CN107550797B - Desensitized anti-inflammation moistening and repairing tea seed shower gel and preparation method thereof - Google Patents
Desensitized anti-inflammation moistening and repairing tea seed shower gel and preparation method thereof Download PDFInfo
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Abstract
45-60 parts of tea seed extracting solution, 10-30 parts of traditional Chinese medicine extracting solution, 10-15 parts of ethoxylated alkyl sodium sulfate, 1-2 parts of coconut oil fatty acid diethanolamide, 3-5 parts of cocamidopropyl betaine, 3-5 parts of alkyl glycoside, 0.5-1 part of camellia oil, 2-8 parts of glycerol, 1-2 parts of salt, 0.1-0.5 part of essence and 0.1-0.3 part of preservative; the traditional Chinese medicine extracting solution is prepared by hot extracting and filtering 3-5 parts of fructus kochiae, 3-5 parts of centella, 1-2 parts of flos caryophyllata and 90-100 parts of deionized water. The tea seed bath lotion realizes complete desensitization of tea seed extract, and has anti-inflammatory and repairing effects after being matched with natural Chinese herbal medicines and camellia oil.
Description
Technical Field
The invention relates to shower gel, in particular to desensitized anti-inflammation moistening and repairing tea seed shower gel and a preparation method thereof.
Background
Household washing and caring articles have a large share in the cosmetic market for a long time, in recent years, products adopting natural active agents and plant source raw materials are more and more in the market, consumers also more and more like purchasing the products, the currently known natural active ingredients comprise tea seed powder, Chinese honeylocust fruit and soapberry, and as a natural active agent, the tea seed powder has allergen, so that skin itch and eruption of an allergen are caused, the tea seed powder product cannot use the tea seed powder raw materials in a large amount, the allergen problem of the tea seed powder is solved, and the tea seed powder product can be better introduced into the market.
Disclosure of Invention
The invention aims to solve the problem of allergy of the existing tea seed extract and provide the desensitized anti-inflammation moisturizing repair tea seed shower gel.
The invention also aims to provide a preparation method of the desensitized anti-inflammation moistening repair tea seed shower gel.
The technical scheme of the invention is as follows:
the desensitized anti-inflammation moistening repair tea seed shower gel is prepared from the following components, by mass, 45-60 parts of a tea seed extracting solution, 10-30 parts of a traditional Chinese medicine extracting solution, 10-15 parts of ethoxylated alkyl sodium sulfate, 1-2 parts of coconut oil fatty acid diethanolamide, 3-5 parts of cocamidopropyl betaine, 3-5 parts of alkyl glycoside, 0.5-1 part of camellia oil, 2-8 parts of glycerol, 1-2 parts of table salt, 0.1-0.5 part of essence and 0.05-0.1 part of a preservative.
Preferably, the camellia oil is special-grade virgin camellia oil rich in vitamin E, squalene, camelliaside and other active substances.
The alkyl glycoside is preferably APG 0810.
The antiseptic is preferably rhizoma Ligustici Chuanxiong extract.
The traditional Chinese medicine extracting solution is prepared by heating 3-5 parts of fructus kochiae, 3-5 parts of centella asiatica, 1-2 parts of flos caryophyllata and 90 parts of deionized water to 80-90 ℃, continuously stirring for 1.5-2 hours, and filtering through a filter cloth of 200 meshes.
The tea seed extracting solution process comprises the following specific steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 30-100-mesh sieve to obtain camellia seed powder;
(4) hot extraction: mixing the camellia seed powder prepared in the step (3) with deionized water according to a mixing ratio of 1 (3-10), heating to 60-100 ℃, stirring at a speed of 20-60 r/min, stirring for 40-60 min, and adding an adsorbent, wherein the addition amount of the adsorbent is (1-2) in terms of the weight ratio of the adsorbent to the camellia seed powder: 10, heating to 60-100 ℃, stirring for 20-30 minutes at a stirring speed of 20-60 revolutions per minute, and filtering by a sedimentation centrifuge to obtain filtrate; the adsorbent is active carbon and active clay, and has an adsorption specific surface area of 1000m2/g-1500m2The/g or the adsorption capacity reaches 80-100%, and the weight ratio of the activated carbon is as follows: activated clay =1: (3-10);
(5) refining: and (4) adding 1-6% of diatomite into the filtrate obtained in the step (4), and filtering by a leaf filter to obtain a clear camellia seed extracting solution.
