CN105747266B - Preparation method of cigarette rod without burning tobacco by heating - Google Patents
Preparation method of cigarette rod without burning tobacco by heating Download PDFInfo
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- CN105747266B CN105747266B CN201610247576.7A CN201610247576A CN105747266B CN 105747266 B CN105747266 B CN 105747266B CN 201610247576 A CN201610247576 A CN 201610247576A CN 105747266 B CN105747266 B CN 105747266B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
- A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a preparation method of a cigarette without burning tobacco by heating, which comprises the following steps: selecting a tobacco raw material, soaking the tobacco raw material in water, filtering, and pulping the filtered tobacco to obtain tobacco pulp; preparing a tobacco substrate; selecting one or more of flue-cured tobacco, air-cured tobacco or sun-cured tobacco, and preparing tobacco essential oil by adopting a molecular distillation method; weighing 1-40 parts of tobacco essential oil, 2-20 parts of tobacco essence and 40-80 parts of atomizing agent by weight, and uniformly mixing to obtain a coating liquid; weighing the coating liquid according to 25-40% of the weight of the tobacco substrate, and spraying the coating liquid on the tobacco substrate; the tobacco substrate is prepared into a heated non-burning tobacco cigarette rod. The cigarette has full smoke and has similar smoking feeling as the traditional cigarette; meanwhile, the aroma is rich, and particularly the tobacco aroma is highlighted; has good satisfaction.
Description
Technical Field
The invention relates to the technical field of tobacco, in particular to a preparation method of a cigarette rod without burning tobacco by heating.
Background
The cigarette without burning is heated to provide nicotine and tobacco characteristic aroma for consumers in a mode of heating the tobacco without burning, so that the requirements of the consumers are met, the release amount of tar and harmful substances in mainstream smoke can be greatly reduced, and the cigarette with burning-free characteristics is an important trend for the development of the tobacco market in the future.
Because the use mode of the cigarette is greatly different from that of the traditional cigarette, the design of heating the cigarette without burning is different from that of the traditional cigarette. Relevant experiments show that ordinary cigarettes without special treatment cannot provide satisfactory smoke quantity and aroma when used in common smoking utensils.
Reconstituted tobacco is an important tobacco raw material and its use in heat not burn tobacco products has three benefits: (1) can be made into sheet materials, and can solve the problem of tobacco falling off to a greater extent; (2) the uniformity of the quality of the tobacco products is ensured to a greater extent, and more consistent smoking feeling is provided; (3) as the chemical components of the tobacco can be changed to a greater extent according to needs in the preparation process of the reconstituted tobacco, the method has obvious advantages for improving and enhancing the quality of the heated non-combustion tobacco products and meeting individual requirements in the market. However, the main purpose of the reconstituted tobacco produced at present is to improve the use efficiency of tobacco raw materials and improve the economic benefit, and the used raw materials are usually waste tobacco powder, tobacco leaves and tobacco stems, so that most of tobacco substrates lack the characteristic aroma of cigarettes on the whole, the original aroma of the tobacco is insufficient, and the miscellaneous gas and the wood gas are heavy. Meanwhile, the reconstituted tobacco is mainly added into cigarettes after being shredded, the content of commonly used humectants is low, and high-concentration smoke cannot be provided in the process of heating non-combustion tobacco products.
Patent document CN 103181613 discloses a method for preparing electrically dry-distilled tobacco sheets. In this patent document, tobacco extracts, plant extracts and smoke agents are applied to a tobacco sheet substrate and applied to an electric dry distillation device to generate smoke. However, the patent document only simply modifies the common sheet in a sheet coating manner, and does not consider the influence on cigarette smoking and the influence on tobacco aroma release after the sheet is rolled.
Disclosure of Invention
Technical problem to be solved
The invention aims to solve the technical problem of how to improve the smoking quantity and the tobacco fragrance of the cigarette without burning during heating, and provide good smoke feeling and rich tobacco fragrance when being used in a smoking set without burning during heating, thereby providing a preparation method of the cigarette without burning during heating.
