CN107670337B - Liquid separator and method for controlling back-pumping of liquid separator - Google Patents

Liquid separator and method for controlling back-pumping of liquid separator Download PDF

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Publication number
CN107670337B
CN107670337B CN201710875890.4A CN201710875890A CN107670337B CN 107670337 B CN107670337 B CN 107670337B CN 201710875890 A CN201710875890 A CN 201710875890A CN 107670337 B CN107670337 B CN 107670337B
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chamber
level sensor
liquid separator
liquid
tube
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CN107670337A (en
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陈悦
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Shenzhen Bluestone Environmental Protection Technology Co ltd
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Shenzhen Bluestone Environmental Protection Technology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • B01D17/0211Separation of non-miscible liquids by sedimentation with baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/28Evaporating with vapour compression
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • B01D17/0214Separation of non-miscible liquids by sedimentation with removal of one of the phases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/048Breaking emulsions by changing the state of aggregation

Abstract

The embodiment of the invention discloses a liquid separator, which comprises a shell (101), a partition plate (102) and a first porous filler (105), wherein the partition plate (102) is arranged in the shell (101) and divides the shell (101) into a first chamber (103) and a second chamber (104), the bottom of the first chamber (103) is communicated with the bottom of the second chamber (104), and the first porous filler (105) is filled at the communication position of the bottom of the first chamber (103) and the bottom of the second chamber (104). Compared with the conventional liquid separator with the same shape and size, in the liquid separator in the technical scheme, the thickness of the suspension layer formed in the first chamber is thicker because the partition plate divides the shell into two chambers, so that the separation is more conveniently realized. Meanwhile, the second chamber is almost free of oil drops and other polluting substances, so that distilled water discharged from the second chamber is cleaner, and the separation effect of the liquid separator is better.

Description

Liquid separator and method for controlling back-suction of liquid separator
Technical Field
The application relates to the field of liquid separation equipment, in particular to a liquid separator. In addition, the application also relates to an MVR evaporation system and a pumpback control method of the liquid separator.
Background
In the process of wastewater treatment, a liquid separation device is often used because the wastewater, especially industrial wastewater, has complex components and often contains pollutants such as solvents, oils and the like.
For example, in the treatment of industrial wastewater by means of MVR (Mechanical Vapor Recompression) evaporation, a small amount of solvent, oil droplets and other polluting substances are often mixed in a condensed liquid condensed in a shell side of an MVR evaporator after being evaporated and separated by the MVR evaporator. Conventionally, a liquid outlet is formed on the side wall of the MVR evaporator, the liquid outlet is communicated with a liquid separator, condensed liquid is led into the liquid separator for layering, and distilled water is discharged from the bottom of the liquid separator, so that distilled water is obtained.
The separation effect of the conventional liquid separator is relatively poor, and the effluent quality is affected, which is a problem to be solved urgently by those skilled in the art.
Disclosure of Invention
In order to solve the technical problem, the application provides a liquid separator with a better separation effect.
Specifically, in a first aspect, a liquid separator is provided, which includes a casing, a partition plate and a first porous filler, wherein the partition plate is disposed in the casing and divides the casing into a first chamber and a second chamber, the bottom of the first chamber is communicated with the bottom of the second chamber, and the first porous filler is filled in a communication part of the bottom of the first chamber and the bottom of the second chamber.
With reference to the first aspect, in a first possible implementation manner of the first aspect, a first liquid level sensor is disposed in the first chamber, a second liquid level sensor is disposed in the second chamber, and a height of the first liquid level sensor is higher than a height of the second liquid level sensor; the first chamber is also communicated with a first pumping-back pipeline and a second pumping-back pipeline, the height of a suction port of the first pumping-back pipeline is lower than that of the first liquid level sensor and higher than or equal to that of the second liquid level sensor, and the height of a suction port of the second pumping-back pipeline is lower than that of the second liquid level sensor.
With reference to the first aspect and the foregoing possible implementation manners, in a second possible implementation manner of the first aspect, the apparatus further includes an expanding pipe communicated with the first chamber, a pipe diameter of one end of the expanding pipe is greater than a pipe diameter of the other end, and the end with the larger pipe diameter is connected with the first chamber.
With reference to the first aspect and the foregoing possible implementation manners, in a second possible implementation manner of the first aspect, a first baffle is fixedly connected to the inner top of the divergent pipe, and a gap is formed between the bottom end of the first baffle and the bottom of the divergent pipe.
With reference to the first aspect and the foregoing possible implementation manners, in a fourth possible implementation manner of the first aspect, a second baffle is further fixedly connected to the top of the inside of the divergent tube, a gap is formed between the bottom end of the second baffle and the bottom of the divergent tube, and a second porous filler is filled in the divergent tube between the first baffle and the second baffle.
