CN107752122B - Interlayer aroma-producing material for cigarette heated without burning and preparation method thereof - Google Patents
Interlayer aroma-producing material for cigarette heated without burning and preparation method thereof Download PDFInfo
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- CN107752122B CN107752122B CN201710838763.7A CN201710838763A CN107752122B CN 107752122 B CN107752122 B CN 107752122B CN 201710838763 A CN201710838763 A CN 201710838763A CN 107752122 B CN107752122 B CN 107752122B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
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Abstract
The invention relates to an aroma-producing material for heating non-combustion cigarettes and a preparation method thereof. The preparation method comprises the steps of preparing coating materials, coating and the like. The aroma-producing material prepared by using the coating material mainly containing the natural extract has the aroma quality closer to that of the traditional cigarette. Meanwhile, the aroma-producing material is applied to heating non-combustion cigarettes, can improve the heat conduction uniformity and the smoke quantity of the cigarettes, achieves the effect of improving the overall smoking quality of the cigarettes, and can be effectively utilized when the heating non-combustion cigarettes are smoked.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of tobacco materials. More particularly, the invention relates to an interlayer aroma-producing material for a cigarette which is not combusted by heating, and also relates to a preparation method of the interlayer aroma-producing material for the cigarette which is not combusted by heating.
[ background of the invention ]
Unlike conventional cigarettes, heated non-burning cigarettes are smoked by heating a non-burning cartridge with electronic equipment, allowing consumers to smoke the tobacco flavor while reducing harmful smoke constituents resulting from combustion and thermal cracking in conventional cigarettes.
The heating non-combustion cigarette smoking product mainly comprises an aerosol generating device, an aerosol cooling device and an aerosol filtering device; the heating element inside the aerosol generating device heats the aerosol generating substrate to generate aerosol, the aerosol is cooled by the heat transfer of the aerosol cooling device to reduce the temperature of the aerosol, and the aerosol is filtered by the aerosol filtering device. The aerosol generating device is composed of a heating element and a fragrance producing substrate, and the fragrance producing substrate is composed of a fragrance producing material. In a heating non-combustion cigarette system, when the aroma-producing material used in the prior art is heated by a heating element, the heat transfer is not uniform, so that the smoking quantity is often insufficient, the smoking quality is not high, and the smoking feeling of a consumer is further influenced; meanwhile, the aroma-producing material is not effectively utilized due to the non-uniformity of heat transfer; therefore, the present inventors have conducted intensive studies on a fragrance-producing material, and have finally completed the present invention.
[ summary of the invention ]
[ problem to be solved ]
The invention aims to provide an interlayer aroma-producing material for a cigarette which is not combusted by heating.
The invention also aims to provide a preparation method of the interlayer aroma-producing material for the cigarette which is not combusted by heating.
[ solution ]
The invention is realized by the following technical scheme.
The invention relates to a preparation method of an aroma-producing material for cigarette which is not combusted by heating.
The preparation method comprises the following steps:
A. preparation of the coating Material
Mixing 20-50 parts by weight of tobacco extract, 3.0-4.5 parts by weight of red date extract, 2-5 parts by weight of licorice extract, 0.5-3.0 parts by weight of fig extract, 1-5 parts by weight of maple extract, 5-15 parts by weight of propylene glycol, 2-3 parts by weight of 1, 3-butanediol and 2-5 parts by weight of water, supplementing the mixture to 100 parts by weight with glycerol, and uniformly mixing and stirring to obtain the coating material;
B. coating of
B, dip-coating the coating material obtained in the step A on the aluminum foil paper by using a coating machine under the conditions of 10-20N of unwinding tension, 50-65 m/min of vehicle speed, 40 ℃ of coating material and 100-140 ℃ of drying temperature to obtain coated aluminum foil paper;
C. preparation of sandwich fragrance-producing material
Under the conditions of the vehicle speed of 42-66 m/min, the unreeling tension of 14-20N and the reeling tension of 10-16N, dividing the coated aluminum foil paper obtained in the step B into two rolls by using a rewinder, overlapping the two rolls of coated aluminum foil paper, and then using a compound machine to apply glue with the glue applying amount of 1.5-4.0 g/m at the vehicle speed of 70-100 m/min and the unreeling tension of 12-18N2And compounding the two layers of coated aluminum foil paper under the compounding pressure of 0.2-0.8 MPa and the compounding temperature of 80-110 ℃ to obtain the interlayer fragrance-producing material.
