CN107974235A - Strong road casting glue of a kind of corrosion resistance and preparation method thereof - Google Patents
Strong road casting glue of a kind of corrosion resistance and preparation method thereof Download PDFInfo
- Publication number
- CN107974235A CN107974235A CN201711322359.0A CN201711322359A CN107974235A CN 107974235 A CN107974235 A CN 107974235A CN 201711322359 A CN201711322359 A CN 201711322359A CN 107974235 A CN107974235 A CN 107974235A
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- CN
- China
- Prior art keywords
- casting glue
- road
- preparation
- parts
- corrosion resistance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J195/00—Adhesives based on bituminous materials, e.g. asphalt, tar, pitch
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
This case is related to strong road casting glue of a kind of corrosion resistance and preparation method thereof, and raw material is made of pitch, SBS modifier, discarded aramid fiber, silicon powder, rubber powder, polystyrene, carbon dust according to specified weight part proportioning；To the order of addition of preparation process items raw material, and temperature during reaction and stir speed (S.S.) by test of many times and determine optimal preparation method；Road gap-grouting glue prepared by the present invention has good corrosion resistance, can weaken it significantly by corrosion damage degrees such as empty gas and water, corrosive substances, and the service life that casting glue is filled in crack extends.
Description
Technical field
The invention belongs to highway pavement patching material field, and in particular to a kind of strong road casting glue of corrosion resistance and its
Preparation method.
Background technology
Crack is the principal mode of road surface early damage, and water penetration causes roadbed into sub-surface structure in order to prevent
Irreversible damage, it is frequently with one of measure remedied using sealing adhesive for crack, that is, casting glue fill up.Rationally utilize
Sealing adhesive for crack can prevent pavement crack from further deteriorating, and extend the service life on road surface.In different types of crack repairing
In packing material, it is the most common type patching material to vulcanize pitch sealing adhesive for crack, its construction is simple, setting time are short,
The usual cementation of fissures is after twenty minutes solidifiable open to traffic, and cheap, cheap compared to cold-penetration sealing more than 50%.
It is to be noted, however, that water in nature, air circulation all can have certain corruption to exposure material therein
Erosion, road gap-grouting glue are no exception.Bituminous paving exposes in atmosphere, and vehicle is by various corrosive substances (such as kerosene, vapour
Oil) it is covered in by wheel on bituminous paving, crack material for repairing is also unable to escape misfortune.The corrosion of empty gas and water, corrosive substance
The repair efficiency of meeting fracture patching material is had a greatly reduced quality, and therefore, road casting glue needs good corrosion resistance.
The content of the invention
For the shortcoming of existing road casting glue, it is an object of the invention to provide a kind of strong road of corrosion resistance
Casting glue and preparation method thereof.
The present invention provides a kind of strong road casting glue of corrosion resistance, it is made of the raw material of following parts by weight：
Preferably, the pitch selects No. 90 matrix pitches.
Preferably, the discarded aramid fiber passes through pulverization process.
Preferably, the particle diameter of the silicon powder is less than 200 mesh；The particle diameter of the rubber powder and carbon dust is in 20-40 mesh.
The preparation method of road casting glue according to the present invention, comprises the following steps：
(1) match somebody with somebody according to parts by weight and take each component；
(2) by asphalt heating to 160-170 DEG C, and it is stirred continuously, successively adds SBS modifier, stirring reaction thereto
40-45 minutes；
(3) 180-190 DEG C is warming up to, polystyrene is added into system, is stirred 30-40 minutes；
(4) 190-200 DEG C is increased the temperature to, uniformly mixed silicon powder, rubber powder and carbon dust are added in system, stirring is anti-
Answer 50-60 minutes；
(5) 180-190 DEG C is cooled to, discarded aramid fiber is added into system, stirs 60-70 minutes, waits to cool to
120-130 DEG C can pack, and road casting glue is prepared.
Preferably, speed of agitator is 2000rpm described in step (2), step (3), step (4) and step (5).
Preferably, the casting glue is repaiied for the sealing of common road, highway, airfield runway crack and seam
It is multiple.