With reference to the first aspect and the foregoing possible implementation manners, in a fifth possible implementation manner of the first aspect, the pipe diameter of the divergent pipe gradually decreases from one end to the other end.
With reference to the first aspect and the foregoing possible implementation manners, in a sixth possible implementation manner of the first aspect, the divergent pipe includes at least one straight pipe section and at least one inclined pipe section, the straight pipe section is connected to the inclined pipe section at an interval, and a caliber of one end of the inclined pipe section is the same as a caliber of the straight pipe section connected to the inclined pipe section.
In a second aspect, there is provided an MVR evaporation system comprising an MVR evaporator, a vapor compressor, and any one of the liquid separators of the first aspect;
the tube pass of the MVR evaporator is communicated with the air inlet of the vapor compressor, the shell pass of the MVR evaporator is communicated with the air outlet of the vapor compressor, and the liquid outlet of the MVR evaporator is communicated with the first chamber of the liquid separator;
and a water intake is formed in the second chamber of the liquid separator and is communicated with the air inlet of the steam compressor.
In a third aspect, there is provided an MVR evaporation system comprising an MVR evaporator, a vapor compressor, and any one of the liquid separators of the first aspect;
the tube pass of the MVR evaporator is communicated with the air inlet of the vapor compressor, the shell pass of the MVR evaporator is communicated with the air outlet of the vapor compressor, and the liquid outlet of the MVR evaporator is communicated with the first chamber of the liquid separator;
and the first pumping-back pipeline and the second pumping-back pipeline of the liquid separator are communicated with the tube pass of the MVR evaporator.
In a fourth aspect, a method for controlling back-pumping of a liquid separator is provided, where the liquid separator includes a casing, a partition plate, and a first porous filler, the partition plate is disposed in the casing and divides the casing into a first chamber and a second chamber, the bottom of the first chamber is communicated with the bottom of the second chamber, and the first porous filler is filled in a communication part between the bottom of the first chamber and the bottom of the second chamber; a first liquid level sensor is arranged in the first chamber, a second liquid level sensor is arranged in the second chamber, and the first liquid level sensor is higher than the second liquid level sensor in arrangement height; a first pumping-back pipeline and a second pumping-back pipeline are communicated with the first chamber, the height of a pumping port of the first pumping-back pipeline is lower than that of the first liquid level sensor and higher than or equal to that of the second liquid level sensor, and the height of a pumping port of the second pumping-back pipeline is lower than that of the second liquid level sensor;
if the second liquid level sensor is triggered and the first liquid level sensor is not triggered, starting the first pumping-back pipeline;
if the first liquid level sensor and the second liquid level sensor are both triggered, starting the second pumping-back pipeline;
if the first level sensor is triggered and the second level sensor is not triggered, the first and second pumpback lines are activated.
When the liquid separator is used, liquid to be separated enters the first chamber, and part of oil drops and other polluting substances in the liquid to be separated gradually float to the liquid level of distilled water in the first chamber due to the fact that the density of the oil drops and other polluting substances is smaller than that of the distilled water, so that a suspension layer is formed. Meanwhile, the liquid to be separated enters the first porous filler, and the other part of fine oil drops and other polluting substances are gathered and enlarged in the first porous filler and gradually float on the liquid level of the distilled water in the first chamber to be converged with the original suspension layer. Due to the presence of the partition, oil drops and other polluting substances in the liquid to be separated are gathered on the surface of the distilled water in the first chamber, while the second chamber is almost free of oil drops and other polluting substances.
In the liquid separator of the present embodiment, since the partition plate divides the housing into two chambers, the thickness of the suspension layer formed in the first chamber is thicker, and thus separation is more easily achieved, compared to a conventional liquid separator of the same shape and size. Meanwhile, the second chamber is almost free of oil drops and other polluting substances, so that distilled water discharged from the second chamber is cleaner, and the separation effect of the liquid separator is better.
Drawings
In order to more clearly explain the technical solution of the present application, the drawings needed to be used in the embodiments will be briefly described below, and it is obvious to those skilled in the art that other drawings can be obtained according to the drawings without any creative effort.
FIG. 1 is a schematic structural view of a first embodiment of a liquid separator of the present application;
FIG. 2 is a schematic structural view of a second embodiment of the liquid separator of the present application;
FIG. 3 is a high level schematic diagram of the components associated with a second embodiment of the liquid separator of the present application;
FIG. 4 is a schematic view of a first state of use of a second embodiment of the liquid separator of the present application;
FIG. 5 is a schematic view of a second embodiment of a liquid separator of the present application in a second state of use;
FIG. 6 is a schematic view of a third state of use of a second embodiment of the liquid separator of the present application;
FIG. 7 is a schematic view of a first embodiment of the present invention;
FIG. 8 is a schematic structural view of a second embodiment of the present invention;
FIG. 9 is a schematic view of a third embodiment of the present invention;
fig. 10 is a schematic structural diagram of one embodiment of the MVR evaporation system of the present application.
