CN107880301A - 一种防紫外线高密度折叠遮阳篷面料的制备方法 - Google Patents
一种防紫外线高密度折叠遮阳篷面料的制备方法 Download PDFInfo
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Abstract
本发明公开了一种防紫外线高密度折叠遮阳篷面料的制备方法,首先制备作为基层的布料层,取用原材料进行混纺得到纱线并通过机器制成布料层备用;然后按照质量分数计取用甲基丙烯酸甲酯、单宁酸、苯胺蓝和丙烯酸‑2‑乙基己酯作为涂料层原料,先将丙烯酸‑2‑乙基己酯按照质量分数比例倒入甲基丙烯酸甲酯中进行加热搅拌10‑20min,然后再向其混合液中加入单宁酸和苯胺蓝并持续搅拌20‑25min即得到涂料;取用薄膜层原材料进行造粒形成改性PVDF颗粒备用;然后将涂料均匀的涂覆在布料层一侧,待其稳定形成涂料层后,将准备好的PVDF颗粒加热并均匀的涂覆在涂料层上并将涂料层完全覆盖;本发明通过设有四层结构且通过在涂料层上设有的薄膜层能够防止涂料在长期使用后磨损较多。
Description
技术领域
本发明涉及布料领域,具体是指一种防紫外线高密度折叠遮阳篷面料的制备方法。
背景技术
遮阳篷具有全面的外遮阳功能,能够彻底阻挡紫外线的辐射,降低室内温度,减少空调负荷;遮阳篷具有节能效果,遮阳篷,从节省能源以及环境保护角度考虑,意义非常重大;遮阳篷,在遮挡炎炎夏日的同时,能够使强烈的阳光以漫射光的形式反射入室内,使室内光线明亮而不眩目,并且不影响从室内看出的窗外景观,将人们的生活空间从室内延伸到室外,创造出了新的居住空间;遮阳篷其遮阳布所具有的特殊防紫外线功能,不仅使人体皮肤免受紫外线的侵袭,而且大大延长了室内装修和家具的使用寿命,遮阳篷有着丰富多彩的遮布花型、颜色,用户可根据需要选择。阻挡高达90%-100%太阳紫外线。所述的遮阳篷面料在水汽的状态下,水颗粒非常细小,根据毛细运动的原理,可以顺利渗透到毛细管到另一侧,从而发生透汽现象。当水汽冷凝变成水珠后,颗粒变大,由于水珠表面张力的作用(水分子之间互相“拉扯抗衡”),水分子就不能顺利脱离水珠渗透到另一侧,也就是防止了水的渗透发生,使透汽膜有了防水的功能。
现有的户外遮阳篷面料通常具备一定的防水效果,但是其材质较为轻薄,导致其结构强度较低,在长期的户外活动中会造成衣物表面出现破损的问题,而且采用多层面料的户外衣物着色单一,为了满足功能性需求从而导致其表面无法附着较为立体的涂料层结构。
发明内容
针对上述现有技术中防水效果较差的问题,本发明的目的在于提供一种通过合理设置达到较高强度且还通过多层材料将涂料层保护起来从而提高防水效果的衣物面料布料的制备方法。
本发明通过下述技术方案实现:一种防紫外线高密度折叠遮阳篷面料的制备方法,具体步骤如下:
A1.首先制备作为基层的布料层,按照质量分数计取用50-75%的聚2,6-萘二甲酸乙二酯纤维、20-40%的聚二正戊基醚纤维和20-35%的聚丁二酸丁二酯纤维作为原材料进行混纺得到纱线并通过机器制成布料层备用;
A2.然后按照质量分数计取用甲基丙烯酸甲酯40-60%、单宁酸15-25%、苯胺蓝10-15%和丙烯酸-2-乙基己酯10-20%作为涂料层原料,先将丙烯酸-2-乙基己酯按照质量分数比例倒入甲基丙烯酸甲酯中进行加热搅拌10-20min,然后再向其混合液中加入单宁酸和苯胺蓝并持续搅拌20-25min即得到涂料;
A3.按照质量分数计取用PVDF40-60%、氯化聚乙烯30-40%和多乙烯多胺20-35%作为薄膜层原材料进行造粒形成改性PVDF颗粒备用;
