CN108004066A - It is a kind of suitable for soap of sensitiveness skin and preparation method thereof - Google Patents

It is a kind of suitable for soap of sensitiveness skin and preparation method thereof Download PDF

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Publication number
CN108004066A
CN108004066A CN201711251469.2A CN201711251469A CN108004066A CN 108004066 A CN108004066 A CN 108004066A CN 201711251469 A CN201711251469 A CN 201711251469A CN 108004066 A CN108004066 A CN 108004066A
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CN
China
Prior art keywords
soap
parts
preparation
fish oil
sodium hydroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711251469.2A
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Chinese (zh)
Inventor
宋文东
魏丹艺
郭健
纪丽丽
蔡璐
王亚宁
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Zhejiang Ocean University ZJOU
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Zhejiang Ocean University ZJOU
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Publication date
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Priority to CN201711251469.2A priority Critical patent/CN108004066A/en
Publication of CN108004066A publication Critical patent/CN108004066A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of suitable for soap of sensitiveness skin and preparation method thereof, comprise the following steps:Comprise the following steps:(1)Fish oil and sodium hydroxide solution are subjected to 1 8h of saponification, then successively saltouts and is analysed with alkali, obtains pure soap base of the content of fatty acid more than 60%;(2)Deionized water is added when stirring soap base, when temperature reaches 70 80 DEG C, sequentially adds alkyl-glucoside, glycerine and stearic acid, it is 67 to adjust pH value of solution;(3)Trehalose and plants essential oil are eventually adding, after stirring 1 10h, is stood up to the soap.The present invention effectively removes oil stain and spot, easily rinsing using natural fish oil as emulsifying agent, gentle non-stimulated, and raw materials used nontoxicity, and production process is environmentally protective, has extensive market value.

