CN108795200A - Lightweight complex building heat insulating coatings and preparation method thereof - Google Patents
Lightweight complex building heat insulating coatings and preparation method thereof Download PDFInfo
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- CN108795200A CN108795200A CN201810698190.7A CN201810698190A CN108795200A CN 108795200 A CN108795200 A CN 108795200A CN 201810698190 A CN201810698190 A CN 201810698190A CN 108795200 A CN108795200 A CN 108795200A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
Abstract
The present invention relates to a kind of lightweight complex building heat insulating coatings, in parts by weight, including 30-50 parts of silicone acrylic emulsion, cellular material 10-15 parts heat-insulated, 10-15 parts of kaolin powder, 1-3 parts of modified ceramic microballoon, 3-5 parts of far-infared ceramic powder, 13-15 parts of rutile type titanium white, 3-5 parts of Ludox, 3-5 parts of re-dispersible glue powder, 1-3 parts of hydroxypropyl methyl cellulose, 1-3 parts of naphthalene water reducer, 2-5 parts of cracking resistance auxiliary agent, 0.3-0.5 parts of antifoaming agent, 20-30 parts of water.The lightweight complex building heat insulating coatings weather resistance of the present invention is excellent, has heat-insulated, reflection double effects, has good heat insulation effect.
Description
Technical field
The present invention relates to a kind of lightweight complex building heat insulating coatings and preparation method thereof, belong to heat-insulating heat-preserving material neck
Domain.
Background technology
With the rapid development of China's building trade and becoming increasingly conspicuous for energy crisis, the energy-saving of building is got over
Send out important.The energy consumption of China's heating and air-conditioning accounts for the 55% of building total energy consumption, but also increases with annual 1 percentage point of speed
Add.Therefore, insulating mold coating for construction is researched and developed, indoor/outdoor temperature-difference is increased, summer reduces warm energy consumption, and winter reduces heating energy consumption
With great economic benefit, environmental benefit and social benefit.Often, hot transfer mode is to conduct, convection current and radiation, accordingly
, insulating mechanism is usually to obstruct, reflection and radiation, so, according to insulating mechanism difference, the heat-insulated painting occurred earliest on the market
Material is divided into three categories：Isolation-type insulating moulding coating, reflective insulation coating and Radiation Heat-insulated Paint；Then, but occur it is a variety of every
Heat engine manages the compound insulating moulding coating that heat-insulated aggregate is used in compounding, although being better than single type insulating moulding coating on heat insulation,
But its there is also problems with：When the additive amount of the heat-insulated aggregate of different insulating mechanisms is small, filler easily forms lonely in coating
Island, heat can transmit around these isolated islands and to base material, to cause coating heat insulation poor；When the heat-insulated bone of different insulating mechanisms
When the additive amount of material is big, heat-insulated aggregate can be unevenly distributed again, influence heat insulation, while also paint film can be caused unstable, be used
Short life.In addition, the shortcomings that such coating also generally existing is long arid cycle, and construction is easily influenced by weather environment.Shen Qing Publication
Number 107760156 A of CN, denomination of invention：A kind of heat insulating reflecting coating and preparation method thereof, the heat insulating reflecting coating is by following heavy
Measure the raw material composition of number：20~35 parts of aqueous epoxy resins, 10~20 parts of waterborne curing agent, 15~30 parts of polyurethane, work(
It can 90~110 parts of filler；The functional stuffing is keyed by the full carbon aerogels of sulfonation and nano meter Fe_3O_4 chemistry, and sulfonation is complete
The mass ratio of carbon aerogels and nano meter Fe_3O_4 is 1:4, it can be effectively improved in current heat insulating reflecting coating different heat-insulated
Mechanism thermal insulating filling is unevenly distributed, and heat insulation is poor, and arid cycle is long, the drawbacks such as bad mechanical property.But still remain with
Lower problem：The heat insulating reflecting performance of whole coating is bad, and especially it is low to have a rate of closed hole in use for hollow ceramic microspheres,
Water absorption rate is big, and the mass defects such as frangible seriously affect the heat insulating effect of hollow ceramic microspheres and its product.
