CN107724116A - 一种猪鬃用染色剂 - Google Patents

一种猪鬃用染色剂 Download PDF

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CN107724116A
CN107724116A CN201710853913.1A CN201710853913A CN107724116A CN 107724116 A CN107724116 A CN 107724116A CN 201710853913 A CN201710853913 A CN 201710853913A CN 107724116 A CN107724116 A CN 107724116A
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parts
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宣永昌
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Yongchang Wuwei County Anhui Province Bristle Brush Manufacturing Co Ltd
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Abstract

本发明公开了一种猪鬃用染色剂，其原料包括：天然染料、铬黄、滑石粉、稀土、硫酸铝铵、硫酸铝钾、碳酸钙、硫酸锌、氯化钾、氢氧化钠、壳聚糖、苯甲酸钠、渗透剂JFC、聚乙烯醇、丙二醇、儿茶素、烷基糖苷、羟甲基纤维素、丙二醇甲醚醋酸酯、三聚磷酸钾、聚丙烯酸酯、苯甲酸乙酯、环氧大豆油、钛酸四丁酯、去离子水。本发明提出的一种猪鬃用染色剂，污染小，染色效率高，上色深且均匀，染色后猪鬃具有良好的耐光性和耐温性，不易褪色，色牢度好，同时提高猪鬃耐磨性和柔韧性，有效延长猪鬃制品的使用寿命。

Description

一种猪鬃用染色剂
技术领域
本发明涉及染色剂技术领域，尤其涉及一种猪鬃用染色剂。
背景技术
猪鬃是指猪颈部和背部生长的5厘米以上的刚毛，常被用于制备日用刷、油漆刷、机器刷等。猪鬃的颜色主要有黑色、白色、黄色和花色。天然黄色猪鬃产量少，无法满足实际生产需要，而目前猪鬃所用染色剂存在污染大，染色效率低，上色浅且不均匀，染色后猪鬃耐光性和耐温性差，易褪色，且不能有效提高猪鬃耐磨性和柔韧性，影响猪鬃制品的使用寿命。
发明内容
基于背景技术存在的技术问题，本发明提出了一种猪鬃用染色剂，污染小，染色效率高，上色深且均匀，染色后猪鬃具有良好的耐光性和耐温性，不易褪色，色牢度好，同时提高猪鬃耐磨性和柔韧性，有效延长猪鬃制品的使用寿命。
本发明提出的一种猪鬃用染色剂，其原料按重量份包括：天然染料12-18份、铬黄1-1.5份、滑石粉0.5-1份、稀土0.5-1份、硫酸铝铵0.2-0.4份、硫酸铝钾0.1-0.3份、碳酸钙0.1-0.2份、硫酸锌0.2-0.4份、氯化钾0.4-0.6份、氢氧化钠0.1-0.4份、壳聚糖0.4-0.8份、苯甲酸钠0.6-0.8份、渗透剂JFC 0.2-0.4份、聚乙烯醇0.2-0.5份、丙二醇0.4-0.8份、儿茶素0.02-0.1份、烷基糖苷0.6-1.2份、羟甲基纤维素0.2-0.4份、丙二醇甲醚醋酸酯0.2-0.5份、三聚磷酸钾0.1-0.3份、聚丙烯酸酯0.2-0.4份、苯甲酸乙酯0.2-0.4份、环氧大豆油0.6-1.5份、钛酸四丁酯0.2-0.6份、去离子水50-80份。