Elaboration to the present invention and its advantage：Road gap-grouting glue prepared by the present invention has good corrosion resistance
Can, it can be weakened significantly by corrosion damage degrees such as empty gas and water, corrosive substances, the use longevity of casting glue is filled in crack
Life extends, it is necessary to safeguard that the cycle of reparation also increases；Wherein, pitch is modified with SBS modifier, enhances the glue of pitch
Stickiness energy, so as to preferably be binded with crack；Polystyrene has preferable acid-alkali-corrosive-resisting performance, and can be with aramid fiber
Fiber interaction, forms elastic anti-corrosion erosion protective layer, avoids the casting glue in filled crack from being corroded easily, especially right
Water, air and faintly acid corrosive deposit are by preferable defence capability；The main composition of silicon powder is silica, can be resisted usually
Soda acid corrode, the present invention in silicon powder particle diameter be far smaller than rubber powder or carbon granules, silicon is micro- when three is uniformly mixed
Powder can be adsorbed in the surface of rubber and carbon granules, and adding in the system containing polyethylene makes silicon powder tight bond and bulky grain table
Face, is then further fixed by aramid fiber, rubber powder or carbon grain surface is protected by silicon powder, so as to reduce pair
Its directly etching, can effectively strengthen the service life of casting glue；Using discarded aramid fiber from superseded in the present invention
The materials such as rope, gloves, protective garment, realize and the effective of waste are recycled.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1
Raw material forms (parts by weight)：No. 90 65 parts of matrix pitches, 8 parts of SBS modifier, discarded 15 parts of aramid fiber, silicon are micro-
10 parts of powder, 6 parts of rubber powder, 12 parts of polystyrene, 8 parts of carbon dust.
Preparation method：
(1) match somebody with somebody according to parts by weight and take each component；
(2) by asphalt heating to 160-170 DEG C, it is stirred continuously under 2000rpm rotating speeds, successively adds SBS thereto and change
Property agent, stirring reaction 40-45 minutes；
(3) 180-190 DEG C is warming up to, polystyrene is added into system, is stirred 30-40 minutes, rotating speed 2000rpm；
(4) 190-200 DEG C is increased the temperature to, uniformly mixed silicon powder, rubber powder and carbon dust are added in system, stirring is anti-
Answer 50-60 minutes, rotating speed 2000rpm；
(5) 180-190 DEG C is cooled to, discarded aramid fiber is added into system, is stirred 60-70 minutes, rotating speed is
2000rpm, 120-130 DEG C to be cooled to can pack, and road casting glue is prepared.
Embodiment 2
Raw material forms (parts by weight)：No. 90 65 parts of matrix pitches, 6 parts of SBS modifier, discarded 12 parts of aramid fiber, silicon are micro-
8 parts of powder, 5 parts of rubber powder, 10 parts of polystyrene, 6 parts of carbon dust.
Preparation method is same as Example 1.
Comparative example 1
Raw material forms (parts by weight)：No. 90 65 parts of matrix pitches, 8 parts of SBS modifier, 15 parts of waste polyester fibers, silicon are micro-
10 parts of powder, 6 parts of rubber powder, 12 parts of polystyrene, 8 parts of carbon dust.
The aramid fiber in embodiment 1 is replaced with the polyester fiber of phase homogenous quantities, preparation method and 1 phase of embodiment
Together.
Comparative example 2
Raw material forms (parts by weight)：No. 90 65 parts of matrix pitches, 8 parts of SBS modifier, discarded 15 parts of aramid fiber, silicon are micro-
10 parts of powder, 6 parts of rubber powder, 12 parts of epoxy resin, 8 parts of carbon dust.
The polystyrene in embodiment 1 is replaced with epoxy resin, preparation method is same as Example 1.
Comparative example 3
Raw material forms (parts by weight)：No. 90 65 parts of matrix pitches, 8 parts of SBS modifier, discarded 15 parts of aramid fiber, talcum
10 parts of powder, 6 parts of rubber powder, 12 parts of polystyrene, 8 parts of carbon dust.
The silicon powder in embodiment 1 is replaced with talcum powder, preparation method is same as Example 1.
Comparative example 4
The hot type face pavement crack fluid sealant road fighter of better performances on the market, selects plain edition product.
First, according to JT/T 740-2015《Road-surface heating type fluid sealant》Code requirement, measures embodiment 1-2 and contrast
Slamp value, cone penetration, softening point, cryogenic tensile and the elastic restoration ratio of road casting glue in example 1-4, in embodiment and comparative example
The indices of product can reach the requirement in professional standard to plain edition casting glue product；Then, in order to test each road
It, is soaked one day when small (24) and taken out afterwards, measure its mass loss, come successively by the corrosion resistance of casting glue in diesel oil respectively
Judge the corrosion resistance of each casting glue, the mass loss of casting glue is bigger after immersion, illustrates that its corrosion resistance is poorer.
For casting glue mass loss rate be recorded in table 1 among, wherein according in the present invention scheme prepare embedding
Glue, i.e. embodiment 1 and embodiment 2, after the corrosion by diesel oil, its quality only have lost about 9%, show preferable resistance to
Corrosive nature；In comparative example 1 aramid fiber, the mass loss after a test of prepared casting glue are instead of with polyester fiber
More than 20%, this explanation aramid fiber plays an important role the corrosion resistance for strengthening fluid sealant, while the experimental result of comparative example 2
It is irreplaceable to illustrate that the polystyrene in raw material also plays the role of, there is synergistic effect energy between aramid fiber and polystyrene
Enough strengthen fluid sealant corrosion resistance；Comparative example 3 test result indicates that silicon powder in raw material to the corrosion-resistant of enhancing fluid sealant
Property has positive effect；Compared by the test result of embodiment 1 and comparative example 3, it is found that the road prepared by the present invention fills
Similar product of the sealing as plain edition fluid sealant in terms of corrosion resistance more on the market is significantly improved.
