CN107557900A - The preparation of multifunctional efficient graphene functional fibre and its application method - Google Patents
The preparation of multifunctional efficient graphene functional fibre and its application method Download PDFInfo
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- CN107557900A CN107557900A CN201710782070.0A CN201710782070A CN107557900A CN 107557900 A CN107557900 A CN 107557900A CN 201710782070 A CN201710782070 A CN 201710782070A CN 107557900 A CN107557900 A CN 107557900A
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Abstract
The present invention relates to the preparation of multifunctional efficient graphene functional fibre and its application method, belong to functional fibre technical field.The preparation of multifunctional efficient graphene functional fibre of the present invention and its application method, the multifunctional efficient graphene functional fibre passes through during final finishing, weaving is combined with each other with anti-mite auxiliary agent, weaving with function additive and basic polyester fiber, formation has anti-mite property and functional terylene composite fibre, antibiotic property, uviolresistance and the static electricity resistance of the addition fiber of graphene, this method technique is simple, it is easy to streamline large-scale operation, easy control of process conditions in production process, production cost are low；A process for preparing the functional fibre come, can pass through repeatedly washing, also with good composite functional, be worth of widely use.
Description
Technical field
The present invention relates to the preparation of multifunctional efficient graphene functional fibre and its application method, belong to functional fibre skill
Art field.
Background technology
At present, as textile technology and life taste, the raising of quality, the garment material of simple function can not expire
The life requirement of sufficient people.Multifunction is the inexorable trend of costume fabric development.
The development of functional fibre is the symbol of modern fiber science progress.Functional fibre, fibre in differentiation and high-performance are fine
The technological innovation for developing into traditional textile industry of dimension, the conversion to high-tech industry creates advantage, is human lives
Horizontal raising contributes.Functional fibre refers in addition to physical and mechanical properties possessed by general fiber, also have
The tencel of certain specific function.Such as:Fiber has health care function (antibacterial, mite killing, physiotherapy and eliminate the unusual smell)
；Safeguard function (radiation proof, antistatic, uvioresistant etc.)；The wet comfortable function (heat absorption, heat release, moisture absorption, moisture releasing etc.) of heat；Doctor
Treat and environment-friendly function (biocompatibility and biological degradability).Common functional fibre, complex manufacturing technology, cost of manufacture
It is higher, and function is not firm enough possessed by fiber, and by washing twice, the function of fiber will have a greatly reduced quality, and be unfavorable for
The manufacture of functional fibre and promote the use of.
It is an object of the invention to provide the preparation of multifunctional efficient graphene functional fibre and its application method, more work(
Energy high-efficient graphite olefinic functionality fiber will be by that during final finishing, will weave with anti-mite auxiliary agent, weaving function additive and basis
Polyester fiber is combined with each other, and formation has anti-mite property and functional terylene composite fibre, and the addition fiber of graphene resists
Bacterium property, uviolresistance and static electricity resistance, this method technique is simple, is easy to streamline large-scale operation, technique in production process
Condition is easily controlled, and production cost is low；A process for preparing the functional fibre come, can pass through repeatedly washing, also has good
Composite functional, be worth of widely use.
The content of the invention
The technical solution adopted for the present invention to solve the technical problems is：The preparation of multifunctional efficient graphene functional fibre
Method, its step are：
（1）, by terylene chips and graphene master batch according to weight than 100:1-10 uniformly after mixing, is prepared into graphene terylene fibre
Dimension, graphene polyester fiber is subjected to fluffy processing, the graphene polyester fiber after fluffy processing is put into terylene mesh bag
In, every bag of weight being put into is 4-6.4 kilograms, and terylene mesh bag is placed on conveyer belt；
（2）, terylene mesh bag entered by conveyer belt in circulation solution case, circulate in solution case that weaving is helped with anti-bacteria and mite-proof functional in solution
Agent, weaving are 1-5 with the weight of function additive and water ratio:1-5:104, the temperature for circulating solution in solution case is Celsius for 50-114
Degree, soak time of the antibiotic polyester fiber in circulation solution case is 3-8 minutes；
（3）, the graphene polyester fiber that soaked is rolled 5 times repeatedly with Pneumatic pressure bar in circulation solution case, roll 1 every time
Minute, the pressure of press rods is 5 kilograms, it is adjacent roll twice between be spaced 1-2 minutes so that antibiotic polyester fiber and solution
Weight ratio be 5:0.1-1；
（4）, the terylene mesh bag that step 3 prepares be put into steam drying box bakeed, stoving temperature is that 80-124 is Celsius
Degree, the baking time is 100-138 minutes；
（5）, the fiber after baking carry out packing encapsulation, that is, be prepared into multifunctional efficient graphene functional fibre.