According to another preferred embodiment of the present invention, in step a, the weight ratio of the tobacco extract, the red date extract, the licorice extract, the fig extract, the maple extract, the propylene glycol, the 1, 3-butanediol and the water is 28-42: 3.4-4.0: 2.8-4.2: 1.2-2.2: 1.6-4.2: 7-12: 2.2-2.8: 2.8 to 4.2.
According to another preferred embodiment of the present invention, the tobacco extract is a yunyan tobacco extract or a Hunan tobacco extract.
According to another preferred embodiment of the present invention, in step B, the aluminum foil is a composite aluminum foil or a transfer aluminum foil.
According to another preferred embodiment of the invention, in the step B, the gram weight of the aluminum foil paper is 35-65 g/m2。
According to another preferred embodiment of the invention, in step B, the coating machine is a forming paper coating machine.
According to another preferred embodiment of the present invention, in step C, the compound machine is a hot melt adhesive compound machine.
According to another preferred embodiment of the present invention, in step C, the coated aluminum foil laminate is a laminate of an aluminum foil layer and an aluminum foil layer or a laminate of a paper layer and a paper layer.
The invention also relates to the interlayer aroma-producing material for the cigarette which is prepared by the preparation method and is not combusted by heating.
The present invention will be described in more detail below.
The invention relates to a preparation method of an aroma-producing material for cigarette which is not combusted by heating.
The preparation method comprises the following steps:
A. preparation of the coating Material
Mixing 20-50 parts by weight of tobacco extract, 3.0-4.5 parts by weight of red date extract, 2-5 parts by weight of licorice extract, 0.5-3.0 parts by weight of fig extract, 1-5 parts by weight of maple extract, 5-15 parts by weight of propylene glycol, 2-3 parts by weight of 1, 3-butanediol and 2-5 parts by weight of water, supplementing the mixture to 100 parts by weight with glycerol, and uniformly mixing and stirring to obtain the coating material;
in the invention, tobacco extract, red date extract, licorice extract, fig extract and maple extract form aroma components; wherein the tobacco extract mainly has the functions of providing the tobacco original fragrance and constructing a tobacco fragrance framework; the red date extract has the main functions of improving the thick feeling and the aroma texture; the main functions of the licorice extract are to improve the taste and improve the mouthfeel; the fig extract has the main functions of improving the suction comfort, improving the taste and reducing the stimulation; the maple extract has the main functions of improving the aroma texture and reducing the miscellaneous gas.
The main effects of the use of propylene glycol and 1, 3-butanediol in the present invention are on the one hand to dissolve the aroma components and act as solvents and on the other hand to generate smoke when the aroma-producing material is smoked.
In the invention, when the using amount of the tobacco extract is 20-50 parts by weight, the red date extract is 3.0-4.5 parts by weight, the licorice extract is 2-5 parts by weight, the fig extract is 0.5-3.0 parts by weight and the maple extract is 1-5 parts by weight, the sensory evaluation aroma amount of aroma components is sufficient, the aroma is rich, the aroma texture is good, the smoke concentration is moderate, the stimulation is small, the offensive odor is low, the comfort is good, and the harmony is good. If the dosage of the tobacco extract, the red date extract, the liquorice extract, the fig extract and the maple extract exceeds the respective dosage range, namely the dosage of the tobacco extract, the red date extract, the liquorice extract, the fig extract and the maple extract is lower than the respective dosage lower limit or higher than the respective dosage upper limit, the sensory evaluation of aroma components or the aroma skeleton is unclear, the aroma amount is slightly insufficient, the aroma richness is poor, the aroma texture is poor, or the stimulation is slightly obvious, the mouthfeel is poor, the offensive odor is large, or the smoking harmony is poor.