(II) technical scheme
In order to solve the technical problems, the invention provides a preparation method of a cigarette without burning tobacco by heating, which comprises the following steps (the used raw materials are purchased in the market):
the method comprises the following steps: preparing a tobacco substrate: selecting tobacco raw materials, soaking the tobacco raw materials in water at the temperature of 60-80 ℃ for 0.5-2h, filtering, and pulping the filtered tobacco to obtain tobacco pulp; weighing 50-80 parts of tobacco pulp, 8-25 parts of wood pulp and 4-8 parts of adhesive in parts by weight, uniformly mixing, feeding the mixed pulp to a paper machine for forming, and drying until the water content is 10-15% to obtain a tobacco substrate;
step two: preparing tobacco essential oil: selecting one or more of flue-cured tobacco, air-cured tobacco or sun-cured tobacco, and preparing a tobacco primary extract by adopting a solvent extraction method; preparing tobacco essential oil from the tobacco primary extract by adopting a molecular distillation method;
step three: preparing a coating liquid: weighing 1-40 parts of tobacco essential oil, 2-20 parts of tobacco essence and 40-80 parts of atomizing agent obtained in the step two by weight, and then uniformly mixing to obtain a coating liquid;
step four: coating a tobacco substrate: weighing the coating liquid obtained in the third step according to 25-40% of the weight of the tobacco substrate obtained in the first step, spraying the coating liquid on the tobacco substrate, and standing for 40-60h under the conditions of constant temperature and constant humidity to obtain a coated tobacco substrate;
step five: preparing tobacco cigarette rods: and D, manufacturing the tobacco substrate obtained in the step four into a tobacco rod according to the size, and connecting the tobacco rod with a filter tip to obtain the cigarette which is heated and does not burn the tobacco.
Preferably, in the first step, the tobacco material comprises one or more of tobacco stems, tobacco powder, broken leaves and short shreds.
Preferably, in the step one, the wood pulp is one or more of spruce bleached kraft pulp, poplar bleached kraft pulp, softwood bleached kraft pulp and eucalyptus bleached kraft pulp.
Preferably, in the first step, the binder is one or more of xanthan gum, arabic gum and guar gum.
Preferably, in the step one, the thickness of the tobacco substrate is 10-300 μm; the thickness gram weight of the tobacco substrate is 20-200g/m2。
Preferably, in the second step, the cured tobacco is one or two of burley tobacco and Maryland tobacco; the sun-cured tobacco is one or more of aromatic tobacco, red sun-cured tobacco, yellow sun-cured tobacco or yellow day-lily tobacco; the molecular distillation conditions were as follows: the feeding speed is 2-10mL/min, the vacuum degree is 15-20Pa, the sample injection temperature is 80 ℃, the heating temperature is 60-80 ℃, the cooling temperature is 10-20 ℃, and the rotating speed is 300-400 r/min.
Preferably, in step three, the essence for the cigarettes is one or more of vanillin, benzoic acid, phenylacetic acid, 10% peru extract, 5% tree moss extract, 90% clove oil, anisic aldehyde, 10% bromelain, benzyl alcohol, phenethyl alcohol, toluophenone, ethyl phenylacetate, bell plum extract, phenylacetaldehyde, acetophenone, angelica lactone, farnesone, dodecanoic acid, isovaleric acid, benzyl butyrate, octanol, tetramethylpyrazine, citric acid, ethyl maltol, sclareol, sclareolide, ambergris ether, sweet wormwood oil, orange leaf oil, valerian oil, vetiver oil, labdanum extract, storax extract, pubescent angelica root tincture, tamarind fluid extract, tamarind extract, chamomile extract, vanilla extract, fig extract, apple juice, megastigmatrienone, dihydroactinidiolide, beta-ionone, palmitic acid and geranylacetone; preferably, the composition comprises 1% of vanillin, 0.2% of benzoic acid, 0.5% of phenylacetic acid, 1.0% of peruvian extract, 5% of tree moss extract, 0.5% of clove oil, 0.5% of anisic aldehyde, 0.5% of bromelain, 0.4% of phenethyl alcohol, 0.2% of toluophenone, 0.2% of ethyl phenylacetate, 25% of ethanol and 65% of propylene glycol in percentage by weight.
Preferably, in the third step, the atomizing agent is one or more of propylene glycol, triethylene glycol, 1, 3-butanediol, glycerol, dipropylene glycol and polyethylene glycol; glycerol is preferred.
The invention also provides the tobacco cigarette prepared by the preparation method of the cigarette without burning tobacco by heating.
The invention also provides the application of the tobacco cigarette prepared by the preparation method of the non-burning tobacco cigarette in heating a non-burning smoking set, namely, the tobacco cigarette is placed in the smoking set, the heating temperature is set to be 200-500 ℃, the heating time is 10-30s, and smoking is started after the heating time is reached.