Description of reference numerals: a liquid separator 100; a housing 101; a partition plate 102; a first chamber 103; a second chamber 104; a first porous filler 105; a first level sensor 106; the second liquid level sensor 107; a first withdrawal line 108; suction port 1081 of the first pumpback line; a second pumpback line 109; a suction port 1091 of the second pumpback line; an expander 110; one end 111 of the divergent tube; the other end 112 of the divergent tube; a first baffle 113; a second baffle 114; a second porous filler 115; a gap 116; a straight tube 117; a chute 118; a water outlet 120; a liquid inlet 130; a distilled water layer 140; a suspension layer 150; a water intake 160; an MVR evaporator 200; a tube pass 201; a shell side 202; a liquid outlet 203; a liquid inlet chamber 204; a cooling water line 300; an exhaust line 400; a vapor compressor 500; a gas-liquid separator 600; an air intake conduit 700.
Detailed Description
The following examples are given for the detailed implementation and the specific operation procedures of the present invention, but the scope of the present invention is not limited to the following examples.
In the description of the present invention and embodiments, it is to be understood that the terms "first", "second", and the like are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implying any number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature.
In the description of the present invention and the embodiments thereof, it is to be understood that the terms "upper", "lower", "top", "bottom", "inner", "outer", and the like, indicate orientations and positional relationships based on the orientations and positional relationships shown in the drawings, are only used for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the device or component parts referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention.
Referring to fig. 1, in a first embodiment of the present invention, a liquid separator is provided, which includes a housing 101, a partition plate 102 and a first porous packing 105, wherein the partition plate 102 is disposed in the housing 101 to divide the housing 101 into a first chamber 103 and a second chamber 104, the bottom of the first chamber 103 is communicated with the bottom of the second chamber 104, and the first porous packing 105 is filled at the communication position of the bottom of the first chamber 103 and the bottom of the second chamber 104.
The first porous filler 105 may be, for example, a stainless steel mesh, an asbestos mesh, or the like.
The partition plate 102 only needs to divide the housing 101 into two chambers, i.e., a left chamber and a right chamber, and the partition plate 102 may be disposed vertically, as shown in fig. 1, or disposed obliquely, which is not limited in this application.
When the liquid separator is used, the liquid to be separated can enter the first chamber 103 from the liquid inlet 130, and part of oil drops and other polluting substances in the liquid to be separated gradually float to the liquid surface of the distilled water layer 140 in the first chamber 103 due to the density of the liquid to be separated being lower than that of the distilled water, so that the suspension layer 150 is formed. Meanwhile, the liquid to be separated enters the first porous packing 105, and the other part of fine oil droplets and other polluting substances are gathered and enlarged in the first porous packing 105, and gradually float to the liquid surface of the distilled water layer 140 in the first chamber 103 to join with the original suspension layer 150. Due to the presence of the baffle 102, oil droplets and other contaminating substances in the liquid to be separated are collected on the surface of the distilled water in the first chamber 103, while the second chamber 104 is almost free of oil droplets and other contaminating substances.
In the liquid separator of the present embodiment, since the partition plate 102 divides the housing 101 into two chambers, the thickness of the suspension layer 150 formed in the first chamber 103 is thicker, and thus separation is more easily achieved, compared to a conventional liquid separator of the same shape and size. Meanwhile, there are almost no oil drops and other polluting substances in the second chamber 104, so the distilled water discharged from the second chamber 104 is cleaner and the separation effect of the liquid separator is better.
Optionally, the water outlet 120 of the liquid separator is disposed on the sidewall of the second chamber 104, and the height of the water outlet 120 is higher than the height of the bottom end of the partition plate 102, so as to ensure that the water flow passes through the whole first porous packing 105 better, and further ensure the cleanliness of the outlet water.
Optionally, referring to fig. 2, a first liquid level sensor 106 is disposed in the first chamber 103, a second liquid level sensor 107 is disposed in the second chamber 104, and a height of the first liquid level sensor 106 is higher than a height of the second liquid level sensor 107; the first chamber 103 is also connected to a first suction line 108 and a second suction line 109, the suction port 1081 of the first suction line is lower than the first level sensor 106 and higher than or equal to the second level sensor 107, and the suction port 1091 of the second suction line is lower than the second level sensor 107.
The first level sensor 106 and the second level sensor 107 described above are triggered when the liquid level reaches the respective set height.
In the embodiment, it is assumed that the height of the first liquid level sensor 106 relative to the bottom of the casing 101 is H1, the height of the second liquid level sensor 107 relative to the bottom of the casing 101 is H2, the height of the suction port 1081 of the first suction line relative to the bottom of the casing 101 is H3, and the height of the suction port 1091 of the second suction line relative to the bottom of the casing 101 is H4, as shown in fig. 3, H1 > H3 ≧ H2 > H4.