具体实施方式中，天然染料的重量份还可以为13、14、15、16、17份，铬黄的重量份还可以为1.1、1.2、1.25、1.3、1.4份，滑石粉的重量份还可以为0.6、0.7、0.75、0.8、0.9份，稀土的重量份还可以为0.6、0.7、0.75、0.8、0.9份，硫酸铝铵的重量份还可以为0.24、0.28、0.3、0.32、0.35、0.38份，硫酸铝钾的重量份还可以为0.14、0.18、0.22、0.25、0.28份，碳酸钙的重量份还可以为0.12、0.14、0.15、0.16、0.18份，硫酸锌的重量份还可以为0.24、0.28、0.3、0.32、0.35、0.38份，氯化钾的重量份还可以为0.44、0.48、0.5、0.52、0.55、0.58份，氢氧化钠的重量份还可以为0.15、0.2、0.25、0.3、0.35份，壳聚糖的重量份还可以为0.45、0.5、0.55、0.6、0.65、0.7份，苯甲酸钠的重量份还可以为0.64、0.68、0.72、0.75、0.78份，渗透剂JFC的重量份还可以为0.24、0.28、0.3、0.32、0.35、0.38份，聚乙烯醇的重量份还可以为0.25、0.3、0.35、0.4、0.45份，丙二醇的重量份还可以为0.25、0.3、0.35、0.4、0.45份，儿茶素的重量份还可以为0.14、0.18、0.22、0.25、0.28份，烷基糖苷的重量份还可以为0.7、0.8、0.85、0.9、1、1.1份，羟甲基纤维素的重量份还可以为0.24、0.28、0.3、0.32、0.35、0.38份，丙二醇甲醚醋酸酯的重量份还可以为0.25、0.3、0.35、0.4、0.45份，三聚磷酸钾的重量份还可以为0.14、0.18、0.2、0.22、0.25、0.28份，聚丙烯酸酯的重量份还可以为0.24、0.28、0.3、0.32、0.35、0.38份，苯甲酸乙酯的重量份还可以为0.24、0.28、0.3、0.32、0.35、0.38份，环氧大豆油的重量份还可以为0.7、0.8、1、1.2、1.3、1.4份，钛酸四丁酯的重量份还可以为0.25、0.3、0.35、0.4、0.5份，去离子水的重量份还可以为55、60、65、70、75份。
优选地，其原料按重量份包括：天然染料14-17份、铬黄1.1-1.4份、滑石粉0.6-0.9份、稀土0.6-0.9份、硫酸铝铵0.25-0.35份、硫酸铝钾0.15-0.25份、碳酸钙0.12-0.18份、硫酸锌0.25-0.35份、氯化钾0.45-0.55份、氢氧化钠0.2-0.3份、壳聚糖0.5-0.7份、苯甲酸钠0.65-0.75份、渗透剂JFC0.25-0.35份、聚乙烯醇0.3-0.4份、丙二醇0.5-0.7份、儿茶素0.04-0.08份、烷基糖苷0.7-1.1份、羟甲基纤维素0.25-0.35份、丙二醇甲醚醋酸酯0.3-0.4份、三聚磷酸钾0.15-0.25份、聚丙烯酸酯0.25-0.35份、苯甲酸乙酯0.25-0.35份、环氧大豆油0.8-1.2份、钛酸四丁酯0.3-0.5份、去离子水60-70份。
优选地，天然染料按以下工艺进行制备：
S1、将大黄和芒果核清洗，晒干，粉碎，然后加入溶剂A提取2-4次，合并提取液得到物料B；
S2、将香蕉皮粉碎后与玉米粉混合，加入溶剂C，微波处理，抽滤，浓缩，得到物料D；
S3、将物料B、物料D与姜黄素混合，得到天然染料。
优选地，S1中，大黄、芒果核与溶剂A之间的重量比为1-3:2-5:25-30。
优选地，S1中，溶剂A为体积分数为55-62％的乙醇水溶液。
优选地，S1中，提取温度为82-90℃，提取时间为30-40min。
优选地，S2中，香蕉皮、玉米粉、溶剂C之间的重量比为1-2:2-4:25-30。
优选地，S2中，溶剂C为体积分数为72-80％的乙醇水溶液。
优选地，S2中，微波处理过程中工艺参数如下：微波功率为300-350W，微波时间为7-13min。
