CN107384611A - A kind of preparation method of cleaning agent for glassware - Google Patents

A kind of preparation method of cleaning agent for glassware Download PDF

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Publication number
CN107384611A
CN107384611A CN201710646280.7A CN201710646280A CN107384611A CN 107384611 A CN107384611 A CN 107384611A CN 201710646280 A CN201710646280 A CN 201710646280A CN 107384611 A CN107384611 A CN 107384611A
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CN
China
Prior art keywords
parts
solution
preparation
powder
cleaning agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710646280.7A
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Chinese (zh)
Inventor
武娟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hefei Yutai Glass Products Co Ltd
Original Assignee
Hefei Yutai Glass Products Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hefei Yutai Glass Products Co Ltd filed Critical Hefei Yutai Glass Products Co Ltd
Priority to CN201710646280.7A priority Critical patent/CN107384611A/en
Publication of CN107384611A publication Critical patent/CN107384611A/en
Withdrawn legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C11D1/721—End blocked ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2006—Monohydric alcohols
    • C11D3/201—Monohydric alcohols linear
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2006—Monohydric alcohols
    • C11D3/2034—Monohydric alcohols aromatic
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2079—Monocarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/28—Heterocyclic compounds containing nitrogen in the ring
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/30—Amines; Substituted amines ; Quaternized amines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776—Heterocyclic compounds, e.g. lactam

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Detergent Compositions (AREA)

Abstract

A kind of preparation method of cleaning agent for glassware, including following preparation process：A, PVP, AEO and deionized water are mixed, obtains solution one；B, nano-colloid particle, additive and decontamination promoting agent are added in solution one, heats and stir to obtain solution two；C, hydroxy compounds, stalk fibre powder are added into solution two, heats and stirs, obtain solution three；D, the pH value of solution three, filtering, you can obtain finished product are adjusted.Present invention process flow is succinct, and reasonable raw material proportioning, raw material is cheap and easy to get, nontoxic, does not have any pollution to environment not only, while long-term use of, and air is pleasant, is easy to promote and uses.