The specific height difference between the first liquid level sensor 106, the suction port 1081 of the first pumpback line, the second liquid level sensor 107 and the suction port 1091 of the second pumpback line can be determined according to actual conditions. For example, the heights of the suction ports 1081 and 1091 of the first and second evacuation lines can be adjusted to adjust the specific height difference according to the densities of different types of aerosol layers.
Since the bottoms of the first chamber 103 and the second chamber 104 are connected, the pressure at the top is the same, and therefore the pressure of the liquid in the first chamber 103 and the pressure of the liquid in the second chamber 104 are equal to each other at the bottoms. By using the U-tube density difference principle, assuming that the density of water is ρ 1, the density of suspended matter is ρ 2, the gravitational acceleration is g, the height of the distilled water layer in the first chamber 103 is Hb, the height of the suspended matter layer is Hc, and the height of the distilled water in the second chamber 104 is Ha, the pressure of the liquid can be obtained by the formula:
ρ1gHa=ρ1gHb+ρ2gHc,
namely: ρ 1Ha = ρ 1Hb + ρ 2Hc.
Ha < Hb + Hc, since the density of water is greater than the density of the suspension, i.e. p 1 > p 2.
Taking Δ H = Hb + Hc-Ha, it is clear that the value of Δ H is also greater when the thickness Hb of the suspension layer is greater.
Referring to FIG. 4, when the second level sensor 107 is activated and the first level sensor 106 is not activated, it is illustrated that the height of the distilled water layer plus the height of the suspension layer Hb + Hc in the first chamber 103 is less than H1, i.e., H1 > (Hb + Hc); while the height Ha of the distilled water layer in the second chamber 104 is equal to H2, i.e. H2= Ha. Therefore, (H1-H2) > (Hb + Hc-Ha) = Δ H. It can be seen that at this time, the thickness of the suspension layer in the first chamber 103 is relatively thin, the first pumping-back line 108 is activated, and since H1 > H3 ≧ H2, the first pumping-back line 108 can pump back the liquid layer whose height is greater than or equal to H3.
Referring to fig. 5, when the first liquid level sensor 106 and the second liquid level sensor 107 are triggered simultaneously, it is illustrated that the height of the distilled water layer in the first chamber 103 plus the height Hb + Hc of the suspension layer is equal to H1, i.e., (Hb + Hc) = H1; meanwhile, the height Ha of the distilled water layer in the second chamber 104 is equal to H2, that is, ha = H2. Thus, Δ H = (H1-H2). It can be seen that, at this time, the thickness of the suspension layer in the first chamber 103 is relatively thick, the second evacuation line 109 can be activated, and since H1 > H4, the second evacuation line 109 can evacuate liquid layers having a height higher than and equal to H4.
Referring to fig. 6, when the first liquid level sensor 106 is triggered and the second liquid level sensor 107 is not triggered, it is illustrated that the height of the distilled water layer in the first chamber 103 plus the height Hb + Hc of the suspension layer is equal to H1, i.e., (Hb + Hc) = H1; meanwhile, the height Ha of the distilled water layer in the second chamber 104 is less than H2, i.e., ha < H2. Therefore,. DELTA.h > (H1-H2). It can be seen that at this point, the layer of suspension in the first chamber 103 is relatively thick, and the second evacuation line 109 can be activated, so that the liquid layer having a height greater than or equal to H4 can be evacuated back, since H1 > H4. Preferably, the first and second evacuation lines 108 and 109 can be activated at the same time to evacuate the liquid layer with a height higher than or equal to H4 more quickly, further reducing the risk of volatile substances in the suspension layer volatilizing into gas and being discharged into the atmosphere, and further reducing the risk of remixing of the suspension layer with distilled water.
By adopting the liquid separator in this embodiment, the suspended matter in the first chamber 103 can be pumped back, on one hand, volatile substances in the suspended matter layer can be prevented from being emitted into gas, and the exhaust system can cause pollution to the atmosphere; on the other hand, the method avoids the polluting substances in the suspension layer from staying in the liquid separator for a long time and mixing with the distilled water again to form a mixture which is difficult to separate, and the quality of the distilled water discharged from the liquid separator is influenced. Meanwhile, by adopting the liquid separator in this embodiment, distilled water separated from the condensed liquid can be pumped back as little as possible while the suspension layer is pumped back, improving the treatment efficiency of the liquid separator.
Optionally, referring to fig. 7 to 9, the liquid separator further includes an expanding pipe 110 communicated with the first chamber 103 and used for introducing the liquid to be separated, a pipe diameter of one end 111 of the expanding pipe is larger than that of the other end 112, and the end 111 with the larger pipe diameter is connected with the first chamber 103.
