CN107619720A - A kind of sweet osmanthus aromatic liquid water extracting method - Google Patents
A kind of sweet osmanthus aromatic liquid water extracting method Download PDFInfo
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- CN107619720A CN107619720A CN201710998881.4A CN201710998881A CN107619720A CN 107619720 A CN107619720 A CN 107619720A CN 201710998881 A CN201710998881 A CN 201710998881A CN 107619720 A CN107619720 A CN 107619720A
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- sweet osmanthus
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Abstract
A kind of sweet osmanthus aromatic liquid water extracting method, is carried out in the steps below：The first step, sweet osmanthus is placed in Rotary Evaporators, temperature be 50 DEG C to 66 DEG C, vacuum be that 0.10Mpa becomes a cadre to 0.12Mpa backspins and evaporates 30min to 45min, in destructive distillation, sweet osmanthus cell liquid separates out and forms steam, extract steam it is condensed after obtain condensate liquid；Second step, continue the rotation destructive distillation 55min to 65min in Rotary Evaporators in the case where temperature is 50 DEG C to 66 DEG C, vacuum is 0.10Mpa to 0.12Mpa to the sweet osmanthus after destructive distillation, in destructive distillation, sweet osmanthus cell liquid continues to separate out and formed steam, and condensate liquid is obtained after extraction steam is condensed；3rd step, repeat second step and operate 2 times to 3 times, fragrant plant sweet osmanthus cellular water is obtained after then each condensate liquid is merged.For the sweet osmanthus aromatic liquid taste of acquisition close to fresh flower flavor, retention time is more longlasting, can volume production, improve added value of product.
Description
Technical field
The present invention relates to aromatic liquid technical field, is a kind of sweet osmanthus aromatic liquid water extracting method.
Background technology
Contain plurality of active ingredients in osmanthus flowers cell liquid, there is strong fragrant smell, fragrant agent, but existing osmanthus can be done
Flower fresh flower cell water extracting method is that sweet osmanthus flower bud or osmanthus flowers are carried out under conditions of high temperature mostly, finally obtains the osmanthus of drying
Bud or sweet osmanthus（Valve）, thus lost many fragrance components and nutriment, because sweet osmanthus is thermal sensitivity fragrance
Raw material, under the steaming of high temperature, some lower boiling fragrance ingredients, which are just easily lost in, to vapor away.
The content of the invention
The invention provides a kind of sweet osmanthus aromatic liquid water extracting method, the deficiency of above-mentioned prior art is overcome.
The technical scheme is that realized by following measures：A kind of sweet osmanthus aromatic liquid water extracting method, is pressed
State step progress：
The first step, sweet osmanthus is placed in Rotary Evaporators, temperature be 50 DEG C to 66 DEG C, vacuum be 0.10Mpa extremely
0.12Mpa backspins, which are become a cadre, evaporates 30min to 45min, and in destructive distillation, sweet osmanthus cell liquid separates out and forms steam, and it is condensed to extract steam
After obtain condensate liquid；
Second step, the sweet osmanthus after destructive distillation is continued in the case where temperature is 50 DEG C to 66 DEG C, vacuum is 0.10Mpa to 0.12Mpa
Destructive distillation 55min to 65min is rotated in Rotary Evaporators, in destructive distillation, sweet osmanthus cell liquid continues to separate out and formed steam, extracts steam
Condensate liquid is obtained after condensed；
3rd step, repeat second step and operate 2 times to 3 times, fragrant plant sweet osmanthus cell is obtained after then each condensate liquid is merged
Water.
Further, the sweet osmanthus is fresh sweet osmanthus.
Further, sweet osmanthus of the sweet osmanthus for fresh sweet osmanthus after chilled, the temperature of freezing is 0 DEG C to 5 DEG C, freezing
Time is 10h to 15h.
Further, the speed of rotation of the Rotary Evaporators is 21 revs/min to 35 revs/min.
Further, the condensation is condensed with cooling tower, and the temperature of cooling tower is 14 DEG C to 17 DEG C.
Present invention has the advantages that：For the sweet osmanthus aromatic liquid taste of acquisition close to fresh flower flavor, retention time is more longlasting, can measure
Production, improve added value of product.
Embodiment
The present invention is not limited by following embodiments, can technique according to the invention scheme and actual conditions it is specific to determine
Embodiment.
A kind of sweet osmanthus aromatic liquid water extracting method, is carried out in the steps below：
The first step, sweet osmanthus is placed in Rotary Evaporators, temperature be 50 DEG C to 66 DEG C, vacuum be 0.10Mpa extremely
0.12Mpa backspins, which are become a cadre, evaporates 30min to 45min, and in destructive distillation, sweet osmanthus cell liquid separates out and forms steam, and it is condensed to extract steam
After obtain condensate liquid；Second step, to the sweet osmanthus after destructive distillation temperature be 50 DEG C to 66 DEG C, vacuum be 0.10Mpa extremely
Continue to rotate destructive distillation 55min to 65min in Rotary Evaporators under 0.12Mpa, in destructive distillation, sweet osmanthus cell liquid continues to separate out and shape
Into steam, condensate liquid is obtained after extraction steam is condensed；3rd step, repeat second step and operate 2 times to 3 times, then will be cold every time
Lime set obtains fragrant plant sweet osmanthus cellular water after merging.
