CN107550948A - Ganoderma spove powder microcapsule powder and preparation method thereof - Google Patents
Ganoderma spove powder microcapsule powder and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of ganoderma spove powder microcapsule powder and preparation method thereof, it belongs to drugs and health care products technical field.Ganoderma spove powder microcapsule powder, it is to be prepared by following raw materials by the parts by weight：43~47 parts of ganoderma spove powder, 25~30 parts of ocentyl succinic list Arabic gum ester, 10~15 parts of maltodextrin, 10~15 parts of soybean protein, 1~4 part of Sucrose Fatty Acid Ester, 1~4 part of Sodium Caseinate, 5~10 parts of Arabic gum.Stability of the present invention is good, can effectively wrap up ganoderma lucidum spore oil, preferably solves the problems, such as that ganoderma spove powder is oxidizable rotten.Strengthen the dissolubility of active ingredient, be advantageous to absorbing for ganoderma spove powder.Preferably remain the active component of ganoderma spove powder.
Description
Technical field
The present invention relates to a kind of ganoderma spove powder microcapsule powder and preparation method thereof, and it belongs to drugs and health care products technology neck
Domain.
Background technology
《Sheng Nong's herbal classic》、《Compendium of Materia Medica》In have very recording certainly to the medical functions of ganoderma lucidum.If any heat-clearing
Removing toxic substances, kidney-nourishing liver protection, nourishing and fit keeping function, strengthen the body resistance to consolidate the constitution, beautifying face and moistering lotion, strengthening the essence of calming the nerves gas and other effects.Therefore, ganoderma lucidum is considered as first-class
Health-care hospital good merchantable brand.Lucidum spore powder is the fine particle that ganoderma lucidum growth and maturity phase ejects from cap, is the reproduction of ganoderma lucidum
Cell, there are whole genetic activities materials of ganoderma lucidum.The amount of its active material is 70 times of ganoderma lucidum entity according to surveying and determination, is primarily present
In ganoderma lucidum spore oil, rich in materials such as essential amino acid, sterol, alkaloid, organic germanium, polysaccharide and triterpenes, it has
The content of machine germanium it is more taller than ginseng go out 4 to 6 times, have been shown to effectively to strengthen human immunological competence and each portion of regulation body
Extension set energy, have and suppress tumour, antiviral, guarantor's kidney protect liver, hypoglycemic, immunological regulation anti-aging and other effects, Reishi sporule
Broken wall is currently mainly used in powder, and it is easier to absorb than the conidia powder of non-broken wall.
For lucidum spore powder oil content up to 20%~30%, the lipid components therefrom extracted are ganoderma lucidum spore oil, are mainly contained
Ganoderma lucidum triterpene compounds, unrighted acid, sterol, vitamin, volatile oil isoreactivity composition；Wherein unrighted acid contains
Amount is more than 60%, and based on the aliphatic acid such as oleic acid, linoleic acid, triterpene compound pharmacological activity is strong, and in ganoderma lucidum spore oil
Main active, the mainly ganoderma spove powder for using and selling in the market, spore after ganoderma lucidium spore powder wall breaking
Oily lubricant component almost all is overflowed, and is mixed with conidia powder, after the lubricant component and air contact of spilling, its activity
Composition is very easy to oxidation deterioration, peroxide value increase, harmful components increase, leverages the effective of product quality and storage
Time limit, the method used at present are substantially wrapped up with outer packing, but because packaging exists ventilative or opens situation, still can oxygen
Change.Therefore how to avoid ganoderma spove powder from aoxidizing, it is extremely important to improve stability.On the other hand due to wall-broken ganoderma spore
Contain a large amount of oils in powder, compressibility is very poor, and cause makes it difficult to prepare other such as tablets, capsule formulation.
