CN107936668A - A kind of novel environment-friendly heat insulating coating and preparation method thereof - Google Patents
A kind of novel environment-friendly heat insulating coating and preparation method thereof Download PDFInfo
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- CN107936668A CN107936668A CN201711192076.9A CN201711192076A CN107936668A CN 107936668 A CN107936668 A CN 107936668A CN 201711192076 A CN201711192076 A CN 201711192076A CN 107936668 A CN107936668 A CN 107936668A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D197/00—Coating compositions based on lignin-containing materials
- C09D197/02—Lignocellulosic material, e.g. wood, straw or bagasse
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
Abstract
The present invention provides a kind of novel environment-friendly heat insulating coating and preparation method thereof, is related to technical field of coatings.Novel environment-friendly heat insulating coating of the present invention includes following raw material：Plant fiber, borosilicate hollow glass micropearl, citric acid, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, acrylonitrile butadient styrene, defoamer.Novel environment-friendly heat insulating coating of the present invention has the advantages that good insulation, sound insulation, water-fast, acidproof, alkaline-resisting; it is easy to brush on building inner-outer wall surface; after brushing effective heat insulation layer can be formed in film; also there is good reflection function when being especially coated in exterior wall; at the same time; novel environment-friendly heat insulating coating preparation process is simple, of low cost, is adapted for scale industrial production.
Description
Technical field
The present invention relates to technical field of coatings, more particularly to a kind of novel environment-friendly heat insulating coating and preparation method thereof.
Background technology
Today's society, the energy is the big problem paid close attention to by various countries, and the importance of building energy conservation is by more and more people
Paid attention to.In building the consumption of electric power and the energy can be reduced using the coating with heat-insulation and heat-preservation.China is built
Build energy consumption and occupy very big proportion in national total energy consumption, the heat insulation and preservation effect of building coating is also by more and more engineerings
Used.
Traditional coating pollution environment is again harmful, with the raising of people's quality of the life, it is now of concern not
Only coating is attractive and durable, is more its safety and environmental protection performance, the safety and environmental protection and coating for possessing multiple functions has been not
Carry out the trend of paint development.With developing rapidly for China's building trade and becoming increasingly conspicuous for energy crisis, the section of building
It can lower consumption just important all the more.The building energy consumption in China accounts for the 27% of national energy aggregate consumption, occupies first of all kinds of energy consumptions in the whole nation.
The energy consumption of heating and air-conditioning accounts for the 55% of building total energy consumption, but also in the speed increase with annual 1 percentage point.Because a bit, grinding
Study carefully has great economic benefit, environmental benefit and social benefit with development architecture insulating moulding coating.Have in external wall use
The coating of heat insulating function can not only realize the original decoration of coating, protection and the function such as mould proof, but also make coating have every
The function of heat, keeps indoor temperature constant, increases the temperature difference of indoor and outdoor, and warm energy consumption is reduced in summer, reduces heating fee in the winter time
With.
Thermal insulation coatings are a kind of energy-saving and heat-insulating materials for being gradually subject to people to pay attention in recent years, it is to combine coating and guarantor
Adiabator dual characteristics, can reduce a kind of coating in the thick shape lotion of fiber of thermal loss.It is applied to and requires insulation
Equipment pipe or building surface, it is dry after the insulating layer formed with some strength and elasticity, heat insulation effect is notable, and expense compared with
General thermal insulation material is cheap.
With the rapid development of science and technology, continuous progressive, the continuous enhancing of people's sense of self-protection of human society,
The further realization of sustainable development, thermal insulation coatings as a kind of new functional coating will have more wide market and
Application prospect.
Therefore, it is particularly important that inventing a kind of novel high-performance, environment-friendly heat insulating coating.
The content of the invention
For problem of the prior art, a kind of novel environment-friendly heat insulating coating and preparation method thereof is provided for the present invention.
The present invention uses following technical scheme：
A kind of novel environment-friendly heat insulating coating, the novel environment-friendly heat insulating coating include the raw material of following parts by weight：Plant is fine
15-25 parts of dimension, 23-37 parts of borosilicate hollow glass micropearl, 5-8 parts of citric acid, 2-7 parts of water-reducing agent, nanometer rubber powder 10-17
Part, 10-15 parts of sepiolite, 25-40 parts of functional stuffing, 3-7 parts of acrylonitrile-butadiene-styrene copolymer, 1-6 parts of defoamer.
