CN108821581A - A kind of rough flambe and preparation method thereof for walking mud line with earthworm - Google Patents
A kind of rough flambe and preparation method thereof for walking mud line with earthworm Download PDFInfo
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- CN108821581A CN108821581A CN201810668549.6A CN201810668549A CN108821581A CN 108821581 A CN108821581 A CN 108821581A CN 201810668549 A CN201810668549 A CN 201810668549A CN 108821581 A CN108821581 A CN 108821581A
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- earthworm
- glaze
- mud line
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Road Paving Structures (AREA)
Abstract
The invention discloses a kind of rough flambes that mud line is walked with earthworm, it is prepared by following raw material：50-70 parts of melilite, 12-18 parts of calcite, 8-12 parts of quartz, 4-6 parts of Copper Ores, 5-7 parts of Suzhou soil, 2-4 parts of black wool soil, 0.5-1.5 parts of talcum, 0.3-0.7 parts of copper oxide, 6-10 parts of zircon, 6-10 parts of wollastonite.The rough flambe preparation method that mud line is walked with earthworm, includes the following steps：（1）Mixing and ball milling after above-mentioned raw materials crush, adds water that the mass concentration of glaze is made to reach 55-56%, wet-milling 8-10 hours, wet-grinded slurry crossed 120-300 mesh and obtains glaze slip；（2）Green body soaks glaze 2-3 times；（3）Firing, firing temperature are 1280-1320 DEG C.The lines flow smoothly in the glaze layer being fired into, mellow and full nature, tone are soft, the beautiful trace got in sposh just like earthworm, and yield rate is 70% or more.
Description
Technical field
The present invention relates to pottery manufacturing technology fields, and in particular to a kind of rough flambe and its preparation that mud line is walked with earthworm
Method.
Background technique
Pottery is originated in the Eastern Han Dynasty, is one of five big kiln porcelain of Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, referred to as
National treasure, rarity are world-famous for unique transmutation art, are known as " the valuable an ancient unit of weight of gold is priceless " and " there is ten thousand strings of cash in family, is not so good as pottery
One " good reputation.
Pottery is the exclusive national treasure porcelain in the Henan Province Xuchang City Yuzhou City town mind Hou, by its simple and unsophisticated moulding, consummate
Technique, the complicated magical transmutation with glaze, " it is color to enter kiln kiln discharge ten thousand of the same colour ", the beautiful scenery of lakes and mountains, rosy clouds fog, people's beast flower, bird, insect, and fish etc.
Varied figure color and marvellous charm is known as first of Chinese " five big porcelain ".
In the prior art, formula of rough flambe of mud line and preparation method thereof is walked with earthworm also seldom, the production being fired into
There is low in glossiness in product, the problem crystallized and mechanical strength is not high occurs in glaze, there is 70% or so product during firing
It can scrap, yield rate is low, therefore huge to the waste of raw material, and cost of manufacture is too high.
Summary of the invention
The present invention provides a kind of raw material and the novel rough flambe and preparation method thereof that mud line is walked with earthworm is matched, with
Formula and the preparation method for solving the existing rough flambe that mud line is walked with earthworm are few, and low in glossiness, glaze crystallizes, mechanical strong
Spend the not high problem low with yield rate.
The purpose of the present invention is what is realized with following technical proposals：
A kind of rough flambe for walking mud line with earthworm, it is prepared by the raw material of following parts by weight：50-70 parts of melilite,
12-18 parts of calcite, 8-12 parts of quartz, 4-6 parts of Copper Ores, 5-7 parts of Suzhou soil, 2-4 parts of black wool soil, 0.5-1.5 parts of talcum, oxygen
Change copper 0.3-0.7 parts, 6-10 parts of zircon, 6-10 parts of wollastonite.
Preferably, the rough flambe that mud line is walked with earthworm, it is prepared by the raw material of following parts by weight：It is yellow
60 parts of feldspar, 15 parts of calcite, 10 parts of quartz, 5 parts of Copper Ores, 6 parts of Suzhou soil, black wool native 3 parts, 1 part of talcum, copper oxide 0.5
Part, 8 parts of zircon, 8 parts of wollastonite.
The preparation method of the rough flambe that mud line is walked with earthworm, includes the following steps：
（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and water, which is added, makes the mass concentration of glaze reach 55-56%, wet
Mill 8-10 hours, wet-grinded slurry crosses 120-300 mesh and obtains glaze slip；
（2）Green body soaks glaze 2-3 times；
（3）Firing, firing temperature are 1280-1320 DEG C.