The preparation method of preferable described multifunctional efficient graphene functional fibre, it is characterised in that the step（2）
Middle weaving is that weaving is helped with far-infrared functional auxiliary agent, weaving with anion function auxiliary agent, weaving with function of driving mosquitoes with function additive
Agent, weaving deodorization functions auxiliary agent, weave with formaldehyde-removing antibiotic deodorization functions auxiliary agent, weaving moisture absorption sweat discharging functions auxiliary agent, spin
Knit and use cool feeling function additive, weaving accumulation of heat temperature storage heat-preserving function auxiliary agent or weaving phase-change constant-temperature function additive.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that its step is：
（1）, the multifunctional efficient graphene functional fibre for preparing claim 1 and polyester fiber, eutectic polyester fiber by
According to weight than 1：1-2：0.1-0.5 carries out uniformly mixing and unclamps combing；
（2）, according to needed for fabric grammes per square metre carry out multiple lapping in length and breadth successively, the grammes per square metre of every layer of lapping is at 15-40 grams；
（3）, then in step（2）The upper and lower surface for the Multilayer Network being paved into carries out glue spraying processing；
（4）, then after upper and lower surface glue spraying Multilayer Network be sent into baking oven in bakeed, stoving temperature be 180-188 it is Celsius
Degree so that eutectic polyester fiber melts, and the baking time is the 50-60 seconds；
（5）, it is baked after, roll coiled, that is, be prepared into multifunctional efficient graphene functional fibre flocculus.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that use multifunctional efficient stone
The fabric that black olefinic functionality fiber is prepared.
It is an object of the invention to provide the preparation of multifunctional efficient graphene functional fibre and its application method, more work(
Energy high-efficient graphite olefinic functionality fiber will be by that during final finishing, will weave with anti-mite auxiliary agent, weaving function additive and basis
Polyester fiber is combined with each other, and formation has anti-mite property and functional terylene composite fibre, and the addition fiber of graphene resists
Bacterium property, uviolresistance and static electricity resistance, this method technique is simple, is easy to streamline large-scale operation, technique in production process
Condition is easily controlled, and production cost is low；A process for preparing the functional fibre come, can pass through repeatedly washing, also has good
Composite functional, be worth of widely use.
Embodiment
Specific embodiment one：The preparation method of multifunctional efficient graphene functional fibre, its step are：
（1）, by terylene chips and graphene master batch according to weight than 100:After 1 uniformly mixes, graphene polyester fiber is prepared into,
Graphene polyester fiber is subjected to fluffy processing, the graphene polyester fiber after fluffy processing is put into terylene mesh bag,
Every bag of weight being put into is 4 kilograms, and terylene mesh bag is placed on conveyer belt；
（2）, terylene mesh bag entered by conveyer belt in circulation solution case, circulate in solution case that weaving is helped with anti-bacteria and mite-proof functional in solution
Agent, weaving are 1-5 with the weight of function additive and water ratio:1-5:104, the temperature for circulating solution in solution case is 50 degrees Celsius,
Soak time of the antibiotic polyester fiber in circulation solution case is 3-8 minutes；
（3）, the graphene polyester fiber that soaked is rolled 5 times repeatedly with Pneumatic pressure bar in circulation solution case, roll 1 every time
Minute, the pressure of press rods is 5 kilograms, it is adjacent roll twice between be spaced 1 minute so that antibiotic polyester fiber and solution
Weight ratio is 5:0.1-1；
（4）, by step（3）The terylene mesh bag prepared, which is put into steam drying box, to be bakeed, and stoving temperature is 80 degrees Celsius,
It is 100 minutes to bakee the time；
（5）, the fiber after baking carry out packing encapsulation, that is, be prepared into multifunctional efficient graphene functional fibre.