优选地，S3中，物料B、物料D、姜黄素之间的重量比为6-10:3-5:1-1.5。
本发明制品采用常规制备工艺制得。
本发明中提出的一种猪鬃用染色剂中，天然染料通过优化制备工艺，有效提取大黄、芒果核、香蕉皮与玉米粉中的色素，与姜黄素混合，得到的天然染料绿色环保，生物降解性好，具有良好的抗菌、防紫外线等功能，加入本发明制品中，染色效果明显，色彩鲜艳，与铬黄、滑石粉、稀土、硫酸铝铵、硫酸铝钾、碳酸钙、硫酸锌、氯化钾、氢氧化钠、壳聚糖、苯甲酸钠、渗透剂JFC、聚乙烯醇、丙二醇、儿茶素、烷基糖苷、羟甲基纤维素、丙二醇甲醚醋酸酯、三聚磷酸钾、聚丙烯酸酯、苯甲酸乙酯、环氧大豆油、钛酸四丁酯和去离子水配合，具有协同作用，对猪鬃具有良好的润湿及疏通毛孔等作用，有效改善猪鬃表面活性，渗透效果好，染色深，上染率高，上色均匀，色牢度好，有效改善猪鬃耐磨性、耐光性、耐温性，且有效提高猪鬃弹性、柔韧性等力学性能，综合提高了猪鬃质量，有效延长猪鬃制品的使用寿命。
具体实施方式
下面，通过具体实施例对本发明的技术方案进行详细说明。
实施例1
本发明提出的一种猪鬃用染色剂，其原料按重量份包括：天然染料12份、铬黄1.5份、滑石粉0.5份、稀土1份、硫酸铝铵0.2份、硫酸铝钾0.3份、碳酸钙0.1份、硫酸锌0.4份、氯化钾0.4份、氢氧化钠0.4份、壳聚糖0.4份、苯甲酸钠0.8份、渗透剂JFC 0.2份、聚乙烯醇0.5份、丙二醇0.4份、儿茶素0.1份、烷基糖苷0.6份、羟甲基纤维素0.4份、丙二醇甲醚醋酸酯0.2份、三聚磷酸钾0.3份、聚丙烯酸酯0.2份、苯甲酸乙酯0.4份、环氧大豆油0.6份、钛酸四丁酯0.6份、去离子水50份。
实施例2
本发明提出的一种猪鬃用染色剂，其原料按重量份包括：天然染料18份、铬黄1份、滑石粉1份、稀土0.5份、硫酸铝铵0.4份、硫酸铝钾0.1份、碳酸钙0.2份、硫酸锌0.2份、氯化钾0.6份、氢氧化钠0.1份、壳聚糖0.8份、苯甲酸钠0.6份、渗透剂JFC 0.4份、聚乙烯醇0.2份、丙二醇0.8份、儿茶素0.02份、烷基糖苷1.2份、羟甲基纤维素0.2份、丙二醇甲醚醋酸酯0.5份、三聚磷酸钾0.1份、聚丙烯酸酯0.4份、苯甲酸乙酯0.2份、环氧大豆油1.5份、钛酸四丁酯0.2份、去离子水80份。
其中，天然染料按以下工艺进行制备：
S1、将大黄和芒果核清洗，晒干，粉碎，然后加入溶剂A提取2次，合并提取液得到物料B；
S2、将香蕉皮粉碎后与玉米粉混合，加入溶剂C，微波处理，抽滤，浓缩，得到物料D；
S3、将物料B、物料D与姜黄素混合，得到天然染料。
实施例3
本发明提出的一种猪鬃用染色剂，其原料按重量份包括：天然染料14.5份、铬黄1.25份、滑石粉0.8份、稀土0.75份、硫酸铝铵0.32份、硫酸铝钾0.22份、碳酸钙0.15份、硫酸锌0.3份、氯化钾0.52份、氢氧化钠0.25份、壳聚糖0.62份、苯甲酸钠0.7份、渗透剂JFC 0.3份、聚乙烯醇0.35份、丙二醇0.6份、儿茶素0.06份、烷基糖苷1份、羟甲基纤维素0.32份、丙二醇甲醚醋酸酯0.35份、三聚磷酸钾0.22份、聚丙烯酸酯0.3份、苯甲酸乙酯0.3份、环氧大豆油1份、钛酸四丁酯0.4份、去离子水70份。
其中，天然染料按以下工艺进行制备：
S1、将大黄和芒果核清洗，晒干，粉碎，然后加入溶剂A提取3次，合并提取液得到物料B；其中，大黄、芒果核与溶剂A之间的重量比为2:3:28；溶剂A为体积分数为60％的乙醇水溶液；提取温度为85℃，提取时间为35min；
S2、将香蕉皮粉碎后与玉米粉混合，加入溶剂C，微波处理，抽滤，浓缩，得到物料D；其中，香蕉皮、玉米粉、溶剂C之间的重量比为1.5:3:28；溶剂C为体积分数为75％的乙醇水溶液；微波处理过程中工艺参数如下：微波功率为320W，微波时间为10min；