In use, the liquid to be separated may have already been subjected to separation by other separation means before being passed to the liquid separator. For example, in an MVR evaporation system, referring to fig. 10, the liquid separator 100 may be in communication with the liquid outlet 203 of the MVR evaporator 200. The liquid to be separated is firstly subjected to evaporation separation by the MVR evaporator 200, so that most of the polluting substances such as solvents, oils and the like are separated from the water, and a small amount of the polluting substances such as volatile substances, oil droplets and the like are released heat and condensed in the shell pass 202 of the MVR evaporator 200 and then enter the liquid separator 100 together with distilled water through the liquid outlet 203 of the MVR evaporator. At this moment, adopt divergent pipe 110 to connect MVR evaporimeter liquid outlet 203 and first cavity 103, can let and keep the natural gentle flow under the effect of gravity from waiting to separate and enter into first cavity 103 and separate to avoid the disturbance that rapid flow caused, make distilled water and polluting substances mix, and then be favorable to liquid separator's separation.
Alternatively, the height of the second liquid level sensor 107 may be equal to the lowest point where the divergent pipe 110 and the first chamber 103 communicate with each other, or slightly lower than the height of the divergent pipe 110 at the interface with the first chamber 103. The first level sensor 106 may be positioned at a height slightly greater than the height of the second level sensor 107.
Alternatively, referring to fig. 8, the diverging pipe 110 may be a inclined pipe 118 whose pipe diameter gradually decreases from one end 111 to the other end 112. The inclined pipe in the embodiment of the application refers to a pipeline with the pipe diameter gradually increasing or decreasing.
Referring to fig. 7 and 9, the divergent pipe 110 may further include at least one straight pipe 117 and at least one inclined pipe 118, the straight pipe 117 is connected to the inclined pipe 118 at intervals, and an aperture of one end of the inclined pipe 118 is the same as an aperture of the straight pipe 117 connected to the inclined pipe 118 adjacently. In contrast, the height of the bottom of the straight tube 117 or the inclined tube 118 relatively close to the first chamber 103 is not higher than the height of the bottom of the straight tube 117 or the inclined tube 118 relatively far from the liquid outlet 203, so that the distilled water and the polluting substances can flow under the action of gravity. The divergent tube 110 formed by connecting the straight tube 117 and the inclined tube 118 at intervals can reduce the flow rate of the distilled water and the polluting substances, so that the distilled water and the polluting substances can flow more stably and gently, further, the distilled water and the polluting substances are prevented from being mixed in the continuous acceleration flow process, the separation of a liquid separator is facilitated, and the quality of separated water is further improved.
Optionally, referring to fig. 7 to fig. 9, the first baffle 113 is fixedly connected to the top of the divergent pipe 110, and a gap 116 is formed between the bottom of the first baffle 113 and the bottom of the divergent pipe 110. A second baffle plate 114 is further fixedly connected to the top of the interior of the divergent tube 110, a gap 116 is formed between the bottom end of the second baffle plate 114 and the bottom of the divergent tube 110, and a second porous filler 115 is filled in the divergent tube between the first baffle plate 113 and the second baffle plate 114. The size of the gap 116 between the first baffle 113 and the bottom of the divergent pipe 110, the second baffle 114 and the bottom of the divergent pipe 110 can be adjusted according to practical situations, which is not limited in this application. The second porous filler 115 may be, for example, a wire mesh, organic cotton, or the like.
Referring to fig. 10, when the liquid separator is applied to an MVR evaporation system and is communicated with the liquid outlet 203 of the MVR evaporator, there may be uncondensed gas in the shell side 202 of the MVR evaporator, and most of the gas is discharged from the gas exhaust pipeline 400, but a small part of the gas enters the divergent pipe 110 through the liquid outlet 203 and then enters the shell 101 of the liquid separator. These gases, on the one hand, agitate the distilled water and the polluting substances which are originally in a natural, gentle flow; on the other hand, since the top of the first chamber 103 and the top of the second chamber 104 are also connected in a normal condition, volatile gas and fine oil droplets in the gas directly enter the first chamber 103 and the second chamber 104 to be condensed, aggregated and re-dissolved, and continuously pollute the distilled water which is originally separated in the second chamber 104.
In the present embodiment, since the bottom end of the first baffle 113 is higher than the bottom of the divergent pipe 110, a gap 116 exists between the bottom end of the first baffle 113 and the bottom of the divergent pipe 110. Distilled water and contaminants continue to flow smoothly through the diverging tube 110 and continue to flow smoothly into the liquid separator through the gap 116. The volatile gas and oil droplets in the gas in the shell side 202 are blocked to some extent by the first baffle 113, and the gas entering the liquid separator through the divergent pipe 110 is reduced, so that the risk of contamination of the distilled water in the second chamber 104 by the volatile gas and oil droplets in the gas is reduced.