The application method of described multifunctional efficient graphene functional fibre, its step are：
（1）, the multifunctional efficient graphene functional fibre for preparing claim 1 and polyester fiber, eutectic polyester fiber by
According to weight than 1：1：0.1, which carries out uniformly mixing, unclamps combing；
（2）, according to needed for fabric grammes per square metre carry out multiple lapping in length and breadth successively, the grammes per square metre of every layer of lapping is at 15 grams；
（3）, then in step（2）The upper and lower surface for the Multilayer Network being paved into carries out glue spraying processing；
（4）, then after upper and lower surface glue spraying Multilayer Network be sent into baking oven in bakeed, stoving temperature be 180 degrees Celsius, make
The fusing of eutectic polyester fiber is obtained, it is 50 seconds to bakee the time；
（5）, it is baked after, roll coiled, that is, be prepared into multifunctional efficient graphene functional fibre flocculus.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that use multifunctional efficient stone
The fabric that black olefinic functionality fiber is prepared.
Specific embodiment two：The preparation method of multifunctional efficient graphene functional fibre, its step are：
（1）, by terylene chips and graphene master batch according to weight than 100:After 7 uniformly mix, graphene polyester fiber is prepared into,
Graphene polyester fiber is subjected to fluffy processing, the graphene polyester fiber after fluffy processing is put into terylene mesh bag,
Every bag of weight being put into is 5 kilograms, and terylene mesh bag is placed on conveyer belt；
（2）, terylene mesh bag entered by conveyer belt in circulation solution case, circulate in solution case that weaving is helped with anti-bacteria and mite-proof functional in solution
Agent, weaving are 1-5 with the weight of function additive and water ratio:1-5:104, the temperature for circulating solution in solution case is Celsius for 50-114
Degree, soak time of the antibiotic polyester fiber in circulation solution case is 3-8 minutes；
（3）, the graphene polyester fiber that soaked is rolled 5 times repeatedly with Pneumatic pressure bar in circulation solution case, roll 1 every time
Minute, the pressure of press rods is 5 kilograms, it is adjacent roll twice between be spaced 1 minute so that antibiotic polyester fiber and solution
Weight ratio is 5:0.1-1；
（4）, the terylene mesh bag that step 3 prepares be put into steam drying box bakeed, stoving temperature is 92 degrees Celsius, is dried
It is 122 minutes to roast the time；
（5）, the fiber after baking carry out packing encapsulation, that is, be prepared into multifunctional efficient graphene functional fibre.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that its step is：
（1）, the multifunctional efficient graphene functional fibre for preparing claim 1 and polyester fiber, eutectic polyester fiber by
According to weight than 1：1.6：0.35, which carries out uniformly mixing, unclamps combing；
（2）, according to needed for fabric grammes per square metre carry out multiple lapping in length and breadth successively, the grammes per square metre of every layer of lapping is at 28 grams；
（3）, then in step（2）The upper and lower surface for the Multilayer Network being paved into carries out glue spraying processing；
（4）, then after upper and lower surface glue spraying Multilayer Network be sent into baking oven in bakeed, stoving temperature be 186 degrees Celsius, make
The fusing of eutectic polyester fiber is obtained, it is 54 seconds to bakee the time；
（5）, it is baked after, roll coiled, that is, be prepared into multifunctional efficient graphene functional fibre flocculus.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that use multifunctional efficient stone
The fabric that black olefinic functionality fiber is prepared.
Specific embodiment three：The preparation method of multifunctional efficient graphene functional fibre, its step are：
（1）, by terylene chips and graphene master batch according to weight than 10:After 1 uniformly mixes, graphene polyester fiber is prepared into,
Graphene polyester fiber is subjected to fluffy processing, the graphene polyester fiber after fluffy processing is put into terylene mesh bag,
Every bag of weight being put into is 6.4 kilograms, and terylene mesh bag is placed on conveyer belt；
（2）, terylene mesh bag entered by conveyer belt in circulation solution case, circulate in solution case that weaving is helped with anti-bacteria and mite-proof functional in solution
Agent, weaving are 1-5 with the weight of function additive and water ratio:1-5:104, the temperature for circulating solution in solution case is 114 degrees Celsius,
Soak time of the antibiotic polyester fiber in circulation solution case is 3-8 minutes；
（3）, the graphene polyester fiber that soaked is rolled 5 times repeatedly with Pneumatic pressure bar in circulation solution case, roll 1 every time
Minute, the pressure of press rods is 5 kilograms, it is adjacent roll twice between be spaced 2 minutes so that antibiotic polyester fiber and solution
Weight ratio is 5:0.1-1；
（4）, the terylene mesh bag that step 3 prepares be put into steam drying box bakeed, stoving temperature is 124 degrees Celsius,
It is 138 minutes to bakee the time；
（5）, the fiber after baking carry out packing encapsulation, that is, be prepared into multifunctional efficient graphene functional fibre.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that its step is：
（1）, the multifunctional efficient graphene functional fibre for preparing claim 1 and polyester fiber, eutectic polyester fiber by
According to weight than 1： 2：0.5, which carries out uniformly mixing, unclamps combing；
（2）, according to needed for fabric grammes per square metre carry out multiple lapping in length and breadth successively, the grammes per square metre of every layer of lapping is at 40 grams；
（3）, then in step（2）The upper and lower surface for the Multilayer Network being paved into carries out glue spraying processing；
（4）, then after upper and lower surface glue spraying Multilayer Network be sent into baking oven in bakeed, stoving temperature be 188 degrees Celsius, make
The fusing of eutectic polyester fiber is obtained, it is 60 seconds to bakee the time；
（5）, it is baked after, roll coiled, that is, be prepared into multifunctional efficient graphene functional fibre flocculus.