Invention content
The present invention provides a kind of lightweight complex building heat insulating coatings and preparation method thereof, solve existing heat-insulated guarantor
The problem of thermo-paint entirety heat preservation and insulation difference.
In order to solve the above technical problems, the technical solution adopted by the present invention：
A kind of lightweight complex building heat insulating coatings, in parts by weight, including 30-50 parts of silicone acrylic emulsion, heat-insulated honeycomb material
10-15 parts of material, 10-15 parts of kaolin powder, 1-3 parts of modified ceramic microballoon, 3-5 parts of far-infared ceramic powder, rutile type titanium white
13-15 parts, 3-5 parts of Ludox, 3-5 parts of re-dispersible glue powder, 1-3 parts of hydroxypropyl methyl cellulose, 1-3 parts of naphthalene water reducer,
2-5 parts of cracking resistance auxiliary agent, 0.3-0.5 parts of antifoaming agent, 20-30 parts of water.
Further, a preferred embodiment of the present invention is：The preparation method of the heat-insulated cellular material is as follows：By carbon fiber
Tie up 40-50 parts by weight, thickener 5-10 parts by weight, nano-silicon hybrid resin 15-20 parts by weight, montmorillonite 3-5 parts by weight, swelling
Native 1-2 parts by weight, silica 6-8 parts by weight are uniformly mixed, and are pressed into the thin plate of 10-20mm, are cured, low-temperature carbonization, then powder
It is broken, 150 mesh sieve is crossed, heat-insulated cellular material is obtained.
Further, a preferred embodiment of the present invention is：The thickener is appointing for chitosan, sodium alginate and agar
Meaning is one or more of.
Further, a preferred embodiment of the present invention is：The cured temperature is 160 DEG C~200 DEG C, the cured time
For 1h~2h；The temperature of the carbonization is 600 DEG C~800 DEG C, and the time of carbonization is 2h~3h.
Further, a preferred embodiment of the present invention is：The cracking resistance auxiliary agent is the polypropylene cracking resistance that length is 1~10mm
Fiber.
Further, a preferred embodiment of the present invention is：The preparation method of the modified ceramic microballoon：By 10 parts by weight
Polylactic resin, the dispersible rubber powder of 3 parts by weight and 0.1 part of titania powder are uniformly mixed, fusing, then convertible mixed
It closes in reaction kettle, 100 parts by weight ceramic microspheres is heated to 90-95 DEG C, the mixture of molten condition is sprayed at glass bead
Surface, overturning mixing 25-30 minutes.
Present invention provides a kind of preparation methods of lightweight complex building heat insulating coatings, include the following steps：
（1）Raw material is weighed by weight, by Ludox, re-dispersible glue powder, hydroxypropyl methyl cellulose, naphthalene water reducer, is resisted
It splits auxiliary agent, antifoaming agent and water to be uniformly mixed, 10-20min is disperseed with the stir speed (S.S.) of 400-800r/min, it is spare；
（2）Raw material is weighed by weight, by kaolin powder, modified ceramic microballoon, far-infared ceramic powder and rutile type titanium white
It is uniformly mixed, is added to the（1）In the solution of step, 10-20min is disperseed with the stir speed (S.S.) of 1000-1200r/min, it is spare；Point
It dissipates uniform；
（3）Raw material is weighed by weight, and silicone acrylic emulsion, heat-insulated cellular material, kaolin powder and modified ceramic microballoon are added to
（2）In step, 30-40min is disperseed with the stir speed (S.S.) of 100-150r/min, is stirred evenly to get the heat-insulated guarantor of lightweight complex building
Thermo-paint.