A4.然后将涂料均匀的涂覆在布料层一侧,待其稳定形成涂料层后,将准备好的PVDF颗粒加热并均匀的涂覆在涂料层上并将涂料层完全覆盖;
A5.再以质量分数计选取氯化聚乙烯橡胶45-85%、丙酮8-16%和石蜡20-30%作为压胶层的原材料进行熔融共聚得到改性氯化聚乙烯橡胶并通过烫金工艺贴合在布料层设有涂料层相对一侧面上形成压胶层,从而得到衣物面料。
进一步地,所述步骤A1中混纺成纱为40-60支,并将得到的混纺纱按照90*50的纱织密度进行纺织成布料层。
进一步地,所述步骤A2中具体在123-156℃的条件下进行甲基丙烯酸甲酯的加热搅拌过程。
进一步地,所述步骤A3中中造粒挤出温度范围为110-156℃;造粒挤出机前端温度为110-115℃,中端温度150-156℃,后端为135-138℃。
进一步地,所述步骤A5中的烫金工艺为塑料冷烫金工艺。
冷烫金技术是近年来欧美印刷行业中的高科技成果。它打破了传统烫金依靠热压转移电化铝箔的传统工艺,而使用一种全新的的概念——冷压技术来转移电化箔。冷烫金技术不仅解决了许多印刷行业过去难以解决的工艺问题,而且更重要的是节约了能源,并避免了制作金属印版过程中对环境产生的污染。将冷烫金技术用于在窄幅轮转印刷机上印刷不干胶材料时,只需在原有设备上附加一些装置即可。以下介绍了冷烫金的工艺流程原理及其附加设备等情况。
本发明与现有技术相比,具有以下优点及有益效果:
本发明的方法通过合理控制各反应物之间的配比,合理控制反应条件而制备出一种适高强度且具有较好防水效果的衣物面料,本发明的防水基层为表面覆盖的薄膜层和内部的压胶层得到的固化物,耐湿性优异,并且抗冲击性等机械特性也优异的性能,粘接性能好,耐久性能好,且制备方法简单易行,适合工业化生产力。
具体实施方式
下面详细描述本发明的实施例。
实施例1:
本实施例的一种防紫外线高密度折叠遮阳篷面料,以布料层为基层,并在布料层一侧设有用来增加观感的涂料层,并在涂料层上覆盖有用来保持涂料层长期使用稳定附着在布料层上的薄膜层;在布料层另一侧设有采用烫金工艺贴合在布料层表面的压胶层,其中每层材料的具体配方如下:布料层:包括以质量分数计的聚2,6-萘二甲酸乙二酯纤维45-75%、聚二正戊基醚纤维15-45%和聚丁二酸丁二酯纤维35-45%;涂料层:包括以质量分数计的甲基丙烯酸甲酯35-62%、单宁酸14-24%、苯胺蓝11-13%和丙烯酸-2-乙基己酯14-25%;薄膜层:包括以质量分数计的PVDF50-70%、氯化聚乙烯20-30%和多乙烯多胺20-35%;压胶层:包括以质量分数计的氯化聚乙烯橡胶55-80%、丙酮8-16%和石蜡25-35%。
本发明的制备方法,具体步骤为:
(1)布料层的制备:首先制备作为基层的布料层,按照质量分数计取用的聚2,6-萘二甲酸乙二酯纤维、聚二正戊基醚纤维和聚丁二酸丁二酯纤维作为原材料进行混纺得到纱线并通过机器制成布料层备用;其中混纺成纱为40-60支,并将得到的混纺纱按照90*50的纱织密度进行纺织成布料层。
(2)然后按照质量分数计取用甲基丙烯酸甲酯、单宁酸、苯胺蓝10-15%和丙烯酸-2-乙基己酯作为涂料层原料,先将丙烯酸-2-乙基己酯按照质量分数比例倒入甲基丙烯酸甲酯中进行加热搅拌10-20min,然后再向其混合液中加入单宁酸和苯胺蓝并持续搅拌20-25min即得到涂料;其中具体在123-156℃的条件下进行甲基丙烯酸甲酯的加热搅拌过程。
(3)按照质量分数计取用PVDF、氯化聚乙烯和多乙烯多胺作为薄膜层原材料进行造粒形成改性PVDF颗粒备用;其中造粒挤出温度范围为110-156℃;造粒挤出机前端温度为110-115℃,中端温度150-156℃,后端为135-138℃。