The preparation method of the desensitized anti-inflammation moistening repair tea seed shower gel sequentially comprises the following steps:
(1) adding Chinese herbal medicine extract, ethoxylated alkyl sodium sulfate, coconut oil fatty acid diethanolamide into the tea seed extract, and heating for dissolving;
(2) then adding the cocamidopropyl betaine and the alkyl glycoside into the mixture and stirring the mixture evenly;
(3) cooling, adding camellia oil, glycerol, essence, preservative and salt, and stirring uniformly to obtain the shower gel.
The invention has the beneficial effects that:
the obtained tea seed shower gel has good rinsing effect, and can moisturize, diminish inflammation and relieve itching.
The main raw materials used are described below:
camellia seeds: the camellia oleifera abel is a fruit of camellia oleifera abel, is a main woody oil tree in China, is known as an "east tree", belongs to camellia of the family Theaceae, belongs to a evergreen small tree, is a unique woody plant oil resource in China, is 3-6 meters high, has a breast diameter of 24-30 cm, and has a smooth and grayish brown bark. The camellia oleifera tree grows with single leaf and flower is in amphoteric white, and fruits can be ripe within 10 months of the next year after blooming for 10 months, so that the camellia oleifera tree has rare flower and fruit homologous phenomenon; the fruit is capsule, mostly elliptical and has fine hair. The seeds are mostly yellow brown, glossy and triangular; the tea-oil tree grows in a deep mountain, absorbs natural nutrients, is evergreen and has long life, and the tree age can reach more than 200 years.
Centella asiatica: herba Centellae has effects of clearing away heat and toxic materials, removing dampness, relieving swelling, nourishing, relieving inflammation, and tranquilizing; the skin softening agent can stimulate deep skin cells to replace, tighten the connecting part of the epidermis and the dermis, soften the skin, help to solve the phenomenon of skin relaxation, make the skin smooth and elastic, promote the formation of collagen in the dermis, regenerate fibrin, and reconnect to make the skin compact and smooth; can help the injured tissue to heal and compact the skin, can promote the close connection between the epidermis and the dermis, can inhibit the increase of fat cells, and can prevent skin edema and obesity; centella asiatica is suitable for various skin types, and water extract of its plumule has antibacterial and anti-inflammatory effects, and belongs to the family of dicotyledonous plants, Umbelliferae, and can be used for relieving swelling, removing toxic substance and removing abscess.
Flos caryophyllata: flos caryophylli is a common traditional Chinese medicine, is one of the traditional imported south medicines in China, and is listed in the treatise on the property of the medicine, and the modern research shows that the flos caryophylli contains volatile oil which mainly contains components such as syringoleic acid, acetyl syringoleic acid, caryophyllene, methyl n-pentanone, methyl n-heptanone, vanillin and the like, has the effects of inhibiting bacteria and expelling worms, and is used as an aromatic, spasmolytic and wind-dispelling agent.
The preparation method comprises the following steps of (1) preparing broom cypress fruit: is dry mature fruit of Kochia scoparia belonging to Chenopodiaceae, and has effects of clearing heat, promoting diuresis, dispelling pathogenic wind and relieving itching.
Ethoxylated sodium alkyl sulfate, colorless, white or light yellow viscous liquid, and alkaline anionic surfactant with typical soap smell; the detergent is easy to dissolve in water, has excellent decontamination, emulsification and foaming performances and hard water resistance, and does not damage skin due to mild washing property; widely applied to washing cosmetics such as shampoo, bath lotion, tableware detergent, compound soap and the like; it can be used as wetting agent and cleaning agent in textile industry.