The application method of described multifunctional efficient graphene functional fibre, it is characterised in that use multifunctional efficient stone
The fabric that black olefinic functionality fiber is prepared.
It is an object of the invention to provide the preparation of multifunctional efficient graphene functional fibre and its application method, more work(
Energy high-efficient graphite olefinic functionality fiber will be by that during final finishing, will weave with anti-mite auxiliary agent, weaving function additive and basis
Polyester fiber is combined with each other, and formation has anti-mite property and functional terylene composite fibre, and the addition fiber of graphene resists
Bacterium property, uviolresistance and static electricity resistance, this method technique is simple, is easy to streamline large-scale operation, technique in production process
Condition is easily controlled, and production cost is low；A process for preparing the functional fibre come, can pass through repeatedly washing, also has good
Composite functional, be worth of widely use.
Obviously, above-described embodiment is only intended to clearly illustrate example, and is not the restriction to embodiment.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or
Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (4)
1. the preparation method of multifunctional efficient graphene functional fibre, it is characterised in that its step is：
（1）, by terylene chips and graphene master batch according to weight than 100:1-10 uniformly after mixing, is prepared into graphene terylene fibre
Dimension, graphene polyester fiber is subjected to fluffy processing, the graphene polyester fiber after fluffy processing is put into terylene mesh bag
In, every bag of weight being put into is 4-6.4 kilograms, and terylene mesh bag is placed on conveyer belt；
（2）, terylene mesh bag entered by conveyer belt in circulation solution case, circulate in solution case that weaving is helped with anti-bacteria and mite-proof functional in solution
Agent, weaving are 1-5 with the weight of function additive and water ratio:1-5:104, the temperature for circulating solution in solution case is Celsius for 50-114
Degree, soak time of the antibiotic polyester fiber in circulation solution case is 3-8 minutes；
（3）, the graphene polyester fiber that soaked is rolled 5 times repeatedly with Pneumatic pressure bar in circulation solution case, roll 1 every time
Minute, the pressure of press rods is 5 kilograms, it is adjacent roll twice between be spaced 1-2 minutes so that antibiotic polyester fiber and solution
Weight ratio be 5:0.1-1；
（4）, the terylene mesh bag that step 3 prepares be put into steam drying box bakeed, stoving temperature is that 80-124 is Celsius
Degree, the baking time is 100-138 minutes；
（5）, the fiber after baking carry out packing encapsulation, that is, be prepared into multifunctional efficient graphene functional fibre.
2. the preparation method of multifunctional efficient graphene functional fibre according to claim 1, it is characterised in that the step
Suddenly（2）Middle weaving is weaving far-infrared functional auxiliary agent, weaving anion function auxiliary agent, weaving mosquito repellent work(with function additive
Energy auxiliary agent, weaving are helped with deodorization functions auxiliary agent, weaving with formaldehyde-removing antibiotic deodorization functions auxiliary agent, weaving with moisture absorption sweat discharging functions
Agent, weaving cool feeling function additive, weaving use phase-change constant-temperature function additive with accumulation of heat temperature storage heat-preserving function auxiliary agent or weaving.
3. the application method of multifunctional efficient graphene functional fibre according to claim 1, it is characterised in that its step
For：
（1）, the multifunctional efficient graphene functional fibre for preparing claim 1 and polyester fiber, eutectic polyester fiber by
According to weight than 1：1-2：0.1-0.5 carries out uniformly mixing and unclamps combing；
（2）, according to needed for fabric grammes per square metre carry out multiple lapping in length and breadth successively, the grammes per square metre of every layer of lapping is at 15-40 grams；
（3）, then in step（2）The upper and lower surface for the Multilayer Network being paved into carries out glue spraying processing；
（4）, then after upper and lower surface glue spraying Multilayer Network be sent into baking oven in bakeed, stoving temperature be 180-188 it is Celsius
Degree so that eutectic polyester fiber melts, and the baking time is the 50-60 seconds；
（5）, it is baked after, roll coiled, that is, be prepared into multifunctional efficient graphene functional fibre flocculus.