Beneficial effects of the present invention：
The present invention increases the material for being conducive to light reflection so that the modified pottery in its surface by the modification to modified ceramic microballoon
Porcelain microballoon not cracky, ensure that inorganic heat insulation mortar body unit weight stability, to ensure that the stability of thermal coefficient；In addition
Light reflective properties are effectively increased, its heat-insulating property is made to effectively improve.By modified ceramic microballoon, far-infared ceramic powder,
Major ingredient of the rutile type titanium white as light reflection so that coating has the effect of good reflection photo-thermal.
Heat-insulated cellular material is filler, 80~120mg/cm3 of density of heat-insulated cellular material, good mechanical performance, intensity
Height, overall structure are stablized, and foam is uniform in bee-hole, and rate of closed hole is high, and thermal coefficient is small, reduces heat radiation, heat transfer and sky
Gas convection current improves heat insulation and preservation effect.Heat-insulated cellular material and modified ceramic microballoon are used in combination, and can effectively improve coating
Heat-proof quality.
The lightweight complex building heat insulating coatings weather resistance of the present invention is excellent, has heat-insulated, reflection double effects, tool
There is good heat insulation effect.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme of the present invention is clearly and completely described, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
The every other embodiment that those of ordinary skill in the art are obtained without creative efforts, belongs to this hair
The range of bright protection.
The preparation method of heat-insulated cellular material used in embodiment is as follows：By 40 parts by weight of carbon fiber, 8 weight of thickener
Part, 15 parts by weight of nano-silicon hybrid resin, 4 parts by weight of montmorillonite, 1 parts by weight of bentonite, 6 parts by weight of silica, mixing are equal
It is even, it is pressed into the thin plate of 10-20mm, then solidification, low-temperature carbonization crush, cross 150 mesh sieve, obtain heat-insulated cellular material.
Nano-silicon hybrid resin uses the COMPOCERAN SQ502-8 of Arakawa Chemical Industries, Ltd..
Thickener is agar.
Cured temperature is 160 DEG C, and the cured time is 1h；The temperature of the carbonization is 600 DEG C, and the time of carbonization is
3h。
Cracking resistance auxiliary agent is the polypropylene anti-crack fiber that length is 1~10mm.
The preparation method of modified ceramic microballoon：By 10 parts by weight polylactic resin, the dispersible rubber powder of 3 parts by weight and 0.1 part
Titania powder be uniformly mixed, fusing, then in convertible hybrid reactor, by 100 parts by weight ceramic microspheres heat
To 90-95 DEG C, the mixture of molten condition is sprayed at glass bead surface, overturning mixing 25-30 minutes.
Embodiment 1
A kind of lightweight complex building heat insulating coatings, in parts by weight, including 30 parts of silicone acrylic emulsion, heat-insulated cellular material 15
Part, 10 parts of kaolin powder, 1 part of modified ceramic microballoon, 5 parts of far-infared ceramic powder, 13 parts of rutile type titanium white, 3 parts of Ludox,
5 parts of re-dispersible glue powder, 1 part of hydroxypropyl methyl cellulose, 3 parts of naphthalene water reducer, 2 parts of cracking resistance auxiliary agent, 0.3 part of antifoaming agent, water
20 parts.
Its preparation method, includes the following steps：
（1）Raw material is weighed by weight, by Ludox, re-dispersible glue powder, hydroxypropyl methyl cellulose, naphthalene water reducer, is resisted
It splits auxiliary agent, antifoaming agent and water to be uniformly mixed, 20min is disperseed with the stir speed (S.S.) of 400r/min, it is spare；
（2）Raw material is weighed by weight, by kaolin powder, modified ceramic microballoon, far-infared ceramic powder and rutile type titanium white
It is uniformly mixed, is added to the（1）In the solution of step, 20min is disperseed with the stir speed (S.S.) of 1000r/min, it is spare；It is uniformly dispersed；
（3）Raw material is weighed by weight, and silicone acrylic emulsion, heat-insulated cellular material, kaolin powder and modified ceramic microballoon are added to
（2）In step, 30min is disperseed with the stir speed (S.S.) of 100r/min, is stirred evenly to get lightweight complex building heat insulating coatings.
