CN107963812A - A kind of pottery hacking yellowish pea green glaze and preparation method thereof - Google Patents
A kind of pottery hacking yellowish pea green glaze and preparation method thereof Download PDFInfo
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- CN107963812A CN107963812A CN201710971553.5A CN201710971553A CN107963812A CN 107963812 A CN107963812 A CN 107963812A CN 201710971553 A CN201710971553 A CN 201710971553A CN 107963812 A CN107963812 A CN 107963812A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
- C04B41/5023—Glass-ceramics
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2204/00—Glasses, glazes or enamels with special properties
- C03C2204/04—Opaque glass, glaze or enamel
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Finishing Walls (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of pottery hacking yellowish pea green glaze, it is prepared by the raw material of following parts by weight：28 36 parts of melilite, 18 24 parts of glaze fruit, 8 12 parts of quartz, 6 10 parts of calcite, 8 10 parts of simple substance silica flour, 46 parts of talcum, 1.5 2.5 parts of iron ore, 24 parts of black wool soil, 0.5 1.5 parts of tin oxide, 35 parts of wood ash.The preparation method of the pottery hacking yellowish pea green glaze, comprises the following steps：（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 56 58%, when wet-milling 10 12 is small, and wet-grinded slurry crosses 200 300 mesh sieves and obtains glaze slip；（2）Base substrate leaching glaze 12 times；（3）Burn till, firing temperature is 1,290 1310 DEG C.
Description
Technical field
The present invention relates to pottery manufacturing technology field, and in particular to a kind of pottery hacking yellowish pea green glaze and preparation method thereof.
Background technology
Pottery is the exclusive national treasure porcelain in Henan Province Xuchang City Yuzhou City god Hou towns, by its simple and unsophisticated moulding, consummate
Technique, the complicated magical transmutation with glaze, " it is color to enter kiln kiln discharge ten thousand of the same colour ", the beautiful scenery of lakes and mountains, rosy clouds fog, people's beast flower, bird, insect, and fish etc.
Varied figure color and marvellous charm, are known as first of Chinese " five big porcelain ".
Blue or green glaze is conventional color glaze famous in Chinese porcelain, also known as " celadon glaze ".The celadon of Ancient Times in China, glaze paint colour generation
It is abundant, it is famous have pale blue, plum green, pea green, shadow is blue or green, Bai Hu, careless green grass or young crops, parched rice Huang, crust green etc., it is but how much always general in color
Go out some dark greens.
Cracked glaze is a kind of decorative art of porcelain, its secondary glaze paint is discontented with many crackles, has comb to have close, be coarse and fine,
Have with short, there is Qu Youzhi, the lines of likeness in form cracking, crab claw or ice crack.Glaze paint cracking original is a kind of defect in burning till, but is worked as
The glaze paint cracking of some products is very special, and lines uniformly, clearly, is covered with device face, gives people a kind of special aesthetic feeling.Hacking yellowish pea green glaze
Glaze paint cracks, and the hacking that adds decoration sets off that implements are quaint interesting, also increases the diversity of pottery.The reason for glaze paint cracks
It is that silicon amount excessive in glaze causes the coefficient of expansion of glaze layer and base substrate different, when kiln discharge postcooling is cracking.
In existing public technology, formula of hacking yellowish pea green glaze and preparation method thereof is also seldom, complex production process, fires not
Easily.The product for having 60% or so during firing can be scrapped, and yield rate is low, therefore the waste to raw material is huge, make
Cost is too high.
The content of the invention
The present invention provides a kind of raw material and the pottery hacking yellowish pea green glaze for matching science and preparation method thereof are existing to solve
The problem of formula and preparation method of pottery hacking yellowish pea green glaze are few, and yield rate is low, cost of manufacture and high manufacture difficulty.
