CN107653066A - A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application - Google Patents
A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application Download PDFInfo
- Publication number
- CN107653066A CN107653066A CN201710900570.XA CN201710900570A CN107653066A CN 107653066 A CN107653066 A CN 107653066A CN 201710900570 A CN201710900570 A CN 201710900570A CN 107653066 A CN107653066 A CN 107653066A
- Authority
- CN
- China
- Prior art keywords
- radix glycyrrhizae
- cigarette
- aroma component
- extracting method
- extract solution
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention relates to a kind of cigarette radix glycyrrhizae aroma component and its extracting method and application, belong to tobacco aromaticss field.The extracting method includes：After radix glycyrrhizae is crushed, the mixed solvent for adding second alcohol and water composition carries out homogenate extraction, and extract solution A is obtained after filtering；After extract solution A is concentrated, add ethanol and carry out removing impurity by means of precipitation, obtain extract solution B；After extract solution B is concentrated, add propane diols and be aged, lower clear liquid is cigarette radix glycyrrhizae aroma component.The extracting method of cigarette provided by the invention radix glycyrrhizae aroma component, tobacco aromaticss are made through homogenate extraction, concentration, removing impurity by means of precipitation, concentration, ageing process after radix glycyrrhizae crushing, the aroma component being extracted in radix glycyrrhizae of this method high degree, eliminate the miscellaneous material for influenceing cigarette smoking fragrance.Proved through cigarette smoking evaluation test, the perfuming effect of gained radix glycyrrhizae aroma component is good, reduces the excitant of cigarette smoking and miscellaneous gas, the soft fine and smooth, comfortable taste of flue gas, improves smoke perfume quality.
Description
Technical field
The invention belongs to tobacco aromaticss field, and in particular to a kind of cigarette is with radix glycyrrhizae aroma component and its extracting method and answers
With.
Background technology
Tobacco can not only produce pleasant, pleasant fragrance in combustion, can also produce some miscellaneous gas and bitterness, pungent
Taste.It is based on《Tobacco international framework pact》Implementation, low tar Less harmful cigarette by as the main flow of future world cigarette,
This will inevitably lead to cigarette odor-absorbing reduction, and fragrance is thin out.Therefore, State Tobacco Monopoly Bureau exists《It is long-term in tobacco business
Science and technology development planning outline》In propose flavouring humectation key special subjects work.Develop new with improvement cigarette taste, raising
The natural tobacco aromaticss of cigarette comfort level, it is the active demand of current tobacco industry.
Radix glycyrrhizae is one of conventional herbal species in China, rich in triterpene saponin, flavonoids, polysaccharide isoreactivity composition, tool
Invigorate the spleen and benefit qi, be clearing heat and detoxicating, expelling phlegm and arresting coughing and other effects.Based on the tobacco aromaticss of licorice existing one in tobacco industry
A little achievements in research.
Application publication number is that CN103750573A patent discloses a kind of electronic cigarette tobacco tar and preparation method thereof, the electronics
The preparation of cigarette tobacco tar includes：After radix glycyrrhizae is shredded, the edible alcohol progress refluxing extraction of addition 75~95%, then filtered,
Remove slag, obtain licorice extract；Added after licorice extract is concentrated in ordinary electronic cigarette tobacco tar, stir and get product.
The radix glycyrrhizae aroma component prepared using this kind of method, it is more to influence to aspirate the miscellaneous material of fragrance, the aspiration procedure added after cigarette
Excitant and miscellaneous gas are often brought, have impact on the flavor quality of tobacco product to a certain extent.
The content of the invention
Extracting method it is an object of the invention to provide a kind of cigarette with radix glycyrrhizae aroma component, so as to solve existing extraction side
The miscellaneous material for the radix glycyrrhizae aroma component that method obtains is more, after addition tobacco product the problem of flavor quality difference.
Second object of the present invention is to provide the cigarette radix glycyrrhizae aroma component that said extracted method obtains.
Third object of the present invention is in application of the above-mentioned cigarette of offer with radix glycyrrhizae aroma component in tobacco product.
To achieve the above object, the technical solution adopted in the present invention is：
A kind of cigarette extracting method of radix glycyrrhizae aroma component, comprises the following steps：
1) after radix glycyrrhizae is crushed, the mixed solvent for adding second alcohol and water composition carries out homogenate extraction, is extracted after filtering
Liquid A；
2) after extract solution A is concentrated, add ethanol and carry out removing impurity by means of precipitation, obtain extract solution B；
3) after extract solution B is concentrated, add propane diols and be aged, lower clear liquid is cigarette radix glycyrrhizae aroma component.