4. the application method of multifunctional efficient graphene functional fibre according to claim 1, it is characterised in that use more
The fabric that function high-efficient graphite olefinic functionality fiber is prepared.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108048945A (en) * | 2018-01-24 | 2018-05-18 | 广州联汇技术服务有限公司 | A kind of new polyester fiber |
| CN108456942A (en) * | 2018-03-15 | 2018-08-28 | 杭州海科纤维有限公司 | A kind of graphene three-dimensional hollow polyester staple fiber and its manufacturing method |
| CN109056100A (en) * | 2018-07-29 | 2018-12-21 | 江苏鑫轮纳米生物科技有限公司 | A kind of preparation and its application method of functional form polyester fiber |
| CN109161980A (en) * | 2018-08-30 | 2019-01-08 | 广州市中诚新型材料科技有限公司 | A kind of anion, graphene polyester fiber |
| CN109594174A (en) * | 2018-12-19 | 2019-04-09 | 南通强生石墨烯科技有限公司 | A kind of graphene function of driving mosquitoes fabric and preparation method thereof |
| CN110024673A (en) * | 2018-11-27 | 2019-07-19 | 劳富文 | Cotton and preparation method thereof is planted in the cultivation of graphene polyester fiber water |
| CN110468595A (en) * | 2019-07-23 | 2019-11-19 | 四川亿家云享科技有限公司 | A kind of preparation method of graphene anion phase-transition heat-preserving cloth |
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| CN106350894A (en) * | 2016-07-05 | 2017-01-25 | 福建省晋江市华宇织造有限公司 | Graphene polyester monofilament |
| CN106835496A (en) * | 2016-12-27 | 2017-06-13 | 丹阳市宇晟纺织新材料有限公司 | A kind of preparation method without glue composite that can automatically adjust humiture |
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| CN105113160A (en) * | 2015-08-20 | 2015-12-02 | 江苏鑫轮特种纤维科技发展有限公司 | Fiber after-treatment equipment |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108048945A (en) * | 2018-01-24 | 2018-05-18 | 广州联汇技术服务有限公司 | A kind of new polyester fiber |
| CN108456942A (en) * | 2018-03-15 | 2018-08-28 | 杭州海科纤维有限公司 | A kind of graphene three-dimensional hollow polyester staple fiber and its manufacturing method |
| CN109056100A (en) * | 2018-07-29 | 2018-12-21 | 江苏鑫轮纳米生物科技有限公司 | A kind of preparation and its application method of functional form polyester fiber |
| CN109161980A (en) * | 2018-08-30 | 2019-01-08 | 广州市中诚新型材料科技有限公司 | A kind of anion, graphene polyester fiber |
| CN110024673A (en) * | 2018-11-27 | 2019-07-19 | 劳富文 | Cotton and preparation method thereof is planted in the cultivation of graphene polyester fiber water |
| CN109594174A (en) * | 2018-12-19 | 2019-04-09 | 南通强生石墨烯科技有限公司 | A kind of graphene function of driving mosquitoes fabric and preparation method thereof |
| CN110468595A (en) * | 2019-07-23 | 2019-11-19 | 四川亿家云享科技有限公司 | A kind of preparation method of graphene anion phase-transition heat-preserving cloth |
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Address after: 226000 building 4, 9 new East Road, Nantong economic and Technological Development Zone, Jiangsu Applicant after: JIANGSU XINLUN NANO BIOTECHNOLOGY CO.,LTD. Address before: 226000 building 4, 9 new East Road, Nantong economic and Technological Development Zone, Jiangsu Applicant before: Jiangsu Xin Ling new material technology development Co.,Ltd. Address after: 226000 building 4, 9 new East Road, Nantong economic and Technological Development Zone, Jiangsu Applicant after: Jiangsu Xin Ling new material technology development Co.,Ltd. Address before: 226000 building 4, 9 new East Road, Nantong economic and Technological Development Zone, Jiangsu Applicant before: JIANGSU XINLUN SPECIAL FIBER TECHNOLOGY DEVELOPMENT Co.,Ltd. |
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Application publication date: 20180109 |