At present, the document and patent report on ganoderma lucidum spore oil micro-capsule are only seen using pure spore oil material, are had no pair
Ganoderma spove powder miospore oil prepares the document and patent of micro-capsule.Existing visible document and patent are primarily with regard to broken wall
Lucidum spore powder carries out the report of anti-oxidant treatment and preparation technique, and main literature has：Academic magazine 03 phase in 2015, spirit
The prospect of Ganoderma lucidum spore powder New technical use is inquired into, and oxidation resistant purpose is realized to ganoderma lucidium spore powder wall breaking processing；The food science and technology phase
06 phase in 2009 is printed, lucidum spore powder Wet-process wall breaking and inclusion technique use cyclodextrin encapsulated effect, using colloid mill polishing
Broken wall simultaneously prepares inclusion compound, solves the easy microbiological contamination spoilage problems of active ingredient after ganoderma lucidium spore powder wall breaking hardly possible, broken wall, but this method ring
Dextrin can not wrap up spore oil whole composition, especially easily incomplete to the fatty acid composition parcel of oxidation, have larger
Limitation.Patent includes：Chinese patent CN200610040992.6, a kind of glossy ganoderma spore powder with crushed sporoderm anti-oxidation tech, utilizes oil
The easy adsorptivity of fat, add other and the oil readily oxidizable substances such as traditional Chinese medicine powder foot couple ganodenic acid, unrighted acid can be used
Wrapped up, play antioxidation, this method still falls within adsorption method, and spore oil is still in naked state；Chinese patent
CN102960731A, the preparation method and product of oxidation resistant ganoderma spove powder, ganoderma spove powder and chitin are gathered
Confectionery vinegar colloidal solution is sufficiently mixed, and in the attached last layer chitosan diaphragm in wall-breaking lucidum powder surface, effectively completely cuts off Reishi sporule
Contact of the powder with ambient air outside, so as to reach superior oxidation resistance, extend pot-life, Chinese patent
CN201410139764.9, a kind of oxidation resistant double glue ganoderma spove powders and preparation method thereof, by ganoderma spove powder
It is made through donkey-hide gelatin, pig skin gelatin colloidal solution spraying embedding granulation, fluidized drying technique, the two methods belong to the side of granule coating
Method, because conidia powder belongs to irregular granules, coating can not accomplish integrality；Chinese patent CN 106173779A, a kind of ganoderma lucidum
Spore solid beverage and preparation method thereof, the lucidum spore powder of use have captured the active ingredients such as GL-B by wall breaking technology
Hardly possible extraction, difficult the defects of absorbing.There is a following report on preparing micro-capsule to pure ganoderma lucidum spore oil, fungus periodical 02 phase in 2014,
Ganoderma lucidum spore oil Micro-Encapsulation Technique is dry using spray drying process and freezing using soybean protein isolate and maltodextrin as wall material
Dry method prepares Reishi sporule oil microcapsule；Do not retrieve and microcapsule formulation report or patent are prepared using ganoderma spove powder.With
Upper patent and document are not related to this patent content.Microcapsule technology be currently including one of oil component best technique, can be preferable
Tiny oil droplets are rolled into solid, completely cut off air, while realize oils powdered.At present document and patent report generally be directed to
Pure oil component prepares micro-capsule, have no contained oils in solid material wrap up directly prepare micro-capsule report.
The content of the invention
Present invention aims at provide a kind of stable, oxidation resistant ganoderma spove powder microcapsule powder.
Another object of the present invention is to develop a kind of stabilization, ganoderma spove powder micro-capsule anti-oxidant, easy to process
The preparation method of powder.
Ganoderma spove powder microcapsule powder, it is to be prepared by following raw materials by the parts by weight：Wall-breaking lucidum spore
Sub- 43~47 parts of powder, 25~30 parts of ocentyl succinic list Arabic gum ester, 10~15 parts of maltodextrin, soybean protein 10~15
Part, 1~4 part of Sucrose Fatty Acid Ester, 1~4 part of Sodium Caseinate, 5~10 parts of Arabic gum.
Above-mentioned ganoderma spove powder microcapsule powder, it is to be prepared by following raw materials by the parts by weight：Broken wall
45~47 parts of lucidum spore powder, 26~28 parts of ocentyl succinic list Arabic gum ester, 10~12 parts of maltodextrin, soybean protein
10~12 parts, 1.5~3 parts of Sucrose Fatty Acid Ester, 1.5~3 parts of Sodium Caseinate, 8~10 parts of Arabic gum.
Above-mentioned ganoderma spove powder microcapsule powder, it is to be prepared by following raw materials by the parts by weight：Broken wall
45 parts of lucidum spore powder, 27 parts of ocentyl succinic list Arabic gum ester, 12 parts of maltodextrin, 12 parts of soybean protein, Sucrose Fatty Acid Ester 2
Part, 2 parts of Sodium Caseinate, 10 parts of Arabic gum.