Further, by arranging two baffles and filling the second porous filler 115 in the divergent pipe 110 between the baffles, fine liquid droplets in the gas are further captured by the second porous filler 115, so as to better prevent the fine liquid droplets from entering the second chamber 104, and simultaneously, the water flow flowing to the first chamber 103 through the divergent pipe 110 is more uniform and gentle.
Referring to fig. 10, in a second embodiment of the present application, an MVR evaporation system is provided, which includes an MVR evaporator 200, a vapor compressor 500, and any one of the liquid separators 100 described above, wherein a tube side 201 of the MVR evaporator is connected to an air inlet of the vapor compressor 500, a shell side 202 of the MVR evaporator is connected to an air outlet of the vapor compressor 500, and a liquid outlet 203 of the MVR evaporator is connected to the first chamber 103 of the liquid separator 100; the second chamber 104 of the liquid separator 100 is provided with a water intake 160, and the water intake 160 is communicated with an air inlet of the vapor compressor 500. Preferably, the intake port 160 opens at the bottom of the second chamber 104. The distilled water in the second chamber 104 may also exit the liquid separator 100 through a water outlet 120 disposed in a sidewall of the second chamber 104.
When in use, a gas-liquid separator 600 communicated with the tube pass 201 of the MVR evaporator can be arranged above the MVR evaporator 200 to remove most of liquid drops and foams in the vapor generated by evaporation in the tube pass 201. An exhaust pipeline 400 can be further arranged in the MVR evaporation system, and the exhaust pipeline 400 is communicated with the shell side 202 and is used for exhausting gas which is not condensed in the shell side 202. Preferably, the exhaust pipeline 400 and the air inlet pipeline 700 are respectively disposed on two opposite sides of the sidewall of the MVR evaporator 200, so that the high-quality steam entering the shell side 202 from the air inlet pipeline 700 is fully heat-exchanged with the heat exchange pipe, and then is exhausted from the exhaust pipeline 400 to enter the subsequent processing step of the gas.
In operation, the liquid to be treated enters the tube pass 201 from the liquid inlet cavity 204 at the bottom of the MVR evaporator 200, and is heated and evaporated in the tube pass 201. During the evaporation process, volatile solvent gas, pollutant gas and other pollutant gases, and oil droplets, pollutant droplets and other pollutant droplets are mixed in the water vapor, and most of the droplets and bubbles in the steam generated by evaporation in the tube pass 201 are removed through the gas-liquid separator 600. And then compressed by a vapor compressor 500 to become high quality vapor, which enters the shell side 202. The high-quality steam in the shell pass 202 exchanges heat with the liquid in the tube pass 201 to maintain the heat required by the evaporation of the liquid in the tube pass 201; meanwhile, the steam in the shell side 202 is condensed into condensate after heat exchange. The condensate enters the first chamber 103 of the liquid separator 100 through the liquid outlet 203 of the MVR evaporator and is separated into layers to remove distilled water from the second chamber 104. The water intake 160 of the liquid separator 100 is communicated with the air inlet of the vapor compressor 500 through the cooling water pipeline 300, and clean distilled water is used as cooling water to control the temperature of the vapor compressor 500, so that the condition that the vapor compressor 500 is unstable to cause the change of the working condition of the whole MVR evaporation system is prevented, and the cyclic utilization of the distilled water is realized. The water intake 160 is disposed at the bottom of the second chamber 104, so that clean distilled water can be taken out, and the cooling water can be prevented from being deficient to the greatest extent.
In addition, the MVR evaporation system has better effluent quality and higher cleaning degree, and the MVR evaporation system includes any one of the liquid separators, so the MVR evaporation system also has the beneficial effects of the liquid separator in the embodiments, and the description is omitted here.
Still referring to fig. 10, in a third embodiment of the present application, an MVR evaporation system is provided, which includes an MVR evaporator 200, a vapor compressor 500 and any of the liquid separators 100 described above, wherein a tube side 201 of the MVR evaporator is communicated with an air inlet of the vapor compressor 500, a shell side 202 of the MVR evaporator is communicated with an air outlet of the vapor compressor 500, and a liquid outlet 203 of the MVR evaporator is communicated with the first chamber 103 of the liquid separator 100; both the first withdrawal line 108 and the second withdrawal line 109 of the liquid separator 100 are in communication with the tube side 201 of the MVR evaporator.
When in use, a gas-liquid separator 600 communicated with the tube pass 201 of the MVR evaporator can be arranged above the MVR evaporator 200 to remove most of liquid drops and foams in the steam generated by evaporation in the tube pass 201. The first and second withdrawal lines 108 and 109 are both in communication with the tube side 201 of the MVR evaporator via a gas-liquid separator 600. The gas inlet of the vapor compressor 500 is also in communication with the tube side 201 of the MVR evaporator via a vapor-liquid separator 600.