The extracting method of cigarette provided by the invention radix glycyrrhizae aroma component, through homogenate extraction, concentration, precipitation after radix glycyrrhizae crushing
Tobacco aromaticss are made in removal of impurities, concentration, ageing process, the aroma component being extracted in radix glycyrrhizae of this method high degree, eliminate
Influence the miscellaneous material of cigarette smoking fragrance.Being proved through cigarette smoking evaluation test, the perfuming effect of gained radix glycyrrhizae aroma component is good,
Reduce the excitant of cigarette smoking and miscellaneous gas, the soft fine and smooth, comfortable taste of flue gas, improve smoke perfume quality.
In step 1), the volumetric concentration of in the mixed solvent ethanol is 60~95%.Every gram of licorice raw material corresponds to mixed solvent
Addition be 6~12mL.It is preferred that above-mentioned mixed solvent and solid-liquid ratio, have more preferably extraction effect.It is it is further preferred that mixed
Bonding solvent is by edible alcohol and water by volume 7 that purity is 95%:2 mix.Every gram of licorice raw material corresponds to mixed solvent
Addition be 8mL.
In step 1), the temperature of homogenate extraction is 15~30 DEG C, and the time of homogenate extraction is 0.5~5min.Preferably, dodge
The temperature of formula extraction is 20 DEG C.Homogenate extraction is to carry out material by high speed machine shearing force and super dynamic molecule diafiltration techniques to carry
Take, it is high to the extraction efficiency of aroma component in radix glycyrrhizae under said extracted parameter, and avoid active ingredient because heated and by
Destroy.
In step 1), described be filtered into is filtered using absorbent cotton.Filtered using this kind of mode, there is more preferable adsorbing contaminant
Effect.
In step 2), extract solution A is concentrated into Baume degrees as 38~39.The concentration is to be concentrated under reduced pressure.Extract solution A is concentrated
After obtain concentrate A, the addition of ethanol is counted by 95% edible alcohol of purity, is 4 times of concentrate A volumes.
In step 2), for sedimentation overnight, it is the extract solution B to isolate supernatant to the removing impurity by means of precipitation.The sedimentation
Overnight temperature control is at 0~10 DEG C.
In step 2), under above-mentioned optimizing technology parameters, the loss of radix glycyrrhizae aroma component is lacked, and the effect of removing impurity by means of precipitation is more
It is good.
In step 3), extract solution B is concentrated into Baume degrees as 28~29.The concentration is vacuum concentration.Extract solution B is concentrated
After obtain concentrate B, the addition of propane diols is the 15%~20% of concentrate B weight.
In step 3), concentrate B is obtained after extract solution B concentrations, separatory funnel will be poured into after concentrate B and mixed with propylene glycol
It is aged, distributes lower clear liquid, discard top impurity, lower clear liquid is the radix glycyrrhizae aroma component.The time of the ageing
For 36~48h.The ageing process added by step 3) after propane diols, can further separate impurity, improve radix glycyrrhizae aroma component
Purity.
The radix glycyrrhizae aroma component that said extracted method obtains can be applied in the tobacco products such as reconstituted tobacoo, pipe tobacco.
The tobacco product of above-mentioned radix glycyrrhizae aroma component is added, flavor quality can be promoted in aspiration procedure, reduces excitant
With miscellaneous gas, sense organ comfort level is improved.
Embodiment
Embodiments of the present invention are described further with reference to specific embodiment.In following examples, food used
It is 95% with the purity of alcohol.
Embodiment 1
The extracting method of the cigarette of the present embodiment radix glycyrrhizae aroma component, using following steps：
1) radix glycyrrhizae of natural air drying is crushed, crosses 100 mesh sieves, then added extractant and carry out homogenate extraction, through absorbent cotton
Extract solution is obtained after filtering；Extractant is by edible alcohol and water by volume 7:2 are mixed, and every gram of licorice raw material is corresponding to be added
Extractant 8mL, the temperature of homogenate extraction is 20 DEG C, extraction time 4min；
2) it is 38 extract solution A to be concentrated under reduced pressure into Baume degrees, obtains concentrate A, then adds the edible wine of 4 times of volume ratios
Essence is diluted, and in 0-10 DEG C of sedimentation overnight, is poured out supernatant, is discarded lower sediment impurity, supernatant is extract solution B；Subtract
The pressure of pressure concentration is 0.9Pa, and temperature is 55 DEG C；
3) it is 29 (pressure of vacuum concentration is 0.9Pa, and temperature is 55 DEG C) extract solution B to be concentrated in vacuo into Baume degrees, is obtained
To concentrate B, the propane diols of concentrate B mass 20% is then added, separatory funnel is poured into after mixing, 48h is aged, distributes down
Clear liquid, discards top impurity, and gained lower clear liquid is radix glycyrrhizae aroma component.
