CN107890456A - A kind of eye cream and preparation method thereof - Google Patents

A kind of eye cream and preparation method thereof Download PDF

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Publication number
CN107890456A
CN107890456A CN201711169609.1A CN201711169609A CN107890456A CN 107890456 A CN107890456 A CN 107890456A CN 201711169609 A CN201711169609 A CN 201711169609A CN 107890456 A CN107890456 A CN 107890456A
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weight
parts
eye
dimethyl silicone
eye cream
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柳继成
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Shanghai He Xuan Brand Management Co Ltd
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Shanghai He Xuan Brand Management Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645Proteins of vegetable origin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/68Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin

Abstract

The invention discloses a kind of eye cream, the eye cream uses Wild soybean albumen, hydrolysed rice albumen and superoxide dismutase, for improving eye microcirculation and strengthening protection collagen and elastin matrix, plays prevention and reduces black-eyed effect;Silantriol, Sodium Hyaluronate are used for the elasticity for increasing skin, reduce wrinkle, hydrolyzed wheat protein, the compounding of these collagens of hydrolytic collagen and hydrolytic soya bean protein, the tight of epidermis lipid monofilm is kept, promotes the synthesis of collagen, so as to cooperate with anti-wrinkle effect;Acetyl group hexapeptide 8 has the effect of contraction for suppressing eye muscle, so as to reach the effect for mitigating wrinkle;Ceramide and tocopherol acetate, the moisture in skin can be pinned, repair skin barrier, skin care.The eye cream has the function that moisturizing, prevention and reduces eye livid ring around eye, pouch, desalination eye microgroove, also discloses the preparation method of eye cream, this method is simple, and the eye cream of production is stable.

Description

A kind of eye cream and preparation method thereof
Technical field
The invention belongs to cosmetic field, specifically, is related to a kind of eye cream and preparation method thereof.
Background technology
Eye skin is human body skin position the weakest.The thickness summation of eye epidermis and corium is just about 0.55mm, only skin of face 1/4 thickness, therefore be easier to be injured by the external world.Eye sub-surface porosity connective tissue is rich Rich, soft and high resilience, in the fibre structure of loose connective tissue, it is dispersed with extremely abundant capillary and nerve end The tip, the tube wall of these capillaries is very thin, and has certain permeability.Loose connective tissue is easy to congested, product Water and form hemotoncus or oedema.Eye is subcutaneously almost distributed without sebaceous glands or sweat gland, and the thin thin skin skin around eyes is non- Chang Rongyi is dry, lacks moisture.Because eye part skin lacks sebaceous glands and sweat gland, periocualr skin does not have natural moist ability, The grease that can be supplied wants much less relatively, result in eye part skin and is easy to aging.The skin sensitivity of circumference of eyes is fragile, micro- blood Pipe is extremely fine, it is easy to produces wrinkle, livid ring around eye, pouch.The live load weight of eye part skin, fatiguability, eyes are daily just Often work will blink 2.4-2.8 ten thousand times, and these actions make eye muscle and its skin of surrounding receive great pressure.
With the quickening of Modern Live rhythm, plus the gradual popularization of the pollution of living environment, and computer applications, lead Many eyes such as big pouch, livid ring around eye, crow's feet, fat granule caused by excess eye-using, such as sleep insufficiency occurs to people very much in cause Problem.
In addition as the increase at age, skin gradually follow the string, metabolic ability slowly weakens, and skin can be more next More aging, and wrinkle is the result of skin aging, is that skin lacks moisture, surface fat is reduced, the result of flexibility decrease.Eye Skin be human body part the most fragile, therefore, it is easier to produce wrinkle.The problem of for appearing above, people generally like It is joyous to select cosmetics to change.
Eye skin is very tender and lovely, and a variety of eye creams occurs in the market, although there is certain treatment on eye-care Effect, it is simply most of more chemical composition to be present, there is certain excitant to skin, also some eye cream nutritional ingredient mistakes Height, it is long-term use of easily to produce fat granule, prolong and bear new skin problem.
For these reasons, it is special to propose the present invention.
The content of the invention
In order to solve problem above existing for prior art, the invention provides a kind of eye cream, the eye cream has moisturizing taste Profit, prevention and the effect for reducing eye livid ring around eye, pouch, desalination eye microgroove.