Further, the novel environment-friendly heat insulating coating includes the raw material of following parts by weight：18-23 parts of plant fiber, boron
27-34 parts of silicate hollow glass micropearl, 6-7 parts of citric acid, 3-6 parts of water-reducing agent, 12-15 parts of nanometer rubber powder, sepiolite 11-14
Part, 30-36 parts of functional stuffing, 4-6 parts of acrylonitrile-butadiene-styrene copolymer, 2-5 parts of defoamer.
Further, the novel environment-friendly heat insulating coating includes the raw material of following parts by weight：20 parts of plant fiber, borosilicic acid
30 parts of salt hollow glass micropearl, 6 parts of citric acid, 14 parts of 5 part, nanometer rubber powder of water-reducing agent, 13 parts of sepiolite, 33 parts of functional stuffing,
5 parts of acrylonitrile-butadiene-styrene copolymer, 3.5 parts of defoamer.
Further, the water-reducing agent selects naphthalenesulfonate formaldehyde condensation compound, sulfonated melamine compound condensation product, poly- carboxylic
One kind in sour water-reducing agent.
Further, the functional stuffing is wood-fibred, fly ash float, aerosil, bentonite, ceramic fine bead
At least one of.
Further, the defoamer is three fat of sorbitan alcohol laurate or polypropylene glycol.
A kind of preparation method of novel environment-friendly heat insulating coating, comprises the following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, third
Alkene nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, and constant temperature after being slowly heated to 100-180 DEG C to boiler, is stirred
10-25min postcoolings are mixed to room temperature, add citric acid, defoamer stirs evenly, taking-up pack.
A kind of novel environment-friendly heat insulating coating of the present invention and preparation method thereof, compared with prior art, the characteristics of it is protruded and
Excellent effect is：
Novel environment-friendly heat insulating coating of the present invention has the advantages that good insulation, sound insulation, water-fast, acidproof, alkaline-resisting, easily
In brushing on building inner-outer wall surface, effective heat insulation layer can be formed in film after brushing, especially be coated in exterior wall
When also there is good reflection function, meanwhile, novel environment-friendly heat insulating coating preparation process is simple, of low cost, is adapted for
Scale industrial production；
The addition of plant fiber, borosilicate hollow glass micropearl is in coating in novel environment-friendly heat insulating coating raw material of the present invention
In form " froth bed " phenomenon so as to play well heat preserving heat insulating noise insulation effect, in addition plant fiber addition, also
Play the role of coating enhancing, add impact resistance；Nanometer rubber powder is that one kind reaches nano level gelinite, by length
Nanofiber, nanometer rods and the micro-nano crystal particles to differ are formed, and can improve water resistance, the abrasion resistance of coating, resistance to be stained with
Dirt, and the addition of nanometer rubber powder also has synergistic effect to functional stuffing；Secondly, water-reducing agent, nanometer rubber powder, sepiolite, work(
The raw materials such as energy filler, acrylonitrile-butadiene-styrene copolymer, citric acid fall within environment-friendly type raw material, and the coating of preparation will not
There is volatile harmful gase, beneficial to health.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, following embodiments, carry out the present invention
It is further described.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit
The present invention.
Embodiment 1
The present embodiment novel environment-friendly heat insulating coating includes the raw material of following parts by weight：15 parts of plant fiber, borosilicate are empty
23 parts of heart glass microballoon, 5 parts of citric acid, 10 parts of 2 part, nanometer rubber powder of water-reducing agent, 10 parts of sepiolite, 25 parts of functional stuffing, propylene
3 parts of nitrile-butadiene-styrene copolymer, 1 part of defoamer；
Wherein, water-reducing agent selects naphthalenesulfonate formaldehyde condensation compound；Functional stuffing is wood-fibred, fly ash float, gas phase two
Silica, bentonite, ceramic fine bead mix；Defoamer is three fat of sorbitan alcohol laurate；
The preparation method of the present embodiment novel environment-friendly heat insulating coating, comprises the following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, third
Alkene nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, constant temperature after 100 DEG C are slowly heated to boiler, stirring
10min postcoolings add citric acid, defoamer stirs evenly, taking-up pack to room temperature.