Above-mentioned ganoderma spove powder is that Reishi sporule is made through technology for broken wall.
The preparation method of above-mentioned ganoderma spove powder microcapsule powder, step are as follows：Weigh and meet the pungent of the parts by weight
Alkenyl succinic acid list Arabic gum ester, maltodextrin, soybean protein, add relative to capsule material ocentyl succinic list Arabic gum
The hot water of ester and maltodextrin and 18~22 times of weight of soybean protein gross weight, addition, which takes, under agitation meets the parts by weight
Emulsifying agent Sucrose Fatty Acid Ester, Sodium Caseinate, add the ganoderma spove powder for taking and meeting the parts by weight, then use high shear
Dispersion emulsifying machine shears 5~10min, high-pressure homogeneous, obtains emulsion, the emulsion spray is dried, and obtains powder intermediate original
Material, the powder intermediate feed is put into fluid bed and fluidized, and preparation meets the water that the parts by weight contain 10% Arabic gum
Solution, spray and wrap up to the raw material of fluidisation, obtain ganoderma spove powder microcapsule powder.
Above-mentioned hot water temperature is 60~70 DEG C.
It is above-mentioned it is high-pressure homogeneous be using high pressure homogenizer 30Mpa homogeneous twice.
Invention is invented based on following principles, and ganoderma spove powder usually contains 20%~30% oil component, its
Include unrighted acid and triterpenes oily substance, easily oxidation deterioration, simultaneously because bellding influences compressibility, it is difficult to make
Agent is molded.The present invention is studied through lot of experiments and found, in spore powder with crushed sporoderm ganoderma lucidum spore oil after hot-water soak can separate out,
Micro-capsule core can be used as, and polysaccharide and protein hot-water soak can also extract in spore powder with crushed sporoderm, can be used as part
Wall material, while help the wall material that can be combined with conidia powder to be filtered out through lot of experiments, ganoderma spove powder and pungent
Alkenyl succinic acid list Arabic gum ester, maltodextrin, soybean protein, Sucrose Fatty Acid Ester, Sodium Caseinate combination, are adding emulsifying agent situation
Under, oil-in-water type solution is formed through emulsification, polysaccharide, protein are contained in aqueous phase, it is spray-dried to form micro-capsule.But pass through
Investigation is crossed, not all can may be used to spore powder with crushed sporoderm of the present invention as the material and emulsifying agent of micro-capsule wall material
Micro-capsule, screened by lot of experiments, the wall material and emulsification agent material that the present invention filters out can be used for the present invention, reach broken wall spirit
The effect of Ganoderma lucidum spore powder micro-capsule, envelop rate have the physicochemical property of good stability and preparation of preparation more than 80%.
Using 60~70 DEG C of hot water hot dippings of addition in present invention process so that polysaccharide and protein are by more in spore powder with crushed sporoderm
Good extraction dissolution, and make spore oil separate out.Wall material and emulsifying agent are added, constitutes to form micro-capsule primary condition.
This patent is using the material such as part ganoderma spove powder and ocentyl succinic list Arabic gum ester as capsule material
Ganoderma spove powder micro-capsule is prepared, the ganoderma spove powder and ocentyl succinic list Arabic gum ester, malt added
Dextrin, soybean protein, Sucrose Fatty Acid Ester, the capsule material of Sodium Caseinate combination can effectively embed Reishi sporule in ganoderma spove powder
Oil, form micro-capsule powder.
The ganoderma spove powder micro-capsule powder preparation that the present invention obtains has the following advantages that：
（1）Product stability is good, can effectively wrap up ganoderma lucidum spore oil, and it is oxidizable rotten preferably to solve ganoderma spove powder
Problem.
（2）Strengthen the dissolubility of active ingredient, be advantageous to absorbing for ganoderma spove powder.
（3）Not only ganoderma lucidum spore oil had been contained in product but also had contained other polysaccharide of ganoderma spove powder and protein ingredient, more preferably
The active component for remaining ganoderma spove powder.
Embodiment
With reference to instantiation, the present invention is expanded on further.But these embodiments are only limitted to illustrate rather than
To limit the scope of the present invention, the equivalent variations made according to the spirit and scope limited in the claims in the present invention are still fallen within
The scope that the present invention is covered.