During operation, the liquid to be treated is heated and evaporated in the tube pass 201, volatile solvent gas, pollutant gas and other pollutant gases, and oil droplets, pollutant droplets and other pollutant droplets are mixed in the water vapor in the evaporation process, and most of droplets and bubbles in the steam generated by evaporation in the tube pass 201 are removed through the gas-liquid separator 600. And then compressed by a vapor compressor 500 to become high quality vapor entering the shell side 202. The high-quality steam in the shell pass 202 exchanges heat with the liquid in the tube pass 201 to maintain the heat required by the evaporation of the liquid in the tube pass 201; meanwhile, the steam in the shell side 202 is condensed into condensate after heat exchange. The condensate enters the first chamber 103 of the liquid separator 100 through the liquid outlet 203 of the MVR evaporator, and is separated by layers to remove clean distilled water from the second chamber 104. The layer of suspension suspended on the surface of the liquid in the first chamber 103 is re-sucked into the tube side 201 of the MVR evaporator via the first and second evacuation lines 108, 109.
Because the tube pass 201 of the MVR evaporator is under negative pressure when the MVR evaporation system works, as long as the valves on the first and second pumping back pipelines 108 and 109 are opened, the suspension layer higher than the respective suction ports of the two pumping back pipelines will be sucked into the tube pass 201 of the MVR evaporator again, and no other power is needed to start the pumping back pipeline. Through with the suspension layer back suction tube side 201, can also prevent that the volatile substance in the suspension layer from volatilizing, prevent that the volatile gas in the liquid separator 100 from discharging MVR evaporation system, cause the pollution to the atmosphere.
In addition, the MVR evaporation system has better effluent quality and higher cleaning degree, and the MVR evaporation system includes any one of the liquid separators, so the MVR evaporation system also has the beneficial effects of the liquid separator in the embodiments, and the description is omitted here.
In a fourth embodiment of the present application, a method for controlling the back-suction of a liquid separator is provided, the liquid separator, referring to fig. 2, includes a housing 101, a partition plate 102 and a first porous packing 105, the partition plate 102 is disposed in the housing 101 to divide the housing 101 into a first chamber 103 and a second chamber 104, the bottom of the first chamber 103 is communicated with the bottom of the second chamber 104, and the first porous packing 105 is filled at the communication position of the bottom of the first chamber 103 and the bottom of the second chamber 104; a first liquid level sensor 106 is arranged in the first chamber 103, a second liquid level sensor 107 is arranged in the second chamber 104, and the first liquid level sensor 106 is arranged at a higher height than the second liquid level sensor 107; the first chamber 104 is also communicated with a first pumping-back pipeline 108 and a second pumping-back pipeline 109, the height of a pumping-out opening 1081 of the first pumping-back pipeline 108 is lower than that of the first liquid level sensor 106 and is higher than or equal to that of the second liquid level sensor 107, and the height of a pumping-out opening 1091 of the second pumping-back pipeline 109 is lower than that of the second liquid level sensor 107;
if the second level sensor 107 is triggered and the first level sensor 106 is not triggered, the first pumpback line 108 is activated;
if the first liquid level sensor 106 and the second liquid level sensor 107 are both triggered, the second pumping-back pipeline 109 is started;
if the first level sensor 106 is triggered and the second level sensor 107 is not triggered, the first and second return lines 108, 109 are activated.
Optionally, valves may be disposed on the first and second pumping lines 108 and 109, respectively, and the valves are controlled to open and close according to the trigger signals of the first and second liquid level sensors 106 and 107, respectively.
By adopting the back-pumping control method in this embodiment, the suspended matter in the first chamber 103 can be back-pumped, on one hand, volatile substances in the suspended matter layer are prevented from being emitted into gas, and the exhaust system causes pollution to the atmosphere; on the other hand, it is avoided that the contaminating substances in the suspension layer stay in the liquid separator 100 for a long time and are mixed with the distilled water again to form a mixture which is difficult to separate, and the quality of the distilled water discharged from the second chamber 104 is affected. Meanwhile, by adopting the back-pumping control method in the embodiment, the distilled water separated from the condensed liquid can be back-pumped as little as possible when the suspended matters are back-pumped, and the treatment efficiency of the liquid separator is improved.