The purpose of the present invention is what is realized with following technical proposals：
A kind of pottery hacking yellowish pea green glaze, it is prepared by the raw material of following parts by weight：28-36 parts of melilite, glaze fruit 18-24
Part, 8-12 parts of quartz, 6-10 parts of calcite, 8-10 parts of simple substance silica flour, 4-6 parts of talcum, 1.5-2.5 parts of iron ore, black wool soil 2-
4 parts, 0.5-1.5 parts of tin oxide, 3-5 parts of wood ash.
Preferably, the pottery hacking yellowish pea green glaze, it is prepared by the raw material of following parts by weight：Melilite 32
Part, 21 parts of glaze fruit, 10 parts of quartz, 8 parts of calcite, 9 parts of simple substance silica flour, 5 parts of talcum, 2 parts of iron ore, black wool native 3 parts, tin oxide
1 part, 4 parts of wood ash.
The preparation method of the pottery hacking yellowish pea green glaze, comprises the following steps：
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 56-58%,
When wet-milling 10-12 is small, wet-grinded slurry crosses 200-300 mesh sieves and obtains glaze slip；
(2) base substrate leaching glaze 1-2 times；
(3) burn till, firing temperature is 1290-1310 DEG C.
Preferably, the preparation method of the pottery hacking yellowish pea green glaze, firing process specifically includes following step in step (3)
Suddenly：
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 980- when 4.5-6.5 is small
1030℃；
2. under reducing atmosphere, make temperature is interior when 6-7 is small to be ramped up 1290-1310 DEG C；
3. annealing is cooled to room temperature, it is made.
Beneficial effects of the present invention are as follows：
1st, the invention discloses a kind of pottery hacking yellowish pea green glaze and preparation method thereof, the thermal coefficient of expansion of glaze layer is more than the heat of base substrate
The coefficient of expansion, when burning till postcooling, glaze layer shrinking percentage is big, the cracking microgroove of surface glaze layer.The simple substance silica flour added in glaze
The thermal coefficient of expansion of glaze slip can be increased, there is good mobility under high temperature, black wool soil has good plasticity and caking property, from
And reducing the crackle increase in sintering causes the risk of rupture, a variety of hacking microgrooves are formed, add the diversity of yellowish pea green glaze.
Technical solution disclosed by the invention is easy to operate, and the finished product rate burnt till is 85% or so, therefore reduces raw material and the energy
Waste, greatly reduce cost of manufacture.
2nd, glaze fruit is used in raw material of the present invention, iron oxide content in glaze slip is controlled by varying glaze fruit content.When glaze fruit contains
When amount percentage by weight is 21% or so, sparkling and crystal-clear smooth as jade pea green color is presented in glaze paint.With the increase of glaze fruit content, iron oxide
Content also changes therewith, and iron oxide content also increases at this time, under reducing atmosphere Fe3+/Fe2+Ratio it is increasing, from
And make the colouring effect of glaze paint more and more deeper.
3rd, the calcium crystallization and not molten quartz particles that glaze is formed during high-temperature firing send out the light into glaze layer
Raw scattering, increases refractive index to the suspension and calcite of glaze plus wood ash in glaze, can increase the milkiness sense of glaze layer, improves
Glaze paint glossiness.The application of pottery hacking yellowish pea green glaze, may advantageously facilitate the raising of china industry common technology, promote local
Economic development.
Brief description of the drawings
Fig. 1 is the pottery hacking yellowish pea green glaze schematic diagram that the embodiment of the present invention 2 obtains.
Embodiment
Embodiment 1
A kind of pottery hacking yellowish pea green glaze, is prepared by the raw material of following parts by weight：28-36 parts of melilite, 18-24 parts of glaze fruit,
8-12 parts quartzy, 6-10 parts of calcite, 8-10 parts of simple substance silica flour, 4-6 parts of talcum, 1.5-2.5 parts of iron ore, black wool soil 2-4
Part, 0.5-1.5 parts of tin oxide, 3-5 parts of wood ash.