Method in following embodiments, it is conventional method unless otherwise instructed.
Percentage composition in following embodiments is weight/mass percentage composition unless otherwise instructed.
Micro-capsule powder preparation made from following embodiments can use following known method to be detected, using electron microscopic
Sem observation micro-capsule size, form；Determined using the method for extraction grease outside micro-capsule with fat content in micro-capsule, draw envelop rate；
Using determined by ultraviolet spectrophotometry triterpene and sterol content.
Specific detection method is as follows：
1. electron microscope method
100mg microcapsule powder samples accurately are weighed, glycerol adding is settled to 10ml volumetric flasks, shaken up, and drawing 1 ~ 2 drop of liquid with suction pipe drips
It is added to slide, covered, in electron microscope observation micro-capsule size and form.
2. using the method measure microcapsule powder envelop rate of extraction grease
（1）The measure of microcapsule powder surface Reishi sporule oil content
10g microcapsule powder samples accurately are weighed, by 3 additions of 100ml petroleum ethers point, 2min is vibrated every time, filters, merging filtrate.
Filtrate is placed into heating distillation on the rotary evaporator, petroleum ether is slowly distilled out, produces surface oil quality.Surface oil content
（%）=surface oil quality/sample quality × 100.
（2）The measure of ganoderma lucidum spore oil total amount in micro-capsule
Accurately weigh microcapsule powder sample 10g（m1）It is put into dry triangular flask, adds 100mL hot water, after sample is fully dissolved,
After addition 100mL petroleum ethers fully extract, extract is moved into the triangular flask dried and weighed（m2）, repeat to be extracted twice,
Combining extraction liquid, petroleum ether is sloughed with rotary evaporator, place into 60 DEG C of baking ovens and dry to constant weight（m3）, total oil content（%）=
（m3-m2）/m1×100.
（3）The measure of microcapsule powder envelop rate
Envelop rate（%）=（1- surface oil contents/total oil content）×100
3. use determined by ultraviolet spectrophotometry triterpene and sterol content
The preparation of reference substance solution takes oleanolic acid reference substance appropriate, adds methanol that solution of every 1ml containing 0.2mg is made, produces.
The preparation precision of standard curve measures reference substance solution 0.1,0.2,0.3,0.4,0.5ml, puts 15ml tool plugs respectively
In test tube, volatilize, let cool, precision adds vanillic aldehyde glacial acetic acid solution 0.2ml, the perchloric acid 0.8ml newly prepared, shakes up, 70
Heated 15 minutes in DEG C water-bath, put in ice bath and cool down 5 minutes immediately, taken out, precision adds ethyl acetate 4ml, shakes up, according to purple
Outside-visible spectrophotometry, absorbance is determined at 546nm wavelength, be that abscissa draws mark using absorbance as ordinate, concentration
Directrix curve.
The preparation of need testing solution takes micro-capsule powder about 200mg, accurately weighed, puts in conical flask with cover, adds ethanol
50ml, it is ultrasonically treated 45 minutes, filtration, filtrate is put in 100ml measuring bottles, with ethanol in proper amount, gradation washing nozzle and filter residue, washing lotion
And in the same measuring bottle of people, ethanol is added to shake up, produce to scale.
Determination method precision measures need testing solution 0.2ml, puts in 15ml tool plug test tubes, the side under sighting target directrix curve preparation
Method, from " volatilizing ", is operated with method, determines absorbance, and containing for triterpene and sterol in need testing solution is read from standard curve
Amount, calculate, produce.
Embodiment 1
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
43 parts of powder, 1 part of sucrose ester, 30 parts of ocentyl succinic list Arabic gum ester, 12 parts of maltodextrin, 13 parts of soybean protein, casein
Sour 1 part of sodium, 5 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 30g, maltodextrin 12g, soybean
Albumen 13g, 60~70 DEG C of hot water 990g are added, add sucrose ester 1g, Sodium Caseinate 1g under agitation, add wall-breaking lucidum spore
Sub- powder 43g, then shears 5min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule emulsification
Liquid, the emulsion spray is dried, obtain powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, claimed
Arabic gum 5g is taken, is configured to containing the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtain wall-breaking lucidum spore
Sub- powder microcapsule powder, it is 80.6% to measure envelop rate through the above method, and triterpene and sterol content are 0.91%.
