CN107501993A - Dyeing method on a kind of Burma padauk dyestuff and fabric - Google Patents
Dyeing method on a kind of Burma padauk dyestuff and fabric Download PDFInfo
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- CN107501993A CN107501993A CN201710740089.9A CN201710740089A CN107501993A CN 107501993 A CN107501993 A CN 107501993A CN 201710740089 A CN201710740089 A CN 201710740089A CN 107501993 A CN107501993 A CN 107501993A
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- CN
- China
- Prior art keywords
- dyestuff
- burma padauk
- padauk
- burma
- dye
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/24—Polyamides; Polyurethanes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The present invention relates to field of light chemical industry, it is desirable to provide dyeing method on a kind of Burma padauk dyestuff and fabric.The extracting method of the Burma padauk dyestuff is including step：Burma padauk dead meal is taken, is placed in after mechanical crushing in ethanol water, the pH value of solution is adjusted with plant ash, ultrasonic extraction is simultaneously filtered to extract solution, and Burma padauk dyestuff can be obtained by being evaporated under reduced pressure concentration；Dyeing method includes step on this：Gained Burma padauk dyestuff and alum, levelling agent, deionized water etc. are configured to Burma padauk dye liquor with certain proportion, under the conditions of appropriate bath raio, temperature, pH value, fabric is submerged into water-bath in Burma padauk dye liquor to dye, fabric cold water wash is taken out and dries.Extraction process of the present invention is simple, extraction effect is good, and extraction is environment friendly and pollution-free with dyeing course, and upper dye fabric color fastness is high, lasting fragrance, and dress is safe and very wide with certain anti-inflammation and medicinal health-care effect, market prospects.
Description
Technical field
The present invention relates to a kind of extracting method and its fabric dyeing method of redwood dyestuff, more particularly to a kind of Burma padauk dye
Dyeing method on material and fabric.
Technical background
The chemical composition of Burma padauk inclusion mainly has eucalyptol, nerolidol, pterocarpoid, chromene flavonoids
Pigment etc. [Liu little Jin, Hainan Jianfengling Burma padauk core material ratio and derived essential oil composition, 2017], there is odor type stably to hold
Long, the pharmacological action such as anti-inflammatory antisepsis and sterilization [woods Jin nation, the fungistatic effect of Burma padauk heartwood different solvents extract, 2015].
Great Yong towns are described as in " Chinese mahogany furniture production Professional towns " " Chinese Qian Qiang towns " " Chinese jeans name town " etc.
Title, but the management to Tropical forests especially redwood resource is in the trend kept under strict control successively in the world at present, Asia in addition
The eruptive growth in mahogany furniture market, it is increasingly in short supply to cause to gush greatly redwood precious timber, so that redwood products innovation, industry
The problems such as structure optimization, increasingly impacts the big sustainable development for gushing redwood industry.
It is significantly increased in cost, in the case that the utilization rate of timber is not high, how relies on scientific and technological advances, optimizes redwood industry
Structure, the comprehensive utilization ratio for improving redwood especially corner dead meal is the vital task of redwood market sustainable development.
To sum up, in order to adapt to great Yong towns " 13 " strategic planning of development, realize that redwood textile industryization is green in combination
Development, this invention address that by the use of the corner dead meal of mahogany furniture as dye source, takes environment-friendly colouring method
To lift textile enterprise's Environmental Protection Level, and then expand redwood and the industry development space of weaving.
On the tint applications of Burma padauk natural dye, document report is had no at present.
The content of the invention
Problem solved by the invention there is provided a kind of Burma padauk natural dye and the dyestuff in polyamide fibre and wool etc.
Colouring method on fabric.
In order to solve the above-mentioned technical problem, extraction step of the invention is：Burma padauk is taken to discard leftover pieces sawdust etc., in
2 hours are dried in 60~80 DEG C of baking ovens, low temperature ultra micro mechanical crushing to particle is 50~100 mesh, and the big fruit after crushing is purple
The ethanol solution that wingceltis concentration of volume percent is 50~75% extracts, and feed liquid mass ratio is 1:15~40, and with vegetation tone
Save between pH value is 5~9,2~4h of ultrasonic extraction, is then filtered by vacuum under 60~80 DEG C of temperature conditionss, and filter residue is with side of the same race
Method extracts again, merges filtrate twice, rotated evaporation under reduced pressure distillation and concentration, obtains natural Burma padauk dyestuff.