Embodiment 2
A kind of lightweight complex building heat insulating coatings, in parts by weight, including 40 parts of silicone acrylic emulsion, heat-insulated cellular material 10
Part, 13 parts of kaolin powder, 2 parts of modified ceramic microballoon, 4 parts of far-infared ceramic powder, 14 parts of rutile type titanium white, 4 parts of Ludox,
3 parts of re-dispersible glue powder, 2 parts of hydroxypropyl methyl cellulose, 1 part of naphthalene water reducer, 3 parts of cracking resistance auxiliary agent, 0.4 part of antifoaming agent, water
25 parts.
Its preparation method, includes the following steps：
（1）Raw material is weighed by weight, by Ludox, re-dispersible glue powder, hydroxypropyl methyl cellulose, naphthalene water reducer, is resisted
It splits auxiliary agent, antifoaming agent and water 20-30 to be uniformly mixed, 15min is disperseed with the stir speed (S.S.) of 600r/min, it is spare；
（2）Raw material is weighed by weight, by kaolin powder, modified ceramic microballoon, far-infared ceramic powder and rutile type titanium white
It is uniformly mixed, is added to the（1）In the solution of step, 10min is disperseed with the stir speed (S.S.) of 1200r/min, it is spare；It is uniformly dispersed；
（3）Raw material is weighed by weight, and silicone acrylic emulsion, heat-insulated cellular material, kaolin powder and modified ceramic microballoon are added to
（2）In step, 30min is disperseed with the stir speed (S.S.) of 150r/min, is stirred evenly to get lightweight complex building heat insulating coatings.
Embodiment 3
A kind of lightweight complex building heat insulating coatings, in parts by weight, including 50 parts of silicone acrylic emulsion, heat-insulated cellular material 13
Part, 15 parts of kaolin powder, 3 parts of modified ceramic microballoon, 3 parts of far-infared ceramic powder, 15 parts of rutile type titanium white, 5 parts of Ludox,
4 parts of re-dispersible glue powder, 3 parts of hydroxypropyl methyl cellulose, 2 parts of naphthalene water reducer, 5 parts of cracking resistance auxiliary agent, 0.5 part of antifoaming agent, water
30 parts.
Its preparation method, includes the following steps：
（1）Raw material is weighed by weight, by Ludox, re-dispersible glue powder, hydroxypropyl methyl cellulose, naphthalene water reducer, is resisted
It splits auxiliary agent, antifoaming agent and water to be uniformly mixed, 10min is disperseed with the stir speed (S.S.) of 800r/min, it is spare；
（2）Raw material is weighed by weight, by kaolin powder, modified ceramic microballoon, far-infared ceramic powder and rutile type titanium white
It is uniformly mixed, is added to the（1）In the solution of step, 15min is disperseed with the stir speed (S.S.) of 1200r/min, it is spare；It is uniformly dispersed；
（3）Raw material is weighed by weight, and silicone acrylic emulsion, heat-insulated cellular material, kaolin powder and modified ceramic microballoon are added to
（2）In step, 40min is disperseed with the stir speed (S.S.) of 100r/min, is stirred evenly to get lightweight complex building heat insulating coatings.
According to J C/T1 040--2007 heat-reflecting insulating coating for outer surface of building, the performance of the coating of preparation is measured,
Specifically it see the table below.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (7)
1. a kind of lightweight complex building heat insulating coatings, which is characterized in that in parts by weight, including silicone acrylic emulsion 30-50
Part, cellular material 10-15 parts heat-insulated, 10-15 parts of kaolin powder, 1-3 parts of modified ceramic microballoon, 3-5 parts of far-infared ceramic powder, gold
13-15 parts of red stone-type titanium dioxide, 3-5 parts of Ludox, 3-5 parts of re-dispersible glue powder, 1-3 parts of hydroxypropyl methyl cellulose, naphthalene system
1-3 parts of water-reducing agent, 2-5 parts of cracking resistance auxiliary agent, 0.3-0.5 parts of antifoaming agent, 20-30 parts of water.
