CN107625689B - Camellia oleifera fruit washing-free hair cleaning agent, preparation method and use method - Google Patents
Camellia oleifera fruit washing-free hair cleaning agent, preparation method and use method Download PDFInfo
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Abstract
The oil tea fruit washing-free hair cleaning agent is prepared from the following components in parts by mass: 40-70 parts of freshly squeezed tea fruit emulsion, 1-15 parts of caprylic/capric triglyceride, 3-5 parts of absolute ethyl alcohol, 5-8 parts of rice starch, 5-8 parts of modified corn starch, 2-5 parts of phospholipid, 0.1-0.3 part of chitosan and 0.02-0.05 part of rosemary extract. The camellia oleifera fruit no-washing hair cleaner adopts fresh camellia oleifera fruit pulp as a basic raw material, is rich in substances such as camellia oil, tea saponin, tea polysaccharide, tea protein and flavone, is compounded into the hair cleaner, has very good effects of moisturizing, moistening, resisting bacteria, cleaning and the like on hair, does not need washing, and is easier.
Description
Technical Field
The invention relates to a washing-free hair cleaning spray, in particular to a tea-oil camellia fruit washing-free hair cleaning agent.
Background
In the industrial society, dust due to various pollutions and unclean hair due to external stimuli are generated. Thus, the hair that has become unclean is washed by the shampoo, but there is also generated a side effect that the shampoo is used almost every day in the modern industrial society with the improved living standard, thereby causing damage to the hair; generally, when synthesizing the existing shampoo, the shampoo is composed by adding anionic surfactant with washing and foaming functions, nonionic surfactant with dissolving and emulsifying decomposition functions, shampoo base component formed by pH regulator, thickener, antiseptic and water, and optionally adding additives such as repairing agent, humectant, perfume, pigment, etc., especially, the surfactant content of the main component accounts for 40-50 wt% of the whole shampoo composition, and the water content accounts for 45-55 wt%; the conventional shampoo cream (shampoo composition) having the above-mentioned synthesis has a high viscosity; the method for washing hair is carried out as follows: 1) first, the hair is soaked, 2) the shampoo is applied to the hair, massaged to produce foam, 3) it is washed again with a large amount of water, and then 4) the water is wiped off with a dry towel.
However, the conventional shampoo as described above has a problem that although the hygienic state and the moisturizing state are improved, the components of the detergent contain a large amount of synthetic surfactant which is irritant to the skin and hair, and particularly, the skin and hair of a person having sensitive skin and hair are irritant, so that the skin and hair are damaged or the skin is damaged; in addition, the conventional shampoo having a high viscosity and a viscous property has a problem that the washing method using the shampoo is required to wash the hair with a large amount of water after the hair is soaked in water, the shampoo is applied to the hair, and then the hair is foamed.
Particularly, the existing shampoo has the problems that the old and the weak with inconvenient actions, the patients in hospital and the serious patients for a long time, the social disadvantaged persons such as the disabled, the maritime crews, the soldiers or the mountaineers, the indigenous travelers, the fishing or camping, the leisure travelers such as the tourists and the motorcycles, the travelers for long-time traveling, and the water-deficient areas, such as the desert areas and the cold areas, are restricted by time and places when washing hair; in particular, the washing method thereof is cumbersome, and there is a disadvantage that after the occurrence of foam, washing with a large amount of water is necessary, limiting the use by people as described above.
Therefore, there is a need for a non-washing hair-care agent.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the oil tea fruit no-washing hair-cleaning agent and the preparation method thereof. The obtained hair-washing-free hair-cleaning agent adopts fresh tea fruit pulp as a basic raw material, is rich in substances such as camellia oil, tea saponin, tea polysaccharide, tea protein, flavone and the like, is compounded into a hair-cleaning agent, and has very good effects of moisturizing, moistening, resisting bacteria, cleaning and the like on hair; does not need water washing and is easier.