Preferably, the preparation method of the rough flambe that mud line is walked with earthworm, it is characterised in that step（3）Middle firing
Technique specifically comprises the following steps：
1. the green body after glazing is put into kiln, fired under oxidizing atmosphere, temperature is made to be ramped up 1000- at 4-6 hours
1020℃；
2. temperature under reducing atmosphere, is made to be ramped up 1300 DEG C in 5-6 hours；
3. annealing is cooled to room temperature, it is made.
Beneficial effects of the present invention are as follows：
1, the invention discloses the formula and production method of a kind of rough flambe for walking mud line with earthworm, by reasonably matching and
Preparation method can be fired to obtain the stable rough flambe for walking mud line with earthworm, because glazing is thicker, gold contained in glaze
It is different to belong to ion weight, some float on surface, some sink to glaze bottom, in addition shrinkage temperature is inconsistent up and down for shaddock when cooling,
Under the difference of the temperature difference and density, glaze layer is made to generate two different movements.One is being affected by gravity down to flow from the top to the bottom, one
Kind be the inside and outside movement between glaze layer inner wall and glaze surface layer, two kinds of interaction between moving, formed in glaze layer the lines flow smoothly, it is mellow and full from
So, tone is soft, the beautiful trace got in sposh just like earthworm, and yield rate is 70% or more.
2, pick diamond stone is used in raw material of the present invention, glaze layer crystal phase is mainly pick cristobalite crystal and glass phase composition, in glaze layer
Pick cristobalite crystal be evenly distributed in glaze layer, it is the main milkiness phase of opaque glaze, and the wearability of glaze layer also can be improved.
3, wollastonite is used in raw material of the present invention, the rambling arrangement of wollastonite acicular crystal forms pilotaxitic texture, quilt
Attached in the melt that partial melting generates, the structural stability and mechanical strength of sintered body can be greatly enhanced.On the other hand former
It wollastonite in material and burns the low loss on ignition of talcum and reduces the drum in glaze slip to reduce the crystallization water in raw material and carbonate,
Keep glaze layer fine and close, promotes mechanical strength.Wollastonite has apparent flux to act on, and the coefficient of expansion is low, is free of the crystallization water and carbonic acid
Salt does not decompose generation gas in sintering process, can reduce the firing time of product, has apparent energy-saving effect, avoids product
Deformation and cracking, the generation of less glaze pin hole, improve glaze quality.
Specific embodiment
Embodiment 1
A kind of rough flambe for walking mud line with earthworm, it is prepared by the raw material of following parts by weight：50-70 parts of melilite,
12-18 parts of calcite, 8-12 parts of quartz, 4-6 parts of Copper Ores, 5-7 parts of Suzhou soil, 2-4 parts of black wool soil, 0.5-1.5 parts of talcum, oxygen
Change copper 0.3-0.7 parts, 6-10 parts of zircon, 6-10 parts of wollastonite.
The preparation method of the rough flambe that mud line is walked with earthworm, includes the following steps：
（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and water, which is added, makes the mass concentration of glaze reach 55-56%, wet
Mill 8-10 hours, wet-grinded slurry crosses 120-300 mesh and obtains glaze slip；
（2）Green body soaks glaze 2-3 times；
（3）Firing, firing temperature are 1280-1320 DEG C.
The present invention is using melilite as primary solvent, and melilite dioxide-containing silica is 77% or so, aluminium oxide 13% or so, oxygen
Change iron 0.6%, magnesia 0.16%.Calcite mainly reduces glaze melting temperature, can increase the refractive index of glaze in glaze, thus mentions
High gloss, and the translucency of glaze can be improved.Quartz plays skeleton function, and the main glossiness for increasing glaze can improve glaze
Mobility.Copper Ores and copper oxide play pigmentation in glaze.The essential mineral of Suzhou soil be tubulose halloysite and
Sheet kaolinite, alumina content are 37%~39%, silica 46%~48%, 1730 DEG C of refractoriness, quality fine and smooth lubricious,
Plasticity is lower.Black wool soil aluminium content is higher, and plasticity and caking property with higher play suspension effect, glaze can be improved
Texture.Oxidation magnesium component contained in talcum is cosolvent, promotes the generation of middle layer between green body and glaze, improves thermostabilization
Property, expand firing range, enhancing milkiness effect.Zircon plays the role of milkiness.Wollastonite crystal generates melt in partial melting
Under the action of united, formed pilotaxitic texture, elevating mechanism intensity.
By the atmosphere and temperature in rational proportion and control sintering process, the glaze prepared is in walk mud line with earthworm
The unique color of copper red color has very high art and economic value.