The coconut oil fatty acid diethanolamide belongs to a nonionic surfactant, has no cloud point, is a yellowish to amber viscous liquid, is easy to dissolve in water, has good functions of foaming, foam stabilization, penetration decontamination, hard water resistance and the like, has a particularly obvious thickening effect when being compatible with an anionic surfactant when the anionic surfactant is acidic, and can be compatible with various surfactants.
Cocamidopropyl betaine is an amphoteric ion surfactant, has excellent stability under acidic and alkaline conditions, respectively presents positive and negative ion properties, is often used together with an anionic surfactant, a cationic surfactant and a nonionic surfactant, has good compatibility, small irritation, is easy to dissolve in water, is stable to acid and alkali, has more foams and strong detergency, has excellent thickening property, softness, performance, antistatic property and hard water resistance, and can remarkably improve the softness, conditioning and low-temperature stability of washing products.
Alkyl glycoside: synthesized by renewable resources, namely natural fatty alcohol and glucose, is a novel nonionic surfactant with comprehensive performance, has the characteristics of common nonionic and anionic surfactants, has high surface activity, good ecological safety and intermiscibility, and is a preferred 'green' functional surfactant internationally recognized.
Camellia oil: the camellia seed kernel is obtained by cleaning, air drying (at a temperature lower than 100 ℃), shelling and seed selection, and then squeezing at a temperature of 20-50 ℃, and has rich active substances, usually containing 200mg/Kg of vitamin E, 30mg/Kg of sterol and 100mg/Kg of squalene.
Glycerol: is colorless, sweet, clear and viscous liquid, has no odor and warm and sweet taste, and has good moisturizing effect.
Deionized water: means pure water from which impurities in the form of ions have been removed, and the definition of "deionization" specified by the international organization for standardization ISO/TC 147 is: "deionized water completely or incompletely removes ionic species. The water is prepared by adopting an RO reverse osmosis method, and anions and cations in the water are removed by using ion exchange resin.
Salt: the main component is NaCl, which can increase the viscosity of the prepared liquid.
Essence: regulating the smell of the finished product to make the finished product pleasant and comfortable.
And (3) ligusticum wallichii extract: the rhizoma Ligustici Chuanxiong extract has inhibitory effect on various gram-negative intestinal bacteria, such as Escherichia coli, Bacillus dysenteriae, Bacillus proteus, Pseudomonas aeruginosa, Salmonella typhi, Salmonella paratyphi and Vibrio cholerae, and has certain inhibitory effect on pathogenic dermatophyte and viruses.
Detailed Description
The alkyl glycoside used in the examples was APG 0810.
The tea seed extract used in the examples was prepared by the following process steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 30-100-mesh sieve to obtain camellia seed powder;
(4) hot extraction: mixing the camellia seed powder prepared in the step (3) with deionized water according to a mixing ratio of 1:4, heating to 70 ℃, stirring at a speed of 50 revolutions per minute, stirring for 50 minutes, and adding an adsorbent, wherein the adding amount of the adsorbent is 2:10, heating at 70 ℃, stirring for 25 minutes at a stirring speed of 40 revolutions per minute, and filtering by a sedimentation centrifuge to obtain filtrate; the adsorbent is active carbon and active clay, and the average adsorption specific surface areas are 1200m respectively2(iv)/g and 1300m2The weight ratio of activated carbon is as follows: activated clay =1: 4;
(5) refining: and (5) adding diatomite accounting for 3% of the weight of the filtrate into the filtrate obtained in the step (4), and filtering through a leaf filter to obtain a clear camellia seed extracting solution.