The technical scheme of the invention is as follows: the oil tea fruit no-clean hair agent is prepared from, by mass, 40-70 parts of oil tea fruit emulsion, 1-15 parts of caprylic/capric triglyceride, 3-5 parts of absolute ethyl alcohol, 5-8 parts of rice starch, 5-8 parts of modified corn starch, 2-5 parts of phospholipid, 0.1-0.3 part of chitosan and 0.02-0.05 part of rosemary extract.
Preferably, the preparation process of the oil tea fruit emulsion comprises the following steps:
(1) screening: selecting fresh and plump oil tea fruits which are just picked, mechanically peeling, removing shells, and cleaning to obtain fresh tea seeds;
(2) crushing: putting the camellia seed obtained in the step (1) into a crusher to obtain camellia seed particles with the water content of 40-60%;
(3) phase separation: putting the camellia seed particles obtained in the step (2) into a juicer, and extruding to obtain solid fiber powder and milk;
(4) purifying: and (3) conveying the milk obtained in the step (3) to a reaction tank, adjusting the pH value to 2.5-4, adding acid protease, heating in a water bath to 50-60 ℃, adding a decolorizing agent after 20-30min at the temperature of 20-40 ℃, stirring for 20-30min at the stirring speed of 20-60 r/min, adding a diatomite filter aid accounting for 1-6% of the weight of the milk, and filtering through a leaf filter to obtain the clarified fresh oil-tea camellia fruit emulsion.
Preferably, the screen hole diameter of the pulverizer in the step (2) is 2-10 mm, the pulverized particles are smaller than 1 mm, and the moisture content is 40% -60%; juicing well; and when the water content is too low, water is added for spraying.
Preferably, the gap between the squeezing seams of the juicer in the step (3) is 0.1-1 mm, and solid-liquid separation is well performed.
Preferably, the weight ratio of the acidic protease to the whey in the step (4) is (0.1-4): 1000.
preferably, the acid protease in the step (4) is prepared by breeding excellent aspergillus usamii through deep fermentation.
Preferably, the decolorizing agent in the step (4) is activated carbon and clay, and the weight ratio of the activated carbon: activated clay = 1: 3 to 10, and the adsorption specific surface area is 1000m2/g-1500m2The/g or the adsorption capacity reaches 80-100%, and the weight ratio of the decoloring agent to the whey in the step (3) is (2-5): 100, respectively; the active carbon and the active clay are used together, so that the active carbon can effectively remove sensitizers and pigments by matching with protease, and active matters are well reserved.
The preparation method of the camellia oleifera fruit no-washing hair agent comprises the following preparation processes:
(1) fusing: heating the oil tea fruit emulsion to 30-50 ℃, adding caprylic/capric triglyceride, phospholipid, chitosan and rosemary extract according to the proportion, and stirring for 20-30 minutes at the stirring speed of 20-60 revolutions per minute to obtain a fusion;
(2) compounding: in the step (1), cooling to room temperature, adding the rice starch, the modified corn starch and the absolute ethyl alcohol in proportion, mixing and stirring for 20-30 minutes at a stirring speed of 20-60 revolutions per minute to obtain the camellia oleifera fruit no-washing hair agent.
Preferably, the camellia oleifera fruit no-clean hair agent can be prepared into an aerosol.
Preferably, the preparation process of the oil tea fruit washing-free hair-care agent comprises the following steps:
filling the camellia oleifera fruit non-washing hair agent into an aerosol can, introducing compressed gas, and sealing the cap, wherein the input amount of the camellia oleifera fruit non-washing hair agent is 20% -65%.
Preferably, the particle size of the rice starch and the modified corn starch is 0.5 to 5 μm.
Preferably, the compressed gas may be air, CO2、N2。
The invention has the beneficial effects that:
(1) the method has simple process steps, and is a technology for forming a stable system by fusing natural plant juice;
(2) the obtained hair-washing-free hair-cleaning agent adopts fresh tea fruit pulp as a basic raw material, is rich in substances such as camellia oil, tea saponin, tea polysaccharide, tea protein, flavone and the like, is compounded into a hair-cleaning agent, and has very good effects of moisturizing, moistening, resisting bacteria, cleaning and the like on hair;
(3) no bubble, no need of water washing and more relaxed.