According to the invention, the fuming component is composed of propylene glycol, 1, 3-butanediol, water and glycerol, when the using amount of the propylene glycol is 5-15 parts by weight, and 2-3 parts by weight of the 1, 3-butanediol and 2-5 parts by weight of the water, the obtained coating material has good solubility, moderate viscosity and good coating uniformity, and the smoke concentration generated when the fragrance-producing material is sucked is high. When the propylene glycol, 1, 3-butylene glycol and water are used in amounts exceeding their respective ranges, i.e., the amounts are below their respective lower limits or above their respective upper limits, the resulting coating has poor solubility, too low or too high a coating viscosity, poor coating uniformity, or low smoke concentration when the fragrance-producing material is smoked.
Therefore, the weight ratio of the tobacco extract, the red date extract, the licorice extract, the fig extract, the maple extract, the propylene glycol, the 1, 3-butanediol and the water is 20-50: 3.0-4.5: 2-5: 0.3-3.0: 1-5: 5-15: 2-3: 2 to 5 is reasonable.
Preferably, the weight ratio of the tobacco extract, the red date extract, the licorice extract, the fig extract, the maple extract, the propylene glycol, the 1, 3-butanediol and the water is 28-42: 3.4-4.0: 2.8-4.2: 1.2-2.2: 1.6-4.2: 7-12: 2.2-2.8: 2.8 to 4.2.
The tobacco extract, the red date extract, the licorice extract, the fig extract and the maple extract used in the invention are all products sold in the current market, for example, the tobacco extract is a product sold by Henban scientific and technological Limited in Yunnan under the trade name of Yunyan tobacco extract or a product sold by Hendezhengyang biological scientific and technological Limited in Henan under the trade name of Hunan tobacco extract; the red date extract, the liquorice extract, the fig extract and the maple extract are products sold by Xinzheng gold leaf essence perfume company Limited under the trade names of the red date extract, the liquorice extract, the fig extract and the maple extract respectively; the products are sold by Kaihe elegant essence and flavor Limited company under the trade names of red date extract and maple extract respectively.
In the present invention, propylene glycol, 1, 3-butylene glycol, and glycerol are all food grade products currently marketed, such as those sold under the trade names propylene glycol and glycerol by guangzhou exhibition chemical company; a product sold under the trade name 1, 3-butanediol by lucidesco chemical ltd.
B. Coating of
B, dip-coating the coating material obtained in the step A on the aluminum foil paper by using a coating machine under the conditions of 10-20N of unwinding tension, 50-65 m/min of vehicle speed, 40 ℃ of coating material and 100-140 ℃ of drying temperature to obtain coated aluminum foil paper;
in the invention, the aluminum foil paper is composite aluminum foil paper or transfer aluminum foil paper; the composite aluminum foil paper is a paper and aluminum foil composite paper; the transfer aluminum foil paper is an aluminized paper.
In the invention, the gram weight of the aluminum foil paper is 35-65 g/m2。
The aluminum foil used in the present invention is a product generally used in the field of tobacco production, and includes, for example, a composite aluminum foil sold under the trade name CH-0017 by Yuxichun and tipping paper manufacturing Co., Ltd, and a transfer aluminum foil sold under the trade name CH-0104 by Yuxichun and tipping paper manufacturing Co., Ltd
In the present invention, the coater used is a forming paper coater, which is a product currently marketed, for example, by Virgie fine mechanical packaging, Inc. of Changzhou under the trade name coater LZ-0704Z.