The sweet osmanthus is fresh sweet osmanthus；The sweet osmanthus be fresh sweet osmanthus it is chilled after sweet osmanthus, the temperature of freezing for 0 DEG C extremely
5 DEG C, the time of freezing is 10h to 15h；The speed of rotation of the Rotary Evaporators is 21 revs/min to 35 revs/min；It is described
Condensation is condensed with cooling tower, and the temperature of cooling tower is 14 DEG C to 17 DEG C；The sweet osmanthus aromatic liquid taste that the present invention obtains approaches
Fresh flower flavor, retention time is more longlasting, can volume production, improve added value of product.
Above technical characteristic constitutes embodiments of the invention, and it has stronger adaptability and implementation result, can basis
The non-essential technical characteristic of increase and decrease is actually needed, to meet the needs of different situations.
Claims (5)
1. a kind of sweet osmanthus aromatic liquid water extracting method, is carried out in the steps below：
The first step, sweet osmanthus is placed in Rotary Evaporators, temperature be 50 DEG C to 66 DEG C, vacuum be 0.10Mpa extremely
0.12Mpa backspins, which are become a cadre, evaporates 30min to 45min, and in destructive distillation, sweet osmanthus cell liquid separates out and forms steam, and it is condensed to extract steam
After obtain condensate liquid；
Second step, the sweet osmanthus after destructive distillation is continued in the case where temperature is 50 DEG C to 66 DEG C, vacuum is 0.10Mpa to 0.12Mpa
Destructive distillation 55min to 65min is rotated in Rotary Evaporators, in destructive distillation, sweet osmanthus cell liquid continues to separate out and formed steam, extracts steam
Condensate liquid is obtained after condensed；
3rd step, repeat second step and operate 2 times to 3 times, fragrant plant sweet osmanthus cell is obtained after then each condensate liquid is merged
Water.
A kind of 2. sweet osmanthus aromatic liquid water extracting method according to claim 1, it is characterised in that：The sweet osmanthus is fresh osmanthus
Flower.
A kind of 3. sweet osmanthus aromatic liquid water extracting method according to claim 1, it is characterised in that：The sweet osmanthus is fresh sweet osmanthus
Sweet osmanthus after chilled, the temperature of freezing is 0 DEG C to 5 DEG C, and the time of freezing is 10h to 15h.
A kind of 4. sweet osmanthus aromatic liquid water extracting method according to claim 1, it is characterised in that：The rotation of the Rotary Evaporators
Rotational speed rate is 21 revs/min to 35 revs/min.
A kind of 5. sweet osmanthus aromatic liquid water extracting method according to claim 1, it is characterised in that：The condensation is entered with cooling tower
Row condensation, the temperature of cooling tower is 14 DEG C to 17 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710998881.4A CN107619720A (en) | 2017-10-24 | 2017-10-24 | A kind of sweet osmanthus aromatic liquid water extracting method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710998881.4A CN107619720A (en) | 2017-10-24 | 2017-10-24 | A kind of sweet osmanthus aromatic liquid water extracting method |
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| CN107619720A true CN107619720A (en) | 2018-01-23 |
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| CN201710998881.4A Pending CN107619720A (en) | 2017-10-24 | 2017-10-24 | A kind of sweet osmanthus aromatic liquid water extracting method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110645774A (en) * | 2019-09-26 | 2020-01-03 | 云南农业大学 | Method for producing tsaoko amomum fruits and volatile substances thereof through low-temperature vacuum dry distillation |
| WO2021027056A1 (en) * | 2019-08-13 | 2021-02-18 | 湖南艾达伦科技有限公司 | Composition having mogroside sweetness and flavor and preparation method therefor and application thereof |
| CN113456543A (en) * | 2020-03-31 | 2021-10-01 | 海南艾纳香生物科技发展股份有限公司 | Method for extracting blumea balsamifera leaf cell water and blumea balsamifera oil and application |
| CN113662994A (en) * | 2020-05-14 | 2021-11-19 | 广东省禾基生物科技有限公司 | Extraction method of peach blossom cell water and application of peach blossom cell water |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| GB232552A (en) * | 1924-04-19 | 1926-01-21 | Eugene Foray | Process for the extraction of the essential principles of plants, flowers, fruit and the like |
| CN101117614A (en) * | 2007-08-30 | 2008-02-06 | 宋永快 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
| CN106562908A (en) * | 2016-11-01 | 2017-04-19 | 新疆天然芳香农业科技有限公司 | Aromatic plant rose cell water extraction method |
-
2017
- 2017-10-24 CN CN201710998881.4A patent/CN107619720A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB232552A (en) * | 1924-04-19 | 1926-01-21 | Eugene Foray | Process for the extraction of the essential principles of plants, flowers, fruit and the like |
| CN101117614A (en) * | 2007-08-30 | 2008-02-06 | 宋永快 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
| CN106562908A (en) * | 2016-11-01 | 2017-04-19 | 新疆天然芳香农业科技有限公司 | Aromatic plant rose cell water extraction method |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021027056A1 (en) * | 2019-08-13 | 2021-02-18 | 湖南艾达伦科技有限公司 | Composition having mogroside sweetness and flavor and preparation method therefor and application thereof |
| CN110645774A (en) * | 2019-09-26 | 2020-01-03 | 云南农业大学 | Method for producing tsaoko amomum fruits and volatile substances thereof through low-temperature vacuum dry distillation |
| CN113456543A (en) * | 2020-03-31 | 2021-10-01 | 海南艾纳香生物科技发展股份有限公司 | Method for extracting blumea balsamifera leaf cell water and blumea balsamifera oil and application |
| CN113662994A (en) * | 2020-05-14 | 2021-11-19 | 广东省禾基生物科技有限公司 | Extraction method of peach blossom cell water and application of peach blossom cell water |
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