The main raw materials used in the present invention are described as follows:
oil tea fruit: is the fruit of the oil tea tree, the oil tea tree is the main woody oil tree in China, is known as the "east tree", belongs to the camellia family, belongs to the evergreen small tree, and is the unique woody plant oil resource in China; the tree is 3-6 m high, the diameter at breast height can reach 24-30 cm, and the bark is smooth and grey brown; the camellia oleifera tree grows with single leaf and flower is in amphoteric white, and fruits can be ripe within 10 months of the next year after blooming for 10 months, so that the camellia oleifera tree has rare flower and fruit homologous phenomenon; the fruit is capsule, mostly elliptical and has fine hair; the seeds are mostly yellow brown, glossy and triangular; the tea-oil tree grows in a deep mountain, absorbs natural nutrients, is evergreen and has long life, and the tree age can reach more than 200 years.
The oil tea fruit no-washing hair agent: the tea cake is prepared by squeezing camellia seeds and extracting oil, and is refined through a series of processing, wherein the main component of the tea cake is tea saponin; the tea saponin is a natural nonionic surfactant with excellent performance, not only has good active effects of emulsification, foaming, dispersion, permeation, lubrication and the like, but also has pharmacological effects of diminishing inflammation, easing pain, sterilizing, relieving itching and the like, and the tea saponin has the advantages of hair loosening, smoothness, dandruff removal, itching relieving, hair blackening and the like when used for washing hair, and has the effects of cleaning and protecting hair.
Caprylic/capric triglyceride: clear to light yellow, is high-definition tasteless grease, belongs to palm oil or coconut oil derivatives, and is extracted by a thermal fractionation method; because the skin care product has compatible characteristics with human skin, the skin care product is easily absorbed by the skin, so the skin care product is also suitable for oily skin and cannot block pores; it has non-greasy texture, and can be added into cream or lotion to improve extensibility, and has effects of lubricating and softening skin; and has the function of filtering ultraviolet light; the caprylic/capric triglyceride has stable storage property, can be stored for more than 6 months after being unsealed, and has proper storage conditions such as low-temperature storage and direct sunlight prevention; caprylic/capric triglyceride can be used as base material of moisturizing factor, cosmetic stabilizer, antifreeze, and homogenizing agent; the product is listed in GB2760-96< hygienic standards for food additive use > >, and GB12493-90< classification and code > standards for food additives, has been widely applied to industries of food, medicine, cosmetics and the like and has been proved to have no irritation to human bodies.
Phospholipid: has strong emulsification, moistening and dispersion effects, and plays an important role in promoting fat metabolism in vivo, muscle growth, nervous system development, oxidation injury resistance in vivo and the like.
And (3) chitosan: the chitin is polysaccharide substance obtained by deacetylating chitin such as crab, shrimp, insect, etc., and has strong inhibiting effect on Escherichia coli, Proteus vulgaris, Bacillus subtilis, and Staphylococcus aureus.
Pure water: the pure water without ion impurities is prepared by RO reverse osmosis method, and anion and cation in water are removed by ion exchange resin as solvent and carrier.
Anhydrous ethanol: the colorless clear liquid has burning smell and easy flowing, and is easy to absorb water from air to serve as a diluting dispersant.
Rice starch: the rice starch is not only tasteless, small in particle size, uniform and fine, but also has unique physicochemical properties, including low sensitivity and digestibility, is the smallest particle in the grains, the size is between 2 mu m and 7 mu m, and the surface of the starch particle is smooth and is polygonal or polygonal; the functional properties of starch are determined by its physicochemical properties, such as mean particle size, particle size distribution, amylose to amylopectin ratio, mineral content, the complexity of starch biosynthesis giving the amylose and amylopectin molecules a natural variability, thus giving the starch granules a diversity in morphology; the size and shape of starch granules are closely related to their functional properties, processing and nutritional quality; the rice starch mainly comprises amylose, amylopectin and other trace components, and has a very good adsorption effect.
Modified corn starch: the natural corn starch with changed properties after secondary processing, which is also called modified corn starch, has super-strong oil absorption.