C. Preparation of sandwich fragrance-producing material
Under the conditions that the vehicle speed is 42-66 m/min, the unreeling tension is 14-20N and the reeling tension is 10-16N, the aluminum foil paper obtained in the step B is divided into two rolls by using a rewinder, and the two rolls are coated with aluminumLaminating the foil paper, and then using a compound machine to carry out the laminating at the speed of 70-100 m/min, the unreeling tension of 12-18N and the compound glue application amount of 1.5-4 g/m2And compounding the two layers of coated aluminum foil paper under the compounding pressure of 0.2-0.8 MPa and the compounding temperature of 80-110 ℃ to obtain the interlayer fragrance-producing material.
In the present invention, the described rewinding machine is a vertical slitter rewinding machine, which is a product currently marketed, for example, by the Yangtze machinery factory, a subsidiary area of the Weifang City, under the name G02 vertical slitter rewinding machine.
The complex machine used in the present invention is a hot melt adhesive complex machine, which is a product currently marketed, for example, by Yong standing waves by antidune machine, Inc., of Dongguan, under the trade name YG-PUR1 hot melt adhesive coating complex machine.
In the present invention, the composite adhesive is a hot melt adhesive, which is a product currently sold in the market, for example, a product sold under the trade name of hot melt adhesive N-658NA by Prime Adhesives Co., Ltd, Dongguan.
In the invention, the coating aluminum foil paper is laminated by an aluminum foil layer and an aluminum foil layer or laminated by a paper layer and a paper layer.
The invention also relates to the interlayer aroma-producing material for the cigarette which is prepared by the preparation method and is not combusted by heating.
Compared with the conventional heating non-combustion cigarette product, the interlayer flavor-producing material is applied to producing the heating non-combustion cigarette, a roller is not stuck when a flavor-producing substrate is prepared in a loading machine, the loading speed is high, the prepared flavor-producing substrate can improve the heat conduction uniformity of the heating non-combustion cigarette, for example, the flavor-producing substrate consisting of the interlayer flavor-producing material is divided into 3 sections at equal intervals and placed in a cigarette filter stick, each section is provided with a middle point, the aerosol temperature of the middle points is measured under the conditions that the temperature is 22 +/-2 ℃ and the relative humidity is 60 +/-2% according to a thermocouple method (standard GB/T16839.1-1997), and the temperature of the flavor-producing substrate is sequentially improved by more than 60 ℃, more than 35 ℃ and more than 30 ℃ from the middle point close to an electronic heating element section; meanwhile, according to the sensory quality evaluation method of the YCT 138-.
[ advantageous effects ]
The invention has the beneficial effects that: the interlayer aroma-producing material prepared from the coating material mainly containing the natural extract has the aroma quality closer to that of the traditional cigarette. Meanwhile, the interlayer aroma-producing material is applied to heating non-combustion cigarettes, so that the heat conduction uniformity and the smoke quantity of the cigarettes can be improved, and the effect of improving the overall smoking quality of the cigarettes is achieved. The interlayer aroma-producing material is applied to heating non-combustion cigarettes, and can be effectively utilized when the heating non-combustion cigarettes are smoked. In addition, when the interlayer aroma-producing material is used for preparing a heating non-combustion aroma-producing base body, the feeding speed is high, and the interlayer aroma-producing material is not easy to stick to a roller.