Embodiment 2
The present embodiment novel environment-friendly heat insulating coating includes the raw material of following parts by weight：25 parts of plant fiber, borosilicate are empty
37 parts of heart glass microballoon, 8 parts of citric acid, 17 parts of 7 part, nanometer rubber powder of water-reducing agent, 15 parts of sepiolite, 40 parts of functional stuffing, propylene
7 parts of nitrile-butadiene-styrene copolymer, 6 parts of defoamer；
Wherein, water-reducing agent selects sulfonated melamine compound condensation product；Functional stuffing for wood-fibred, aerosil,
Bentonite, ceramic fine bead mix；Defoamer is polypropylene glycol；
The preparation method of the present embodiment novel environment-friendly heat insulating coating, comprises the following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, third
Alkene nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, constant temperature after 180 DEG C are slowly heated to boiler, stirring
25min postcoolings add citric acid, defoamer stirs evenly, taking-up pack to room temperature
Embodiment 3
The present embodiment novel environment-friendly heat insulating coating includes the raw material of following parts by weight：20 parts of plant fiber, borosilicate are empty
30 parts of heart glass microballoon, 6 parts of citric acid, 14 parts of 5 part, nanometer rubber powder of water-reducing agent, 13 parts of sepiolite, 33 parts of functional stuffing, propylene
5 parts of nitrile-butadiene-styrene copolymer, 3.5 parts of defoamer；
Wherein, water-reducing agent selects polycarboxylate water-reducer；Functional stuffing for wood-fibred, fly ash float, aerosil,
Bentonite, ceramic fine bead mix；Defoamer is three fat of sorbitan alcohol laurate；
The preparation method of the present embodiment novel environment-friendly heat insulating coating, comprises the following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, third
Alkene nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, constant temperature after 140 DEG C are slowly heated to boiler, stirring
18min postcoolings add citric acid, defoamer stirs evenly, taking-up pack to room temperature.
Embodiment 4
The present embodiment novel environment-friendly heat insulating coating includes the raw material of following parts by weight：18 parts of plant fiber, borosilicate are empty
27 parts of heart glass microballoon, 6 parts of citric acid, 12 parts of 3 part, nanometer rubber powder of water-reducing agent, 11 parts of sepiolite, 30 parts of functional stuffing, propylene
4 parts of nitrile-butadiene-styrene copolymer, 2 parts of defoamer；
Wherein, water-reducing agent selects naphthalenesulfonate formaldehyde condensation compound；Functional stuffing is bentonite；Defoamer is sorbitan
Three fat of alcohol laurate；
The preparation method of the present embodiment novel environment-friendly heat insulating coating, comprises the following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, third
Alkene nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, constant temperature after 120 DEG C are slowly heated to boiler, stirring
15min postcoolings add citric acid, defoamer stirs evenly, taking-up pack to room temperature.
Embodiment 5
The present embodiment novel environment-friendly heat insulating coating includes the raw material of following parts by weight：23 parts of plant fiber, borosilicate are empty
34 parts of heart glass microballoon, 7 parts of citric acid, 15 parts of 6 part, nanometer rubber powder of water-reducing agent, 14 parts of sepiolite, 36 parts of functional stuffing, propylene
6 parts of nitrile-butadiene-styrene copolymer, 5 parts of defoamer；
Wherein, water-reducing agent selects sulfonated melamine compound condensation product；Functional stuffing is aerosil；Defoamer is
Polypropylene glycol；
The preparation method of the present embodiment novel environment-friendly heat insulating coating, comprises the following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, third
Alkene nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, constant temperature after 160 DEG C are slowly heated to boiler, stirring
23min postcoolings add citric acid, defoamer stirs evenly, taking-up pack to room temperature.
Coating prepared by embodiment 1-5 carries out external wall film, is slaughtered in identical structure, building of the same area
Coating prepared by magic embodiment 1-5, summer outdoor temperature is asked as 40 DEG C, and indoor temperature is tested, and other performances are surveyed
Examination, the testing standard of sun luminous reflectance is ASTM C1549-2009, and hemispherical emissivity testing standard is ASTM C371-
2004a (2010) e1, the results are shown in Table 1.