The first object of the present invention provides a kind of eye cream, and described eye cream includes following component:Parleam, gather Dimethyl siloxane, Glyceryl stearate citrate, dimethiconol, methoxyl group PEG/PPG-25/4 poly dimethyls Siloxanes, silantriol, Sodium Hyaluronate, hydrolyzed wheat protein, hydrolytic collagen, hydrolytic soya bean protein, serine, arginine, Proline, ceramide, tocopherol acetate, Argireline, Pseudoalteromonas tunning extract, Wild soybean egg In vain, the hard ester alcohol of hydrolysed rice albumen, superoxide dismutase, glycerine, propane diols, ring five dimethyl silicone polymer, spermaceti, card ripple It is nurse, Chondrus crispus extract, caprylic/capric triglyceride, glycine betaine, trehalose, xanthans, allantoin, EDETATE SODIUM, right Hydroxy acetophenone, 1,2- hexylene glycols, vinyl dimethicone cross polymer, bisabolol, triethanolamine and essence.
The present invention uses Wild soybean albumen, hydrolysed rice albumen and superoxide dismutase, for improving eye microcirculation And strengthen protection collagen and elastin matrix, play prevention and reduce black-eyed effect.
Silantriol, Sodium Hyaluronate are used for the elasticity for increasing skin, the plentiful skin of consolidation, reduce wrinkle, and increase is protected, Hydrolyzed wheat protein, the compounding of these collagens of hydrolytic collagen and hydrolytic soya bean protein, forms moisturizing on a skin surface Property diaphragm, promoting epidermal cell epimatrix sticks together, and keeps the tight of epidermis lipid monofilm, improves cell egg White matter is horizontal, promotes the synthesis of collagen, so as to cooperate with anti-wrinkle effect.
Argireline has the effect of contraction for suppressing eye muscle, so as to reach the effect for mitigating wrinkle;Neural acyl Amine and tocopherol acetate, promote skin metabolism, prevent pigment deposition, improve skin elasticity, the water in skin can be pinned Point, repair skin barrier, skin care.
The eye cream of the present invention is a kind of translucent liquid.
Further, described eye cream includes according to parts by weight:Parleam 3-5 parts by weight, polydimethylsiloxanes Alkane 3-5 parts by weight, Glyceryl stearate citrate 0.2-0.5 parts by weight, dimethiconol 1-2 parts by weight, methoxy Base PEG/PPG-25/4 dimethyl silicone polymer 0.1-0.5 parts by weight, silantriol 3-5 parts by weight, Sodium Hyaluronate 0.1-0.2 Parts by weight, hydrolyzed wheat protein 0.5-1 parts by weight, hydrolytic collagen 0.5-1 parts by weight, hydrolytic soya bean protein 0.5-1 parts by weight, silk Propylhomoserin 0.5-1 parts by weight, arginine 0.5-1 parts by weight, proline 0.5-1 parts by weight, ceramide 0.5-1 parts by weight, fertility Phenol acetic acid esters 0.5-1 parts by weight, Argireline 1-3 parts by weight, Pseudoalteromonas tunning extract 1-2 weight Part, Wild soybean albumen 1-2 parts by weight, hydrolysed rice albumen 1-2 parts by weight, superoxide dismutase 1-2 parts by weight, glycerine 2-5 Parts by weight, propane diols 2-5 parts by weight, ring five dimethyl silicone polymer 3-5 parts by weight, the hard ester alcohol 0.5-1 parts by weight of spermaceti, card ripple Nurse 0.1-0.5 parts by weight, Chondrus crispus extract 8-10 parts by weight, caprylic/capric triglyceride 3-5 parts by weight, glycine betaine 0.5-1 parts by weight, trehalose 0.5-1 parts by weight, xanthans 0.05-1 parts by weight, allantoin 0.1-0.2 parts by weight, EDETATE SODIUM 0.01-0.05 parts by weight, parahydroxyacet-ophenone 0.04-0.08 parts by weight, 1,2- hexylene glycol 0.04-0.06 parts by weight, vinyl Dimethicone Crosspolymer 0.05-0.08 parts by weight, bisabolol 0.01-0.03 parts by weight, triethanolamine 0.1- 0.2 parts by weight and essence 0.01-0.05 parts by weight.