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: preparation of aroma-producing material for cigarette
The implementation steps of this example are as follows:
A. preparation of the coating Material
Mixing 20 parts by weight of Yunyan tobacco extract sold by Henan gang Hengji scientific and technological Limited, 3 parts by weight of red date extract sold by Kaifeng river elegant essence and perfume Limited, 2 parts by weight of licorice extract sold by Kaifeng river elegant essence and perfume Limited, 0.5 part by weight of fig extract sold by Henan Xinzheng essence and perfume Limited, 1 part by weight of maple extract sold by Kaifeng river elegant essence and perfume Limited, 5 parts by weight of propylene glycol, 2.0 parts by weight of 1, 3-butanediol and 2 parts by weight of water, then supplementing to 100 parts by weight with glycerol, mixing and stirring uniformly, thus obtaining the coating material;
B. coating of
The coating obtained in step A was applied to a roll using a coater sold under the trade name of coater LZ-0704Z by Virgie Seiko, VanDipping and coating 35g/m under the conditions of 10N tension, 50m/min vehicle speed, 40 ℃ coating material temperature and 100 ℃ drying temperature2Coating transfer aluminum foil paper is obtained on the transfer aluminum foil paper sold under the trade name CH-0104 by Yuxichun and tipping paper manufacturing company Limited;
C. preparation of sandwich fragrance-producing material
Dividing the coated transfer aluminum foil paper obtained in the step B into two rolls by using a rewinder sold under the trade name G02 vertical slitting rewinder by Shaofang city workshop subregion Yangyang machinery factory under the conditions of the vehicle speed of 42m/min, the unwinding tension of 14N and the winding tension of 10N, superposing two aluminum foil layers of the two rolls of coated transfer aluminum foil paper, and using a compound machine sold under the trade name YG-PUR1 hot melt adhesive coating compound machine by Yong standing waves by antidune mechanical Limited company of Dongguan city at the vehicle speed of 70m/min, the unwinding tension of 12N and the compound adhesive application amount sold under the trade name N-658NA by Dongguan adhesive Limited company of Yongguan City2And compounding the two layers of coated aluminum foil paper under the compounding pressure of 0.2MPa and the compounding temperature of 80 ℃ to obtain the interlayer aroma-producing material of the transfer aluminum foil layer in the paper interlayer.
The interlayer aroma-producing material prepared in the embodiment is used for producing the heating non-combustion cigarettes, the roller is not stuck when the aroma-producing base body is prepared on an upper machine, the loading speed is high, the prepared aroma-producing base body can improve the heat conduction uniformity of the heating non-combustion cigarettes, the aroma-producing base body consisting of the aroma-producing material is divided into 3 sections at equal intervals and placed in a cigarette filter stick, the middle point of each section is selected, and the temperature of the aroma-producing base body is sequentially improved by 65 ℃, 40 ℃ and 30 ℃ from the middle point close to the electronic heating element section; meanwhile, sensory evaluation results show that when the aroma-producing material is applied to the cigarette with the heating non-combustion cigarette, the aroma texture and richness are good, the comfort of the oral cavity is good, the overall smoking quality is high, and the smoke output is also high.
Example 2: preparation of aroma-producing material for cigarette
The implementation steps of this example are as follows:
A. preparation of the coating Material
Mixing 30 parts by weight of Yunyan tobacco extract sold by Henan gang Hengji scientific and technological Limited, 3.5 parts by weight of red date extract sold by Kaifeng river elegant essence and spice Limited, 3 parts by weight of licorice extract sold by Henan Xinzheng essence and spice Limited, 1.3 parts by weight of fig extract sold by Henan Xinzheng essence and spice Limited, 2.3 parts by weight of maple extract sold by Kaifeng river elegant essence and spice Limited, 8 parts by weight of propylene glycol, 2.5 parts by weight of 1, 3-butanediol and 3 parts by weight of water, then supplementing to 100 parts by weight with glycerol, mixing and stirring uniformly, thus obtaining the coating material;
B. coating of
The coating obtained in step A was dip-coated at 45g/m under the conditions of unwinding tension of 13N, vehicle speed of 55m/min, coating temperature of 40 ℃ and drying temperature of 113 ℃ using a coater sold under the trade name of coating machine LZ-0704Z by Virgie Fine mechanical packaging Co., Ltd2Coating transfer aluminum foil paper is obtained on the transfer aluminum foil paper sold under the trade name CH-0104 by Yuxichun and tipping paper manufacturing company Limited;
C. preparation of sandwich fragrance-producing material
Dividing the coating transfer aluminum foil paper obtained in the step B into two rolls by using a rewinding machine sold by Shaofang city workshop subregion Yangyo machinery factory under the trade name G02 vertical slitting rewinding machine under the conditions of the vehicle speed of 50m/min, the unreeling tension of 16N and the reeling tension of 12N, laminating the two aluminum foil layers of the two rolls of coating transfer aluminum foil paper, and applying the compound adhesive with the adhesive amount of 2.3G/m sold by Dongguan Chengguan adhesive Limited company under the trade name hot melt adhesive N-658NA at the vehicle speed of 80m/min, the unreeling tension of 14N and the compound adhesive amount of 2.3G/m2The two-layer coated aluminum foil paper was combined using a compounding machine sold under the trade name of YG-PUR1 hot melt adhesive coating compounding machine by the company yong standing waves by antidune machines ltd, dongguan at a compounding pressure of 0.4MPa and a compounding temperature of 90 c to obtain an interlayer fragrance-producing material in which the transfer aluminum foil layer was present in the interlayer of the paper.