Rosemary extract: the product has good effects of resisting oxidation, caring skin, etc., and has effects of delaying aging by effectively improving in vivo antioxidant enzyme activity and inhibiting lipid peroxidation; in addition, rosmarinic acid and carnosic acid in the rosemary extract have strong affinity with natural organic lipids, so rosemary is often combined with organic lipids to produce a curdled product. The active ingredients of rosemary have affinity with the skin epidermis layer while having affinity with the coagulated fat, and the affinity exceeds the affinity with water, so that most of the active ingredients of rosemary can be still absorbed by the skin in the cleaning process to play the role of antioxidation.
Detailed Description
The phospholipid in the examples is soybean phospholipid.
The preparation process of the oil tea fruit emulsion in the embodiment comprises the following steps:
(1) screening: selecting fresh and plump oil tea fruits which are just picked, mechanically peeling, removing shells, and cleaning to obtain fresh tea seeds;
(2) crushing: putting the camellia seeds obtained in the step (1) into a grinder (the sieve pore size of the grinder is 4 mm) to obtain plant raw material particles (the particles are less than 1 mm), wherein the water content is 51%;
(3) phase separation: putting the camellia seed raw material particles obtained in the step (2) into a juicer (the gap between squeezing seams is 0.5 mm), and squeezing to obtain solid fiber powder and milk;
(4) purifying: conveying the milk obtained in the step (3) to a reaction tank, adjusting the pH to 3.5, adding acid protease (the acid protease is prepared by deep fermentation of excellent aspergillus usamii selected for breeding, the weight ratio of the acid protease to the filtrate 1 is 0.5: 1000), and the weight ratio of the acid protease to the milk is (0.5): 1000, heating to 55 ℃ in a water bath, and adding a decolorizing agent after 25min, wherein the decolorizing agent is activated carbon and carclazyte, and the weight ratio of the decolorizing agent to the whey is 3: 100, respectively; calculated according to the weight ratio, the activated carbon: activated clay = 1: 6, the adsorption specific surface areas are respectively 1200m2G and 1500m2At the temperature of 25 ℃, the stirring time is 25 minutes, the stirring speed is 40 revolutions per minute, 3 percent (by weight) of diatomite filter aid of the milk is added, and the clear fresh oil-tea camellia fruit emulsion is obtained by filtering through a leaf filter.
Example 1
The preparation process of the oil tea fruit no-clean hair cleaning agent comprises the following steps:
(1) fusing: heating the fresh oil tea fruit emulsion to 40 ℃, adding caprylic/capric triglyceride, phospholipid, chitosan and rosemary extract according to the proportion, and stirring for 25 minutes at the stirring speed of 40 revolutions per minute to obtain the fusion.
(2) Compounding: in the step (1), cooling to room temperature, adding the rice starch, the modified corn starch and the absolute ethyl alcohol in proportion, mixing and stirring at the stirring speed of 40 revolutions per minute for 25 minutes to obtain the oil tea fruit no-washing hair agent.
Examples 2 to 6
The preparation process conditions of the camellia oleifera fruit no-clean hair agent of the embodiments 2 to 6 are basically the same as the embodiment 1, except that the conditions of reaction raw materials, ingredient proportion, temperature, time and the like are slightly different, and are specifically listed in table 1.
TABLE 1 preparation of Camellia oleifera fruit leave-in hair cleanser of examples 1-6
The formulations of comparative example 1 and comparative example 2 were identical to example 6 except that the preparation method of the oil tea fruit emulsion was different, and the neutral protease-serrapeptase was used in comparative example 1 and the alkaline protease-subtilisin was used in comparative example 2.
Comparative example 3
The amount of camellia oleifera fruit emulsion used in the formulation of comparative example 3 was 90, and the rest was the same as in example 6.
The leave-in hair cleanser of camellia oleifera fruits obtained in examples 1-6 and comparative examples 1-3 was tested for cold and heat resistance stability, scalp allergy, moisture and cleanness.