(4)然后将涂料均匀的涂覆在布料层一侧,待其稳定形成涂料层后,将准备好的PVDF颗粒加热并均匀的涂覆在涂料层上并将涂料层完全覆盖;
(5)再以质量分数计选取氯化聚乙烯橡胶、丙酮和石蜡作为压胶层的原材料进行熔融共聚得到改性氯化聚乙烯橡胶并通过烫金工艺贴合在布料层设有涂料层相对一侧面上形成压胶层,从而得到衣物面料。
实施例2:
本实施例是在上述实施例1的基础上,进一步地限定,包括以质量分数计的聚2,6-萘二甲酸乙二酯纤维50%、聚二正戊基醚纤维15%和聚丁二酸丁二酯纤维35%;涂料层:包括以质量分数计的甲基丙烯酸甲酯55%、单宁酸15%、苯胺蓝13%和丙烯酸-2-乙基己酯17%;薄膜层:包括以质量分数计的PVDF52%、氯化聚乙烯28%和多乙烯多胺20%;压胶层:包括以质量分数计的氯化聚乙烯橡胶65%、丙酮10%和石蜡25%。本实施例的其他部分与上述实施例相同,不再赘述。
实施例3:
本实施例是在上述实施例1的基础上,进一步地限定,所述布料层包括以质量分数计的聚2,6-萘二甲酸乙二酯纤维45%、聚二正戊基醚纤维15%和聚丁二酸丁二酯纤维40%;涂料层:包括以质量分数计的甲基丙烯酸甲酯43%、单宁酸19%、苯胺蓝13%和丙烯酸-2-乙基己酯25%;薄膜层:包括以质量分数计的PVDF50%、氯化聚乙烯25%和多乙烯多胺25%;压胶层:包括以质量分数计的氯化聚乙烯橡胶60%、丙酮15%和石蜡35%。本实施例的其他部分与上述实施例相同,不再赘述。
实施例4:
本实施例是在上述实施例1的基础上,进一步地限定,所述布料层包括以质量分数计的聚2,6-萘二甲酸乙二酯纤维48%、聚二正戊基醚纤维16%和聚丁二酸丁二酯纤维36%;涂料层:包括以质量分数计的甲基丙烯酸甲酯51%、单宁酸19%、苯胺蓝11%和丙烯酸-2-乙基己酯19%;薄膜层:包括以质量分数计的PVDF53%、氯化聚乙烯20%和多乙烯多胺27%;压胶层:包括以质量分数计的氯化聚乙烯橡胶55%、丙酮16%和石蜡34%。本实施例的其他部分与上述实施例相同,不再赘述。
实施例5:
本实施例是在上述实施例1的基础上,进一步地限定其制备方法,具体步骤为:(1)布料层的制备:首先制备作为基层的布料层,按照质量分数计取用的聚2,6-萘二甲酸乙二酯纤维、聚二正戊基醚纤维和聚丁二酸丁二酯纤维作为原材料进行混纺得到纱线并通过机器制成布料层备用;其中混纺成纱为70支,并将得到的混纺纱按照90*50的纱织密度进行纺织成布料层。(2)然后按照质量分数计取用甲基丙烯酸甲酯、单宁酸、苯胺蓝10-15%和丙烯酸-2-乙基己酯作为涂料层原料,先将丙烯酸-2-乙基己酯按照质量分数比例倒入甲基丙烯酸甲酯中进行加热搅拌15min,然后再向其混合液中加入单宁酸和苯胺蓝并持续搅拌26min即得到涂料;其中具体在156℃的条件下进行甲基丙烯酸甲酯的加热搅拌过程。(3)按照质量分数计取用PVDF、氯化聚乙烯和多乙烯多胺作为薄膜层原材料进行造粒形成改性PVDF颗粒备用;其中造粒挤出温度范围为110-156℃;造粒挤出机前端温度为120℃,中端温度140℃,后端为138℃;(4)然后将涂料均匀的涂覆在布料层一侧,待其稳定形成涂料层后,将准备好的PVDF颗粒加热并均匀的涂覆在涂料层上并将涂料层完全覆盖;(5)再以质量分数计选取氯化聚乙烯橡胶、丙酮和石蜡作为压胶层的原材料进行熔融共聚得到改性氯化聚乙烯橡胶并通过烫金工艺贴合在布料层设有涂料层相对一侧面上形成压胶层,从而得到衣物面料。
实施例6:
