CN107556879A - 一种隔热纳米复合涂料及其制备方法 - Google Patents
一种隔热纳米复合涂料及其制备方法 Download PDFInfo
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- CN107556879A CN107556879A CN201710961848.4A CN201710961848A CN107556879A CN 107556879 A CN107556879 A CN 107556879A CN 201710961848 A CN201710961848 A CN 201710961848A CN 107556879 A CN107556879 A CN 107556879A
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- heat
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- 238000000576 coating method Methods 0.000 title claims abstract description 59
- 239000011248 coating agent Substances 0.000 title claims abstract description 54
- 239000002114 nanocomposite Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000001913 cellulose Substances 0.000 claims abstract description 32
- 229920002678 cellulose Polymers 0.000 claims abstract description 32
- 229910052688 Gadolinium Inorganic materials 0.000 claims abstract description 28
- UIWYJDYFSGRHKR-UHFFFAOYSA-N gadolinium atom Chemical compound [Gd] UIWYJDYFSGRHKR-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000004964 aerogel Substances 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000004593 Epoxy Substances 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 239000000945 filler Substances 0.000 claims abstract description 15
- 239000012452 mother liquor Substances 0.000 claims abstract description 15
- 239000011858 nanopowder Substances 0.000 claims abstract description 14
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 14
- 239000002131 composite material Substances 0.000 claims abstract description 13
- 239000003822 epoxy resin Substances 0.000 claims abstract description 13
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 238000009413 insulation Methods 0.000 claims description 17
- CMIHHWBVHJVIGI-UHFFFAOYSA-N gadolinium(iii) oxide Chemical class [O-2].[O-2].[O-2].[Gd+3].[Gd+3] CMIHHWBVHJVIGI-UHFFFAOYSA-N 0.000 claims description 12
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 8
- 239000000839 emulsion Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 229910002609 Gd2Zr2O7 Inorganic materials 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 4
- 229910006213 ZrOCl2 Inorganic materials 0.000 claims description 4
- 150000001768 cations Chemical class 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 238000000975 co-precipitation Methods 0.000 claims description 4
- 244000144992 flock Species 0.000 claims description 4
- 229910001938 gadolinium oxide Inorganic materials 0.000 claims description 4
- 229910017604 nitric acid Inorganic materials 0.000 claims description 4
- 239000002244 precipitate Substances 0.000 claims description 4
- 238000009938 salting Methods 0.000 claims description 4
- 238000007873 sieving Methods 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000000725 suspension Substances 0.000 claims description 4
- 230000009514 concussion Effects 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000001291 vacuum drying Methods 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- NZSLBYVEIXCMBT-UHFFFAOYSA-N chloro hypochlorite;zirconium Chemical class [Zr].ClOCl NZSLBYVEIXCMBT-UHFFFAOYSA-N 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims 1
- 238000001354 calcination Methods 0.000 claims 1
- 239000008107 starch Substances 0.000 claims 1
- 235000019698 starch Nutrition 0.000 claims 1
- IPCAPQRVQMIMAN-UHFFFAOYSA-L zirconyl chloride Chemical compound Cl[Zr](Cl)=O IPCAPQRVQMIMAN-UHFFFAOYSA-L 0.000 claims 1
- 229920006334 epoxy coating Polymers 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 description 5
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 239000002086 nanomaterial Substances 0.000 description 4