The preparation method of above-mentioned pottery hacking yellowish pea green glaze comprises the following steps：
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 56-58%,
When wet-milling 10-12 is small, wet-grinded slurry crosses 200-300 mesh sieves and obtains glaze slip；
(2) base substrate leaching glaze 1-2 times；
(3) burn till, firing temperature is 1290-1310 DEG C.
Firing process specifically comprises the following steps in step (3)：
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 980- when 4.5-6.5 is small
1030℃；
2. under reducing atmosphere, make temperature is interior when 6-7 is small to be ramped up 1290-1310 DEG C；
3. annealing is cooled to room temperature, it is made.
For the present invention using melilite, calcite and spodumene as primary solvent, melilite dioxide-containing silica is 77% or so,
Aluminium oxide 13% or so, iron oxide 0.6%, magnesia 0.16%.Calcite mainly reduces glaze melting temperature, can increase in glaze
The refractive index of big glaze, thus glossiness is improved, and the translucency of glaze can be improved.Simple substance silica flour has flowing well at high temperature
Property, and thermal coefficient of expansion is higher, and when cooling can make glaze layer produce hacking line.Glaze fruit is a kind of porcelain stone, and component is sericite, quartz
And feldspar, also containing elements such as some iron, magnesium, sulphur, zinc, the iron oxide content in control glaze slip is played to change glaze paint colour generation effect
The effect of fruit.Quartz plays skeleton function, improves the melting temperature of glaze, increases the glossiness of glaze, can improve the flowing of glaze
Property.Talcum is natural hydrous magnesium silicate mineral, is the cosolvent of glaze.Tin oxide is assistant toner, and main helps glaze slip color development to make
With making color and luster more bright-coloured.Iron ore plays main pigmentation.Wood ash plays the role of milkiness.Black wool soil aluminium content is higher, tool
There are higher plasticity and caking property, play suspension effect, the texture of glaze can be improved.Pass through rational proportion and control sintering process
In atmosphere and temperature, the pottery hacking yellowish pea green glaze color and luster prepared is simple and elegant, makings is noble and unsullied, there is very high artistic value and economy
Value.
Embodiment 2
A kind of pottery hacking yellowish pea green glaze, is prepared by the raw material of following parts by weight：32 parts of melilite, 21 parts of glaze fruit, quartz 10
Part, 3 parts of 8 parts of calcite, 9 parts of simple substance silica flour, 5 parts of talcum, 2 parts of iron ore, black wool soil, 1 part of tin oxide, 4 parts of wood ash.
The preparation method of above-mentioned pottery hacking yellowish pea green glaze, comprises the following steps：
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 57%, wet-milling
12 it is small when, wet-grinded slurry crosses 250 mesh sieves and obtains glaze slip；
(2) base substrate leaching glaze 2 times；
(3) burn till, specifically comprise the following steps：
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1010 DEG C when 6 is small；
2. under reducing atmosphere, make temperature is interior when 7 is small to be ramped up 1300 DEG C；
3. annealing is cooled to room temperature, it is made.
By rational proportion and control sintering process in atmosphere and temperature, the pottery hacking yellowish pea green glaze glaze colours prepared with
Light changes, and color development temperature text is soft, under the conditions of light is stronger, sees the glaze paint of yellowish pea green glaze, its glaze paint color and luster is " light such as lake water
It is green ", under conditions of light is weaker, see the glaze paint of yellowish pea green glaze, its glaze paint color and luster is " dark green middle yellowing ", gentle simple and unsophisticated, color and luster
Simple and elegant, makings is noble and unsullied, and glaze paint forms the segmentation crack of uniqueness, and lines uniformly, clearly, is covered with device face, gives people a kind of special beautiful
Sense.