Description

A kind of preparation method of cleaning agent for glassware
Technical field
The invention belongs to glass cleaner technical field, and in particular to a kind of preparation side of cleaning agent for glassware Method.
Background technology
Glass is fused together by sand and other chemical substances and formed, and contiguous network structure is formed in melting, Viscosity gradually increases and hardened and non crystallized silicates nonmetallic materials in cooling procedure.The chemical composition of simple glass is Na2OCaO6SiO2, main component are silica.It is widely used in building, for every wind printing opacity, belonging to mixture, Separately there are the oxide for being mixed into some metals or salt and show the coloured glass of color, and by made from specific process Safety glass etc..
Glass cleaner is used to be primarily adapted for use in the various glass such as lucite, unorganic glass, optical glass, plexiglas Product and optical mirror slip, eyeglass, swimming glasses eyeglass, photographic goods camera lens, the high-efficiency cleaning preparation of high-grade precision glass instrument.
In actual life, people replace glass cleaner to be used for the clear of glass commonly using running water or liquid detergent It is clean, because glass is highly corrosion resistant product in people's impression, but in fact, when glass uses in the medium such as air and weak acid After a period of time, the signs such as coarse glass surface, pollution and dot etching with the naked eye can be observed.Long-term use of running water or Not only cleaning performance is poor for glass cleaner inferior cleaning glassware, and may cause the damage of precision glass component corrosion, with The generation for situations such as the zero of glass connection is corroded and is stained with metal parts.
In summary, it is therefore desirable to which a kind of preferably cleaning agent improves the deficiencies in the prior art.
The content of the invention
It is an object of the invention to provide a kind of preparation method of the cleaning agent for glassware, the letter of present invention process flow Clean, reasonable raw material proportioning, raw material is cheap and easy to get, nontoxic, does not have any pollution to environment not only, while long-term use of, empty Gas is pleasant, is easy to promote and uses.
The invention provides following technical scheme：
A kind of preparation method of cleaning agent for glassware, including following preparation process：
A, PVP, AEO and deionized water are mixed, obtains solution one；
B, nano-colloid particle, additive and decontamination promoting agent are added in solution one, heats and stir at 60-70 DEG C, when Between be 30-40min, obtain solution two；
C, hydroxy compounds, stalk fibre powder are added into solution two, heating and high-speed stirred, mixing speed at 80-100 DEG C For 200-300r/min, time 25-35min, solution three is obtained；
D, the pH value of solution three is adjusted in 7.5-9, filter 23-5 times, you can obtain finished product.
Preferably, the cleaning agent includes the raw material of following parts by weight：PVP 32-38 parts, poly alkyl alcohol Oxygen vinethene 25-29 parts, deionized water 45-49 parts, nano-colloid particle 24-28 parts, additive 18-22 parts, decontamination promoting agent 17-24 parts, hydroxy compounds 22-25 parts and stalk fibre powder 45-55 parts.
Preferably, the nano-colloid particle of the step b is in nano silicone diatomaceous earth, carclazyte, talcum powder and bentonite Any one or more mixing.
Preferably, the additive of the step b is any of dyestuff, spices and preservative or a variety of mixing.
Preferably, the decontamination promoting agent of the step b is triethanolamine, acetic acid, BTA, quaternary ammonium salt and polyethylene Than any of pyrrolidone or a variety of mixing.
Preferably, the hydroxy compounds of the step c is any in isopropanol and methanol, ethanol, propyl alcohol and phenol Kind or a variety of mixing.
Preferably, the stalk fibre powder of the step c is Wheat Straw powder, rice straw powder, corn stalk powder, rape stalk Any of powder and broomcorn straw powder or a variety of mixing.
Preferably, the stalk fibre powder was milled to 500-600 mesh sieves using ball mill, in 60-70 DEG C of environment Dry to water content below 5%.
The beneficial effects of the invention are as follows：
Present invention process flow is succinct, and reasonable raw material proportioning, raw material is cheap and easy to get, nontoxic, not only not any to environment Pollution, at the same it is long-term use of, and air is pleasant, is easy to promote and uses.
Glass cleaner prepared by the present invention is metal ion, cleaning performance be not good, it is easy to removes each on glass Kind dirt, including dust, various edible oils, shellac etc., and precision glass part is not damaged.
Glass cleaner prepared by the present invention is in alkalescent, after being cleaned to glassware, without any residual thing, dirt-removing power Up to more than 98%.
