CN107858197A - A kind of production and processing method of low acid value high-quality edible oil tea-seed oil - Google Patents
A kind of production and processing method of low acid value high-quality edible oil tea-seed oil Download PDFInfo
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- CN107858197A CN107858197A CN201711051335.6A CN201711051335A CN107858197A CN 107858197 A CN107858197 A CN 107858197A CN 201711051335 A CN201711051335 A CN 201711051335A CN 107858197 A CN107858197 A CN 107858197A
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- seed oil
- separating still
- acid value
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/106—Production of fats or fatty oils from raw materials by extracting using ultra-sounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Edible Oils And Fats (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of production and processing method of low acid value high-quality edible oil tea-seed oil, including multi-stage separation supercritical CO2Extraction and molecular distillation refining.Multi-stage separation supercritical CO2Extraction camellia seed oil had both possessed higher recovery rate, and because the presence of multi-stage separation can separate moisture, free fatty, malodorous elements and pigment composition etc. simultaneously.Refining treatment is carried out by molecular distillation technique again, low acid value high-quality edible oil tea-seed oil is produced, for its oil yield up to more than 90%, acid value is less than 0.6, unsaturated fatty acid content more than 90%, rich in the natural anti-oxidation active component such as vitamin E, squalene, Sitosterolum.The production and processing method avoids " five is de- " technical process of traditional complexity, have the advantages that oil-collecting ratio is high, life cycle is short, avoid product from aoxidizing and become sour, keeps oily in nutritional ingredient, in the absence of inflammable and explosive dangerous, free from environmental pollution, solvent-free and heavy-metal residual, the natural quality of guarantee tea oil.
Description
Technical field
The present invention relates to edible oil preparing technical field, more particularly to a kind of life of low acid value high-quality edible oil tea-seed oil
Produce processing method.
Background technology
Oil tea (Camellia oleifera Abel.) is the distinctive woody oil tree species in China, and camellia seed oil is with oil
The oil that tea seed refines out, rich in multiple nutritional components such as unrighted acid, glyceride and various vitamins.Camellia seed oil is not only
Good in color, smell and taste, because of its aliphatic acid composition, high-quality grease --- the composition of olive oil is closely similar with universally acknowledged, and it is not
Saturated fatty acid content is higher than olive oil, and " smoke point " is high, is preferable high nutrition, low in calories, high-grade edible health-care oil.In recent years
Camellia seed oil has been classified as the health type edible oil of emphasis popularization by international food and agricultural organization.The camellia seed oil quality of China is white through the U.S.
Palace Institutes of Health Research and Chinese Center for Disease Control, which examine, to be confirmed, is superior to universally acknowledged olive oil, is described as " east olive
Oil ".
The traditional oil plant fats and oils processing production in China is main to be squeezed using organic solvent leaching or high temperature, is then heated, is added
The modes such as soda acid, adding assistant are decolourized, depickling, dehydration, dewaxing, degumming, technique and equipment extremely fall behind.On the one hand, grease
Middle active skull cap components can largely lose in the preparation process of complexity, and fats and oils processing enterprise is integrally still in a height
The situation of energy resource consumption.On the other hand, in oil production, a certain amount of waste liquid, waste gas is inevitably resulted from and is given up
Slag.
It is presently disclosed on camellia seed oil production and processing method, such as《A kind of processing method of edible tea-seed oil》(application
Number：CN201310042924.3)、《A kind of preparation method of edible oil tea-seed oil》(application number：CN201510954378.X)、
《A kind of high camellia seed oil production method of natural plant sterol content》(application number：CN201610442779.1)、《A kind of selenium-rich
The processing method for refining tea oil》(application number：CN201610569049.8) there is preparation for processing complicated, the production time is longer
The deficiencies of.For utilizing supercritical CO2It is less to extract camellia seed oil Patents, such as《A kind of supercritical CO2Abstraction purification oil tea
The method of seed oil》(application number：CN201510646529.5), its production process lacks supercritical CO2The system of extraction process is ground
Study carefully, the investigation of extraction process technological parameter is not complete, the change of each technological parameter in extraction process, can influence grease obtained product
Matter, such as separation temperature, separating pressure, this patent supercritical CO2Extraction gained camellia seed oil contains moisture, it is necessary to enter to advance
One step dewater treatment, the result is relevant with lacking other technological parameters, equally because its technological parameter lacked can cause patent without
Method is implemented.Patent《The preparation method of camellia seed essential oil》(application number：201310070893.2) in equally employ supercritical CO2
Extraction and molecular distillation, but because of its supercritical CO2Extraction equipment and gained camellia seed essential oil is caused the problems such as preparation technology to prepare
Technique is still relative complex, the step such as while dehydration is added, can not still avoid being deodorized, decolourize, and molecular distillation takes off
Smelly process parameter investigation is not complete, and such as molecular distillation knifing rotating speed, molecular distillation condensation temperature, the process conditions can influence
The working effect of molecular distillation and grease obtained quality, equally because the technological parameter that it lacks can cause patent not implement,
And gained camellia seed essential oil quality is difficult to ensure that the standard for meeting edible oil.