The interlayer aroma-producing material prepared in the embodiment is used for heating non-burning cigarettes, the roller is not stuck when the aroma-producing base body is prepared in an upper machine, the loading speed is high, the heat conduction uniformity of the heated non-burning cigarettes can be improved, the aroma-producing base body consisting of the aroma-producing material is divided into 3 sections at equal intervals and placed in a cigarette filter stick, the middle point of each section is selected, and the temperature of the aroma-producing base body is sequentially increased by 70 ℃, 45 ℃ and 35 ℃ from the middle point close to an electronic heating element section; meanwhile, the sensory evaluation results were similar to those of example 1.
Example 3: preparation of aroma-producing material for cigarette
The implementation steps of this example are as follows:
A. preparation of the coating Material
Mixing 40 parts by weight of Yunyan tobacco extract sold by Henan gang Hengji scientific and technology Limited, 4 parts by weight of red date extract sold by Kaifeng river elegant essence and perfume Limited, 4 parts by weight of licorice extract sold by Henan Xinzheng essence and perfume Limited, 2.1 parts by weight of fig extract sold by Henan Xinzheng essence and perfume Limited, 3.6 parts by weight of maple extract sold by Kaifeng river elegant essence and perfume Limited, 12 parts by weight of propylene glycol, 3 parts by weight of 1, 3-butanediol and 4 parts by weight of water, then supplementing to 100 parts by weight with glycerol, mixing and stirring uniformly, thus obtaining the coating material;
B. coating of
The coating obtained in step A was dip-coated at 55g/m using a coater sold under the trade name of coater LZ-0704Z by Virgie Seiko, Van.2Coating composite aluminum foil paper obtained by Yuxichun and tipping paper manufacturing company Limited under the trade name CH-0017;
C. preparation of sandwich fragrance-producing material
Dividing the coated composite aluminum foil paper obtained in the step B into two rolls by using a rewinder sold under the trade name G02 vertical slitting rewinder by Shaofang city workshop subregion Yang-raising machinery factory under the conditions of the vehicle speed of 58m/min, the unreeling tension of 18N and the reeling tension of 14N, superposing two aluminum foil layers of the coated composite aluminum foil paper, and coating a compound machine sold under the trade name YG-PUR1 by Yong standing waves by antidune machinery Limited company of Dongguan city by using a hot melt adhesive,the glue application amount of the compound glue sold by Namepi adhesive company Limited in Dongguan city under the trade name of hot melt glue N-658NA at the vehicle speed of 90m/min and the unreeling tension of 16N is 3.1g/m2And compounding the two layers of coated composite aluminum foil paper under the conditions of the compounding pressure of 0.6MPa and the compounding temperature of 100 ℃ to obtain the interlayer aroma-producing material which is the composite aluminum foil layer in the interlayer of the paper.
The interlayer aroma-producing material prepared in the embodiment is applied to producing the heating non-combustion cigarettes, the roller is not stuck when the aroma-producing base body is prepared on an upper machine, the loading speed is high, the prepared aroma-producing base body can improve the heat conduction uniformity of the heating non-combustion cigarettes, the aroma-producing base body consisting of the aroma-producing material is divided into 3 sections at equal intervals and placed in a cigarette filter stick, the middle point of each section is selected, and the temperature of the aroma-producing base body is sequentially improved by 63 ℃, 37 ℃ and 34 ℃ from the middle point close to the electronic heating element section; meanwhile, the sensory evaluation results were similar to those of example 1.