Embodiment 2
A kind of rough flambe for walking mud line with earthworm, it is prepared by the raw material of following parts by weight：60 parts of melilite, Fang Xie
15 parts of stone, quartz 10 parts, 5 parts of Copper Ores, 6 parts of Suzhou soil, black wool soil 3 parts, 1 part of talcum, 0.5 part of copper oxide, 8 parts of zircon,
8 parts of wollastonite.
The preparation method of the rough flambe that mud line is walked with earthworm, includes the following steps：
（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and water, which is added, makes the mass concentration of glaze reach 55-56%, wet
Mill 8-10 hours, wet-grinded slurry crosses 120-300 mesh and obtains glaze slip；
（2）Green body soaks glaze 2-3 times；
（3）Firing, firing temperature are 1280-1320 DEG C.
It is characterized in that step（3）Middle firing process specifically comprises the following steps：
1. the green body after glazing is put into kiln, fired under oxidizing atmosphere, temperature is made to be ramped up 1000- at 4-6 hours
1020℃；
2. temperature under reducing atmosphere, is made to be ramped up 1300 DEG C in 5-6 hours；
3. annealing is cooled to room temperature, it is made.
By the atmosphere and temperature in rational proportion and control sintering process, the rough flambe color prepared is full, rich
Gloss also walks the effect unique of mud line with earthworm, and stability is strong, and the rough flambe for walking mud line with earthworm being fired into is mechanical
Intensity is high and more beautiful.
Embodiment 3
A kind of rough flambe for walking mud line with earthworm, it is prepared by the raw material of following parts by weight：60 parts of melilite, Fang Xie
15 parts of stone, quartz 10 parts, 5 parts of Copper Ores, 6 parts of Suzhou soil, black wool soil 3 parts, 1 part of talcum, 0.5 part of copper oxide, 8 parts of zircon,
8 parts of wollastonite.
The preparation method of the rough flambe that mud line is walked with earthworm, includes the following steps：
（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and water, which is added, makes the mass concentration of glaze reach 56%, wet-milling 9
Hour, wet-grinded slurry crosses 200 meshes and obtains glaze slip；
（2）Green body soaks glaze 3 times；
（3）Firing, firing temperature are 1300 DEG C.
It is characterized in that step（3）Middle firing process specifically comprises the following steps：
1. the green body after glazing is put into kiln, fired under oxidizing atmosphere, temperature is made to be ramped up 1000 DEG C at 5 hours；
2. temperature under reducing atmosphere, is made to be ramped up 1300 DEG C in 6 hours；
3. annealing is cooled to room temperature, it is made.
By the atmosphere and temperature in rational proportion and control sintering process, for preparing walks the copper red of mud line with earthworm
The full and rich glossiness effect unique of glaze color, and stability is strong, high mechanical strength and more beautiful.
Comparative example 1
A kind of rough flambe for walking mud line with earthworm, it is prepared by the raw material of following parts by weight：60 parts of red feldspar, Fang Xie
15 parts of stone, quartz 10 parts, 5 parts of Copper Ores, 6 parts of Suzhou soil, black wool soil 3 parts, 1 part of talcum, 0.5 part of copper oxide, 8 parts of zircon,
8 parts of wollastonite.Preparation method is the same as embodiment 3.This example is compared with Example 3 compared with using red feldspar instead of melilite.Melilite
Compared to red feldspar, silicon, iron content are higher, and the glossiness on chun glaze surface can be improved.Using in glaze after red feldspar silicon and iron contain
Measure it is less, be fired into earthworm walk mud line rough flambe color it is darker, glossiness is low, and product is more easily-deformable, yield rate only
Have 48% or so.
Comparative example 2
A kind of rough flambe for walking mud line with earthworm, is prepared by the raw material of following parts by weight：60 parts of melilite, calcite 15
Part, 10 parts of quartz, 5 parts of Copper Ores, 6 parts of Suzhou soil, black wool native 3 parts, 1 part of talcum, 0.5 part of copper oxide, 8 parts of wollastonite.Preparation
Method is the same as embodiment 3.This example compared with Example 3 compared with, in raw material be not used pick diamond stone, because lacking pick diamond stone, the band being fired into
The opacity and glossiness for having earthworm to walk the rough flambe of mud line are lower than the copper red for walking mud line with earthworm prepared in embodiment 3
Glaze, wearability is relatively poor, and yield rate only has 45% or so.
Comparative example 3
A kind of rough flambe for walking mud line with earthworm, is prepared by the raw material of following parts by weight：68 parts of melilite, calcite 15
Part, 10 parts of quartz, 5 parts of Copper Ores, 6 parts of Suzhou soil, black wool native 3 parts, 1 part of talcum, 0.5 part of copper oxide, 8 parts of zircon.This example
Compared with Example 3 compared with unused wollastonite, the usage amount of melilite increase to 68 parts in raw material, and what is be fired into has earthworm
The rough flambe surface for walking mud line is not smooth enough, and glaze pinprick easy to form, color is dimer, and hardness is not so good as to prepare in embodiment 3
Walk the rough flambe of mud line with earthworm, yield rate only has 51%.