Embodiment 2
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
47 parts of powder, 3 parts of sucrose ester, 27 parts of ocentyl succinic list Arabic gum ester, 10 parts of maltodextrin, 10 parts of soybean protein, casein
Sour 3 parts of sodium, 8 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 27g, maltodextrin 10g, soybean
Protein 10 g, 60~70 DEG C of hot water 893g are added, add sucrose ester 3g, Sodium Caseinate 3g under agitation, add wall-breaking lucidum spore
Sub- powder 47g, then shears 7min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule emulsification
Liquid.The emulsion spray is dried, obtains powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, is claimed
Arabic gum 8g is taken, preparation contains the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtains wall-broken ganoderma spore
Powder microcapsule powder, it is 82.5% to measure envelop rate through the above method, and triterpene and sterol content are 0.88%.
Embodiment 3
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
47 parts of powder, 11 parts of maltodextrin, 12 parts of soybean protein, 2 parts of Sodium Caseinate, 2 parts of sucrose ester, ocentyl succinic list Arabic gum
26 parts of ester, 9 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 26g, maltodextrin 11g, soybean
Protein 12 g, 60~70 DEG C of hot water 980g are added, add sucrose ester 2g, Sodium Caseinate 2g under agitation, add wall-breaking lucidum spore
Sub- powder 47g, then shears 8min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule emulsification
Liquid, the emulsion spray is dried, obtain powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, claimed
Arabic gum 9g is taken, preparation contains the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtains wall-broken ganoderma spore
Powder microcapsule powder, it is 83.1% to measure envelop rate through the above method, and triterpene and sterol content are 0.94%.
Embodiment 4
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
43 parts of powder, 25 parts of ocentyl succinic list Arabic gum ester, 15 parts of maltodextrin, 15 parts of soybean protein, 1 part of Sodium Caseinate, sugarcane
1 part of sugar ester, 10 parts of Arabic gum.
Preparation method comprises the following steps：Weigh maltodextrin 15g, ocentyl succinic list Arabic gum ester 25g, soybean
Protein 15 g, 60~70 DEG C of hot water 1155g are added, add Sodium Caseinate 1g, sucrose ester 1g under agitation, add wall-breaking lucidum
Conidia powder 43g, then shears 8min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule emulsification
Liquid, the emulsion spray is dried, obtain powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, claimed
Arabic gum 10g is taken, is configured to containing the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtain wall-breaking lucidum spore
Sub- powder microcapsule powder, it is 81.2% to measure envelop rate through the above method, and triterpene and sterol content are 0.92%.
Embodiment 5
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
46 parts of powder, 26 parts of ocentyl succinic list Arabic gum ester, 10 parts of soybean protein, 10 parts of maltodextrin, 4 parts of Sodium Caseinate, sugarcane
4 parts of sugar ester, 8 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 26g, soybean protein 10g, malt
Dextrin 10g, 60~70 DEG C of hot water 1012g are added, add sucrose ester 4g, Sodium Caseinate 4g under agitation, add wall-breaking lucidum
Conidia powder 46g, 10min then is sheared with high-shearing dispersion emulsifying machine, micro-capsule emulsion is obtained, the emulsion spray is dried,
Powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, weighs Arabic gum 8g, be configured to containing
The 10% Arabic gum aqueous solution, spray and wrap up to the raw material of fluidisation, obtain ganoderma spove powder microcapsule powder, surveyed through the above method
It is 81.3% to obtain envelop rate, and triterpene and sterol content are 0.88%.
Embodiment 6
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
It is 46 parts of powder, 1.5 parts of sucrose ester, 27 parts of ocentyl succinic list Arabic gum ester, 12 parts of maltodextrin, 1.5 parts of Sodium Caseinate, big
12 parts of legumin, 10 parts of Arabic gum.
Preparation method comprises the following steps：Ocentyl succinic list Arabic gum ester 27g, the g of soybean protein 12, malt paste
Smart 12g, 60~70 DEG C of hot water 1020g are added, add Sodium Caseinate 1.5g, sucrose ester 1.5g under agitation, add broken wall spirit
Ganoderma lucidum spore powder 46g, then shears 5min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule breast
Change liquid.The emulsion spray is dried, obtains powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized,
Arabic gum 10g is weighed, is configured to containing the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtain wall-breaking lucidum
Conidia powder microcapsule powder, it is 80.5% to measure envelop rate through the above method, and triterpene and sterol content are 0.90%.