Example 4: preparation of aroma-producing material for cigarette
The implementation steps of this example are as follows:
A. preparation of the coating Material
Mixing 50 parts by weight of Yunyan tobacco extract sold by Henan gang Hengji scientific and technology Limited, 4.5 parts by weight of red date extract sold by Kaifeng river elegant essence and perfume Limited, 5 parts by weight of licorice extract sold by Henan Xinzheng essence and perfume Limited, 3 parts by weight of fig extract sold by Henan Xinzheng essence and perfume Limited, 5 parts by weight of maple extract sold by Kaifeng river elegant essence and perfume Limited, 15 parts by weight of propylene glycol, 2.5 parts by weight of 1, 3-butanediol and 5 parts by weight of water, then supplementing to 100 parts by weight with glycerol, mixing and stirring uniformly, thus obtaining the coating material;
B. coating of
The coating obtained in step A was applied to a forming paper coater sold under the trade name of coater LZ-0704Z by Virgi Seiko, Van at a unwind tension of 20N, a vehicle speed of 65m/min, a coating temperature of 40 ℃ and a drying temperature of 140 DEG CUnder the condition of (1), dip-coating at 65g/m2Coating composite aluminum foil paper obtained by Yuxichun and tipping paper manufacturing company Limited under the trade name CH-0017;
C. preparation of sandwich fragrance-producing material
Dividing the coated composite aluminum foil paper obtained in the step B into two rolls by using a rewinder sold under the trade name G02 vertical slitting rewinder by Shaofang city workshop subregion Yangyang machinery factory under the conditions of the vehicle speed of 66m/min, the unwinding tension of 20N and the winding tension of 16N, superposing the two aluminum foil layers of the coated composite aluminum foil paper, and using a compound sold under the trade name YG-PUR1 hot melt adhesive coating compound machine by Yong standing waves by antidune machinery Limited in Dongguan city to apply the compound glue with the glue application amount of 4G/m sold under the trade name N-658NA hot melt adhesive by Yongguan Ming adhesive Limited in Dongguan city at the vehicle speed of 100m/min, the unwinding tension of 18N and the winding tension of 16N2And compounding the two layers of coated composite aluminum foil paper under the conditions of the compounding pressure of 0.8MPa and the compounding temperature of 110 ℃ to obtain the interlayer aroma-producing material which is the composite aluminum foil layer in the interlayer of the paper.
The interlayer aroma-producing material prepared in the embodiment is applied to producing the heating non-combustion cigarettes, the roller is not stuck when the aroma-producing base body is prepared on an upper machine, the loading speed is high, the prepared aroma-producing base body can improve the heat conduction uniformity of the heating non-combustion cigarettes, the aroma-producing base body consisting of the aroma-producing material is divided into 3 sections at equal intervals and placed in a cigarette filter stick, the middle point of each section is selected, and the temperature of the aroma-producing base body is sequentially improved by 65 ℃, 40 ℃ and 34 ℃ from the middle point close to the electronic heating element section; meanwhile, the sensory evaluation results were similar to those of example 1.