S3、将物料B、物料D与姜黄素以重量比为8:4:1.2混合，得到天然染料。
实施例4
本发明提出的一种猪鬃用染色剂，其原料按重量份包括：天然染料13.5份、铬黄1.25份、滑石粉0.6份、稀土0.65份、硫酸铝铵0.25份、硫酸铝钾0.15份、碳酸钙0.12份、硫酸锌0.25份、氯化钾0.45份、氢氧化钠0.2份、壳聚糖0.55份、苯甲酸钠0.65份、渗透剂JFC0.25份、聚乙烯醇0.25份、丙二醇0.45份、儿茶素0.04份、烷基糖苷0.75份、羟甲基纤维素0.25份、丙二醇甲醚醋酸酯0.25份、三聚磷酸钾0.15份、聚丙烯酸酯0.25份、苯甲酸乙酯0.25份、环氧大豆油0.75份、钛酸四丁酯0.3份、去离子水60份。
其中，天然染料按以下工艺进行制备：
S1、将大黄和芒果核清洗，晒干，粉碎，然后加入溶剂A提取4次，合并提取液得到物料B；其中，大黄、芒果核与溶剂A之间的重量比为3:5:30；溶剂A为体积分数为62％的乙醇水溶液；提取温度为90℃，提取时间为30min；
S2、将香蕉皮粉碎后与玉米粉混合，加入溶剂C，微波处理，抽滤，浓缩，得到物料D；其中，香蕉皮、玉米粉、溶剂C之间的重量比为2:4:30；溶剂C为体积分数为80％的乙醇水溶液；微波处理过程中工艺参数如下：微波功率为350W，微波时间为7min；
S3、将物料B、物料D与姜黄素以重量比为10:5:1.5混合，得到天然染料。
实施例5
本发明提出的一种猪鬃用染色剂，其原料按重量份包括：天然染料16.5份、铬黄1.4份、滑石粉0.85份、稀土0.8份、硫酸铝铵0.35份、硫酸铝钾0.25份、碳酸钙0.18份、硫酸锌0.35份、氯化钾0.5份、氢氧化钠0.3份、壳聚糖0.7份、苯甲酸钠0.75份、渗透剂JFC 0.35份、聚乙烯醇0.4份、丙二醇0.7份、儿茶素0.08份、烷基糖苷1份、羟甲基纤维素0.35份、丙二醇甲醚醋酸酯0.45份、三聚磷酸钾0.25份、聚丙烯酸酯0.34份、苯甲酸乙酯0.35份、环氧大豆油1.4份、钛酸四丁酯0.5份、去离子水70份。
其中，天然染料按以下工艺进行制备：
S1、将大黄和芒果核清洗，晒干，粉碎，然后加入溶剂A提取2次，合并提取液得到物料B；其中，大黄、芒果核与溶剂A之间的重量比为1:2:25；溶剂A为体积分数为55％的乙醇水溶液；提取温度为82℃，提取时间为40min；
S2、将香蕉皮粉碎后与玉米粉混合，加入溶剂C，微波处理，抽滤，浓缩，得到物料D；其中，香蕉皮、玉米粉、溶剂C之间的重量比为1:2:25；溶剂C为体积分数为72％的乙醇水溶液；微波处理过程中工艺参数如下：微波功率为300W，微波时间为13min；
S3、将物料B、物料D与姜黄素以重量比为6:3:1混合，得到天然染料。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。

Claims (10)

1.一种猪鬃用染色剂，其特征在于，其原料按重量份包括：天然染料12-18份、铬黄1-1.5份、滑石粉0.5-1份、稀土0.5-1份、硫酸铝铵0.2-0.4份、硫酸铝钾0.1-0.3份、碳酸钙0.1-0.2份、硫酸锌0.2-0.4份、氯化钾0.4-0.6份、氢氧化钠0.1-0.4份、壳聚糖0.4-0.8份、苯甲酸钠0.6-0.8份、渗透剂JFC 0.2-0.4份、聚乙烯醇0.2-0.5份、丙二醇0.4-0.8份、儿茶素0.02-0.1份、烷基糖苷0.6-1.2份、羟甲基纤维素0.2-0.4份、丙二醇甲醚醋酸酯0.2-0.5份、三聚磷酸钾0.1-0.3份、聚丙烯酸酯0.2-0.4份、苯甲酸乙酯0.2-0.4份、环氧大豆油0.6-1.5份、钛酸四丁酯0.2-0.6份、去离子水50-80份。