Comparative example 1
A kind of pottery hacking yellowish pea green glaze, is prepared by the raw material of following parts by weight：32 parts of melilite, 21 parts of glaze fruit, quartz 10
Part, 3 parts of 8 parts of calcite, 25 parts of simple substance silica flour, 5 parts of talcum, 2 parts of iron ore, black wool soil, 1 part of tin oxide, 4 parts of wood ash.Prepare
Method is the same as embodiment 2.This example is compared with Example 2 compared with the usage amount of simple substance silica flour increases to 25 parts in raw material.The production burnt till
For product compared with the product in embodiment 2, the crackle that glaze paint is formed is excessive, does not form uniform pattern cracking, yield rate only has
63% or so.
Comparative example 2
A kind of pottery hacking yellowish pea green glaze, is prepared by the raw material of following parts by weight：32 parts of melilite, 30 parts of glaze fruit, quartz 10
Part, 3 parts of 8 parts of calcite, 9 parts of simple substance silica flour, 5 parts of talcum, 2 parts of iron ore, black wool soil, 1 part of tin oxide, 4 parts of wood ash.Prepare
Method is the same as embodiment 2.This example is compared with Example 2 compared with the usage amount of glaze fruit increases to 30 parts in raw material.The product and reality burnt till
The product applied in example 2 compares, and deeper green is presented in glaze face color, and yield rate only has 66% or so.
Comparative example 3
A kind of pottery hacking yellowish pea green glaze, is prepared by the raw material of following parts by weight：32 parts of melilite, 15 parts of glaze fruit, quartz 10
Part, 3 parts of 8 parts of calcite, 9 parts of simple substance silica flour, 5 parts of talcum, 2 parts of iron ore, black wool soil, 1 part of tin oxide, 4 parts of wood ash.Prepare
Method is the same as embodiment 2.This example is compared with Example 2 compared with the usage amount of glaze fruit is reduced to 15 parts in raw material.The product and reality burnt till
The product applied in example 2 compares, and Bluish white is presented in glaze face color, and glaze paint has a small amount of tiny pin hole, and yield rate only has 72%
Left and right.
The formula for the pottery hacking yellowish pea green glaze that 3-26 of the embodiment of the present invention is provided is shown in Table 2-5, the same embodiment of its preparation method
2。
Table 2
Table 3
| Raw material | Embodiment 9 | Embodiment 10 | Embodiment 11 | Embodiment 12 | Embodiment 13 | Embodiment 14 |
| Melilite | 28 | 32 | 35 | 29 | 32 | 36 |
| Glaze fruit | 19 | 21 | 18 | 24 | 21 | 24 |
| Quartz | 8 | 10 | 12 | 8 | 12 | 10 |
| Calcite | 9 | 8 | 7 | 6 | 9 | 8 |
| Simple substance silica flour | 8 | 9 | 10 | 8 | 10 | 9 |
| Talcum | 6 | 4 | 5 | 4 | 6 | 5 |
| Iron ore | 2 | 1.6 | 2 | 1.5 | 2.5 | 1.9 |
| Black wool soil | 2 | 3 | 4 | 2 | 4 | 3 |
| Tin oxide | 1.5 | 0.5 | 1 | 1.5 | 1 | 0.5 |
| Wood ash | 5 | 4 | 3 | 5 | 3 | 4 |
Table 4
Table 5
| Raw material | Embodiment 21 | Embodiment 22 | Embodiment 23 | Embodiment 24 | Embodiment 25 | Embodiment 26 |
| Melilite | 31 | 32 | 33 | 34 | 35 | 36 |
| Glaze fruit | 18 | 21 | 24 | 23 | 22 | 23 |
| Quartz | 10 | 12 | 8 | 10 | 12 | 11 |
| Calcite | 10 | 6 | 6 | 8 | 10 | 8 |
| Simple substance silica flour | 8 | 9 | 10 | 8 | 10 | 9 |
| Talcum | 4 | 5 | 6 | 6 | 5 | 4 |
| Iron ore | 1.5 | 2.5 | 2.3 | 1.5 | 2 | 2.5 |
| Black wool soil | 2 | 3 | 4 | 4 | 2 | 3 |
| Tin oxide | 1 | 0.5 | 1.5 | 0.5 | 1.5 | 1 |
| Wood ash | 5 | 4 | 3 | 3 | 4 | 5 |
Claims (4)
- A kind of 1. pottery hacking yellowish pea green glaze, it is characterised in that：It is prepared by the raw material of following parts by weight：Melilite 28- 36 parts, 18-24 parts of glaze fruit, 8-12 parts of quartz, 6-10 parts of calcite, 8-10 parts of simple substance silica flour, 4-6 parts of talcum, iron ore 1.5- 2.5 parts, 2-4 parts of black wool soil, 0.5-1.5 parts of tin oxide, 3-5 parts of wood ash.