Description

It is a kind of suitable for soap of sensitiveness skin and preparation method thereof
Technical field
The present invention relates to daily chemical product processing technique field, more particularly, to a kind of fertilizer suitable for sensitiveness skin Soap and preparation method thereof.
Background technology
In recent years, with the prosperity and development of modern industry, oil, printing and dyeing, chemical industry, agricultural and the production of mankind's everyday life Raw amount of pollutants increases sharply, and the hazard weather such as haze, sandstorm just increasingly encroaches on the tender and lovely skin of people, with skin Patient's group's accounting is growing.Sensitiveness skin is a kind of skin being at any time in high alert, and skin allergy can cause skin Skin is dried, decortication, rubescent, greasy or even sensitive shouting pain.Common soap is the surfactant with chemical synthesis mostly on the market What saponification obtained, such soap pH value is higher, and human skin is in faintly acid, therefore can destroy the tender and lovely guarantor of skin surface Barrier is protected, aggravates skin allergy.
Up to the present, existing many refines grease from natural materials and makes soap as emulsifying agent in the prior art Relevant report, such as:
The Chinese patent of Application No. CN201510238587.4 discloses a kind of wild fragrant fruit liquid soap manufacture method, by open country It is prepared by raw natural perfume fruit oil, liquid sodium hydroxide, cocounut oil acyl, fatty alcohol polyoxyethylene ether, sodium chloride, glycerine and deionized water Form;In the inventive solutions, main raw material(s) is oily for the fragrant fruit of the wild fragrant fruit refining of Gaoligong Shan Mountain, Baoshan City Tengchong County, Longyang District, Longling County and Changning County are the main producing regions of wild fragrant fruit oil plant, and periphery Dehong prefecture Luxi City, Yingjiang County also have Distribution, belongs to renewable resource, has strong dirt-removing power, easily foaming abundancy, rinsing, power saving, province using the liquid soap of its production Water, antistatic, feel is submissive, the performance of energy-saving and environmental protection.The invention is not added with essence, keeps wild fragrant fruit ecosystem fragrant.
The Chinese patent of Application No. CN201510918857.6 discloses a kind of preparation method of pollution-free soap of refreshing oneself, Belong to soap preparing technical field.The present invention is using peppermint, borneol, lilac, gardenia, essence, Schisandra chinensis as raw material, by powder After broken addition aloe extract, stir evenly, add vitamin mixtures, finally by saponification and injection molding, so as to obtain A kind of pollution-free soap of refreshing oneself.Example proves that the method for the present invention is unique novel, the obtained pollution-free soap not only operative employee that refreshes oneself Skill is simple and practicable, is produced without any sewage, and the preparing raw material of soap is of low cost, significant effect of refreshing oneself after use.
Application No. CN201010107594.8 Chinese patents disclose a kind of by Kazak's conventional soap-black soap Preparation method is combined with modern soapmaking technology, prepares a kind of natural soap, its raw material includes plant ass, animal and plant fat and food Salt etc., natural soap of the present invention in the trace element of health, have environmentally protective rich in multiple beneficial, and formula is simple, and cost is low It is honest and clean, many advantages, such as finished product impurity is few, and color and luster is light, and preparation skin disease to a variety of soap and local disease have good treat Effect.
The Chinese patent of Application No. CN201610144529.X disclose a kind of disposable luffa energy-saving soap and its Preparation method.The present invention is softened by luffa, luffa heat treatment, makes luffa soft easy to sizing, Ran Houtong Cross and be mixed and made into soap with soap lye.The present invention soap have lightweight, dosage does not waste, is small, intensity is good, it is easy to process and The features such as packaging;The present invention is also non-breakable with soap body when washing one's hands at the same time, and common fertilizer is brought in function and visually The characteristics of soap does not possess, is especially suitable for carrying with during travel in holiday.
Emulsifying agent used is often prepared by chemistry is artificial synthesized in the prior art, is irritating to the skin, or by natural Extracted in fruits and vegetables, manufacturing cost is high.
The content of the invention
The present invention is in order to overcome emulsifying agent used in the above-mentioned prior art to be often prepared by chemistry is artificial synthesized, to skin The problem of skin has stimulation, or by being extracted in natural fruit and vegetables, and manufacturing cost is high, there is provided a kind of soap suitable for sensitiveness skin and Its preparation method, using natural fish oil as emulsifying agent, having soap, component is simple, the performance such as effective decontamination and health environment-friendly.
To achieve these goals, the present invention uses following technical scheme:
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight:
25-30 parts of fish oil
5-10 parts of sodium hydroxide
1-3 parts of alkyl-glucoside
1-3 parts of trehalose
0.5-2 parts of plants essential oil
1-5 parts of glycerine
1-3 parts of stearic acid
55-60 parts of deionized water;
Raw material employed in the present invention is environmentally protective, nontoxic, non-stimulated to skin.