Embodiment 2
The extracting method of the cigarette of the present embodiment radix glycyrrhizae aroma component, using following steps：
1) radix glycyrrhizae of natural air drying is crushed, crosses 100 mesh sieves, then added extractant and carry out homogenate extraction, through absorbent cotton
Extract solution is obtained after filtering；Extractant is mixed by edible alcohol and water, and the volumetric concentration of edible alcohol is 60%, and every gram sweet
Grassland material is corresponding to add extractant 6mL, and the temperature of homogenate extraction is 15 DEG C, extraction time 2min；
2) it is 38 extract solution A to be concentrated under reduced pressure into Baume degrees, obtains concentrate A, then adds the edible wine of 4 times of volume ratios
Essence is diluted, and in 0-10 DEG C of sedimentation overnight, is poured out supernatant, is discarded lower sediment impurity, supernatant is extract solution B；Subtract
The pressure of pressure concentration is 0.9Pa, and temperature is 55 DEG C；
3) it is 28 (pressure of vacuum concentration is 0.9Pa, and temperature is 55 DEG C) extract solution B to be concentrated in vacuo into Baume degrees, is obtained
To concentrate B, the propane diols of concentrate B mass 20% is then added, separatory funnel is poured into after mixing, 48h is aged, distributes down
Clear liquid, discards top impurity, and gained lower clear liquid is radix glycyrrhizae aroma component.
Embodiment 3
The extracting method of the cigarette of the present embodiment radix glycyrrhizae aroma component, using following steps：
1) radix glycyrrhizae of natural air drying is crushed, crosses 100 mesh sieves, then added extractant and carry out homogenate extraction, through absorbent cotton
Extract solution is obtained after filtering；Extractant is mixed by edible alcohol and water, and the volumetric concentration of edible alcohol is 75%, and every gram sweet
Grassland material is corresponding to add extractant 10mL, and the temperature of homogenate extraction is 25 DEG C, extraction time 4.5min；
2) it is 38 extract solution A to be concentrated under reduced pressure into Baume degrees, obtains concentrate A, then adds the edible wine of 4 times of volume ratios
Essence is diluted, and in 0-10 DEG C of sedimentation overnight, is poured out supernatant, is discarded lower sediment impurity, supernatant is extract solution B；Subtract
The pressure of pressure concentration is 0.9Pa, and temperature is 55 DEG C；
3) it is 29 (pressure of vacuum concentration is 0.9Pa, and temperature is 55 DEG C) extract solution B to be concentrated in vacuo into Baume degrees, is obtained
To concentrate B, the propane diols of concentrate B mass 20% is then added, separatory funnel is poured into after mixing, 48h is aged, distributes down
Clear liquid, discards top impurity, and gained lower clear liquid is radix glycyrrhizae aroma component.
Embodiment 4
The extracting method of the cigarette of the present embodiment radix glycyrrhizae aroma component, using following steps：
1) radix glycyrrhizae of natural air drying is crushed, crosses 100 mesh sieves, then added extractant and carry out homogenate extraction, through absorbent cotton
Extract solution is obtained after filtering；Extractant is mixed by edible alcohol and water, and the volumetric concentration of edible alcohol is 95%, and every gram sweet
Grassland material is corresponding to add extractant 12mL, and the temperature of homogenate extraction is 30 DEG C, extraction time 5min；
2) it is 38 extract solution A to be concentrated under reduced pressure into Baume degrees, obtains concentrate A, then adds the edible wine of 4 times of volume ratios
Essence is diluted, and in 0-10 DEG C of sedimentation overnight, is poured out supernatant, is discarded lower sediment impurity, supernatant is extract solution B；Subtract
The pressure of pressure concentration is 0.9Pa, and temperature is 55 DEG C；
3) it is 29 extract solution B to be concentrated in vacuo into Baume degrees, obtains concentrate B, then adds concentrate B mass 20%
Propane diols, separatory funnel is poured into after mixing, be aged 48h, distribute lower clear liquid, discard top impurity, gained lower clear liquid is as sweet
Careless aroma component.
Test example
The gained radix glycyrrhizae aroma component of embodiment 1 is added in pipe tobacco, volume is made by production of cigarettes process by this test example
Cigarette, cigarette smoking evaluation is then carried out, as a result as shown in table 1.
The cigarette smoking effect of the radix glycyrrhizae aroma component of the embodiment of table 1
From the Cigarette evaluation result of table 1, the cigarette for adding the radix glycyrrhizae aroma component of the present invention adds in aspiration procedure
Fragrant positive effect, reduce the excitant of cigarette smoking and miscellaneous gas, the soft fine and smooth, comfortable taste of flue gas, improve smoke perfume
Quality.