Embodiment 7
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
45 parts of powder, 12 parts of maltodextrin, 12 parts of soybean protein, 2 parts of Sodium Caseinate, 2 parts of sucrose ester, ocentyl succinic list Arabic gum
27 parts of ester, 10 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 27g, maltodextrin 12g, soybean
Protein 12 g, 60~70 DEG C of hot water 1020g are added, add sucrose ester 2g, Sodium Caseinate 2g under agitation, add wall-breaking lucidum
Conidia powder 45g, then shears 10min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule breast
Change liquid.The emulsion spray is dried, obtains powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized,
Arabic gum 10g is weighed, is configured to containing the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtain wall-breaking lucidum
Conidia powder microcapsule powder, it is 85.7% to measure envelop rate through the above method, and triterpene and sterol content are 0.96%.
Embodiment 8
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
46 parts of powder, 10 parts of maltodextrin, 10 parts of soybean protein, 3 parts of Sodium Caseinate, 3 parts of sucrose ester, ocentyl succinic list Arabic gum
28 parts of ester, 10 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 28g, maltodextrin 10g, soybean
Protein 10 g, 60~70 DEG C of hot water 960g are added, add sucrose ester 3g, Sodium Caseinate 3g under agitation, add wall-breaking lucidum spore
Sub- powder 46g, then shears 10min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule emulsification
Liquid.The emulsion spray is dried, obtains powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, is claimed
Arabic gum 10g is taken, is configured to containing the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtain wall-breaking lucidum spore
Sub- powder microcapsule powder, it is 82.9% to measure envelop rate through the above method, and triterpene and sterol content are 0.93%.
Embodiment 9
The ganoderma spove powder microcapsule powder of the present invention, raw material are made up of the component of following parts by weight content：Wall-broken ganoderma spore
43 parts of powder, 2 parts of sucrose ester, 30 parts of ocentyl succinic list Arabic gum ester, 12 parts of maltodextrin, 11 parts of soybean protein, casein
Sour 2 parts of sodium, 10 parts of Arabic gum.
Preparation method comprises the following steps：Weigh ocentyl succinic list Arabic gum ester 30g, maltodextrin 12g, soybean
Protein 11 g, 60~70 DEG C of hot water 1100g are added, add sucrose ester 2g, Sodium Caseinate 2g under agitation, add wall-breaking lucidum
Conidia powder 43g, then shears 5min with high-shearing dispersion emulsifying machine, and high pressure homogenizer 30Mpa homogeneous twice, obtains micro-capsule emulsification
Liquid, the emulsion spray is dried, obtain powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, claimed
Arabic gum 10g is taken, is configured to containing the 10% Arabic gum aqueous solution, sprays and wraps up to the raw material of fluidisation, obtain wall-breaking lucidum spore
Sub- powder microcapsule powder, it is 80.9% to measure envelop rate through the above method, and triterpene and sterol content are 0.90%.
Ganoderma spove powder microcapsule powder made from above-described embodiment is tested below, test method and result are such as
Under：
Influence factor is tested
Ten kinds of the ganoderma spove powder microcapsule powder as made from the method for embodiment 1~9, existing ganoderma spove powder samples is taken to fit
Amount, is carried out as follows hot test, exposure experiments to light respectively：
（1）Hot test
Sample is respectively placed in transparent sealing ampoule bottle, is placed at 60 DEG C 10 days, is determined the 0th day, the 5th day, the 10th day respectively
The acid value and peroxide value of sample.
As a result：Contrasted with 0 day sample, ganoderma spove powder acid value and peroxide value rise are obvious；Ganoderma spove powder is micro-
Capsule powder acid value and peroxide value only change by a small margin, raise unobvious, the significant difference compared with ganoderma spove powder.
（2）Exposure experiments to light
Sample is respectively placed in transparent sealing ampoule bottle, is placed in the lighting box equipped with fluorescent lamp, in 4500 ± 500LX illuminance
Under conditions of place 10 days, determine the 0th day, the 5th day and the 10th day sample acid value and peroxide value.