The tobacco material section of the cigarette is processed by adopting the paper filter stick production equipment. Preferably, the resulting substrate basis weight is from 20 to 120g/m2Preferably 50g/m2(ii) a The width is 60-300mm, preferably 110 mm. Preferably, the production equipment of the paper filter stick is prepared at the speed of 10-80 m/min. Preferably, the substrate needs to pass throughEmbossing, wherein the specific shape is not limited, and strip embossing is preferred; the forming paper can be common forming paper, and preferably is a material with the function of preventing seepage.
The invention also provides a tobacco substrate and filter stick compounding process. In order to ensure that the rolled cigarettes can fully release smoke and aroma under the heating condition, the maximum reduction of suction resistance is followed in the process of compounding the tobacco substrate and the filter stick. The filter stick adopted in the invention is an acetate fiber filter stick, preferably a hollow special-shaped filter stick, and the blocking effect of the filter stick on smoke can be reduced to the greatest extent. Specifically, the specification of the adopted filter stick is 22.0-25.0mm of the circumference, the length of the filter stick is 100-150mm, and the specification of the filament bundle is 1.8-6.0 denier of filament denier. The filter stick of the suction nozzle part can be of a whole hollow structure, and can also be combined with part of common filter sticks, preferably a whole hollow filter stick, and the more preferable filter stick length is 23+7mm, wherein 23mm is a hollow filter stick, and 7mm is a common filter stick. The shape of the hollow filter stick is not limited, and a round, square or other special-shaped structure can be adopted. The base is compounded with the filter stick through the tobacco material section of the cigarette produced by the paper filter stick processing equipment. Designing the length of the filter stick to be 15-40mm, preferably 15-30 mm; the tobacco material has a length of 10-40mm, preferably 20 mm. And compounding to obtain the finished cigarette for heating the non-combustion smoking set.
The invention finally provides the use effect of the compounded cigarettes in the smoking set. Placing the prepared cigarette in a smoking set, setting the heating temperature at 200-; the cigarette starts to be smoked after the set time is reached, and the smoke is full, so that the cigarette has similar smoking feeling to the traditional cigarette; meanwhile, the aroma is rich, and particularly the tobacco aroma is highlighted; has good satisfaction.
(III) advantageous effects
The method can prepare cigarettes with uniform quality, and provides a basis for ensuring the consistency of the smoke quality in the process of mouth-to-mouth suction; the method adopts the original paper-making technology to process the tobacco substrate, thereby ensuring the possibility of the industrial production of cigarettes; the method of the invention adopts the hollow filter stick to ensure the smoke quantity of the novel cigarette and the richness of the tobacco fragrance to the maximum extent. By adopting the matched smoking set, the usage amount of tobacco raw materials is reduced and the production cost is reduced on the premise of ensuring that the number of the smoking openings is consistent with that of the traditional cigarettes; the cigarette has full smoke and has similar smoking feeling as the traditional cigarette; meanwhile, the aroma is rich, and particularly the tobacco aroma is highlighted; has good satisfaction.
Detailed Description
The following examples further describe embodiments of the present invention in detail. The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
Example 1
Mixing tobacco stems and tobacco powder, adding 3-4 times of water, heating, and filtering to obtain filter residue; pulping the filter residues to obtain tobacco pulp, uniformly mixing 65Kg of tobacco pulp, 20Kg of wood pulp and 4Kg of xanthan gum, and then making paper on a paper machine to obtain a substrate; preparing a coating liquid, wherein the coating liquid comprises the following components in percentage by weight: flue-cured tobacco essential oil: 15 percent; essence for tobacco: 10 percent; glycerol: 75 percent, and uniformly spraying the coating liquid accounting for 30 percent of the weight of the tobacco substrate onto the tobacco substrate by a throat sprayer; balancing for 48 hours in a constant temperature and humidity chamber under the conditions that the environmental temperature is adjusted to be (22 +/-1) DEG C and the relative humidity is adjusted to be (60 +/-2)% to obtain a No. 1 sample;
the selected quantitative rate is 50g/m2(ii) a Processing a substrate with the width of 80mm by processing equipment to obtain an embossed tobacco rod, wherein the speed of the production equipment is controlled at 40m/min in the production process; the tobacco rod and the filter tip are connected through the compound equipment to form a cigarette, wherein the length of the filter tip is 30mm, and the length of the tobacco rod is 20 mm.