Further, described eye cream includes according to parts by weight:The parts by weight of Parleam 4, dimethyl silicone polymer 4 Parts by weight, the parts by weight of Glyceryl stearate citrate 0.3, the parts by weight of dimethiconol 1.5, methoxyl group PEG/PPG- The parts by weight of 25/4 dimethyl silicone polymer 0.3, the parts by weight of silantriol 4, the parts by weight of Sodium Hyaluronate 0.15, hydrolyzed wheat protein 0.8 parts by weight, the parts by weight of hydrolytic collagen 0.8, the parts by weight of hydrolytic soya bean protein 0.8, the parts by weight of serine 0.8, the weight of arginine 0.8 Measure part, the parts by weight of proline 0.8, the parts by weight of ceramide 0.8, the parts by weight of tocopherol acetate 0.8, the weight of Argireline 2 Measure part, the parts by weight of Pseudoalteromonas tunning extract 1.5, the parts by weight of Wild soybean albumen 1.5, hydrolysed rice albumen 1.5 Parts by weight, the parts by weight of superoxide dismutase 1.5, the parts by weight of glycerine 3.5, the parts by weight of propane diols 3.5, the polydimethylsiloxanes of ring five The hard parts by weight of ester alcohol 0.8 of the parts by weight of alkane 4, spermaceti, the parts by weight of carbomer 0.3, the parts by weight of Chondrus crispus extract 9, the octanoic acid/last of the ten Heavenly stems The parts by weight of acid glycerol three ester 4, the parts by weight of glycine betaine 0.75, the parts by weight of trehalose 0.75, the parts by weight of xanthans 0.75, allantoin 0.15 parts by weight, the parts by weight of EDETATE SODIUM 0.03, the parts by weight of parahydroxyacet-ophenone 0.06, the parts by weight of 1,2- hexylene glycols 0.06, second The parts by weight of alkenyl Dimethicone Crosspolymer 0.065, the parts by weight of bisabolol 0.02, the parts by weight of triethanolamine 0.15 With the parts by weight of essence 0.03.
The second object of the present invention, there is provided a kind of preparation method of eye cream recited above, comprise the following steps:
(1) weight weighing according to described each component is standby;
(2) water is thrown in aqueous phase pot, the glycerine weighed, propane diols, glycine betaine, Huang is separately added under heating stirring Virgin rubber, carbomer, allantoin, trehalose, Sodium Hyaluronate and EDETATE SODIUM, it is stand-by as aqueous phase;
(3) temperature is sweet by the cetostearyl alcohol weighed, Parleam, caprylic/capric respectively at 80-85 DEG C Oily three esters, Glyceryl stearate citrate, ring five dimethyl silicone polymer, dimethyl silicone polymer, dimethyl silicone polymer Alcohol, methoxyl group PEG/PPG-25/4 dimethyl silicone polymers and vinyl dimethicone cross polymer add oil phase pot In, it is mixed evenly, it is stand-by as oil phase;
(4) will be pumped under oil phase vacuum in aqueous phase, stirring, homogeneous, insulation emulsification, cooling down;
(5) hydroxy acetophenone, 1,2- hexylene glycols, the essence weighed is added into the solution after cooling, cooling, is added wild Soybean protein, hydrolysed rice albumen, superoxide dismutase, silantriol, serine, arginine, proline, Chondrus crispus Extract, Argireline, ceramide, tocopherol acetate, hydrolyzed wheat protein, hydrolytic collagen, hydrolytic soya bean protein, Glycine betaine, Pseudoalteromonas tunning extract solution, bisabolol and triethanolamine, stir, and obtain described eye cream.
Further, heating-up temperature is 80-85 DEG C in step (2).
Further, step (2) reclaimed water is 40-45 parts by weight.
Further, stir speed (S.S.) is 3200-3500rpm in step (4).
Further, homogenizing time is 3-5 minutes in step (4).
Further, insulation emulsifying temperature is 80-85 DEG C in step (4), and emulsification times are 15-20 minutes.
Further, the temperature of step (4) cooling down is less than 45 DEG C.
Further, the cooling in step (5) is that temperature is less than 40 DEG C.
Further, the stir speed (S.S.) in step (2) and (3) is 45-50rpm.
The eye cream preparation method of the present invention is simple, consumes few, the eye cream stable performance of production to production equipment, to skin without Stimulation.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) eye cream of the invention can be obviously improved pouch and livid ring around eye, and can substantially mitigate the wrinkle of eye;
(2) active material in eye cream of the invention is stable, non-stimulated to skin, securely and reliably;
(3) eye cream of the invention also has the effect of moisturizing.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below Detailed description.Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Base Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned Other embodiment, belong to the scope that the present invention is protected.
Embodiment 1
The eye cream of the present embodiment includes:Parleam 3g, dimethyl silicone polymer 3g, stearine lemon Acid esters 0.2g, dimethiconol 1g, methoxyl group PEG/PPG-25/4 dimethyl silicone polymers 0.1g, silantriol 3g, Sodium Hyaluronate 0.1g, hydrolyzed wheat protein 0.5g, hydrolytic collagen 0.5g, hydrolytic soya bean protein 0.5g, serine 0.5g, smart ammonia Sour 0.5g, proline 0.5g, ceramide 0.5g, tocopherol acetate 0.5g, Argireline 1g, Pseudoalteromonas Tunning extract 1g, Wild soybean albumen 1g, hydrolysed rice albumen 1g, superoxide dismutase 1g, glycerine 2g, propane diols The hard ester alcohol 0.5g of 2g, ring five dimethyl silicone polymer 3g, spermaceti, carbomer 0.1g, Chondrus crispus extract 8g, the octanoic acid/last of the ten Heavenly stems Acid glycerol three ester 3g, glycine betaine 0.5g, trehalose 0.5g, xanthans 0.05g, allantoin 0.1g, EDETATE SODIUM 0.01g, to hydroxyl Benzoylformaldoxime 0.04g, 1,2- hexylene glycol 0.04-g, vinyl dimethicone cross polymer 0.05g, bisabolol 0.01g, triethanolamine 0.1g and essence 0.01g.