The present invention is had the technical effect that using Burma padauk natural dye：Burma padauk furniture is gushing mahogany furniture middle-end greatly
Market accounts for more than 50% share, and its corner dead meal supplied materials is extensive, is directly lost with conventional Burma padauk corner dead meal sawdust
Abandon or sold with per ton hundred yuan of even lower prices and compared in power plant, wash water station-service in burning, the present invention looks forward to for mahogany furniture
The corner dead meal processing of industry provides new approaches, avoids the environmental pollution burned and brought, is advantageous to environment-friendly development.And
Extraction process of the present invention is simple, and effect is good, and process is pollution-free.
The invention provides colouring method of the Burma padauk on polyamide fibre and wool fabric, specific step：
(1) dye liquor is prepared：By obtained Burma padauk dyestuff, alum, levelling agent and water in claim 1 with following quality percentage
Than being formulated, 3~6 parts of the Burma padauk dyestuff, 3~8 parts of the alum, the levelling agent is 1~2 part, and surplus is to go
Ionized water；
(2) dye：Bath raio during dyeing is 1:40~80；With industrial vinegar regulation dye liquor PH=4~6, dyeing temperature is 60~
95, dyeing time is 60~120min；
(3) post-process：Take out after dye liquor is down to room temperature after upper dye, dried with being placed in after cold water flush in baking oven at 60 DEG C.
The colouring method of the present invention, gained dye product odor type is elegant, good color fastness, and there is antiphlogistic antibacterial and medicinal health-care to make
With.
Embodiment
With reference to embodiment, the present invention will be further described, but the present invention does not limit to and these embodiments, should
, it is noted that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, if can also make
Dry modification and improvement, these belong to protection scope of the present invention.
Embodiment 1
The extraction step of the present embodiment Burma padauk dyestuff is：Burma padauk dead meal etc. is taken, 2 are dried in 60 DEG C of baking ovens
Individual hour, low temperature ultra micro mechanical crushing to 100 mesh, by the ethanol that the Burma padauk concentration of volume percent after crushing is 75%
Solution extracts, and feed liquid mass ratio is 1:30, PH=8 is adjusted with plant ash, ultrasonic extraction 2h, vacuum are taken out under 60 DEG C of temperature conditionss
Filter, filter residue are extracted again with method of the same race, are merged filtrate twice, rotated evaporation under reduced pressure distillation and concentration, are obtained natural dye.
Upper dyeing technique step of the present embodiment Burma padauk dyestuff on the fabrics such as polyamide fibre and wool be：
(1) dye liquor is prepared：By obtained Burma padauk dyestuff, alum, levelling agent and water in claim 1 with following quality percentage
Than being formulated, 6 parts of the Burma padauk dyestuff, 3 parts of the alum, the levelling agent is 2 parts, and surplus is deionized water；
(2) dye：Bath raio during dyeing is 1:80；Dye liquor PH=5, dyeing temperature 95, dyeing time are adjusted with industrial vinegar
For 90min；
(3) post-process：Take out after dye liquor is down to room temperature after upper dye, dried with being placed in after cold water flush in baking oven at 60 DEG C.
Embodiment 2
The extraction step of the present embodiment dyestuff is：Burma padauk dead meal etc. is taken, 2 hours are dried in 60 DEG C of baking ovens,
Low temperature ultra micro mechanical crushing carries the Burma padauk after crushing with the ethanol water that concentration of volume percent is 75% to 50 mesh
Take, feed liquid mass ratio is 1:30, the pH value that solution is adjusted with plant ash is 8 or so, ultrasonic extraction 2h, vacuum under the conditions of 60 DEG C
Filter, filter residue is extracted again with method of the same race, is merged filtrate twice, rotated evaporation under reduced pressure distillation and concentration, is obtained naturally big fruit
Red sandalwood dyestuff.
The upper dyeing technique step of Burma padauk dyestuff described in claim 1 on the fabrics such as polyamide fibre and wool is：
(1) dye liquor is prepared：By obtained Burma padauk dyestuff, alum, levelling agent and water in claim 1 with following quality percentage
Than being formulated, 4 parts of the Burma padauk dyestuff, 2 parts of the alum, the levelling agent is 2 parts, and surplus is deionized water；
(2) dye：Bath raio during dyeing is 1:60；Dye liquor PH=8, dyeing temperature 90, dyeing time are adjusted with industrial vinegar
For 100min；
(3) post-process：Take out after dye liquor is down to room temperature after upper dye, dried with being placed in after cold water flush in baking oven at 60 DEG C.