The content of the invention
Extremely fall behind to solve technique in the prior art and equipment, preparation temperature is high, introduce organic solvent, oil product is received
The deficiencies of rate is low, life cycle is long, energy consumption is big, the present invention provide a kind of multi-stage separation supercritical CO2Extract binding molecule distillation
The method that refinery practice produces and processes low acid value high-quality edible oil tea-seed oil.
The purpose of the present invention will be achieved through the following technical solutions：A kind of production of low acid value high-quality edible oil tea-seed oil
Processing method, the tea seed that will shell add multi-stage separation supercritical CO after crushing2In extraction equipment, extraction conditions is set, and
The temperature and pressure of separating stills at different levels is adjusted, carries out camellia seed oil extraction, camellia seed oil crude oil is obtained in separating still I；By more fractions
From supercritical CO2Extraction gained camellia seed oil crude oil, which is added in molecular distillation, carries out refining treatment, regulation vacuum, distillation temperature
Degree, knifing rotating speed, charging rate and condensation temperature carry out refining treatment, and gained oil is low acid value high-quality edible oil tea seed
Oil.
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, the supercritical CO2
Extraction temperature is 40~50 DEG C, the supercritical CO2Extracting pressure is 30~45MPa, and extraction time is 1~2 hour.
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, in the separating still
The temperature of separating still I is 45~60 DEG C, and the pressure of separating still I is 10~20MPa.
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, in the separating still
The temperature of separating still II is 30~50 DEG C, and the pressure of separating still II is 4~8MPa.
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, in the separating still
The temperature of separating still III is 30~50 DEG C, and the pressure of separating still III is 4~8MPa.
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, the molecular distillation
Middle vacuum is 2~9Pa, and vapo(u)rizing temperature is 120~180 DEG C.
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, the molecular distillation
Middle knifing rotating speed is 100~300rmin-1。
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, the molecular distillation
Middle charging rate is 10~50mLmin-1。
Preferably, the production and processing method of described a kind of low acid value high-quality edible oil tea-seed oil, the molecular distillation
Middle condensation temperature is 20-50 DEG C.
Compared with prior art, beneficial effects of the present invention：
Take multi-stage separation supercritical CO2Extraction camellia seed oil had both possessed higher recovery rate, and depositing because of multi-stage separation
Moisture, free fatty, malodorous elements and pigment composition etc. can be being separated simultaneously.Multi-stage separation supercritical CO2Extraction can be once
Property in separating still I collect the preferable camellia seed oil of relative quality, its impurity component for example moisture, free fatty, malodorous elements and
Pigment composition etc. can be separated in separating still II, separating still III, and it, which extracts gained camellia seed oil, has had relatively
High quality, then pass through the edible oil tea-seed oil that simple molecular distillation refining process can obtain low acid value high-quality, acid value
Less than 0.6, unsaturated fatty acid content more than 90%, rich in the natural anti-oxidations such as vitamin E, squalene, cupreol activity
Composition.
The production and processing method avoids " five is de- " (decolouring, depickling, dehydration, dewaxing, degumming) technique mistake of traditional complexity
Journey, has that oil-collecting ratio is high, life cycle is short, avoid product from aoxidizing and become sour, keeps nutritional ingredient in oil, in the absence of inflammable easy
Quick-fried dangerous, free from environmental pollution, solvent-free and heavy-metal residual, ensure the advantages that natural quality of tea oil.
Brief description of the drawings
A kind of flow chart of the production and processing method of low acid value high-quality edible oil tea-seed oil described in Fig. 1.