The eye cream preparation method of the present embodiment comprises the following steps:
(1) weight weighing according to described each component is standby;
(2) 40g water is thrown in aqueous phase pot, be separately added under the stirring of 80 DEG C of temperature the glycerine weighed, propane diols, Glycine betaine, xanthans, carbomer, allantoin, trehalose, Sodium Hyaluronate and EDETATE SODIUM, it is stand-by as aqueous phase;
(3) temperature is at 80 DEG C, respectively by the cetostearyl alcohol weighed, Parleam, caprylic/capric glycerine three Ester, Glyceryl stearate citrate, ring five dimethyl silicone polymer, dimethyl silicone polymer, dimethiconol, first Epoxide PEG/PPG-25/4 dimethyl silicone polymers and vinyl dimethicone cross polymer are added in oil phase pot, are mixed Conjunction stirs, stand-by as oil phase;
(4) it will be pumped under oil phase vacuum in aqueous phase, stirring, stir speed (S.S.) 3200rpm, homogeneous 3 minutes, be incubated 80 DEG C, Emulsification 15 minutes, cools to 44 DEG C;
(5) hydroxy acetophenone, 1,2- hexylene glycols, the essence weighed is added into the solution after cooling, cools to 39 DEG C, Add Wild soybean albumen, hydrolysed rice albumen, superoxide dismutase, silantriol, serine, arginine, proline, ripple Chondrus extract, Argireline, ceramide, tocopherol acetate, hydrolyzed wheat protein, hydrolytic collagen, hydrolysis are big Legumin, glycine betaine, Pseudoalteromonas tunning extract solution, bisabolol and triethanolamine, stir, and obtain described Eye cream.
Embodiment 2
The eye cream of the present embodiment includes:Parleam 4g, dimethyl silicone polymer 4g, stearine citric acid Ester 0.3g, dimethiconol 1.5g, methoxyl group PEG/PPG-25/4 dimethyl silicone polymers 0.3g, silantriol 4g, Sodium Hyaluronate 0.15g, hydrolyzed wheat protein 0.8g, hydrolytic collagen 0.8g, hydrolytic soya bean protein 0.8g, serine 0.8g, essence Propylhomoserin 0.8g, proline 0.8g, ceramide 0.8g, tocopherol acetate 0.8g, Argireline 2g, false Alteromonas Bacterium tunning extract 1.5g, Wild soybean albumen 1.5g, hydrolysed rice albumen 1.5g, superoxide dismutase 1.5g, glycerine The hard ester alcohol 0.8g of 3.5g, propane diols 3.5g, ring five dimethyl silicone polymer 4g, spermaceti, carbomer 0.3g, Chondrus crispus extraction Thing 9g, caprylic/capric triglyceride 4g, glycine betaine 0.75g, trehalose 0.75g, xanthans 0.75g, allantoin 0.15g, EDTA Disodium 0.03g, parahydroxyacet-ophenone 0.06g, 1,2- hexylene glycol 0.06g, vinyl dimethicone cross polymer 0.065g, bisabolol 0.02g, triethanolamine 0.15g and essence 0.03g.
The eye cream preparation method of the present embodiment comprises the following steps:
(1) weight weighing according to described each component is standby;
(2) 43g water is thrown in aqueous phase pot, be separately added under the stirring of 83 DEG C of temperature the glycerine weighed, propane diols, Glycine betaine, xanthans, carbomer, allantoin, trehalose, Sodium Hyaluronate and EDETATE SODIUM, it is stand-by as aqueous phase;
(3) temperature is at 83 DEG C, respectively by the cetostearyl alcohol weighed, Parleam, caprylic/capric glycerine three Ester, Glyceryl stearate citrate, ring five dimethyl silicone polymer, dimethyl silicone polymer, dimethiconol, first Epoxide PEG/PPG-25/4 dimethyl silicone polymers and vinyl dimethicone cross polymer are added in oil phase pot, are mixed Conjunction stirs, stand-by as oil phase;
(4) it will be pumped under oil phase vacuum in aqueous phase, stirring, stir speed (S.S.) 3300rpm, homogeneous 4 minutes, be incubated 83 DEG C Under, emulsify 18 minutes, cool to 42 DEG C;
(5) hydroxy acetophenone, 1,2- hexylene glycols, the essence weighed is added into the solution after cooling, cools to 35 DEG C, Add Wild soybean albumen, hydrolysed rice albumen, superoxide dismutase, silantriol, serine, arginine, proline, ripple Chondrus extract, Argireline, ceramide, tocopherol acetate, hydrolyzed wheat protein, hydrolytic collagen, hydrolysis are big Legumin, glycine betaine, Pseudoalteromonas tunning extract solution, bisabolol and triethanolamine, stir, and obtain described Eye cream.