Inserting the obtained cigarette into smoking set, setting heating temperature of smoking set at 250 deg.C, heating for 20s, and starting smoking.
Example 2
Mixing tobacco stems and tobacco powder, adding 3-4 times of water, heating, and filtering to obtain filter residue; pulping the filter residues to obtain tobacco pulp, uniformly mixing 80Kg of tobacco pulp, 25Kg of wood pulp and 8Kg of xanthan gum, and then making paper on a paper machine to obtain a substrate; preparing a coating liquid, wherein the coating liquid comprises the following components in percentage by weight: flue-cured tobacco essential oil: 15 percent; essence for tobacco: 10 percent; glycerol: 75 percent of the coating solution is uniformly sprayed on the selected tobacco substrate by a throat sprayer, wherein the weight of the coating solution is 15 percent of the weight of the tobacco substrate. Balancing for 48 hours in a constant temperature and humidity chamber under the conditions that the environmental temperature is adjusted to be (22 +/-1) DEG C and the relative humidity is adjusted to be (60 +/-2)% to obtain a No. 2 sample;
the selection ration is 35g/m2(ii) a Processing a substrate with the width of 110mm by processing equipment to obtain an embossed tobacco rod, wherein the speed of the production equipment is controlled at 60m/min in the production process; the tobacco rod and the filter tip are connected through the compound equipment to form a cigarette, wherein the length of the filter tip is 30mm, and the length of the tobacco rod is 20 mm.
Inserting the obtained cigarette into smoking set, setting the heating temperature of smoking set at 300 deg.C, heating for 10s, and starting smoking.
Example 3
Mixing tobacco stems and tobacco powder, adding 3-4 times of water, heating, and filtering to obtain filter residue; pulping the filter residues to obtain tobacco pulp, uniformly mixing 50Kg of tobacco pulp, 8Kg of wood pulp and 6Kg of arabic gum, and then making paper on a paper machine to obtain a substrate; preparing a coating liquid, wherein the coating liquid comprises the following components in percentage by weight: flue-cured tobacco essential oil: 40 percent; essence for tobacco: 10 percent; glycerol: 50 percent, and uniformly spraying the coating solution accounting for 45 percent of the weight of the tobacco substrate onto the tobacco substrate by using a throat sprayer. Balancing for 48 hours in a constant temperature and humidity chamber under the conditions that the environmental temperature is adjusted to be (22 +/-1) DEG C and the relative humidity is adjusted to be (60 +/-2)% to obtain a 3# sample;
the selected quantitative value is 70g/m2(ii) a Processing a substrate with the width of 220mm by processing equipment to obtain an embossed tobacco rod, wherein the speed of the production equipment is controlled at 20m/min in the production process; the tobacco rod and the filter tip are connected through the compound equipment to form a cigarette, wherein the length of the filter tip is 30mm, and the length of the tobacco rod is 20 mm.
Inserting the obtained cigarette into smoking set, setting heating temperature of smoking set at 200 deg.C, heating for 15s, and starting smoking.
The results show that: the smoke generated by the heating non-combustible tobacco product in the embodiment under the low-temperature heating condition has less irritation to throat, rich fragrance, prominent tobacco, unique style, good satisfaction, pure and comfortable aftertaste and sufficient smoke quantity.
The above embodiments are merely illustrative of the present invention and are not to be construed as limiting the invention. Although the present invention has been described in detail with reference to the embodiments, it should be understood by those skilled in the art that various combinations, modifications or equivalents may be made to the technical solution of the present invention without departing from the spirit and scope of the technical solution of the present invention, and the technical solution of the present invention is covered by the claims of the present invention.