Embodiment
To more fully understand the present invention, make further specific elaboration, but not to the present invention below by following examples
Limitation of the invention is can be regarded as, some made for those skilled in the art according to foregoing invention content are nonessential
Improve and adjust, be also considered as being within the scope of the present invention.
Embodiment 1
The tea seed that will shell is crushed, and is crossed 20 mesh sieves, is weighed 500g oil tea powder of seeds, and adds that multi-stage separation is super to face
Boundary CO2In extraction equipment, 40 DEG C of extraction temperature, extracting pressure 30MPa, extraction time 120min, the temperature 45 of separating still I are set
DEG C, the pressure 10MPa of separating still I, 30 DEG C of II temperature of separating still, the pressure 4MPa of separating still II, 30 DEG C of III temperature of separating still, separating still
III pressure 4MPa carries out camellia seed oil extraction, and camellia seed oil crude oil is obtained in separating still I.
By multi-stage separation supercritical CO2Extraction gained camellia seed oil crude oil, which is added in molecular distillation, carries out refining treatment,
Vacuum 2Pa, 120 DEG C of vapo(u)rizing temperature, knifing rotating speed 100rmin are set-1, charging rate 10mLmin-1, condensation temperature 20
DEG C carry out refining treatment, gained oil edible oil tea seed oil recovery rate be 85.64%, gained oil physical and chemical index such as table 1-1, aliphatic acid
Composition such as table 1-2, nutritional ingredient such as table 1-3.
Table 1-1 camellia seed oil physical and chemical indexs
Table 1-2 aliphatic acid forms and content
Table 1-3 nutritional ingredients form and content
Embodiment 2
The tea seed that will shell is crushed, and is crossed 40 mesh sieves, is weighed 1000g oil tea powder of seeds, and add multi-stage separation and surpass
Critical CO2In extraction equipment, 45 DEG C of extraction temperature, extracting pressure 45MPa, extraction time 60min, the temperature 50 of separating still I are set
DEG C, the pressure 16MPa of separating still I, the temperature 45 C of separating still II, the pressure 6MPa of separating still II, the temperature 45 C of separating still III, separating still
III pressure 6MPa carries out camellia seed oil extraction, and camellia seed oil crude oil is obtained in separating still I.
By multi-stage separation supercritical CO2Extraction gained camellia seed oil crude oil, which is added in molecular distillation, carries out refining treatment,
Vacuum 8Pa, 130 DEG C of vapo(u)rizing temperature, knifing rotating speed 250rmin are set-1, charging rate 20mLmin-1, condensation temperature 50
DEG C carry out refining treatment, gained oil edible oil tea seed oil recovery rate be 91.23%, gained oil physical and chemical index such as table 2-1, aliphatic acid
Composition such as table 2-2, nutritional ingredient such as table 2-3.
Table 2-1 camellia seed oil physical and chemical indexs
Table 2-2 aliphatic acid forms
Table 2-3 nutritional ingredients form and content
Embodiment 3
The tea seed that will shell is crushed, and is crossed 60 mesh sieves, is weighed 4000g oil tea powder of seeds, and add multi-stage separation and surpass
Critical CO2In extraction equipment, 50 DEG C of extraction temperature, extracting pressure 35MPa, extraction time 60min, the temperature 60 of separating still I are set
DEG C, the pressure 20MPa of separating still I, the temperature 50 C of separating still II, the pressure 8MPa of separating still II, the temperature 50 C of separating still III, separating still
III pressure 8MPa carries out camellia seed oil extraction, and camellia seed oil crude oil is obtained in separating still I.
By multi-stage separation supercritical CO2Extraction gained camellia seed oil crude oil, which is added in molecular distillation, carries out refining treatment,
Vacuum 9Pa, 150 DEG C of vapo(u)rizing temperature, knifing rotating speed 150rmin are set-1, charging rate 50mLmin-1, condensation temperature 40
DEG C carry out refining treatment, gained oil edible oil tea seed oil recovery rate be 87.34%, gained oil physical and chemical index such as table 3-1, aliphatic acid
Composition such as table 3-2, nutritional ingredient such as table 3-3.
Table 3-1 camellia seed oil physical and chemical indexs
Table 3-2 aliphatic acid forms
Table 3-3 nutritional ingredients form and content
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
God any modification, equivalent substitution and improvements made etc., should be included in the scope of the protection with principle.