Glass cleaner prepared by the present invention has long-acting anti-fog function, clean and bright after wiping, and need not wash, and avoids glass Glass product produces mist film in the case where there is the temperature difference with steam, is brought convenience for daily life.
Embodiment
Embodiment 1
A kind of preparation method of cleaning agent for glassware, including following preparation process：
A, PVP, AEO and deionized water are mixed, obtains solution one；
B, nano-colloid particle, additive and decontamination promoting agent are added in solution one, heats and stir at 60 DEG C, the time is 40min, obtain solution two；
C, hydroxy compounds, stalk fibre powder are added into solution two, heating and high-speed stirred, mixing speed are at 80 DEG C 300r/min, time 25min, obtain solution three；
D, the pH value of solution three is adjusted 9, is filtered 4 times, you can obtain finished product.
Cleaning agent includes the raw material of following parts by weight：38 parts of PVP, 25 parts of AEO, go 49 parts of ionized water, 24 parts of nano-colloid particle, 22 parts of additive, 17 parts of decontamination promoting agent, 25 parts of hydroxy compounds and stalk are fine Tie up 45 parts of powder.
Step b nano-colloid particle is nano silicone diatomaceous earth, carclazyte, talcum powder and bentonitic mixing.
Step b additive is the mixing of dyestuff, spices and preservative.
Step b decontamination promoting agent is triethanolamine, acetic acid, BTA, quaternary ammonium salt and PVP Mixing.
Step c hydroxy compounds is the mixing of isopropanol and methanol, ethanol, propyl alcohol and phenol.
Step c stalk fibre powder is Wheat Straw powder, rice straw powder, corn stalk powder, rape straw and sorghum stalks The mixing of stalk powder.
Stalk fibre powder was milled to 600 mesh sieves using ball mill, in 60 DEG C of environment dry to water content 5% with Under.
Embodiment 2
A kind of preparation method of cleaning agent for glassware, including following preparation process：
A, PVP, AEO and deionized water are mixed, obtains solution one；
B, nano-colloid particle, additive and decontamination promoting agent are added in solution one, heats and stir at 60 DEG C, the time is 40min, obtain solution two；
C, hydroxy compounds, stalk fibre powder are added into solution two, heating and high-speed stirred, mixing speed are at 100 DEG C 200r/min, time 25min, obtain solution three；
D, the pH value of solution three is adjusted 7.5, is filtered 5 times, you can obtain finished product.
Cleaning agent includes the raw material of following parts by weight：32 parts of PVP, 25 parts of AEO, go 45 parts of ionized water, 24 parts of nano-colloid particle, 18 parts of additive, 17 parts of decontamination promoting agent, 22 parts of hydroxy compounds and stalk are fine Tie up 45 parts of powder.
Step b nano-colloid particle is nano silicone diatomaceous earth, carclazyte, talcum powder and bentonitic mixing.
Step b additive is the mixing of dyestuff, spices and preservative.
Step b decontamination promoting agent is triethanolamine, acetic acid, BTA, quaternary ammonium salt and PVP Mixing.
Step c hydroxy compounds is the mixing of isopropanol and methanol, ethanol, propyl alcohol and phenol.
Step c stalk fibre powder is Wheat Straw powder, rice straw powder, corn stalk powder, rape straw and sorghum stalks The mixing of stalk powder.
Stalk fibre powder was milled to 500 mesh sieves using ball mill, in 60 DEG C of environment dry to water content 5% with Under.
Embodiment 3
A kind of preparation method of cleaning agent for glassware, including following preparation process：
A, PVP, AEO and deionized water are mixed, obtains solution one；
B, nano-colloid particle, additive and decontamination promoting agent are added in solution one, heats and stir at 70 DEG C, the time is 40min, obtain solution two；
C, hydroxy compounds, stalk fibre powder are added into solution two, heating and high-speed stirred, mixing speed are at 100 DEG C 300r/min, time 35min, obtain solution three；
D, the pH value of solution three is adjusted 9, filter 23, you can obtain finished product.
Cleaning agent includes the raw material of following parts by weight：38 parts of PVP, 29 parts of AEO, go 45 parts of ionized water, 28 parts of nano-colloid particle, 18 parts of additive, 24 parts of decontamination promoting agent, 25 parts of hydroxy compounds and stalk are fine Tie up 45 parts of powder.
Step b nano-colloid particle is nano silicone diatomaceous earth, carclazyte, talcum powder and bentonitic mixing.
Step b additive is the mixing of dyestuff, spices and preservative.
Step b decontamination promoting agent is triethanolamine, acetic acid, BTA, quaternary ammonium salt and PVP Mixing.
Step c hydroxy compounds is the mixing of isopropanol and methanol, ethanol, propyl alcohol and phenol.
Step c stalk fibre powder is Wheat Straw powder, rice straw powder, corn stalk powder, rape straw and sorghum stalks The mixing of stalk powder.
Stalk fibre powder was milled to 600 mesh sieves using ball mill, in 70 DEG C of environment dry to water content 5% with Under.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention God any modification, equivalent substitution and improvements made etc., should be included in the scope of the protection with principle.