Table 1
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Realize other modification, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details.
Claims (7)
1. strong road casting glue of a kind of corrosion resistance and preparation method thereof, it is characterised in that by the raw material group of following parts by weight
Into：
2. road casting glue according to claim 1, it is characterised in that the pitch selects No. 90 matrix pitches.
3. road casting glue according to claim 1, it is characterised in that the discarded aramid fiber passes through pulverization process.
4. road casting glue according to claim 1, it is characterised in that the particle diameter of the silicon powder is less than 200 mesh；It is described
The particle diameter of rubber powder and carbon dust is in 20-40 mesh.
5. the preparation method of road casting glue according to claim 1, it is characterised in that comprise the following steps：
(1) match somebody with somebody according to parts by weight described in claim 1 and take each component；
(2) by asphalt heating to 160-170 DEG C, and it is stirred continuously, successively adds SBS modifier, stirring reaction 40-45 thereto
Minute；
(3) 180-190 DEG C is warming up to, polystyrene is added into system, is stirred 30-40 minutes；
(4) 190-200 DEG C is increased the temperature to, uniformly mixed silicon powder, rubber powder and carbon dust, stirring reaction are added in system
50-60 minutes；
(5) 180-190 DEG C is cooled to, discarded aramid fiber is added into system, is stirred 60-70 minutes, 120-130 to be cooled to
It DEG C can pack, road casting glue is prepared.
6. preparation method according to claim 5, it is characterised in that step (2), step (3), step (4) and step (5)
Described in speed of agitator be 2000rpm.
7. road casting glue according to claim 1, it is characterised in that the casting glue is used for common road, at a high speed public affairs
The sealing reparation on road, airfield runway crack and seam.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711322359.0A CN107974235A (en) | 2017-12-12 | 2017-12-12 | Strong road casting glue of a kind of corrosion resistance and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711322359.0A CN107974235A (en) | 2017-12-12 | 2017-12-12 | Strong road casting glue of a kind of corrosion resistance and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107974235A true CN107974235A (en) | 2018-05-01 |
Family
ID=62010004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711322359.0A Pending CN107974235A (en) | 2017-12-12 | 2017-12-12 | Strong road casting glue of a kind of corrosion resistance and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107974235A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111234319A (en) * | 2020-01-17 | 2020-06-05 | 遵义市聚源建材有限公司 | High-density polymer regulator and preparation method thereof |
| CN113265151A (en) * | 2021-05-17 | 2021-08-17 | 四川统揽建设集团有限公司 | Asphalt modifier and modified asphalt prepared from same |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102936420A (en) * | 2011-08-16 | 2013-02-20 | 赵金叶 | Modified asphalt joint grouting glue for severe-cold roads |
| TW201710313A (en) * | 2015-07-16 | 2017-03-16 | Asahi Chemical Ind | Partially hydrogenated block copolymer, adhesive composition, adhesive tape, label, modified asphalt composition﹑modified asphalt mixture, and paving binder composition |
| CN106947416A (en) * | 2017-04-06 | 2017-07-14 | 江苏中路交通科学技术有限公司 | A kind of self-healing high osmosis casting glue |
-
2017
- 2017-12-12 CN CN201711322359.0A patent/CN107974235A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102936420A (en) * | 2011-08-16 | 2013-02-20 | 赵金叶 | Modified asphalt joint grouting glue for severe-cold roads |
| TW201710313A (en) * | 2015-07-16 | 2017-03-16 | Asahi Chemical Ind | Partially hydrogenated block copolymer, adhesive composition, adhesive tape, label, modified asphalt composition﹑modified asphalt mixture, and paving binder composition |
| CN106947416A (en) * | 2017-04-06 | 2017-07-14 | 江苏中路交通科学技术有限公司 | A kind of self-healing high osmosis casting glue |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111234319A (en) * | 2020-01-17 | 2020-06-05 | 遵义市聚源建材有限公司 | High-density polymer regulator and preparation method thereof |
| CN111234319B (en) * | 2020-01-17 | 2021-06-01 | 遵义市聚源建材有限公司 | High-density polymer regulator and preparation method thereof |
| CN113265151A (en) * | 2021-05-17 | 2021-08-17 | 四川统揽建设集团有限公司 | Asphalt modifier and modified asphalt prepared from same |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180501 |
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| RJ01 | Rejection of invention patent application after publication |