Embodiment 3
The extraction step of the present embodiment dyestuff is：Burma padauk dead meal etc. is taken, 2 hours are dried in 70 DEG C of baking ovens,
Low temperature ultra micro mechanical crushing is to 50 mesh, by the Burma padauk PH=7 after crushing, the ethanol grass that concentration of volume percent is 75%
The wood ash aqueous solution is extractant, and feed liquid mass ratio is 1:40, under the conditions of temperature is 60 DEG C after ultrasonic extraction 2h, it is filtered by vacuum, filter
Slag is extracted again with method of the same race, is merged filtrate twice, rotated evaporation under reduced pressure distillation, concentration, is obtained natural dye.
The upper dyeing technique step of Burma padauk dyestuff described in claim 1 on the fabrics such as polyamide fibre and wool is：
(1) dye liquor is prepared：By obtained Burma padauk dyestuff, alum, levelling agent and water in claim 1 with following quality percentage
Than being formulated, 5 parts of the Burma padauk dyestuff, 3 parts of the alum, the levelling agent is 2 parts, and surplus is deionized water；
(2) dye：Bath raio during dyeing is 1:60；Dye liquor PH=4, dyeing temperature 80, dyeing time are adjusted with industrial vinegar
For 120min；
(3) post-process：Take out after dye liquor is down to room temperature after upper dye, dried with being placed in after cold water flush in baking oven at 70 DEG C.
Claims (4)
1. dyeing method on a kind of Burma padauk dyestuff and fabric, it is characterised in that step is：Burma padauk dead meal etc. is taken, in
2 hours, low temperature ultra micro mechanical crushing to 50~100 mesh, by the Burma padauk body after crushing are dried in 60~80 DEG C of baking ovens
The ethanol solution that product percent concentration is 50~75% extracts, and feed liquid mass ratio is 1:15~40, and adjust pH value with plant ash
For 5~9,2~4h of ultrasonic extraction, is then filtered by vacuum under 60~80 DEG C of temperature conditionss, and filter residue is extracted again with method of the same race,
Merge filtrate twice, the rotated evaporation under reduced pressure distillation and concentration of filtrate, obtain natural Burma padauk dyestuff.
2. the upper dyeing technique step of Burma padauk dyestuff described in claim 1 on the fabrics such as polyamide fibre and wool is：
(1) dye liquor is prepared：By obtained Burma padauk dyestuff, alum, levelling agent and water in claim 1 with following quality percentage
Than being formulated, 3~6 parts of the Burma padauk dyestuff, 3~8 parts of the alum, the levelling agent is 1~2 part, and surplus is to go
Ionized water；
(2) dye：Bath raio during dyeing is 1:40~80；With industrial vinegar regulation dye liquor PH=4~6, dyeing temperature is 60~
95, dyeing time is 60~120min；
(3) post-process：Take out after dye liquor is down to room temperature after upper dye, dried with being placed in after cold water flush in baking oven at 60~80 DEG C
It is dry.
3. the Burma padauk dead meal described in claim 1 includes but is not limited to heart sapwood offal, sawdust etc..
4. fabric described in claim 2 includes but is not limited to polyamide fibre and wool etc..
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710740089.9A CN107501993A (en) | 2017-08-25 | 2017-08-25 | Dyeing method on a kind of Burma padauk dyestuff and fabric |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710740089.9A CN107501993A (en) | 2017-08-25 | 2017-08-25 | Dyeing method on a kind of Burma padauk dyestuff and fabric |
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| CN107501993A true CN107501993A (en) | 2017-12-22 |
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| CN201710740089.9A Pending CN107501993A (en) | 2017-08-25 | 2017-08-25 | Dyeing method on a kind of Burma padauk dyestuff and fabric |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108864742A (en) * | 2018-09-13 | 2018-11-23 | 爱慕股份有限公司 | The method of plant ash method extraction pigment |
| CN113389069A (en) * | 2021-07-02 | 2021-09-14 | 浙江理工大学 | Blue-violet natural dye color matching and dyeing method based on natural eutectic solvent and microwave extraction technology |
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| CN101397407A (en) * | 2007-09-27 | 2009-04-01 | 马中华 | Bacterial extracted from broad-leaf species and natural antibacterial dye of adoukdeafric combinations |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108864742A (en) * | 2018-09-13 | 2018-11-23 | 爱慕股份有限公司 | The method of plant ash method extraction pigment |
| CN113389069A (en) * | 2021-07-02 | 2021-09-14 | 浙江理工大学 | Blue-violet natural dye color matching and dyeing method based on natural eutectic solvent and microwave extraction technology |
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Application publication date: 20171222 |