Claims (8)

1. the preparation method of a kind of cleaning agent for glassware, it is characterised in that including following preparation process：
A, PVP, AEO and deionized water are mixed, obtains solution one；
B, nano-colloid particle, additive and decontamination promoting agent are added in solution one, heats and stir at 60-70 DEG C, when Between be 30-40min, obtain solution two；
C, hydroxy compounds, stalk fibre powder are added into solution two, heating and high-speed stirred, mixing speed at 80-100 DEG C For 200-300r/min, time 25-35min, solution three is obtained；
D, the pH value of solution three is adjusted in 7.5-9, filter 23-5 times, you can obtain finished product.
2. the preparation method of a kind of cleaning agent for glassware according to claim 1, it is characterised in that described clear Lotion includes the raw material of following parts by weight：PVP 32-38 parts, AEO 25-29 parts, deionization Water 45-49 parts, nano-colloid particle 24-28 parts, additive 18-22 parts, decontamination promoting agent 17-24 parts, hydroxy compounds 22-25 Part and stalk fibre powder 45-55 parts.
A kind of 3. preparation method of cleaning agent for glassware according to claim 1, it is characterised in that the step Rapid b nano-colloid particle is any of nano silicone diatomaceous earth, carclazyte, talcum powder and bentonite or a variety of mixing.
A kind of 4. preparation method of cleaning agent for glassware according to claim 1, it is characterised in that the step Rapid b additive is any of dyestuff, spices and preservative or a variety of mixing.
A kind of 5. preparation method of cleaning agent for glassware according to claim 1, it is characterised in that the step Rapid b decontamination promoting agent for any of triethanolamine, acetic acid, BTA, quaternary ammonium salt and PVP or A variety of mixing.
A kind of 6. preparation method of cleaning agent for glassware according to claim 1, it is characterised in that the step Rapid c hydroxy compounds is any of isopropanol and methanol, ethanol, propyl alcohol and phenol or a variety of mixing.
A kind of 7. preparation method of cleaning agent for glassware according to claim 1, it is characterised in that the step Rapid c stalk fibre powder is appointing in Wheat Straw powder, rice straw powder, corn stalk powder, rape straw and broomcorn straw powder One or more mixing.
A kind of 8. preparation method of cleaning agent for glassware according to claim 7, it is characterised in that the straw Stalk fiber powder was milled to 500-600 mesh sieves using ball mill, was dried in 60-70 DEG C of environment to water content below 5%.
CN201710646280.7A 2017-08-01 2017-08-01 A kind of preparation method of cleaning agent for glassware Withdrawn CN107384611A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108277095A (en) * 2017-12-30 2018-07-13 安徽杜氏高科玻璃有限公司 A kind of cleaning treatment technique of glass

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103103027A (en) * 2012-12-10 2013-05-15 苏州丰儒软件有限公司 Glass product cleaning agent and preparation method thereof
CN105154255A (en) * 2015-08-24 2015-12-16 安徽万宝玻璃有限公司 Plant-source glass cleaning agent and preparation method thereof
CN105586166A (en) * 2016-03-04 2016-05-18 苏州圣谱拉新材料科技有限公司 Corrosion-resistant glass cleaner and preparation method thereof
CN105695134A (en) * 2016-03-04 2016-06-22 苏州圣谱拉新材料科技有限公司 Glass cleaning agent with antifogging function

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103103027A (en) * 2012-12-10 2013-05-15 苏州丰儒软件有限公司 Glass product cleaning agent and preparation method thereof
CN105154255A (en) * 2015-08-24 2015-12-16 安徽万宝玻璃有限公司 Plant-source glass cleaning agent and preparation method thereof
CN105586166A (en) * 2016-03-04 2016-05-18 苏州圣谱拉新材料科技有限公司 Corrosion-resistant glass cleaner and preparation method thereof
CN105695134A (en) * 2016-03-04 2016-06-22 苏州圣谱拉新材料科技有限公司 Glass cleaning agent with antifogging function

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108277095A (en) * 2017-12-30 2018-07-13 安徽杜氏高科玻璃有限公司 A kind of cleaning treatment technique of glass

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Application publication date: 20171124