Performing spot test on the tea seed extract, wherein the result of the spot test is no anaphylactic reaction; the test method is as follows:
the method comprises the following steps: cutting four layers of gauze into 8 circles with the diameter of 1cm by using a pair of scissors, respectively sucking 25uL of tea seed extracting solution by using a liquid-transferring gun, dripping the tea seed extracting solution on the circular gauze, and performing blank comparison by using deionized water;
step two: clamping gauze with forceps, placing on the anteflexion arm of the subject (allergic to tea seed extractive solution), fixing with adhesive tape, and timing;
step three: after 48h the tape was removed and the gauze covered skin was immediately observed for reaction.
The traditional Chinese medicine extracting solution used in the embodiment is prepared by heating 4 parts of fructus kochiae, 4 parts of centella, 2 parts of flos caryophyllata and 90 parts of deionized water to 85 ℃, continuously stirring for 2 hours, and filtering through 200-mesh filter cloth.
Example 1
408.9 g of tea seed extract is taken and added with 300 g of Chinese herbal medicine extract, 120 g of ethoxylated alkyl sodium sulfate and 20 g of coconut oil fatty acid diethanolamide, the mixture is heated and dissolved, 50 g of cocamidopropyl betaine and 50 g of alkyl glycoside are added and stirred uniformly, after cooling, 10 g of camellia oil, 25g of glycerol, 1 g of essence, 1 g of ligusticum wallichii extract and 15 g of salt are added, and after stirring uniformly, the shower gel is obtained.
Examples 2 to 5
The preparation process conditions of the shower gel of the embodiments 2 to 5 are basically the same as the embodiment 1, except that the conditions such as the reaction raw materials, the ingredient proportion and the like are slightly different, and the conditions are specifically listed in the table 1.
TABLE 1 preparation methods of shower gels of examples 1-5 and comparative examples 1-2
Comparative example 3
Comparative example 3 the same procedure as in example 1 was repeated except that centella was removed from the test sample 1 and 6 parts of cloves were used.
Comparative example 4
Comparative example 4 the same procedure as in example 1 was repeated except that Kochia scoparia was removed from example 1 and 6 parts of Syzygium aromaticum was used.
Comparative example 5
Comparative example 5 the same procedure as in example 1 was repeated except that cloves were removed and centella was used in an amount of 6 parts based on example 1.
Comparative example 6
The difference between the comparative example 6 and the example 1 is only that the preparation method of the tea seed extracting solution is different, and the tea seed extracting solution used in the comparative example 6 is prepared by the following process steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 30-100-mesh sieve to obtain camellia seed powder;
(4) hot extraction: mixing the camellia seed powder prepared in the step (3) with deionized water according to a mixing ratio of 1:4, heating to 70 ℃, stirring at a speed of 50 revolutions per minute, stirring for 50 minutes, and adding an adsorbent, wherein the adding amount of the adsorbent is 2:10, heating at 70 ℃, stirring for 25 minutes at a stirring speed of 40 revolutions per minute, and filtering by a sedimentation centrifuge to obtain filtrate; the adsorbent is only activated carbon, and the dosage of the activated carbon is the same as the total dosage of the activated carbon and the activated clay in the example 1;
(5) refining: and (5) adding diatomite accounting for 3% of the weight of the filtrate into the filtrate obtained in the step (4), and filtering through a leaf filter to obtain a clear camellia seed extracting solution.
The shower gel obtained in examples 1 to 5 and comparative examples 1 to 6 was tested for foaming, rinsing, moisturizing, antipruritic repair.