Claims (8)
1. A preparation method of an interlayer aroma-producing material for cigarette by heating and non-combustion is characterized by comprising the following steps:
A. preparation of the coating Material
Mixing 20-50 parts by weight of tobacco extract, 3.0-4.5 parts by weight of red date extract, 2-5 parts by weight of licorice extract, 0.5-3.0 parts by weight of fig extract, 1-5 parts by weight of maple extract, 5-15 parts by weight of propylene glycol, 2-3 parts by weight of 1, 3-butanediol and 2-5 parts by weight of water, supplementing the mixture to 100 parts by weight with glycerol, and uniformly mixing and stirring to obtain the coating material;
B. coating of
B, dip-coating the coating material obtained in the step A on the aluminum foil paper by using a coating machine under the conditions of 10-20N of unwinding tension, 50-65 m/min of vehicle speed, 40 ℃ of coating material and 100-140 ℃ of drying temperature to obtain coated aluminum foil paper; the gram weight of the aluminum foil paper is 35-65 g/m2；
C. Preparation of sandwich fragrance-producing material
Under the conditions of the vehicle speed of 42-66 m/min, the unreeling tension of 14-20N and the reeling tension of 10-16N, dividing the coated aluminum foil paper obtained in the step B into two rolls by using a rewinder, overlapping the two rolls of coated aluminum foil paper, and then using a compound machine to apply glue with the glue applying amount of 1.5-4.0 g/m at the vehicle speed of 70-100 m/min and the unreeling tension of 12-18N2And compounding the two layers of coated aluminum foil paper under the compounding pressure of 0.2-0.8 MPa and the compounding temperature of 80-110 ℃ to obtain the interlayer fragrance-producing material.
2. The preparation method according to claim 1, wherein in the step A, the weight ratio of the tobacco extract, the red date extract, the licorice extract, the fig extract, the maple extract, the propylene glycol, the 1, 3-butanediol and the water is 28-42: 3.4-4.0: 2.8-4.2: 1.2-2.2: 1.6-4.2: 7-12: 2.2-2.8: 2.8 to 4.2.
3. The method according to claim 1 or 2, wherein the tobacco extract is Yunyan tobacco extract or Hunan tobacco extract.
4. The method according to claim 1, wherein in step a, the aluminum-foil paper is a composite aluminum-foil paper or a transfer aluminum-foil paper.
5. The method according to claim 1, wherein in step B, the coater is a forming paper coater.
6. The method of claim 1, wherein in step B, said compounding machine is a hot melt adhesive compounding machine.
7. The method of claim 1, wherein in step C, the coated aluminum foil laminate is an aluminum foil layer and an aluminum foil layer or a paper layer and a paper layer.
8. An interlayer flavor-producing material for a heat-not-burn cigarette produced by the production method according to any one of claims 1 to 7.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710838763.7A CN107752122B (en) | 2017-09-18 | 2017-09-18 | Interlayer aroma-producing material for cigarette heated without burning and preparation method thereof |
Applications Claiming Priority (1)
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| CN108523206B (en) * | 2018-05-14 | 2021-06-01 | 四川三联新材料有限公司 | Preparation method of cigar flavor cooling and flavoring section and heating non-combustion cigarette base rod |
| CN108720077B (en) * | 2018-07-25 | 2021-04-20 | 河南中烟工业有限责任公司 | Application of low-sugar high-fragrance maple extract in cigarette without burning under heating |
| CN109512015B (en) * | 2018-10-29 | 2021-07-20 | 云南巴菰生物科技有限公司 | Heating non-combustion solid essence for cigarettes and preparation method thereof |
| CN111084414A (en) * | 2019-12-17 | 2020-05-01 | 云南中烟工业有限责任公司 | Method for improving smoking stability of heated cigarette |
| CN114027546A (en) * | 2021-10-27 | 2022-02-11 | 深圳市真味生物科技有限公司 | Heating non-combustible tobacco original flavor fuming feed liquid, fuming particles and preparation method of fuming particles |
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Address after: No. 280, north section of Yizhou Avenue, high tech Zone, Chengdu, Sichuan 610040 Patentee after: SICHUAN SANLIAN CIGARETTE MATERIALS CO.,LTD. Patentee after: Yunnan Bazi Biotechnology Co., Ltd Address before: No. 280, north section of Yizhou Avenue, high tech Zone, Chengdu, Sichuan 610040 Patentee before: SICHUAN SANLIAN CIGARETTE MATERIALS CO.,LTD. Patentee before: Yunnan Bazi Biotechnology Co., Ltd |
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