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps:(1)By fish oil and sodium hydroxide Solution carries out saponification 1-8h, then successively saltouts and analysed with alkali, obtains pure soap base of the content of fatty acid more than 60%; (2)Add deionized water when stirring soap base, when temperature reaches 70-80 DEG C, sequentially add alkyl-glucoside, glycerine and Stearic acid, adjusting pH value of solution are 6-7;(3)Trehalose and plants essential oil are eventually adding, after stirring 1-10h, is stood up to the fertilizer Soap.Saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed and once arrange by alkali twice and obtain fat Pure soap base of the fat acid content more than 60%, uses the soap that technical solution of the present invention is prepared to be used as emulsification using natural fish oil Agent, by the selection and optimization of component, effectively removes oil stain and spot, easily rinsing, gentle non-stimulated and raw materials used nontoxic Property, production process is environmentally protective, has extensive market value.
Preferably, step(1)Described in sodium hydroxide solution pH be 8-10, fish oil and sodium hydroxide solution weight Than for 1:2-10.
Preferably, step(1)Described in saponification carried out in the reaction pot equipped with steam openings.
Preferably, step(2)In, the ionized water added into soap base is the 60-90% of required deionization total Water, remaining Under be used for adjust solution ph.
Preferably, step(2)In, the ionized water added into soap base carries out under the conditions of steam is turned over and boiled.
Preferably, the fish oil is refined to obtain by band fish pomace.It is environmentally protective using the leftover bits and pieces refinement fish oil of fish, Belong to regenerative resource.
Therefore, the present invention has the advantages that:(1)Using natural fish oil as emulsifying agent, oil stain and dirt are effectively removed Stain;(2)Easily rinsing, it is gentle non-stimulated;(3)Raw materials used nontoxicity, production process is environmentally protective, has extensive market price Value.
Embodiment
Technical solution of the present invention is further described with reference to embodiment.
Embodiment 1:
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight:
25 parts of fish oil, 5 parts of sodium hydroxide, 1 part of alkyl-glucoside, 3 parts of trehalose, 2 parts of plants essential oil, 5 parts of glycerine are stearic 3 parts of acid, 60 parts of deionized water;
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps:By fish oil be provided with blender and It is open in the reaction pot of steam and the sodium hydroxide solution progress saponification that pH is 8, the weight of fish oil and sodium hydroxide solution Than for 1:2, saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed by alkali twice and once arranged To pure soap base of the content of fatty acid more than 60%, deionized water is added in the case where steam is turned over and boiled with turn on agitator, is added Water stops when reaching required total Water 80% plus water, treats that temperature reaches 70 DEG C and keeps, sequentially adds alkyl grape while stirring Glucosides, glycerine, stearic acid, it is 7 to adjust pH value of solution, is eventually adding trehalose, plants essential oil, after stirring 1h, is stood up to institute State soap.Under normal temperature and pressure, the cloth 30min of lard is infected with this product immersion, frequency is washed by rubbing with the hands and is maintained at 60 times/min, only It is 20.8% to wash rate, and the pH of finished product is 7 in addition, and human skin is faintly acid, is not stimulated gently.
Embodiment 2:
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight:
30 parts of fish oil, 10 parts of sodium hydroxide, 3 parts of alkyl-glucoside, 1 part of trehalose, 0.5 part of plants essential oil, 1 part of glycerine, 1 part of stearic acid, 55 parts of deionized water;
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps:By fish oil be provided with blender and It is open in the reaction pot of steam and the sodium hydroxide solution progress saponification that pH is 10, the weight of fish oil and sodium hydroxide solution Than for 1:10, saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed by alkali twice and once arranged Pure soap base of the content of fatty acid more than 60% is obtained, deionized water is added in the case where steam is turned over and boiled with turn on agitator, Amount of water stops when reaching required total Water 90% plus water, treats that temperature reaches 80 DEG C and keeps, sequentially adds alkyl Portugal while stirring Polyglycoside, glycerine, stearic acid, it is 6 to adjust pH value of solution, is eventually adding trehalose, plants essential oil, after stirring 10h, is stood to obtain the final product The soap.The cloth 30min of lard is infected with this product immersion, frequency is washed by rubbing with the hands and is maintained at 60 times/min, washing rate is 25.3%, the pH of finished product is 6 in addition, and human skin is faintly acid, is not stimulated gently.
Embodiment 3:
A kind of soap suitable for sensitiveness skin, is made from the following raw materials in parts by weight:
27 parts of fish oil, 8 parts of sodium hydroxide, 2 parts of alkyl-glucoside, 2 parts of trehalose, 1 part of plants essential oil, 3 parts of glycerine are stearic 2 parts of acid, 57 parts of deionized water;
A kind of preparation method of soap suitable for sensitiveness skin, comprises the following steps:By fish oil be provided with blender and It is open in the reaction pot of steam and the sodium hydroxide solution progress saponification that pH is 9, the weight of fish oil and sodium hydroxide solution Than for 1:6, saltoutd by saponification twice and remove natural fish oil secondary impurity and pigment, then analysed by alkali twice and once arranged To pure soap base of the content of fatty acid more than 60%, deionized water is added in the case where steam is turned over and boiled with turn on agitator, is added Water stops when reaching required total Water 60% plus water, treats that temperature reaches 75 DEG C and keeps, sequentially adds alkyl grape while stirring Glucosides, glycerine, stearic acid, it is 6.5 to adjust pH value of solution, is eventually adding trehalose, plants essential oil, after stirring 5h, is stood to obtain the final product The soap.The cloth 30min of lard is infected with this product immersion, frequency is washed by rubbing with the hands and is maintained at 60 times/min, washing rate is 23.5%, the pH of finished product is 6.5 in addition, and human skin is faintly acid, is not stimulated gently.