Claims (9)
- A kind of 1. production and processing method of low acid value high-quality edible oil tea-seed oil, it is characterised in that：To have been shelled tea seed powder Multi-stage separation supercritical CO is added after broken2In extraction equipment, regulation extraction temperature, extracting pressure, extraction time, the temperature of separating still I Degree, the pressure of separating still I, the temperature of separating still II, the pressure of separating still II, the temperature of separating still III and the pressure of separating still III carry out tea seed Oil extraction, obtains camellia seed oil crude oil from separating still I；By multi-stage separation supercritical CO2Extraction gained camellia seed oil crude oil adds Refining treatment is carried out into molecular distillation, regulation vacuum, vapo(u)rizing temperature, knifing rotating speed, charging rate and condensation temperature are carried out Refining treatment, gained oil are low acid value high-quality edible oil tea-seed oil.
- 2. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：The supercritical CO2Extraction temperature is 40~50 DEG C, the supercritical CO2Extracting pressure is 30~45MPa, and extraction time is 1~2 hour.
- 3. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：The temperature of separating still I is 45~60 DEG C in the separating still, and the pressure of separating still I is 10~20MPa.
- 4. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：The temperature of separating still II is 30~50 DEG C in the separating still, and the pressure of separating still II is 4~8MPa.
- 5. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：The temperature of separating still III is 30~50 DEG C in the separating still, and the pressure of separating still III is 4~8MPa.
- 6. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：Vacuum is 2~9Pa in the molecular distillation, and vapo(u)rizing temperature is 120~180 DEG C.
- 7. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：Knifing rotating speed is 100~300rmin in the molecular distillation-1。
- 8. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：Charging rate is 10~50mLmin in the molecular distillation-1。
- 9. a kind of production and processing method of low acid value high-quality edible oil tea-seed oil according to claim 1, its feature exist In：Condensation temperature is 20-50 DEG C in the molecular distillation.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109349364A (en) * | 2018-11-28 | 2019-02-19 | 乌鲁木齐上善元生物科技有限公司 | A kind of reducing blood lipid, norcholesterol fortification oil producing method |
| CN109362898A (en) * | 2018-12-28 | 2019-02-22 | 大连工业大学 | A kind of preparation method of mushroom flavored oils |
| CN109456829A (en) * | 2018-11-22 | 2019-03-12 | 西南林业大学 | A kind of preparation method of rubber seed oil |
| CN110643420A (en) * | 2019-11-13 | 2020-01-03 | 贵州航天乌江机电设备有限责任公司 | Process for extracting and refining oil from idesia polycarpa |
| CN112159706A (en) * | 2020-10-12 | 2021-01-01 | 贵州航天乌江机电设备有限责任公司 | Efficient perilla seed oil preparation process |
| CN113684092A (en) * | 2021-09-03 | 2021-11-23 | 南京益唯森生物科技有限公司 | Preparation method of nitraria seed oil for increasing vitamin E content |
| CN115678671A (en) * | 2022-11-16 | 2023-02-03 | 广东金妮宝科技发展有限公司 | Preparation method of low-trans fatty acid high-quality camellia seed oil |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109456829A (en) * | 2018-11-22 | 2019-03-12 | 西南林业大学 | A kind of preparation method of rubber seed oil |
| CN109349364A (en) * | 2018-11-28 | 2019-02-19 | 乌鲁木齐上善元生物科技有限公司 | A kind of reducing blood lipid, norcholesterol fortification oil producing method |
| CN109362898A (en) * | 2018-12-28 | 2019-02-22 | 大连工业大学 | A kind of preparation method of mushroom flavored oils |
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| CN112159706A (en) * | 2020-10-12 | 2021-01-01 | 贵州航天乌江机电设备有限责任公司 | Efficient perilla seed oil preparation process |
| CN113684092A (en) * | 2021-09-03 | 2021-11-23 | 南京益唯森生物科技有限公司 | Preparation method of nitraria seed oil for increasing vitamin E content |
| CN115678671A (en) * | 2022-11-16 | 2023-02-03 | 广东金妮宝科技发展有限公司 | Preparation method of low-trans fatty acid high-quality camellia seed oil |
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Application publication date: 20180330 |