2.根据权利要求1所述猪鬃用染色剂，其特征在于，其原料按重量份包括：天然染料14-17份、铬黄1.1-1.4份、滑石粉0.6-0.9份、稀土0.6-0.9份、硫酸铝铵0.25-0.35份、硫酸铝钾0.15-0.25份、碳酸钙0.12-0.18份、硫酸锌0.25-0.35份、氯化钾0.45-0.55份、氢氧化钠0.2-0.3份、壳聚糖0.5-0.7份、苯甲酸钠0.65-0.75份、渗透剂JFC 0.25-0.35份、聚乙烯醇0.3-0.4份、丙二醇0.5-0.7份、儿茶素0.04-0.08份、烷基糖苷0.7-1.1份、羟甲基纤维素0.25-0.35份、丙二醇甲醚醋酸酯0.3-0.4份、三聚磷酸钾0.15-0.25份、聚丙烯酸酯0.25-0.35份、苯甲酸乙酯0.25-0.35份、环氧大豆油0.8-1.2份、钛酸四丁酯0.3-0.5份、去离子水60-70份。
3.根据权利要求1或2所述猪鬃用染色剂，其特征在于，天然染料按以下工艺进行制备：
S1、将大黄和芒果核清洗，晒干，粉碎，然后加入溶剂A提取2-4次，合并提取液得到物料B；
S2、将香蕉皮粉碎后与玉米粉混合，加入溶剂C，微波处理，抽滤，浓缩，得到物料D；
S3、将物料B、物料D与姜黄素混合，得到天然染料。
4.根据权利要求1-3中任一项所述猪鬃用染色剂，其特征在于，S1中，大黄、芒果核与溶剂A之间的重量比为1-3:2-5:25-30。
5.根据权利要求1-4中任一项所述猪鬃用染色剂，其特征在于，S1中，溶剂A为体积分数为55-62％的乙醇水溶液。
6.根据权利要求1-5中任一项所述猪鬃用染色剂，其特征在于，S1中，提取温度为82-90℃，提取时间为30-40min。
7.根据权利要求1-6中任一项所述猪鬃用染色剂，其特征在于，S2中，香蕉皮、玉米粉、溶剂C之间的重量比为1-2:2-4:25-30。
8.根据权利要求1-7中任一项所述猪鬃用染色剂，其特征在于，S2中，溶剂C为体积分数为72-80％的乙醇水溶液。
9.根据权利要求1-8中任一项所述猪鬃用染色剂，其特征在于，S2中，微波处理过程中工艺参数如下：微波功率为300-350W，微波时间为7-13min。
10.根据权利要求1-9中任一项所述猪鬃用染色剂，其特征在于，S3中，物料B、物料D、姜黄素之间的重量比为6-10:3-5:1-1.5。
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111021102A (zh) * 2019-12-30 2020-04-17 珠海华大浩宏化工有限公司 一种免除硅复染助剂及其制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107177993A (zh) * 2017-07-03 2017-09-19 吴江市意胜纺织有限公司 一种添加有壳聚糖的纺织染料及其制备方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107177993A (zh) * 2017-07-03 2017-09-19 吴江市意胜纺织有限公司 一种添加有壳聚糖的纺织染料及其制备方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
何瑾馨: "《染料化学 第2版》", 31 October 2016, 中国纺织出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111021102A (zh) * 2019-12-30 2020-04-17 珠海华大浩宏化工有限公司 一种免除硅复染助剂及其制备方法

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