本实施例是在上述实施例1的基础上,进一步地限定其制备方法,具体步骤为:(1)布料层的制备:首先制备作为基层的布料层,按照质量分数计取用的聚2,6-萘二甲酸乙二酯纤维、聚二正戊基醚纤维和聚丁二酸丁二酯纤维作为原材料进行混纺得到纱线并通过机器制成布料层备用;其中混纺成纱为70支,并将得到的混纺纱按照90*50的纱织密度进行纺织成布料层。(2)然后按照质量分数计取用甲基丙烯酸甲酯、单宁酸、苯胺蓝10-15%和丙烯酸-2-乙基己酯作为涂料层原料,先将丙烯酸-2-乙基己酯按照质量分数比例倒入甲基丙烯酸甲酯中进行加热搅拌17min,然后再向其混合液中加入单宁酸和苯胺蓝并持续搅拌22min即得到涂料;其中具体在155℃的条件下进行甲基丙烯酸甲酯的加热搅拌过程;(3)按照质量分数计取用PVDF、氯化聚乙烯和多乙烯多胺作为薄膜层原材料进行造粒形成改性PVDF颗粒备用;其中造粒挤出温度范围为110-156℃;造粒挤出机前端温度为124℃,中端温度145℃,后端为136℃;(4)然后将涂料均匀的涂覆在布料层一侧,待其稳定形成涂料层后,将准备好的PVDF颗粒加热并均匀的涂覆在涂料层上并将涂料层完全覆盖;(5)再以质量分数计选取氯化聚乙烯橡胶、丙酮和石蜡作为压胶层的原材料进行熔融共聚得到改性氯化聚乙烯橡胶并通过烫金工艺贴合在布料层设有涂料层相对一侧面上形成压胶层,从而得到衣物面料。
尽管已经示出和描述了本发明的实施例,本领域的普通技术人员可以理解:在不脱离本发明的原理和宗旨下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由权利要求及其等同物限定。
Claims (5)
1.一种防紫外线高密度折叠遮阳篷面料的制备方法,其特征在于:具体步骤如下:
A1.首先制备作为基层的布料层,取用以质量分数计的聚2,6-萘二甲酸乙二酯纤维45-75%、聚二正戊基醚纤维15-45%和聚丁二酸丁二酯纤维35-45%作为原材料进行混纺得到纱线并通过机器制成布料层备用;
A2.然后取用质量分数计的甲基丙烯酸甲酯35-62%、单宁酸14-24%、苯胺蓝11-13%和丙烯酸-2-乙基己酯14-25%作为涂料层原料,先将丙烯酸-2-乙基己酯按照质量分数比例倒入甲基丙烯酸甲酯中进行加热搅拌10-20min,然后再向其混合液中加入单宁酸和苯胺蓝并持续搅拌20-25min即得到涂料;
A3.取用质量分数计的PVDF50-70%、氯化聚乙烯20-30%和多乙烯多胺20-35%作为薄膜层原材料进行造粒形成改性PVDF颗粒备用;
A4.然后将涂料均匀的涂覆在布料层一侧,待其稳定形成涂料层后,将准备好的PVDF颗粒加热并均匀的涂覆在涂料层上并将涂料层完全覆盖;
A5.再选取质量分数计的氯化聚乙烯橡胶55-80%、丙酮8-16%和石蜡25-35%作为压胶层的原材料进行熔融共聚得到改性氯化聚乙烯橡胶并通过烫金工艺贴合在布料层设有涂料层相对一侧面上形成压胶层,从而得到衣物面料。
2.根据权利要求1所述的一种防紫外线高密度折叠遮阳篷面料的制备方法,其特征在于:所述步骤A1中混纺成纱为40-60支,并将得到的混纺纱按照90*50的纱织密度进行纺织成布料层。
3.根据权利要求1所述的一种防紫外线高密度折叠遮阳篷面料的制备方法,其特征在于:所述步骤A2中具体在123-156℃的条件下进行甲基丙烯酸甲酯的加热搅拌过程。
4.根据权利要求1所述的一种防紫外线高密度折叠遮阳篷面料的制备方法,其特征在于:所述步骤A3中中造粒挤出温度范围为110-156℃;造粒挤出机前端温度为110-115℃,中端温度150-156℃,后端为135-138℃。
5.根据权利要求1所述的一种防紫外线高密度折叠遮阳篷面料的制备方法,其特征在于:所述步骤A5中的烫金工艺为塑料冷烫金工艺。
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