Claims (7)

1. a kind of soap suitable for sensitiveness skin, it is characterised in that be made from the following raw materials in parts by weight:
25-30 parts of fish oil
5-10 parts of sodium hydroxide
1-3 parts of alkyl-glucoside
1-3 parts of trehalose
0.5-2 parts of plants essential oil
1-5 parts of glycerine
1-3 parts of stearic acid
55-60 parts of deionized water.
A kind of 2. preparation method of soap suitable for sensitiveness skin according to claim 1, it is characterised in that including Following steps:(1)Fish oil and sodium hydroxide solution are subjected to saponification 1-8h, then successively saltouts and is analysed with alkali, obtains fat Pure soap base of the fat acid content more than 60%;(2)Deionized water is added when stirring soap base, when temperature reaches 70-80 DEG C, Alkyl-glucoside, glycerine and stearic acid are sequentially added, adjusting pH value of solution is 6-7;(3)It is eventually adding trehalose and plant essence Oil, after stirring 1-10h, stands up to the soap.
A kind of 3. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step (1)Described in the pH of sodium hydroxide solution be 8-10, the weight ratio of fish oil and sodium hydroxide solution is 1:2-10.
A kind of 4. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step (1)Described in saponification carried out in the reaction pot equipped with steam openings.
A kind of 5. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step (2)In, the ionized water added into soap base is the 60-90% of required deionization total Water, remaining to be used to adjust solution ph.
A kind of 6. preparation method of soap suitable for sensitiveness skin according to claim 2, it is characterised in that step (2)In, the ionized water added into soap base carries out under the conditions of steam is turned over and boiled.
7. a kind of preparation method of soap suitable for sensitiveness skin according to claim 1-6 any one, it is special Sign is that the fish oil is refined to obtain by band fish pomace.
CN201711251469.2A 2017-12-01 2017-12-01 It is a kind of suitable for soap of sensitiveness skin and preparation method thereof Pending CN108004066A (en)

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Application Number Priority Date Filing Date Title
CN201711251469.2A CN108004066A (en) 2017-12-01 2017-12-01 It is a kind of suitable for soap of sensitiveness skin and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711251469.2A CN108004066A (en) 2017-12-01 2017-12-01 It is a kind of suitable for soap of sensitiveness skin and preparation method thereof

Publications (1)

Publication Number Publication Date
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110577864A (en) * 2019-08-13 2019-12-17 安徽天祥粮油食品有限公司 Skin-moistening soap prepared by taking fish oil as animal fat
CN114717063A (en) * 2022-01-13 2022-07-08 郑州工业应用技术学院 Refining of tea seed oil soap base and preparation method of detergent thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1078258A (en) * 1992-03-20 1993-11-10 普罗格特-甘布尔公司 The neutral pH cleaning soap
CN104862131A (en) * 2015-06-05 2015-08-26 浙江海洋学院 Fruit and vegetable tableware detergent based on marine fish oil and preparation method thereof
CN104962408A (en) * 2015-07-01 2015-10-07 浙江海洋学院 Marine fish oil washing product and preparation method thereof
CN105861202A (en) * 2016-03-18 2016-08-17 杭州稞恩生物科技有限公司 Floating soap and preparation method thereof
CN106318724A (en) * 2016-08-19 2017-01-11 跨越生物科技(滁州)有限公司 Moisturizing and toxin expelling congealed fat essential oil handmade soap

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1078258A (en) * 1992-03-20 1993-11-10 普罗格特-甘布尔公司 The neutral pH cleaning soap
CN104862131A (en) * 2015-06-05 2015-08-26 浙江海洋学院 Fruit and vegetable tableware detergent based on marine fish oil and preparation method thereof
CN104962408A (en) * 2015-07-01 2015-10-07 浙江海洋学院 Marine fish oil washing product and preparation method thereof
CN105861202A (en) * 2016-03-18 2016-08-17 杭州稞恩生物科技有限公司 Floating soap and preparation method thereof
CN106318724A (en) * 2016-08-19 2017-01-11 跨越生物科技(滁州)有限公司 Moisturizing and toxin expelling congealed fat essential oil handmade soap

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110577864A (en) * 2019-08-13 2019-12-17 安徽天祥粮油食品有限公司 Skin-moistening soap prepared by taking fish oil as animal fat
CN110577864B (en) * 2019-08-13 2021-03-16 安徽天祥粮油食品有限公司 Skin-moistening soap prepared by taking fish oil as animal fat
CN114717063A (en) * 2022-01-13 2022-07-08 郑州工业应用技术学院 Refining of tea seed oil soap base and preparation method of detergent thereof

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Application publication date: 20180508