The formula for the rough flambe for walking mud line with earthworm that 4-27 of the embodiment of the present invention is provided is shown in Table 1-4, preparation method
With embodiment 3.
Claims (4)
1. a kind of rough flambe for walking mud line with earthworm, it is characterised in that：It is prepared by the raw material of following parts by weight：It is yellow
50-70 parts of feldspar, 12-18 parts of calcite, 8-12 parts of quartz, 4-6 parts of Copper Ores, 5-7 parts of Suzhou soil, 2-4 parts of black wool soil, talcum
0.5-1.5 parts, 0.3-0.7 parts of copper oxide, 6-10 parts of zircon, 6-10 parts of wollastonite.
2. the rough flambe according to claim 1 for walking mud line with earthworm, it is characterised in that：It is by following parts by weight
Raw material is prepared：60 parts of melilite, 10 parts of quartz, 5 parts of Copper Ores, 6 parts of Suzhou soil, 3 parts of black wool soil, is slided 15 parts of calcite
1 part of stone, 0.5 part of copper oxide, 8 parts of zircon, 8 parts of wollastonite.
3. a kind of preparation method for the rough flambe for walking mud line with earthworm as claimed in claim 1 or 2, it is characterised in that including
Following steps：
（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and water, which is added, makes the mass concentration of glaze reach 55-56%, wet
Mill 8-10 hours, wet-grinded slurry crosses 120-300 mesh and obtains glaze slip；
（2）Green body soaks glaze 2-3 times；
（3）Firing, firing temperature are 1280-1320 DEG C.
4. the preparation method of the rough flambe of mud line is walked with earthworm as claimed in claim 3, it is characterised in that step（3）Middle burning
Specifically comprise the following steps at technique：
1. the green body after glazing is put into kiln, fired under oxidizing atmosphere, temperature is made to be ramped up 1000- at 4-6 hours
1020℃；
2. temperature under reducing atmosphere, is made to be ramped up 1300 DEG C in 5-6 hours；
3. annealing is cooled to room temperature, it is made.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810668549.6A CN108821581A (en) | 2018-06-26 | 2018-06-26 | A kind of rough flambe and preparation method thereof for walking mud line with earthworm |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810668549.6A CN108821581A (en) | 2018-06-26 | 2018-06-26 | A kind of rough flambe and preparation method thereof for walking mud line with earthworm |
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| CN108821581A true CN108821581A (en) | 2018-11-16 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109502978A (en) * | 2018-12-28 | 2019-03-22 | 福建省德化县顺兴达陶瓷工艺有限公司 | A kind of preparation method of shrinking pattern glaze ceramics and products thereof |
| CN115557702A (en) * | 2022-11-10 | 2023-01-03 | 福建省德化非凡陶瓷有限公司 | Earthworm mud-streak-running multilayer composite thick-glaze white porcelain and manufacturing process thereof |
| CN116535096A (en) * | 2023-05-12 | 2023-08-04 | 陕西科技大学 | Silver glaze building cup with earthworm mud pattern and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107721172A (en) * | 2017-10-17 | 2018-02-23 | 禹州市锦丰源瓷业有限公司 | A kind of high rigidity an ancient unit of weight fancy glaze and preparation method thereof |
-
2018
- 2018-06-26 CN CN201810668549.6A patent/CN108821581A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107721172A (en) * | 2017-10-17 | 2018-02-23 | 禹州市锦丰源瓷业有限公司 | A kind of high rigidity an ancient unit of weight fancy glaze and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109502978A (en) * | 2018-12-28 | 2019-03-22 | 福建省德化县顺兴达陶瓷工艺有限公司 | A kind of preparation method of shrinking pattern glaze ceramics and products thereof |
| CN115557702A (en) * | 2022-11-10 | 2023-01-03 | 福建省德化非凡陶瓷有限公司 | Earthworm mud-streak-running multilayer composite thick-glaze white porcelain and manufacturing process thereof |
| CN115557702B (en) * | 2022-11-10 | 2023-12-22 | 福建省德化非凡陶瓷有限公司 | Earthworm mud grain multilayer composite thick glaze white porcelain and manufacturing process thereof |
| CN116535096A (en) * | 2023-05-12 | 2023-08-04 | 陕西科技大学 | Silver glaze building cup with earthworm mud pattern and preparation method thereof |
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