- 2. pottery hacking yellowish pea green glaze according to claim 1, it is characterised in that：It is the raw material preparation by following parts by weight Form：It is 32 parts of melilite, 21 parts of glaze fruit, 10 parts of quartz, 8 parts of calcite, 9 parts of simple substance silica flour, 5 parts of talcum, 2 parts of iron ore, black 3 parts of hair soil, 1 part of tin oxide, 4 parts of wood ash.
- 3. a kind of preparation method of pottery hacking yellowish pea green glaze as claimed in claim 1 or 2, it is characterised in that including following step Suddenly：（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 56-58%, wet When mill 10-12 is small, wet-grinded slurry crosses 200-300 mesh sieves and obtains glaze slip；（2）Base substrate leaching glaze 1-2 times；（3）Burn till, firing temperature is 1290-1310 DEG C.
- 4. the preparation method of pottery hacking yellowish pea green glaze as claimed in claim 3, it is characterised in that step（3）Middle firing process tool Body includes the following steps：1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 980- when 4.5-6.5 is small 1030℃；2. under reducing atmosphere, make temperature is interior when 6-7 is small to be ramped up 1290-1310 DEG C；3. annealing is cooled to room temperature, it is made.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020213A (en) * | 2018-09-21 | 2018-12-18 | 王晟鸣 | A kind of your porcelain sky blue glaze and preparation method thereof, your porcelain |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104987042A (en) * | 2015-06-17 | 2015-10-21 | 郑州大学 | Light blue jun porcelain and method for experimental verification of furnace transmutation features thereof |
| CN106242288A (en) * | 2016-08-18 | 2016-12-21 | 温书强 | A kind of pottery coal gloss firing material |
| CN107010834A (en) * | 2017-05-24 | 2017-08-04 | 禹州市神器钧窑有限公司 | A kind of Lu's chun glaze |
| CN107021634A (en) * | 2017-05-24 | 2017-08-08 | 禹州市神器钧窑有限公司 | A kind of red glaze of an ancient unit of weight |
| CN107098587A (en) * | 2017-06-05 | 2017-08-29 | 任合超 | A kind of pottery sky blue cracked glaze |
-
2017
- 2017-10-18 CN CN201710971553.5A patent/CN107963812A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104987042A (en) * | 2015-06-17 | 2015-10-21 | 郑州大学 | Light blue jun porcelain and method for experimental verification of furnace transmutation features thereof |
| CN106242288A (en) * | 2016-08-18 | 2016-12-21 | 温书强 | A kind of pottery coal gloss firing material |
| CN107010834A (en) * | 2017-05-24 | 2017-08-04 | 禹州市神器钧窑有限公司 | A kind of Lu's chun glaze |
| CN107021634A (en) * | 2017-05-24 | 2017-08-08 | 禹州市神器钧窑有限公司 | A kind of red glaze of an ancient unit of weight |
| CN107098587A (en) * | 2017-06-05 | 2017-08-29 | 任合超 | A kind of pottery sky blue cracked glaze |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020213A (en) * | 2018-09-21 | 2018-12-18 | 王晟鸣 | A kind of your porcelain sky blue glaze and preparation method thereof, your porcelain |
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Application publication date: 20180427 |