As a result：Contrasted with 0 day sample, ganoderma spove powder acid value and peroxide value rise are obvious；Wall-broken ganoderma spore
Powder microcapsule powder acid value and peroxide value only change by a small margin, raise unobvious, the difference compared with ganoderma spove powder sample
Significantly, wherein best results of embodiment 7.
Claims (7)
1. ganoderma spove powder microcapsule powder, it is characterised in that it is to be prepared by following raw materials by the parts by weight：It is broken
43~47 parts of wall lucidum spore powder, 25~30 parts of ocentyl succinic list Arabic gum ester, 10~15 parts of maltodextrin, soybean egg
White 10~15 parts, 1~4 part of Sucrose Fatty Acid Ester, 1~4 part of Sodium Caseinate, 5~10 parts of Arabic gum.
2. ganoderma spove powder microcapsule powder according to claim 1, it is characterised in that it is by described by following raw materials
Parts by weight are prepared：45~47 parts of ganoderma spove powder, 26~28 parts of ocentyl succinic list Arabic gum ester, malt
10~12 parts of dextrin, 10~12 parts of soybean protein, 1.5~3 parts of Sucrose Fatty Acid Ester, 1.5~3 parts of Sodium Caseinate, Arabic gum 8~10
Part.
3. ganoderma spove powder microcapsule powder according to claim 1, it is characterised in that it is by described by following raw materials
Parts by weight are prepared：45 parts of ganoderma spove powder, 27 parts of ocentyl succinic list Arabic gum ester, maltodextrin 12
Part, 12 parts of soybean protein, 2 parts of Sucrose Fatty Acid Ester, 2 parts of Sodium Caseinate, 10 parts of Arabic gum.
4. according to the ganoderma spove powder microcapsule powder described in claim 1,2 or 3, it is characterised in that described wall-breaking lucidum spore
Sub- powder is that Reishi sporule is made through technology for broken wall.
5. the preparation method of the ganoderma spove powder microcapsule powder of claim 1,2 or 3, it is characterised in that step is as follows：Claim
Ocentyl succinic list Arabic gum ester, maltodextrin, the soybean protein for meeting the parts by weight are taken, is added relative to capsule material
The hot water of ocentyl succinic list Arabic gum ester and maltodextrin and 18~22 times of weight of soybean protein gross weight, under agitation
The emulsifying agent Sucrose Fatty Acid Ester for taking and meeting the parts by weight is added, Sodium Caseinate, adds the broken wall for taking and meeting the parts by weight
Lucidum spore powder, 5~10min then is sheared with high-shearing dispersion emulsifying machine, it is high-pressure homogeneous, emulsion is obtained, by the emulsion
Spray drying, obtains powder intermediate feed, the powder intermediate feed is put into fluid bed and fluidized, and preparation meets the weight
Number contains the aqueous solution of 10% Arabic gum, sprays and wraps up to the raw material of fluidisation, obtains ganoderma spove powder microcapsule powder.
6. the preparation method of ganoderma spove powder microcapsule powder according to claim 5, it is characterised in that described hot water
Temperature is 60~70 DEG C.
7. the preparation method of ganoderma spove powder microcapsule powder according to claim 5, it is characterised in that described high pressure
Homogeneous is to use high pressure homogenizer 30Mpa homogeneous twice.
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| CN112675793A (en) * | 2020-12-10 | 2021-04-20 | 广州中国科学院先进技术研究所 | Preparation method of ganoderma lucidum spore oil nano microcapsule |
| CN114533770A (en) * | 2022-02-22 | 2022-05-27 | 西藏天虹科技股份有限责任公司 | Extraction process and device of ganoderma lucidum extract |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110419717A (en) * | 2019-07-18 | 2019-11-08 | 中华全国供销合作总社济南果品研究院 | A kind of preparation method avoiding viscous wall and the ganoderma spove powder for delaying oxidation |
| CN112675793A (en) * | 2020-12-10 | 2021-04-20 | 广州中国科学院先进技术研究所 | Preparation method of ganoderma lucidum spore oil nano microcapsule |
| CN114533770A (en) * | 2022-02-22 | 2022-05-27 | 西藏天虹科技股份有限责任公司 | Extraction process and device of ganoderma lucidum extract |
| CN114533770B (en) * | 2022-02-22 | 2024-02-06 | 西藏天虹科技股份有限责任公司 | Extraction process and device of ganoderma lucidum extract |
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