TABLE 2 results of functional index test of bath cream obtained in examples 1 to 5 and comparative examples 1 to 6
The functional indexes and physicochemical indexes of the shower gel obtained in the examples 1 to 5 and the comparative examples 1 to 6 are as follows:
(1) the testing method of the foaming, rinsing, moistening and moisture-keeping performances is a hand skin test, and the specific method is as follows:
10mL of desensitized, anti-inflammatory, moisturizing and repairing tea seed shower gel obtained in examples 1-5 and comparative examples 1-5 and a commercially available tea seed shower gel are respectively uniformly applied to moistened hands, repeatedly massaged and rubbed, when the foam is sufficiently abundant and cannot be increased any more, the foam abundance is observed, the record is recorded (indicating almost no foam, + indicating a small amount of foam, + indicating more foam, + indicates much foam, and + indicates much foam), then the hands are washed with clean water, the time for washing is recorded until the hands are clean until the hands are not sticky, clean water beads are wiped with a clean towel, and the moisture value of the back of the hands is detected by a digital skin moisture detector after half an hour (note: the moisture value of the back of the hands is detected before the shower gel is used and recorded), and the statistical results are shown in Table 3.
TABLE 3 average score table of trial effect of desensitized anti-inflammatory, moisturizing and repairing tea seed bath lotion
From Table 3, it can be seen that the present invention has low foaming, easy cleaning, and good moisturizing effect.
The method for testing the itching relieving and repairing effect of the desensitized anti-inflammation moisturizing repair tea seed shower gel in the examples 1-5 and the comparative examples 1-6 is as follows:
20 patients with mild dermatitis were selected from the desensitized anti-inflammatory moisturizing repair tea seed bath liquids of examples 1 to 5 and comparative examples 1 to 6 and commercially available tea seed bath liquids (comparative example), and tried for one month to count the number of recovery cases, which are shown in table 4.
TABLE 4 statistics of the anti-inflammatory repair effect of tea seed bath lotion
From table 4, it can be seen that the addition of the tea seed extract and the camellia oil has a significant effect on the recovery of patients with mild dermatitis, and the effect is better after the tea seed extract and the camellia oil are matched with the Chinese herbal medicine extract.
In addition, the desensitized anti-inflammatory moisturizing and repairing tea seed bath liquids obtained in examples 1 to 5 were tested for microbiological indicators and health indicators "technical safety standards for cosmetics" (2015 edition), and the test results shown in table 5 below were obtained.
TABLE 5 microbial hygiene indicators for desensitized anti-inflammatory moisturizing repair tea seed body washes of examples 1-5
The desensitized anti-inflammation moistening repair tea seed shower gel toxicology test comprises the following steps: skin irritation test (multiple skin irritation test)
The purpose of the test is as follows: skin irritation reaction generated after the rabbit intact skin contacts with a test object (the tea seed shower gel provided by the embodiment of the invention) for multiple times for a long time is observed, so that a safety basis is provided for the desensitized anti-inflammation moistening repair tea seed shower gel provided by the embodiment of the invention.
According to the test method, 8 white New Zealand rabbits are selected and randomly divided into 2 groups of 4 rabbits, the group A is an experimental group, the group B is a deionized water control group, both sides of the back spine of a rabbit are sheared 24 hours before the test, the skin surface is not damaged in shearing, the hair removing range is 3cm × 3cm, the smearing area is 2.5cm × 2.5.5 2.5cm., the tested group is the tea seed bath lotion of each embodiment of the invention, 0.5ml of the tested substance is directly smeared on one side of the back spine, 0.5ml of deionized water of the control group is smeared on the other side of the back spine for 1 time every day, the sample is continuously smeared for 14 days, the hair is sheared from the second day, the residual tested substance is removed by deionized water, the result is observed after one hour, and the control area and the test area are graded according to a skin irritation table of the cosmetic safety technical specification (2015 year version).
And (4) evaluating the results: the average integral of each rabbit per day is calculated according to the following formula, the skin irritation intensity of the rabbits is judged according to a standard table, and other toxic effects except irritation are observed.
And (3) test results: after the test object is given with the tea seed shower gel of each embodiment of the invention in a plurality of skin irritation test observation periods, no erythema and edema are seen in the rabbits; the general poisoning and death conditions are not seen, the weight of the animals is increased, and the animals have no influence on respiration, circulation, central nervous system, limb activities and the like.