Embodiment 3
The eye cream of this implementation includes:Parleam 5g, dimethyl silicone polymer 5g, Glyceryl stearate citrate It is 0.5g, dimethiconol 2g, methoxyl group PEG/PPG-25/4 dimethyl silicone polymers 0.5g, silantriol 5g, transparent Matter acid sodium 0.2g, hydrolyzed wheat protein 1g, hydrolytic collagen 1g, hydrolytic soya bean protein 1g, serine 1g, arginine 1g, proline 1g, Cer EOS g, tocopherol acetate 1g, Argireline 3g, Pseudoalteromonas tunning extract 2g, open country Soybean protein 2g, hydrolysed rice albumen 2g, superoxide dismutase 2g, glycerine 5g, propane diols 5g, ring five dimethyl silicone polymer The hard ester alcohol 1g of 5g, spermaceti, carbomer 0.5g, Chondrus crispus extract 10g, caprylic/capric triglyceride 5g, glycine betaine 1g, Trehalose 1g, xanthans 1g, allantoin 0.2g, EDETATE SODIUM 0.05g, parahydroxyacet-ophenone 0.08g, 1,2- hexylene glycol 0.06g, Vinyl dimethicone cross polymer 0.08g, bisabolol 0.03g, triethanolamine 0.2g and essence 0.05g.
The eye cream preparation method of the present embodiment comprises the following steps:
(1) weight weighing according to described each component is standby;
(2) 45g water is thrown in aqueous phase pot, be separately added under the stirring of 85 DEG C of temperature the glycerine weighed, propane diols, Glycine betaine, xanthans, carbomer, allantoin, trehalose, Sodium Hyaluronate and EDETATE SODIUM, it is stand-by as aqueous phase;
(3) temperature is at 85 DEG C, respectively by the cetostearyl alcohol weighed, Parleam, caprylic/capric glycerine three Ester, Glyceryl stearate citrate, ring five dimethyl silicone polymer, dimethyl silicone polymer, dimethiconol, first Epoxide PEG/PPG-25/4 dimethyl silicone polymers and vinyl dimethicone cross polymer are added in oil phase pot, are mixed Conjunction stirs, stand-by as oil phase;
(4) it will be pumped under oil phase vacuum in aqueous phase, stirring, stir speed (S.S.) 3500rpm, homogeneous 5 minutes, be incubated 85 DEG C Under, emulsify 20 minutes, cool to 40 DEG C;
(5) hydroxy acetophenone, 1,2- hexylene glycols, the essence weighed is added into the solution after cooling, cools to 32 DEG C, Add Wild soybean albumen, hydrolysed rice albumen, superoxide dismutase, silantriol, serine, arginine, proline, ripple Chondrus extract, Argireline, ceramide, tocopherol acetate, hydrolyzed wheat protein, hydrolytic collagen, hydrolysis are big Legumin, glycine betaine, Pseudoalteromonas tunning extract solution, bisabolol and triethanolamine, stir, and obtain described Eye cream.
Test example 1
Test specimen 1-3 is respectively eye cream prepared by embodiment 1-3;
Control sample 1:Wild soybean albumen, hydrolysed rice albumen, superoxide dismutase, other groups are not added in eye cream component Divide and preparation method is same as Example 1;
Control sample 2:Do not add hydrolyzed wheat protein, hydrolytic collagen and hydrolyzed soy in eye cream component, other components and Preparation method is same as Example 1;
Control sample 3:It is identical with control sample 2, difference, add wheat gluten.
(1) mouse skin irritant test:
Test method:With reference to (cosmetics health specification) 2007 Ministry of Public Health's legal system and supervision department;
Experimental animal:Small white mouse;
Result of the test:7 days Skin Irritation Tests, sent out using the non-stimulate the reaction of the eye cream of test specimen and control sample It is raw.
(2) crease-resistant experiment
Tested using the test specimen 1-3 and control sample 1-4 eye creams prepared;
The tested people of crowd 120,18-50 year, each 60 people of men and women, skin health, without allergic history, 6 groups are randomly divided into, often 20 people of group.