Table 2 functional index test results of the oil tea fruit no-clean hair lotion of examples 1 to 6 and comparative examples 1 to 3
The functional index and the physicochemical index of the camellia oleifera fruit no-cleaning agent obtained in the embodiments 1 to 6 and the comparative examples 1 to 3 are tested by the following test methods:
(1) cold and heat resistance stability
According to 6.2.1 and 6.2.2 of GB/T29680.
(2) And (3) testing the degree of allergy:
the method comprises the following steps: the gauze with the thickness of four layers is cut into 8 circles with the diameter of 1cm by using a pair of scissors, 1 g of the oil tea fruit no-clean hair agent of the examples 1 to 6 and the comparative examples 1 to 3 is taken by using a steel spoon, and is coated on the circular gauze, and deionized water is used for blank comparison.
Step two: the gauze was held with forceps and placed on the anteflexion arm of the subject, fixed with tape and timed.
Step three: tearing off the adhesive tape after 48h, and immediately observing the reaction of the skin covered by the gauze; and (6) observing the result.
(3) The cleanliness test comprises the following specific steps:
uniformly coating the oil tea fruit no-clean hair cleaning agent obtained in the examples 1-6 and the comparative examples 1-3 on uncleaned hair for three days, rubbing and kneading for 10 minutes by fingers until all hairs are uniformly white, wiping off white scraps by a dry towel after two minutes, wiping the hair again by white oil absorption paper, and checking the oil absorption paper; the hair was compared without any cleansing.
(4) The test method for moistening repair and moisture retention performance is a head test, and the specific method is as follows:
the leave-in hair cleanser of camellia oleifera fruits obtained in examples 1 to 6 and comparative examples 1 to 3 was applied uniformly to rough, dry and damaged hair, and the moisturizing effect and the repairing condition were noted, and the moisturizing time was recorded until there was no moisturizing effect (-indicating almost no, + indicating good, + indicating very good). Compare coarse, dry damaged hair.
From table 2, the camellia oleifera fruit no-washing hair agent disclosed by the invention adopts fresh camellia oleifera fruit pulp as a basic raw material, is rich in substances such as camellia oil, tea saponin, tea polysaccharide, tea protein and flavone, is compounded with decontamination and repair components, can penetrate into hair, has the effects of protecting and moisturizing hair, repairing hair tips, cleaning and the like, and is free of allergy.
In addition, the oil tea fruit non-washing hair-cleansing agent obtained in examples 1 to 6 was tested for the microbial indicators and the health indicators "technical standards for cosmetic safety" (2015 edition), and the following test results were obtained as shown in table 3:
TABLE 3 microbial and hygienic indexes of the oil tea fruit no-cleaning agent obtained in examples 1 to 6
The toxicology test of the oil tea fruit detergent-free hair-care agent comprises the following steps: skin irritation test (multiple skin irritation tests).
The purpose of the test is as follows: skin irritation reactions generated after the rabbit intact skin is contacted with a test object (the camellia oleifera fruit non-washing hair agent in the embodiment of the invention) for multiple times for a long time are observed, so that a safety basis is provided for the camellia oleifera fruit non-washing hair agent in the embodiment of the invention.
The inspection basis is as follows: technical standards for cosmetic safety 2015 edition; the test method comprises the following steps: selecting 8 white New Zealand rabbits, and randomly dividing the white New Zealand rabbits into 2 groups, wherein each group comprises 4 rabbits; group A is experimental group, group B is deionized water control group; shearing hairs on two sides of a spinal column of the back of a rabbit 24 hours before a test, wherein the skin surface is not damaged in the shearing process, the hair removing range is 3cm multiplied by 3cm, the smearing area is 2.5cm multiplied by 2.5cm, a test object is the oil tea fruit non-washing hair agent for each embodiment of the invention, 0.5ml of the test object is directly smeared on one side of the spinal column of the back, 0.5ml of deionized water of a control group is smeared on the other side of the spinal column of the back, and the test object is smeared for 1 time every day and is smeared for 14 days continuously; shearing hair from the next day, and removing residual test substances by using deionized water; the results were observed after one hour and scored according to the skin irritation test table of the technical specifications for cosmetic safety (2015 edition), with the control and test areas treated the same.