And (4) test conclusion: the desensitized anti-inflammation moistening repair tea seed shower gel provided by the embodiments of the invention has no irritation to the intact skin of a white New Zealand rabbit.
Claims (3)
1. The desensitized anti-inflammation moistening and repairing tea seed shower gel is prepared from the following components in parts by mass: 45-60 parts of tea seed extract, 10-30 parts of traditional Chinese medicine extract, 10-15 parts of ethoxylated alkyl sodium sulfate, 1-2 parts of coconut oil fatty acid diethanolamide, 3-5 parts of cocamidopropyl betaine, 3-5 parts of alkyl glycoside, 0.5-1 part of camellia oil, 2-8 parts of glycerol, 1-2 parts of salt, 0.1-0.5 part of essence and 0.1-0.3 part of preservative;
the traditional Chinese medicine extracting solution is prepared by heating 4 parts of fructus kochiae, 4 parts of centella, 2 parts of flos caryophyllata and 90 parts of deionized water to 85 ℃, continuously stirring for 2 hours, and filtering through 200-mesh filter cloth;
the tea seed extracting solution process comprises the following specific steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 30-100-mesh sieve to obtain camellia seed powder;
(4) hot extraction: mixing the camellia seed powder prepared in the step (3) with deionized water according to the mixing ratio of 1:4, heating to 70 ℃, stirring at the speed of 50 revolutions per minute, stirring for 50 minutes, adding an adsorbent, wherein the adding amount of the adsorbent is 2:10 in weight ratio to the camellia seed powder, the heating temperature is 70 ℃, the stirring time is 25 minutes, the stirring speed is 40 revolutions per minute, and filtering by a sedimentation centrifuge to obtain a filtrate; the adsorbent is activated carbon and activated clay with adsorption specific surface areas of 1200m2/g 、1300m2Per g, by weight ratio, activated carbon:activated clay =1: 4;
(5) refining: adding diatomite accounting for 3% of the weight of the filtrate into the filtrate obtained in the step (4), and filtering through a leaf filter to obtain camellia seed extracting solution;
the alkyl glycoside is APG 0810; the antiseptic is rhizoma Ligustici Chuanxiong extract.
2. The desensitized anti-inflammatory moisturizing repair tea seed body wash according to claim 1, wherein: the camellia oil is special-grade virgin camellia oil.
3. The preparation method of the desensitized anti-inflammation moisturizing repair tea seed shower gel according to claim 1, wherein the desensitized anti-inflammation moisturizing repair tea seed shower gel comprises the following steps: the method sequentially comprises the following steps:
(1) adding Chinese herbal medicine extract, ethoxylated alkyl sodium sulfate, coconut oil fatty acid diethanolamide into the tea seed extract, and heating for dissolving;
(2) then adding the cocamidopropyl betaine and the alkyl glycoside into the mixture and stirring the mixture evenly;
(3) cooling, adding camellia oil, glycerol, essence, preservative and salt, and stirring uniformly to obtain the shower gel.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434612A (en) * | 2013-11-25 | 2015-03-25 | 广西三椿生物科技有限公司 | Tea bran shower gel |
| CN105997730A (en) * | 2016-07-12 | 2016-10-12 | 林序彬 | Shower gel |
| CN106635453A (en) * | 2016-12-30 | 2017-05-10 | 湖南林之神生物科技有限公司 | Fruit and vegetable cleaning fluid containing oiltea seed extract and preparation method of fruit and vegetable cleaning fluid |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434612A (en) * | 2013-11-25 | 2015-03-25 | 广西三椿生物科技有限公司 | Tea bran shower gel |
| CN105997730A (en) * | 2016-07-12 | 2016-10-12 | 林序彬 | Shower gel |
| CN106635453A (en) * | 2016-12-30 | 2017-05-10 | 湖南林之神生物科技有限公司 | Fruit and vegetable cleaning fluid containing oiltea seed extract and preparation method of fruit and vegetable cleaning fluid |
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