Claims (8)
1. A preparation method of a cigarette without burning tobacco by heating is characterized by comprising the following steps:
the method comprises the following steps: preparing a tobacco substrate: selecting tobacco raw materials, soaking the tobacco raw materials in water at the temperature of 60-80 ℃ for 0.5-2h, filtering, and pulping the filtered tobacco to obtain tobacco pulp; weighing 65 parts of tobacco pulp, 20 parts of wood pulp and 4 parts of xanthan gum in parts by weight, uniformly mixing, feeding the mixed pulp to a paper machine for forming, drying until the water content is 10-15%, and embossing to obtain a tobacco substrate; the grammage of the tobacco substrate is 50g/m2；
Step two: preparing tobacco essential oil: selecting one or more of flue-cured tobacco, air-cured tobacco or sun-cured tobacco, and preparing a tobacco primary extract by adopting a solvent extraction method; preparing tobacco essential oil from the tobacco primary extract by adopting a molecular distillation method;
step three: preparing a coating liquid: weighing 15 parts by weight of tobacco essential oil, 10 parts by weight of tobacco essence and 75 parts by weight of glycerol obtained in the step two, and uniformly mixing to obtain a coating liquid;
step four: coating a tobacco substrate: weighing the coating liquid obtained in the third step according to 30% of the weight of the tobacco substrate obtained in the first step, spraying the coating liquid on the tobacco substrate, and standing for 40-60h under the conditions of constant temperature and constant humidity to obtain a coated tobacco substrate;
step five: preparing tobacco cigarette rods: preparing the tobacco substrate obtained in the fourth step into a tobacco rod according to the size, and connecting the tobacco rod with a filter tip to obtain a cigarette which is heated and does not burn tobacco;
the filter tip consists of a 23mm hollow filter stick and a 7mm common filter stick, the size of the adopted filter stick is 22.0-25.0mm in circumference, and the size of the filament bundle is 1.8-6.0 denier.
2. The method for preparing a heated non-combustible tobacco cigarette rod as claimed in claim 1, wherein in the first step, the tobacco material includes one or more of tobacco stems, tobacco powder, broken leaves and short shreds.
3. The method for preparing cigarette with non-combustible tobacco by heating according to claim 1, wherein in the first step, the wood pulp is one or more of spruce bleached kraft pulp, poplar bleached kraft pulp, softwood bleached kraft pulp and eucalyptus bleached kraft pulp.
4. The method for preparing a heated non-combustible tobacco cigarette rod according to claim 1, wherein in step one, the tobacco substrate has a thickness of 10 to 300 μm.
5. The method for preparing a cigarette rod without burning tobacco by heating according to claim 1, wherein in the second step, the air-cured tobacco is one or two of burley tobacco and Maryland tobacco; the sun-cured tobacco is one or more of aromatic tobacco, red sun-cured tobacco, yellow sun-cured tobacco or yellow day-lily tobacco; the molecular distillation conditions were as follows: the feeding speed is 2-10mL/min, the vacuum degree is 15-20Pa, the sample injection temperature is 80 ℃, the heating temperature is 60-80 ℃, the cooling temperature is 10-20 ℃, and the rotating speed is 300-400 r/min.
6. The method according to claim 1, wherein in step three, the tobacco flavor is vanillin, benzoic acid, phenylacetic acid, 10% peru extract, 5% moss extract, 90% clove oil, anisic aldehyde, 10% bromelain, benzyl alcohol, phenethyl alcohol, toluophenone, ethyl phenylacetate, bell plum extract, phenylacetaldehyde, acetophenone, angelica lactone, farnesone, dodecanoic acid, isovaleric acid, benzyl butyrate, octanol, tetramethylpyrazine, citric acid, ethyl maltol, sclareol, sclareolide, ambrox, sweet wormwood oil, orange leaf oil, valerian oil, vetiver oil, labdanum extract, storax extract, pubescent angelica root, tamarind fruit fluid extract, tamarind fruit extract, chamomile extract, vanilla, fig extract, apple juice extract, megastigmatrienone, dihydroactinidiolide, 5% tree moss extract, 90% clove oil, cumin, One or more of beta-ionone, palmitic acid and geranylacetone.
7. A tobacco rod made by the method of making a heated non-combustible tobacco cigarette rod according to any one of claims 1 to 6.
8. The use of the tobacco rod of claim 7 in heating a non-burning smoking set, wherein the tobacco rod of claim 7 is placed in the smoking set at a heating temperature of 200 ℃ and 500 ℃ for a heating time of 10-30s, and smoking is started after the heating time is reached.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610247576.7A CN105747266B (en) | 2016-04-20 | 2016-04-20 | Preparation method of cigarette rod without burning tobacco by heating |
| PCT/CN2016/108255 WO2017181684A1 (en) | 2016-04-20 | 2016-12-01 | Method for manufacturing heat-not-burn tobacco cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610247576.7A CN105747266B (en) | 2016-04-20 | 2016-04-20 | Preparation method of cigarette rod without burning tobacco by heating |
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| CN105747266A CN105747266A (en) | 2016-07-13 |
| CN105747266B true CN105747266B (en) | 2021-05-28 |
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| WO (1) | WO2017181684A1 (en) |
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