Method of testing:Using German CK companies manufacture skin elasticity tester MPA580, test eye circumference elasticity of skin with Water content, everyone tests a kind of data, removes maximum and minimum value in each group, and residue is averaged, respectively using experiment Sample 1-3 and control sample 1-3 eye cream tests eye circumference skin skin elasticity index R2, R5, R7 after 2 weeks and 4 weeks, wherein R2, R5, R7 are closer to 1, and skin elasticity is better, R2=Ua/Uf;R5=Ur/Ue;R7=Ur/Uf, it the results are shown in Table 1.
Wherein, Uf --- skin maximum tension amount;
Ue --- after constant negative pressure is added on skin, the amount of tension of skin, positioning elastic part amount of tension at 0.1 second; Ur --- after cancelling negative pressure, skin will restore to the original state rapidly state, equally be divided into elastic portion score value Ur, that is, cancel negative pressure 0.1 second Afterwards, the recovery value of skin and visco-elastic portions value, or plastic value;
Ua --- from cancellation negative pressure to the recovery value of skin when follow-on test skin surface adds negative pressure again next time.
Table 1
As it can be seen from table 1 test specimen 1-3 and control sample 1, using after 4 weeks, R2, R5 and R7 substantially increase, and It is intended to 1, it can thus be appreciated that skin elasticity is greatly improved, wrinkle, control sample 2 and control sample 3 can be significantly reduced In not add hydrolyzed wheat protein, hydrolytic collagen, hydrolyzed soy or addition a kind of, it will be apparent that R2, R5 and R7 increase are less, can be with Illustrating the eye cream of the present invention has preferable anti-wrinkle effect.
(3) livid ring around eye, pouch experiment
The eye conditions after each group uses 4 weeks are observed respectively, the results are shown in Table 2.
Table 2
As can be seen from the table, test specimen 1-3 and control sample 2 and 3 are with preferably removal livid ring around eye and pouch Effect, illustrate that Wild soybean albumen, hydrolysed rice albumen, superoxide dismutase have the function that to remove livid ring around eye and pouch.
The foregoing is only a specific embodiment of the invention, but protection scope of the present invention is not limited thereto, any Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all be contained Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.

Claims (10)

1. a kind of eye cream, it is characterised in that described eye cream includes following component:Parleam, dimethyl silicone polymer, Glyceryl stearate citrate, dimethiconol, methoxyl group PEG/PPG-25/4 dimethyl silicone polymers, silane three Alcohol, Sodium Hyaluronate, hydrolyzed wheat protein, hydrolytic collagen, hydrolytic soya bean protein, serine, arginine, proline, neural acyl Amine, tocopherol acetate, Argireline, Pseudoalteromonas tunning extract, Wild soybean albumen, hydrolysed rice egg In vain, the hard ester alcohol of superoxide dismutase, glycerine, propane diols, ring five dimethyl silicone polymer, spermaceti, carbomer, Chondrus crispus Extract, caprylic/capric triglyceride, glycine betaine, trehalose, xanthans, allantoin, EDETATE SODIUM, parahydroxyacet-ophenone, 1, 2- hexylene glycols, vinyl dimethicone cross polymer, bisabolol, triethanolamine and essence.
2. a kind of eye cream according to claim 1, it is characterised in that described eye cream includes according to parts by weight:Hydrogenation is poly- It is isobutene 3-5 parts by weight, dimethyl silicone polymer 3-5 parts by weight, Glyceryl stearate citrate 0.2-0.5 parts by weight, poly- Dimethyl silica alkanol 1-2 parts by weight, methoxyl group PEG/PPG-25/4 dimethyl silicone polymer 0.1-0.5 parts by weight, silane three Alcohol 3-5 parts by weight, Sodium Hyaluronate 0.1-0.2 parts by weight, hydrolyzed wheat protein 0.5-1 parts by weight, hydrolytic collagen 0.5-1 weight Part, hydrolytic soya bean protein 0.5-1 parts by weight, serine 0.5-1 parts by weight, arginine 0.5-1 parts by weight, proline 0.5-1 weight Measure part, ceramide 0.5-1 parts by weight, tocopherol acetate 0.5-1 parts by weight, Argireline 1-3 parts by weight, false friendship For monad tunning extract 1-2 parts by weight, Wild soybean albumen 1-2 parts by weight, hydrolysed rice albumen 1-2 parts by weight, super Superoxide dismutase 1-2 parts by weight, glycerine 2-5 parts by weight, propane diols 2-5 parts by weight, ring five dimethyl silicone polymer 3-5 weight Part, the hard ester alcohol 0.5-1 parts by weight of spermaceti, carbomer 0.1-0.5 parts by weight, Chondrus crispus extract 8-10 parts by weight, octanoic acid/ Triglyceride DDD 3-5 parts by weight, glycine betaine 0.5-1 parts by weight, trehalose 0.5-1 parts by weight, xanthans 0.05-1 parts by weight, Allantoin 0.1-0.2 parts by weight, EDETATE SODIUM 0.01-0.05 parts by weight, parahydroxyacet-ophenone 0.04-0.08 parts by weight, 1,2- Hexylene glycol 0.04-0.06 parts by weight, vinyl dimethicone cross polymer 0.05-0.08 parts by weight, bisabolol 0.01-0.03 parts by weight, triethanolamine 0.1-0.2 parts by weight and essence 0.01-0.05 parts by weight.