1 coating of table carries out performance test after film
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Indoor temperature DEG C | 28 | 27 | 25 | 27 | 30 |
| Adhesive force, level | 1 | 2 | 2 | 2 | 1 |
| Water resistance | 100h is without exception | 100h is without exception | 100h is without exception | 100h is without exception | 100h is without exception |
| Alkali resistance | 60h is without exception | 60h is without exception | 60h is without exception | 60h is without exception | 60h is without exception |
| Sun luminous reflectance≤0.8 | 0.8856 | 0.8803 | 0.8896 | 0.8895 | 0.8834 |
| Ban ball Fa She Shuai≤0.8 | 0.8898 | 0.8966 | 0.8971 | 0.8562 | 0.8917 |
Shown by 1 data of table, novel environment-friendly heat insulating coating sun luminous reflectance prepared by the present invention is high, hemispherical emissivity
Height, thermal and insulating performance is good, strong adhesive force, water-tolerant, and corrosion resistance is strong.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although ginseng
The present invention is described in detail according to previous embodiment, it will be understood by those of ordinary skill in the art that：It still can be with
Modify to the technical solution described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic；And
These modifications are replaced, and the essence of appropriate technical solution is departed from the spirit and model of various embodiments of the present invention technical solution
Enclose.
Claims (7)
1. a kind of novel environment-friendly heat insulating coating, it is characterised in that the novel environment-friendly heat insulating coating includes the original of following parts by weight
Material：15-25 parts of plant fiber, 23-37 parts of borosilicate hollow glass micropearl, 5-8 parts of citric acid, 2-7 parts of water-reducing agent, nanometre glue
10-17 parts of powder, 10-15 parts of sepiolite, 25-40 parts of functional stuffing, 3-7 parts of acrylonitrile-butadiene-styrene copolymer, defoaming
1-6 parts of agent.
2. novel environment-friendly heat insulating coating according to claim 1, it is characterised in that the novel environment-friendly heat insulating coating includes
The raw material of following parts by weight：18-23 parts of plant fiber, 27-34 parts of borosilicate hollow glass micropearl, 6-7 parts of citric acid, diminishing
3-6 parts of agent, 12-15 parts of nanometer rubber powder, 11-14 parts of sepiolite, 30-36 parts of functional stuffing, acrylonitrile-butadiene-styrene (ABS) are common
4-6 parts of polymers, 2-5 parts of defoamer.
3. novel environment-friendly heat insulating coating according to claim 1, it is characterised in that the novel environment-friendly heat insulating coating includes
The raw material of following parts by weight：20 parts of plant fiber, 30 parts of borosilicate hollow glass micropearl, 6 parts of citric acid, 5 parts of water-reducing agent, receive
14 parts of rice glue powder, 13 parts of sepiolite, 33 parts of functional stuffing, 5 parts of acrylonitrile-butadiene-styrene copolymer, 3.5 parts of defoamer.
4. according to the novel environment-friendly heat insulating coating described in claim 1-3 any one, it is characterised in that the water-reducing agent is selected
One kind in naphthalenesulfonate formaldehyde condensation compound, sulfonated melamine compound condensation product, polycarboxylate water-reducer.
5. according to the novel environment-friendly heat insulating coating described in claim 1-3 any one, it is characterised in that：The functional stuffing is
At least one of wood-fibred, fly ash float, aerosil, bentonite, ceramic fine bead.
6. according to the novel environment-friendly heat insulating coating described in claim 1-3 any one, it is characterised in that：The defoamer is contracting
Three fat of water D-sorbite laurate or polypropylene glycol.
A kind of 7. preparation method of novel environment-friendly heat insulating coating as claimed in any one of claims 1 to 6, it is characterised in that including
Following steps：
S1, according to parts by weight weigh each raw material；
S2, by plant fiber, borosilicate hollow glass micropearl, water-reducing agent, nanometer rubber powder, sepiolite, functional stuffing, propylene
Nitrile-butadiene-styrene copolymer, which is put into, to be stirred under vacuum in boiler, constant temperature after being slowly heated to 100-180 DEG C to boiler, stirring
10-25min postcoolings add citric acid, defoamer stirs evenly, taking-up pack to room temperature.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113563771A (en) * | 2021-08-18 | 2021-10-29 | 广东薄可涂环保科技有限公司 | Anti-cracking sound-insulation composite material and preparation method thereof |
| CN113652111A (en) * | 2021-08-18 | 2021-11-16 | 广东薄可涂环保科技有限公司 | Powder for energy-saving wall and preparation method thereof |
| CN116554746A (en) * | 2023-05-15 | 2023-08-08 | 西南大学 | Environment-friendly heat-insulating anticorrosive paint and preparation method and application thereof |
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| CN116554746A (en) * | 2023-05-15 | 2023-08-08 | 西南大学 | Environment-friendly heat-insulating anticorrosive paint and preparation method and application thereof |
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Application publication date: 20180420 |