry branches and comprehensively utilizing paper mulberry branches | |
| CN108653359A (en) | A kind of preparation method of reed wormwood artemisia general flavone | |
| CN211815147U (en) | A assembly line separation preparation system for pulping of paper mulberry branch | |
| CN106947788A (en) | A kind of method that utilization energy grass prepares fermentation grass juice factor and paper pulp | |
| CN104626310B (en) | A kind of manufacture method of rice straw composite fiber | |
| CN101717438A (en) | Method for extracting leaf protein of sweet potato vine | |
| CN105537248A (en) | Comprehensive utilization method of banana stems and leaves | |
| CN105970717A (en) | Method for preparing unbleached pulp of raw material of egg trays with tail pulp of crop straws |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20231105 Address after: Room 301, Shuangchuang Valley, Economic Development Zone, No. 5 Wangchong Street, Yongchang Town, Beichuan Qiang Autonomous County, Mianyang City, Sichuan Province, 621000 Patentee after: Sichuan Qiangyuan Jiasheng Technology Co.,Ltd. Address before: Building 3, Zone B, Sunshine Tsinghua University, No. 21 Horticultural Street, Science and Technology Innovation Park, Mianyang City, Sichuan Province, 621000 Patentee before: Zhang Mingxun |
|
| TR01 | Transfer of patent right |