2. a kind of lightweight complex building heat insulating coatings according to claim 1, it is characterised in that：The heat-insulated bee
The preparation method of nest material is as follows：By carbon fiber 40-50 parts by weight, thickener 5-10 parts by weight, nano-silicon hybrid resin 15-20
Parts by weight, montmorillonite 3-5 parts by weight, bentonite 1-2 parts by weight, silica 6-8 parts by weight, solidification, low-temperature carbonization, obtain every
Hot cellular material.
3. a kind of lightweight complex building heat insulating coatings according to claim 2, it is characterised in that：The thickener
For any one or a few of chitosan, sodium alginate and agar.
4. a kind of lightweight complex building heat insulating coatings according to claim 2, it is characterised in that：The cured temperature
Degree is 160 DEG C~200 DEG C, and the cured time is 1h~2h；The temperature of the carbonization is 600 DEG C~800 DEG C, and the time of carbonization is
2h~3h.
5. a kind of lightweight complex building heat insulating coatings according to claim 1, it is characterised in that：The cracking resistance auxiliary agent
The polypropylene anti-crack fiber for being 1~10mm for length.
6. a kind of lightweight complex building heat insulating coatings according to claim 1, it is characterised in that：The modified pottery
The preparation method of porcelain microballoon：By 10 parts by weight polylactic resin, the dispersible rubber powder of 3 parts by weight and 0.1 part of titania powder
It is uniformly mixed, 100 parts by weight ceramic microspheres then in convertible hybrid reactor, are heated to 90-95 DEG C, will melted by fusing
The mixture for melting state is sprayed at glass bead surface, overturning mixing 25-30 minutes.
7. a kind of preparation method of lightweight complex building heat insulating coatings described in claim 1, which is characterized in that including with
Lower step：
（1）Raw material is weighed by weight, by Ludox, re-dispersible glue powder, hydroxypropyl methyl cellulose, naphthalene water reducer, is resisted
It splits auxiliary agent, antifoaming agent and water to be uniformly mixed, 10-20min is disperseed with the stir speed (S.S.) of 400-800r/min, it is spare；
（2）Raw material is weighed by weight, by kaolin powder, modified ceramic microballoon, far-infared ceramic powder and rutile type titanium white
It is uniformly mixed, is added to the（1）In the solution of step, 10-20min is disperseed with the stir speed (S.S.) of 1000-1200r/min, it is spare；Point
It dissipates uniform；
（3）Raw material is weighed by weight, and silicone acrylic emulsion, heat-insulated cellular material, kaolin powder and modified ceramic microballoon are added to
（2）In step, 30-40min is disperseed with the stir speed (S.S.) of 100-150r/min, is stirred evenly to get the heat-insulated guarantor of lightweight complex building
Thermo-paint.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111363388A (en) * | 2020-03-27 | 2020-07-03 | 河南宣和钧釉环保材料有限公司 | Inorganic heat-insulating coating and preparation process thereof |
| CN111848103A (en) * | 2020-07-23 | 2020-10-30 | 湖州巨旺墙体材料有限公司 | Preparation method of low-cost heat insulation building block |
| CN112047744A (en) * | 2020-07-17 | 2020-12-08 | 北京盈德化工有限公司 | Heat insulation material and preparation method and application thereof |
| CN114961018A (en) * | 2022-06-07 | 2022-08-30 | 中国建筑第二工程局有限公司 | External wall anchoring type anti-seepage thermal insulation layer external thermal insulation system and construction method thereof |
| CN116285445A (en) * | 2023-04-28 | 2023-06-23 | 广东碧橙材料科技有限公司 | Anti-condensation inorganic silicate paint and preparation method thereof |
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