Claims (10)
1. a kind of cigarette extracting method of radix glycyrrhizae aroma component, it is characterised in that comprise the following steps：
1) after radix glycyrrhizae is crushed, the mixed solvent for adding second alcohol and water composition carries out homogenate extraction, and extract solution A is obtained after filtering；
2) after extract solution A is concentrated, add ethanol and carry out removing impurity by means of precipitation, obtain extract solution B；
3) after extract solution B is concentrated, add propane diols and be aged, lower clear liquid is cigarette radix glycyrrhizae aroma component.
2. the cigarette as claimed in claim 1 extracting method of radix glycyrrhizae aroma component, it is characterised in that in step 1), mixing is molten
The volumetric concentration of ethanol is 60~95% in agent.
3. the cigarette as claimed in claim 1 extracting method of radix glycyrrhizae aroma component, it is characterised in that flash to carry in step 1)
The temperature taken is 15~30 DEG C, and the time of homogenate extraction is 0.5~5min.
4. the cigarette as claimed in claim 1 extracting method of radix glycyrrhizae aroma component, it is characterised in that in step 2), will extract
Liquid A is concentrated into Baume degrees as 38~39.
5. the cigarette as claimed in claim 4 extracting method of radix glycyrrhizae aroma component, it is characterised in that in step 2), extract solution A
Concentrate A is obtained after concentration, the addition of ethanol is counted by 95% edible alcohol of purity, is 4 times of concentrate A volumes.
6. the cigarette as claimed in claim 1 extracting method of radix glycyrrhizae aroma component, it is characterised in that described heavy in step 2)
Removal of impurities of forming sediment is stayed overnight for sedimentation, and it is the extract solution B to isolate supernatant.
7. the cigarette as claimed in claim 1 extracting method of radix glycyrrhizae aroma component, it is characterised in that in step 3), will extract
Liquid B is concentrated into Baume degrees as 28~29.
8. the cigarette as claimed in claim 7 extracting method of radix glycyrrhizae aroma component, it is characterised in that in step 3), extract solution B
Concentrate B is obtained after concentration, the addition of propane diols is the 15%~20% of concentrate B weight.
A kind of 9. cigarette radix glycyrrhizae aroma component that extracting method as described in any one of claim 1~8 obtains.
A kind of 10. application of the cigarette with radix glycyrrhizae aroma component in tobacco product as claimed in claim 9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710900570.XA CN107653066A (en) | 2017-09-28 | 2017-09-28 | A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710900570.XA CN107653066A (en) | 2017-09-28 | 2017-09-28 | A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application |
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|---|---|
| CN107653066A true CN107653066A (en) | 2018-02-02 |
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ID=61117130
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710900570.XA Pending CN107653066A (en) | 2017-09-28 | 2017-09-28 | A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113693264A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Licorice root and mixed fruit tobacco tar and preparation method thereof |
| CN114098139A (en) * | 2021-11-18 | 2022-03-01 | 深圳市真味生物科技有限公司 | Electronic atomized liquid with rich and durable mouth feeling and preparation method thereof |
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| CN101116533A (en) * | 2007-09-04 | 2008-02-06 | 川渝中烟工业公司 | Process for reducing mixed cigarette smoke by using Chinese herbal medicine |
| CN101768514A (en) * | 2008-12-29 | 2010-07-07 | 河南省新郑金叶香料有限公司 | Alhagi sparsifolia extract and preparation method and application thereof |
| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
| CN103750573A (en) * | 2014-01-23 | 2014-04-30 | 深圳市凯神科技股份有限公司 | Electronic cigarette tobacco tar and preparation method thereof |
| CN104147093A (en) * | 2014-07-16 | 2014-11-19 | 华东理工大学 | Method for rapidly extracting licorice flavonoids at room temperature |
-
2017
- 2017-09-28 CN CN201710900570.XA patent/CN107653066A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101116533A (en) * | 2007-09-04 | 2008-02-06 | 川渝中烟工业公司 | Process for reducing mixed cigarette smoke by using Chinese herbal medicine |
| CN101768514A (en) * | 2008-12-29 | 2010-07-07 | 河南省新郑金叶香料有限公司 | Alhagi sparsifolia extract and preparation method and application thereof |
| CN101928640A (en) * | 2010-09-16 | 2010-12-29 | 无锡华海香料有限公司 | Method for extracting natural perfume and application of extract |
| CN103750573A (en) * | 2014-01-23 | 2014-04-30 | 深圳市凯神科技股份有限公司 | Electronic cigarette tobacco tar and preparation method thereof |
| CN104147093A (en) * | 2014-07-16 | 2014-11-19 | 华东理工大学 | Method for rapidly extracting licorice flavonoids at room temperature |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113693264A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Licorice root and mixed fruit tobacco tar and preparation method thereof |
| CN114098139A (en) * | 2021-11-18 | 2022-03-01 | 深圳市真味生物科技有限公司 | Electronic atomized liquid with rich and durable mouth feeling and preparation method thereof |
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