3. a kind of eye cream according to claim 2, it is characterised in that described eye cream includes according to parts by weight:Hydrogenation is poly- The parts by weight of isobutene 4, the parts by weight of dimethyl silicone polymer 4, the parts by weight of Glyceryl stearate citrate 0.3, poly dimethyl silicon The parts by weight of oxygen alkanol 1.5, the parts by weight of methoxyl group PEG/PPG-25/4 dimethyl silicone polymers 0.3, the parts by weight of silantriol 4, thoroughly The bright parts by weight of matter acid sodium 0.15, the parts by weight of hydrolyzed wheat protein 0.8, the parts by weight of hydrolytic collagen 0.8, the weight of hydrolytic soya bean protein 0.8 Measure part, the parts by weight of serine 0.8, the parts by weight of arginine 0.8, the parts by weight of proline 0.8, the parts by weight of ceramide 0.8, tocopherol The parts by weight of acetic acid esters 0.8, the parts by weight of Argireline 2, the parts by weight of Pseudoalteromonas tunning extract 1.5, open country are big The parts by weight of legumin 1.5, the parts by weight of hydrolysed rice albumen 1.5, the parts by weight of superoxide dismutase 1.5, the parts by weight of glycerine 3.5, The parts by weight of propane diols 3.5, the parts by weight of ring five dimethyl silicone polymer 4, the hard parts by weight of ester alcohol 0.8 of spermaceti, the weight of carbomer 0.3 Part, the parts by weight of Chondrus crispus extract 9, the parts by weight of caprylic/capric triglyceride 4, the parts by weight of glycine betaine 0.75, trehalose 0.75 parts by weight, the parts by weight of xanthans 0.75, the parts by weight of allantoin 0.15, the parts by weight of EDETATE SODIUM 0.03, parahydroxyacet-ophenone It is 0.06 parts by weight, the parts by weight of 1,2- hexylene glycols 0.06, the parts by weight of vinyl dimethicone cross polymer 0.065, red The parts by weight of bisabol 0.02, the parts by weight of triethanolamine 0.15 and the parts by weight of essence 0.03.
A kind of 4. preparation method of the eye cream described in claim 1-3 any one, it is characterised in that described preparation method bag Include following steps:
(1) weight weighing according to described each component is standby;
(2) water is thrown in aqueous phase pot, the glycerine weighed, propane diols, glycine betaine, xanthan is separately added under heating stirring Glue, carbomer, allantoin, trehalose, Sodium Hyaluronate and EDETATE SODIUM, it is stand-by as aqueous phase;
(3) temperature is at 80-85 DEG C, respectively by the cetostearyl alcohol weighed, Parleam, caprylic/capric glycerine three Ester, Glyceryl stearate citrate, ring five dimethyl silicone polymer, dimethyl silicone polymer, dimethiconol, first Epoxide PEG/PPG-25/4 dimethyl silicone polymers and vinyl dimethicone cross polymer are added in oil phase pot, are mixed Conjunction stirs, stand-by as oil phase;
(4) will be pumped under oil phase vacuum in aqueous phase, stirring, homogeneous, insulation emulsification, cooling down;
(5) hydroxy acetophenone, 1,2- hexylene glycols, the essence weighed is added into the solution after cooling, cooling, adds Wild soybean Albumen, hydrolysed rice albumen, superoxide dismutase, silantriol, serine, arginine, proline, Chondrus crispus extraction Thing, Argireline, ceramide, tocopherol acetate, hydrolyzed wheat protein, hydrolytic collagen, hydrolytic soya bean protein, beet Alkali, Pseudoalteromonas tunning extract solution, bisabolol and triethanolamine, stir, and obtain described eye cream.
5. preparation method according to claim 4, it is characterised in that heating-up temperature is 80-85 DEG C in step (2).
6. preparation method according to claim 4, it is characterised in that step (2) reclaimed water is 40-45 parts by weight.
7. preparation method according to claim 4, it is characterised in that homogenizing time is 3-5 minutes in step (4).
8. preparation method according to claim 4, it is characterised in that insulation emulsifying temperature is 80-85 DEG C in step (4), Emulsification times are 15-20 minutes.
9. preparation method according to claim 4, it is characterised in that the temperature of step (4) cooling down is less than 45 DEG C.