And (4) evaluating the results: the average integral of each rabbit per day is calculated according to the following formula, the skin irritation intensity of the rabbits is judged according to a standard table, and other toxic effects except irritation are observed.
And (3) test results: after the test object is given with the camellia oleifera fruit non-detergent in each embodiment of the invention within the observation period of multiple skin irritation tests, no erythema and edema are seen in the rabbits; the general poisoning and death conditions are not seen, the weight of the animals is increased, and the animals have no influence on respiration, circulation, central nervous system, limb activities and the like.
And (4) test conclusion: the oil tea fruit no-clean hair cleanser provided by the embodiments of the invention has no irritation to the whole skin of a white New Zealand rabbit.
Claims (6)
1. A cleaning-free oil tea fruit hair lotion is prepared from, by mass, 40-70 parts of oil tea fruit emulsion, 1-15 parts of caprylic/capric triglyceride, 3-5 parts of absolute ethyl alcohol, 5-8 parts of rice starch, 5-8 parts of modified corn starch, 2-5 parts of phospholipid, 0.1-0.3 part of chitosan and 0.02-0.05 part of rosemary extract;
the preparation method of the fresh oil tea fruit emulsion comprises the following steps:
(1) screening: selecting fresh and plump oil tea fruits which are just picked, mechanically peeling, removing shells, and cleaning to obtain fresh tea seeds;
(2) crushing: putting the camellia seed obtained in the step (1) into a crusher to obtain camellia seed particles with the water content of 40-60%;
(3) phase separation: putting the camellia seed particles obtained in the step (2) into a juicer, and extruding to obtain solid fiber powder and milk;
(4) purifying: conveying the milk obtained in the step (3) into a reaction tank, adjusting the pH value to 2.5-4, adding acid protease, heating in a water bath to 50-60 ℃, adding a decolorizing agent after 20-30min at 20-40 ℃, stirring for 20-30min at the stirring speed of 20-60 r/min, adding a diatomite filter aid accounting for 1-6% of the weight of the milk, and filtering through a leaf filter to obtain a clarified fresh oil-tea camellia fruit emulsion;
wherein the weight ratio of the acidic protease to the whey in the step (4) is (0.1-4): 1000, parts by weight; the acid protease is prepared by breeding excellent aspergillus usamii through deep fermentation; the decolorant is active carbon and clay, and the weight ratio of the active carbon: activated clay 1: 3-10, wherein the weight ratio of the decoloring agent to the whey in the step (3) is (2-5): 100.
2. the camellia oleifera fruit no-clean hair agent according to claim 1, characterized in that the particle diameter of the rice starch and modified corn starch is 0.5-5 μm.
3. The preparation method of the camellia oleifera fruit no-wash hair agent according to claim 1, characterized by comprising the steps of:
(1) fusing: heating the oil tea fruit emulsion to 30-50 ℃, adding caprylic/capric triglyceride, phospholipid, chitosan and rosemary extract according to the proportion, and stirring for 20-30 minutes at the stirring speed of 20-60 revolutions per minute to obtain a fusion;
(2) compounding: in the step (1), cooling to room temperature, adding the rice starch, the modified corn starch and the absolute ethyl alcohol in proportion, mixing and stirring for 20-30 minutes at a stirring speed of 20-60 revolutions per minute to obtain the camellia oleifera fruit no-washing hair agent.
4. The use method of the camellia oleifera fruit no-wash hair agent according to claim 1, characterized by preparing into an aerosol.
5. The use method of the camellia oleifera fruit no-wash hair agent according to claim 4, characterized in that the preparation process of the aerosol is as follows: the oil tea fruit no-clean hair detergent is filled into an aerosol can, compressed gas is introduced, the input amount is 20-65% of the oil tea fruit no-clean hair detergent, and the cover is sealed.
6. The use method of the camellia oleifera fruit no-clean hair agent according to claim 5, characterized in that the compressed gas is air, CO2Or N2。
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