The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions, improvements, etc. within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (9)

1. A liquid separator, which is applied to wastewater treatment, wherein the wastewater contains water and pollutant substances, the pollutant substances have lower density than the water, the liquid separator comprises a shell (101), a baffle (102) and a first porous filler (105), the baffle (102) is arranged in the shell (101) and divides the shell (101) into a first chamber (103) and a second chamber (104), the bottom of the first chamber (103) is communicated with the bottom of the second chamber (104), and the first porous filler (105) is filled at the communication part of the bottom of the first chamber (103) and the bottom of the second chamber (104); a first liquid level sensor (106) is arranged in the first chamber (103), a second liquid level sensor (107) is arranged in the second chamber (104), and the first liquid level sensor (106) is arranged at a higher height than the second liquid level sensor (107); the first chamber (103) is also communicated with a first pumping-back pipeline (108) and a second pumping-back pipeline (109), the height of a suction opening (1081) of the first pumping-back pipeline (108) is lower than that of the first liquid level sensor (106) and higher than or equal to that of the second liquid level sensor (107), and the height of a suction opening (1091) of the second pumping-back pipeline (109) is lower than that of the second liquid level sensor (107).
2. A liquid separator according to claim 1, further comprising a divergent tube (110) communicating with the first chamber (103), the divergent tube having a tube diameter larger at one end (111) than at the other end (112), and the end (111) having a larger tube diameter being connected to the first chamber (103).
3. The liquid separator according to claim 2, wherein a first baffle (113) is fixed to the inner top of the divergent tube (110), and a gap (116) is formed between the bottom end of the first baffle (113) and the bottom of the divergent tube (110).
4. The liquid separator according to claim 3, wherein a second baffle (114) is further fixed to the inner top of the divergent tube (110), a gap (116) is formed between the bottom end of the second baffle (114) and the bottom of the divergent tube (110), and a second porous filler (115) is filled in the divergent tube between the first baffle (113) and the second baffle (114).
5. A liquid separator according to any of claims 2-4, characterized in that the pipe diameter of the divergent pipe (110) decreases from one end (111) to the other end (112).
6. A liquid separator according to any one of claims 2-4, characterized in that said divergent tube (110) comprises at least one section of straight tube (117) and at least one section of inclined tube (118), said straight tube (117) is connected with said inclined tube (118) at intervals, and the caliber of one end of said inclined tube (118) is identical to the caliber of said straight tube (117) connected adjacent to it.
7. An MVR evaporation system comprising an MVR evaporator (200), a vapor compressor (500), and a liquid separator (100) according to any of claims 1 to 6;
the tube side (201) of the MVR evaporator (200) is communicated with the air inlet of the vapor compressor (500), the shell side (202) of the MVR evaporator (200) is communicated with the air outlet of the vapor compressor (500), and the liquid outlet (203) of the MVR evaporator (200) is communicated with the first chamber (103) of the liquid separator (100);
a water intake (160) is arranged on the second chamber (104) of the liquid separator (100), and the water intake (160) is communicated with the air inlet of the vapor compressor (500).
8. An MVR evaporation system, comprising an MVR evaporator (200), a vapor compressor (500), and a liquid separator (100) according to any of claims 1 to 6;
a tube pass (201) of the MVR evaporator (200) is communicated with an air inlet of the vapor compressor (500), a shell pass (202) of the MVR evaporator (200) is communicated with an air outlet of the vapor compressor (500), and an liquid outlet (203) of the MVR evaporator (200) is communicated with a first chamber (103) of the liquid separator (100);
the first drawing-back pipeline (108) and the second drawing-back pipeline (109) of the liquid separator (100) are both communicated with the tube pass (201) of the MVR evaporator (200).
9. A method for controlling the back suction of a liquid separator, which is characterized by comprising a shell (101), a baffle plate (102) and a first porous filler (105), wherein the baffle plate (102) is arranged in the shell (101) to divide the shell (101) into a first chamber (103) and a second chamber (104), the bottom of the first chamber (103) is communicated with the bottom of the second chamber (104), and the first porous filler (105) is filled at the communication part of the bottom of the first chamber (103) and the bottom of the second chamber (104); a first liquid level sensor (106) is arranged in the first chamber (103), a second liquid level sensor (107) is arranged in the second chamber (104), and the first liquid level sensor (106) is arranged at a higher height than the second liquid level sensor (107); a first pumping-back pipeline (108) and a second pumping-back pipeline (109) are communicated in the first chamber (103), the height of a suction opening (1081) of the first pumping-back pipeline (108) is lower than that of the first liquid level sensor (106) and higher than or equal to that of the second liquid level sensor (107), and the height of a suction opening (1091) of the second pumping-back pipeline (109) is lower than that of the second liquid level sensor (107);
-activating the first withdrawal line (108) if the second level sensor (107) is triggered and the first level sensor (106) is not triggered;
if the first liquid level sensor (106) and the second liquid level sensor (107) are both triggered, starting the second back-pumping pipeline (109);
-activating the first (108) and the second (109) withdrawal line if the first level sensor (106) is triggered and the second level sensor (107) is not triggered.
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