10. preparation method according to claim 4, it is characterised in that the cooling in step (5) is less than 40 DEG C for temperature.
CN201711169609.1A 2017-11-21 2017-11-21 A kind of eye cream and preparation method thereof Pending CN107890456A (en)

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CN108635272A (en) * 2018-07-06 2018-10-12 广州英桐生物科技有限公司 A kind of anti-age corrective eye treatment cream and preparation method thereof
CN108853000A (en) * 2018-08-17 2018-11-23 广州皓雨投资有限公司 Have effects that moisture-keeping crease-shedding restores the composition of elasticity of skin, facial mask and preparation method thereof
CN108969398A (en) * 2018-08-10 2018-12-11 江西登云健康美业互联有限公司 A kind of Essence and preparation method thereof
CN109602654A (en) * 2018-12-25 2019-04-12 广州葆妍生物科技有限公司 A kind of composition and its preparation method and application with eye-care function
CN110115699A (en) * 2019-04-16 2019-08-13 上海悦目化妆品有限公司 A kind of eye essence and preparation method thereof
CN110403845A (en) * 2019-09-11 2019-11-05 杨立敏 A kind of face cream and skin care item suit
CN111281830A (en) * 2020-02-26 2020-06-16 伊诗芮丝生物科技(上海)有限公司 Preparation process and formula of repair eye cream
CN111631995A (en) * 2020-06-10 2020-09-08 广东柏俐臣生物科技有限公司 Multiplex eye cream and preparation method thereof
CN112641717A (en) * 2021-02-05 2021-04-13 东晟源研究院(广州)有限公司 Eye-protecting cream with upper eyelid and lower eyelid for zone nursing
CN113069393A (en) * 2020-01-06 2021-07-06 广州樱奈儿化妆品有限公司 Eye cream and preparation method thereof
CN114569490A (en) * 2022-03-14 2022-06-03 广州市百好博有限公司 Composition with effects of moisturizing, repairing skin barrier, resisting wrinkles and tightening skin, preparation method and application thereof
CN115844745A (en) * 2022-12-29 2023-03-28 广州旭妆生物科技有限公司 Anti-wrinkle composition, application thereof and cosmetic
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CN108635272B (en) * 2018-07-06 2021-03-30 广州英桐生物科技有限公司 Repairing eye cream and preparation method thereof
CN108635272A (en) * 2018-07-06 2018-10-12 广州英桐生物科技有限公司 A kind of anti-age corrective eye treatment cream and preparation method thereof
CN108969398A (en) * 2018-08-10 2018-12-11 江西登云健康美业互联有限公司 A kind of Essence and preparation method thereof
CN108969398B (en) * 2018-08-10 2021-04-09 江西登云健康美业互联有限公司 Essence and preparation method thereof
CN108853000A (en) * 2018-08-17 2018-11-23 广州皓雨投资有限公司 Have effects that moisture-keeping crease-shedding restores the composition of elasticity of skin, facial mask and preparation method thereof
CN109602654A (en) * 2018-12-25 2019-04-12 广州葆妍生物科技有限公司 A kind of composition and its preparation method and application with eye-care function
CN110115699A (en) * 2019-04-16 2019-08-13 上海悦目化妆品有限公司 A kind of eye essence and preparation method thereof
CN110403845A (en) * 2019-09-11 2019-11-05 杨立敏 A kind of face cream and skin care item suit
CN113069393A (en) * 2020-01-06 2021-07-06 广州樱奈儿化妆品有限公司 Eye cream and preparation method thereof
CN111281830A (en) * 2020-02-26 2020-06-16 伊诗芮丝生物科技(上海)有限公司 Preparation process and formula of repair eye cream
CN111631995A (en) * 2020-06-10 2020-09-08 广东柏俐臣生物科技有限公司 Multiplex eye cream and preparation method thereof
CN112641717A (en) * 2021-02-05 2021-04-13 东晟源研究院(广州)有限公司 Eye-protecting cream with upper eyelid and lower eyelid for zone nursing
CN114569490A (en) * 2022-03-14 2022-06-03 广州市百好博有限公司 Composition with effects of moisturizing, repairing skin barrier, resisting wrinkles and tightening skin, preparation method and application thereof
CN114569490B (en) * 2022-03-14 2022-12-30 广州市百好博有限公司 Composition with effects of moisturizing, repairing skin barrier, resisting wrinkles and tightening skin, preparation method and application thereof
CN115844745A (en) * 2022-12-29 2023-03-28 广州旭妆生物科技有限公司 Anti-wrinkle composition, application thereof and cosmetic
CN115844745B (en) * 2022-12-29 2024-05-14 广州旭妆生物科技有限公司 Anti-wrinkle composition, application thereof and cosmetics

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Application publication date: 20180410