- 239000000758 substrate Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000010422 painting Methods 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 229940075613 gadolinium oxide Drugs 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 238000004378 air conditioning Methods 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical group [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000011256 inorganic filler Substances 0.000 description 1
- 229910003475 inorganic filler Inorganic materials 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
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CN201710961848.4A CN107556879B (zh) | 2017-10-16 | 2017-10-16 | 一种隔热纳米复合涂料及其制备方法 |
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CN201710961848.4A CN107556879B (zh) | 2017-10-16 | 2017-10-16 | 一种隔热纳米复合涂料及其制备方法 |
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CN107556879A true CN107556879A (zh) | 2018-01-09 |
CN107556879B CN107556879B (zh) | 2020-01-21 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115093725A (zh) * | 2022-06-23 | 2022-09-23 | 上海箬宇新材料有限公司 | 一种耐1800℃磷酸盐隔热防火涂料及其制备方法 |
CN115260867A (zh) * | 2022-07-06 | 2022-11-01 | 中城国网(北京)综合能源有限公司 | 一种长效防结露的高分子纳米隔温涂料及其制备方法 |
CN115725209A (zh) * | 2023-01-05 | 2023-03-03 | 曹阳 | 一种纳米复合涂料及其制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102666669A (zh) * | 2009-09-14 | 2012-09-12 | 诺丁汉大学 | 纤维素纳米粒气凝胶、水凝胶和有机凝胶 |
KR20130039028A (ko) * | 2011-10-11 | 2013-04-19 | 엠파워(주) | 다공성 실리카 에어로겔을 이용한 도료 조성물 |
CN106634461A (zh) * | 2016-12-16 | 2017-05-10 | 深圳大学 | 一种氧化石墨烯隔热玻璃双组份涂料及其制备方法 |
CN106747425A (zh) * | 2016-12-01 | 2017-05-31 | 东莞市联洲知识产权运营管理有限公司 | 一种含羟基磷灰石涂层的不裂高致密纳米锆酸钆陶瓷 |
-
2017
- 2017-10-16 CN CN201710961848.4A patent/CN107556879B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102666669A (zh) * | 2009-09-14 | 2012-09-12 | 诺丁汉大学 | 纤维素纳米粒气凝胶、水凝胶和有机凝胶 |
KR20130039028A (ko) * | 2011-10-11 | 2013-04-19 | 엠파워(주) | 다공성 실리카 에어로겔을 이용한 도료 조성물 |
CN106747425A (zh) * | 2016-12-01 | 2017-05-31 | 东莞市联洲知识产权运营管理有限公司 | 一种含羟基磷灰石涂层的不裂高致密纳米锆酸钆陶瓷 |
CN106634461A (zh) * | 2016-12-16 | 2017-05-10 | 深圳大学 | 一种氧化石墨烯隔热玻璃双组份涂料及其制备方法 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115093725A (zh) * | 2022-06-23 | 2022-09-23 | 上海箬宇新材料有限公司 | 一种耐1800℃磷酸盐隔热防火涂料及其制备方法 |
CN115093725B (zh) * | 2022-06-23 | 2023-03-10 | 上海箬宇新材料有限公司 | 一种耐1800℃磷酸盐隔热防火涂料及其制备方法 |
CN115260867A (zh) * | 2022-07-06 | 2022-11-01 | 中城国网(北京)综合能源有限公司 | 一种长效防结露的高分子纳米隔温涂料及其制备方法 |
CN115260867B (zh) * | 2022-07-06 | 2023-10-13 | 中城国网(北京)综合能源有限公司 | 一种长效防结露的高分子纳米隔温涂料及其制备方法 |
CN115725209A (zh) * | 2023-01-05 | 2023-03-03 | 曹阳 | 一种纳米复合涂料及其制备方法 |
CN115725209B (zh) * | 2023-01-05 | 2023-12-22 | 曹阳 | 一种纳米复合涂料及其制备方法 |
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CN107556879B (zh) | 2020-01-21 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A heat insulation nano composite coating and its preparation method Effective date of registration: 20230116 Granted publication date: 20200121 Pledgee: Bank of Jilin Co.,Ltd. Changchun Kaixuan Sub branch Pledgor: CHANGCHUN SHUNFENG NEW MATERIAL CO.,LTD. Registration number: Y2022220000109 |
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Date of cancellation: 20231116 Granted publication date: 20200121 Pledgee: Bank of Jilin Co.,Ltd. Changchun Kaixuan Sub branch Pledgor: CHANGCHUN SHUNFENG NEW MATERIAL CO.,LTD. Registration number: Y2022220000109 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A thermal insulation nanocomposite coating and its preparation method Effective date of registration: 20231122 Granted publication date: 20200121 Pledgee: Bank of Jilin Co.,Ltd. Changchun Kaixuan Sub branch Pledgor: CHANGCHUN SHUNFENG NEW MATERIAL CO.,LTD. Registration number: Y2023220000134 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |