CN107320355A - A kind of collagen protein face and preparation method thereof - Google Patents
A kind of collagen protein face and preparation method thereof Download PDFInfo
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- CN107320355A CN107320355A CN201710624677.6A CN201710624677A CN107320355A CN 107320355 A CN107320355 A CN 107320355A CN 201710624677 A CN201710624677 A CN 201710624677A CN 107320355 A CN107320355 A CN 107320355A
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- collagen
- collagen protein
- protein face
- skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- General Health & Medical Sciences (AREA)
- Public Health (AREA)
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- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Birds (AREA)
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Abstract
The present invention relates to a kind of collagen protein face and preparation method thereof.Collagen protein face disclosed by the invention includes component：Collagen, pH adjusting agent, NMF, skin conditioning agent, preservative and solvent, the molecular weight of the collagen is 1000D 3000D.The collagen protein face that the present invention is provided can infiltrate into deep skin rapidly, supply nutrition, promote cytothesis and improve skin pattern, prevent facial anaphylaxis dermatoses, restrain acceleration of wound reparation, reduce pigmentation and pre- anti-aging effect.
Description
Technical field
The invention belongs to cosmetic composition technical field, more particularly to a kind of collagen protein face and preparation method thereof.
Background technology
Collagen is a kind of biological polymer substance synthesized by fibroblast, be people's in-vivo content it is most abundant,
Widest protein is distributed, the 25%-30% of whole body gross protein is accounted for, the 71.2% of human body skin protein is accounted for.Collagen egg
The positions such as skin, ligament, tendon, cartilage are distributed mainly in vain, the work for the morphosis for maintaining skin and each histoorgan is played
With while being also the important source material material for repairing each injury tissue.
Collagen contains the amino acid such as glycine needed by human, proline and hydroxyproline, because of its high-hydrophilic, low
Toxicity, faint antigenic, good vivo biodistribution compatibility, complete biodegradability, with significant crease-resistant, U.S.
In vain, the beauty functions such as reparation, moisturizing, nourishing, improvement skin elasticity, radioresistance.
With people to the continuous improvement of quality of the life and to the cognitive intensification of collagen effect, people are to containing collagen
The demand of the personal skin quality skin care products of protein peptides can be increasing, wherein, facial mask is used as cleaning, nursing and nutrition skin of face
The single product of cosmetics situation of selling well, obtain the accreditation of more and more people.
Chinese patent CN10376971B discloses a kind of whitening and softening skin facial mask, is made up of following component：Centella, biography are bright
Acid, provitamin, vitamin B3, vitamin C, allantoin, licoflavone, ceramide, glucan, Sodium Hyaluronate, the third two
Alcohol, 1,3 butylene glycol, collagen, amino acid, witch hazel, Matrixyl -3, ethoxy urea, hydroxyethyl cellulose, azone
And deionized water.Although the whitening and softening skin facial mask can skin whitening, bright color, used in the whitening and softening skin facial mask
Collagen handled by gelatin, be collagen hydrolysate for albuminate single-stranded and inactive α, i.e., carried by thermal denaturation
Collagen is produced, part hydrolyzable, material, molecule knot formed by reduction molecular weight are carried out to it using protease
Structure is changed, and degraded is quickly.Though the collagen is soluble in water, activity is lost, it is impossible to repair and other physiology are made
With.
There is no any prior art to provide all advantages and benefit of the present invention.
The content of the invention
It is an object of the invention to the defect for solving prior art presence, there is provided a kind of its preparation side of collagen protein face
Method.The object of the invention to solve the technical problems is realized using following technical scheme.
On the one hand, the invention provides a kind of collagen protein face, using the gross weight of the collagen protein face as base
Standard, including following components：0.01wt%-0.5wt% collagens, 0.1wt%-5.0wt%PH conditioning agents, 6.0wt%-
15.0wt% NMFs, 0.5wt-5.0wt% skin conditioning agents, 0.3wt%-1.0wt% preservatives, surplus is solvent, and institute
The molecular weight for stating collagen is 1000D-3000D.The present inventor has found that said components are effective by substantial amounts of experiment
With reference to, collagen high-hydrophilic, hypotoxicity, faint antigenic, good vivo biodistribution compatibility can be made full use of, it is above-mentioned
Collagen protein face can infiltrate into deep skin rapidly, supply nutrition, promote cytothesis and improve skin pattern, prevention face
Anaphylaxis dermatosis, restrain acceleration of wound reparation, reduce pigmentation and pre- anti-aging effect.The present invention is using spongiform
Collagen product, its molecular weight is 1000D-3000D, retains its original network structure, is a kind of sterile, nontoxic and nonreactive
Originality, still retains original structure and the integrality structural proteins of bioactivity, with significant crease-resistant, whitening, reparation, moisturizing, taste
Support, improve the beauty functions such as skin elasticity, radioresistance.
In certain embodiments, on the basis of the gross weight of the collagen protein face, including following components：With the glue
On the basis of the gross weight of former protein facial mask, including following components：0.1wt%-0.4wt% collagens, 1.0wt%-4.0wt%
PH conditioning agents, 7.0wt%-12.0wt% NMFs, 1.5wt-4.5.0wt% skin conditioning agents, 0.5wt%-0.8wt% anti-corrosions
Agent, surplus is solvent.
In certain embodiments, the collagen is selected from class human-like collagen, ox derived collagen albumen, pig source property glue
The one or more of former albumen or source of fish property collagen.
In certain embodiments, the pH adjusting agent is selected from citric acid, acetic acid, hydrochloric acid, sodium citrate and sodium hydroxide
One or more mixtures.It is further preferred that the pH value of the facial mask is 4.0-5.5.
In certain embodiments, the NMF is selected from glycerine, butanediol, methyl propanediol, panthenol, one kind of trehalose
Or a variety of mixtures.
In certain embodiments, described skin conditioning agent is selected from purslane extract, hyaluronic acid, one kind of niacinamide
Or a variety of mixtures.
In certain embodiments, the preservative is selected from methyl hydroxybenzoate, Nipasol, Chlorphenesin, decoyl hydroximic acid
One or more mixtures.
In certain embodiments, the pH value of the facial mask is 4.0-5.5.
In certain embodiments, the solvent is water.Further preferred the, the solvent is deionized water.
On the other hand, present invention also offers a kind of preparation method of collagen protein face liquid, including step：S1, general
Part water, hydrochloric acid solution, sodium hydroxide solution mixing, pH is between 4.0-5.5 for regulation, obtains mixed solution；S2, by collagen
Above-mentioned mixed solution is added, stirs to being uniformly dissolved, obtains collagen solution；S3, the water for weighing remaining part, NMF, skin
Skin conditioner, preservative are uniformly dissolved to obtain collagen protein face liquid.
The beneficial effects of the present invention are：The collagen protein face that invention is provided has smooth skin, and depth supplies nutrition,
Promote cytothesis and improve skin pattern, prevent facial anaphylaxis dermatoses, restrain acceleration of wound reparation, reduce pigmentation
And pre- anti-aging effect.
Embodiment
In the present invention, unless otherwise indicated, all percentage, number and ratio are with the total of the composition of the present invention
Weight meter.The weight of listed composition is related in terms of its activity substance content, thus it is not commercially available including being possibly comprised in
Carrier or byproduct in product.
The all the components used in the present invention, such as active material and other compositions can be according to their beauty and/or treatment
Effect or the mode of action that they assume are classified or described it should be apparent that in some cases, being used in the present invention
Active material and other compositions can provide more than one beauty and/or therapeutic action or be acted as by way of more than one
With.Therefore, classification of the invention is intended merely to conveniently, and is not intended to a kind of composition being limited in the application or listed of specific descriptions
Using upper." appropriate " of the present invention, which refers to, to be enough substantially to induce positive beneficial effect, preferably good skin appearance or sense
Beneficial effect in terms of feel, the amount of compound or composition independently including beneficial effect disclosed by the invention, is this area
Technical staff can rationally judge what is held.
On the one hand, the invention provides a kind of collagen protein face, including following components：Collagen, pH adjusting agent,
NMF, skin conditioning agent, preservative and solvent, the molecular weight of the collagen is 1000D-3000D.The invention of the present invention
People has found that said components effectively combine by substantial amounts of experiment, can make full use of collagen high-hydrophilic, hypotoxicity, faint
Antigenic, good vivo biodistribution compatibility, above-mentioned collagen protein face can infiltrate into deep skin rapidly, supply nutrition,
Promote cytothesis and improve skin pattern, prevent facial anaphylaxis dermatoses, restrain acceleration of wound reparation, reduce pigmentation
And pre- anti-aging effect.
In certain embodiments, on the basis of the gross weight of the collagen protein face, including following components：
0.01wt%-0.5wt% collagens, 0.1wt%-5.0wt%PH conditioning agents, 6.0wt%-15.0wt% NMFs,
0.5wt-5.0wt% skin conditioning agents, 0.3wt%-1.0wt% preservatives, surplus is solvent.It is highly preferred that with the collagen
On the basis of the gross weight of protein facial mask, including following components：Collagen 0.01wt%-0.3wt%, 0.1mol/L hydrochloric acid solution
0.1wt%-3wt%, sodium hydroxide 0.01wt%-0.5wt%, butanediol 6wt%-10wt%, methyl propanediol 1wt%-
5wt%, trehalose 0.2wt%-2wt%, purslane extract 0.1wt%-3wt%, methyl hydroxybenzoate 0.05wt%-0.4wt%,
Decoyl hydroximic acid 0.1wt%-1.0wt%, surplus is water.Still further preferably, with the gross weight of the collagen protein face
On the basis of, including following components：Collagen 0.2wt%, 0.1mol/L hydrochloric acid solution 0.6wt%, sodium hydroxide 0.02wt%,
Butanediol 8wt%, methyl propanediol 3wt%, trehalose 1wt%, purslane extract 1wt%, Chlorphenesin 0.12wt% are pungent
Acyl hydroximic acid 0.5wt%, surplus is water.
In certain embodiments, the collagen is selected from class human-like collagen, ox derived collagen albumen, pig source property glue
The one or more of former albumen or source of fish property collagen.
In certain embodiments, the pH adjusting agent is selected from citric acid, acetic acid, hydrochloric acid, sodium citrate and sodium hydroxide
One or more mixtures.It is further preferred that the pH value of the facial mask is 4.0-5.5.
In certain embodiments, the NMF is selected from glycerine, butanediol, methyl propanediol, panthenol, one kind of trehalose
Or a variety of mixtures.
In certain embodiments, described skin conditioning agent is selected from purslane extract, hyaluronic acid, one kind of niacinamide
Or a variety of mixtures.
In certain embodiments, the preservative is selected from methyl hydroxybenzoate, Nipasol, Chlorphenesin, decoyl hydroximic acid
One or more mixtures.
In certain embodiments, the pH value of the facial mask is 4.0-5.5.
In certain embodiments, the solvent is water.Further preferred the, the solvent is deionized water.
On the other hand, present invention also offers a kind of preparation method of collagen protein face liquid, including step：S1, general
Part water, hydrochloric acid solution, sodium hydroxide solution mixing, pH is between 4.0-5.5 for regulation, obtains mixed solution；S2, by collagen
Above-mentioned mixed solution is added, stirs to being uniformly dissolved, obtains collagen solution；S3, the water for weighing remaining part, NMF, skin
Skin conditioner, preservative are uniformly dissolved to obtain collagen protein face liquid.
For the ease of it will be appreciated by those skilled in the art that can be with by the preferred specific embodiment of invention now given below
The present invention is further appreciated that, but it is not limitation of the invention.For those skilled in the art according to foregoing invention content
The nonessential improvement of some made and adjustment, are also considered as within the scope of the present invention.
Embodiment 1
Preparation technology：
1) part water, 0.1mol/L hydrochloric acid solutions, sodium hydroxide are weighed, pH is between 4.0-5.5 for regulation, obtains mixed solution
2) class human-like collagen is added in above-mentioned mixed solution, stirs to being uniformly dissolved, obtain collagen solution
3) water, butanediol, methyl propanediol, trehalose and the Chlorphenesin for weighing remaining part dissolve by heating uniform, drop
Warm to room temperature, add purslane extract, decoyl hydroximic acid and above-mentioned collagen solution, be well mixed, obtain collagen face
Film liquid.
Embodiment 2
Preparation technology：
1) part water, 0.1mol/L hydrochloric acid solutions, sodium hydroxide are weighed, pH is between 4.0-5.5 for regulation, obtains mixed solution
2) ox derived collagen albumen is added in above-mentioned mixed solution, stirs to being uniformly dissolved, obtain collagen solution
3) water, butanediol, methyl propanediol, trehalose and the Chlorphenesin for weighing remaining part dissolve by heating uniform, drop
Warm to room temperature, add purslane extract, decoyl hydroximic acid and above-mentioned collagen solution, be well mixed, obtain collagen face
Film liquid.
Embodiment 3
Preparation technology：
1) part water, 0.1mol/L hydrochloric acid solutions, sodium hydroxide are weighed, pH is between 4.0-5.5 for regulation, obtains mixed solution
2) pig derived collagen albumen is added in above-mentioned mixed solution, stirs to being uniformly dissolved, obtain collagen solution
3) water, butanediol, methyl propanediol, trehalose and the Chlorphenesin for weighing remaining part dissolve by heating uniform, drop
Warm to room temperature, add purslane extract, decoyl hydroximic acid and above-mentioned collagen solution, be well mixed, obtain collagen face
Film liquid.
Embodiment 4
Preparation technology：
1) part water, 0.1mol/L hydrochloric acid solutions, sodium hydroxide are weighed, pH is between 4.0-5.5 for regulation, obtains mixed solution
2) property collagen in the source of fish is added in above-mentioned mixed solution, stirs to being uniformly dissolved, obtain collagen solution
3) water, butanediol, methyl propanediol, trehalose and the Chlorphenesin for weighing remaining part dissolve by heating uniform, drop
Warm to room temperature, add purslane extract, decoyl hydroximic acid and above-mentioned collagen solution, be well mixed, obtain collagen face
Film liquid.
Comparative example 1
Preparation technology：
1) part water, 0.1mol/L hydrochloric acid solutions, sodium hydroxide are weighed, pH is between 4.0-5.5 for regulation, obtains mixed solution
2) water, butanediol, methyl propanediol, trehalose and the Chlorphenesin for weighing remaining part dissolve by heating uniform, drop
Warm to room temperature, add purslane extract, decoyl hydroximic acid and above-mentioned mixed solution, be well mixed, obtain facial mask liquid
Comparative example 2
With CN10376971B embodiment 1.
Facial mask liquid to above-described embodiment 1-4 and comparative example 1-2 does following test：
First, physical and chemical testing is done to embodiment 1-4 collagen protein face liquid, it is as a result as follows：
1. outward appearance：Translucent thick liquid
2.pH values：4.5-5.5
3. heat-resistant stability investigates (48 DEG C × 24h):It is qualified
4. cold-resistant study on the stability (- 15 DEG C × 24h):It is qualified.
2nd, in order to prove effect of this product, tests below has been carried out：
1. security test：
120 voluntary testers are chosen, every 30 entitled one group, divides four groups, embodiment 1-4 is tested respectively, every
Tester applies on the inside of mask product 15min of the present invention, the right hand and applied to do control test on the inside of left and right arm every time on the inside of left hand
The facial mask liquid 15min of comparative example 1, twice daily, and records the dermoreaction phenomenon after 24h, 72h.
As a result show：Apply after mask product 24h, 72h of the present invention, have no rubefaction or the allergic phenomenas such as erythema occur,
It is safe to illustrate product collagen protein face of the present invention, without any bad phenomenon.
2. antiallergy is tested
Facial mask liquid made from above-described embodiment and comparative example, continuously tries out 30 through the 300 of 30-55 Sui volunteers respectively
My god, the antiallergic effect of facial mask liquid obtained in the various embodiments described above is evaluated in comparative analysis.Wherein, described antiallergic effect
Itch for skin, tingling sensation, tight feeling, erythema, the improvement situation of the tiny scales of skin that peel off etc..As a result it see the table below 1.
Table 1
3. color spot improves test
Experimental method：
Group one (20 people) product of the embodiment of the present invention 1, it is 3 times a day, continuous to use 2 months；
Group two (20 people) product of the embodiment of the present invention 2, it is 3 times a day, continuous to use 2 months；
Group three (20 people) product of the embodiment of the present invention 3, it is 3 times a day, continuous to use 2 months；
Group four (20 people) product of the embodiment of the present invention 4, it is 3 times a day, continuous to use 2 months
Group five (20 people) product of comparative example 1 of the present invention, it is 3 times a day, continuous to use 2 months；
Group six (20 people) product of comparative example 2 of the present invention, it is 3 times a day, continuous to use 2 months.
Experimental result see the table below 2：
Table 2
| Group | Color spot is significantly reduced | Color spot is slightly reduced | Without improvement |
| Group one | 8 | 12 | 0 |
| Group two | 13 | 7 | 0 |
| Group three | 16 | 4 | 0 |
| Group four | 11 | 9 | 0 |
| Group five | 0 | 4 | 16 |
| Group six | 6 | 8 | 4 |
Interpretation of result：Collagen protein face of the present invention has reduces pigmented effect well, can be effectively
Bright color and effect is notable.
Embodiment described above only expresses the several embodiments of the present invention, and it describes more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, when the technology contents using the disclosure above make a little change or modification
For the equivalent embodiment of equivalent variations, as long as being the technical spirit pair according to the present invention without departing from technical solution of the present invention content
Any simple modification, equivalent variations and modification that above example is made, in the range of still falling within technical solution of the present invention.Cause
This, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of collagen protein face, it is characterised in that on the basis of the gross weight of the collagen protein face, including component：
0.01wt%-0.5wt% collagens, 0.1wt%-5.0wt%pH conditioning agents, 6.0wt%-15.0wt% NMFs,
0.5wt-5.0wt% skin conditioning agents, 0.3wt%-1.0wt% preservatives, surplus is solvent, and the molecule of the collagen
Measure as 1000D-3000D.
2. collagen protein face according to claim 1, it is characterised in that using the gross weight of the collagen protein face as
Benchmark, including following components：0.1wt%-0.4wt% collagens, 1.0wt%-4.0wt%PH conditioning agents, 7.0wt%-
12.0wt% NMFs, 1.5wt-4.5.0wt% skin conditioning agents, 0.5wt%-0.8wt% preservatives, surplus is solvent.
3. collagen protein face according to claim 1, it is characterised in that the collagen is selected from class people source collagen egg
In vain, the one or more of ox derived collagen albumen, pig derived collagen albumen or source of fish property collagen.
4. collagen protein face according to claim 1, it is characterised in that the pH adjusting agent be selected from citric acid, acetic acid,
One or more mixtures of hydrochloric acid, sodium citrate and sodium hydroxide.
5. collagen protein face according to claim 1, it is characterised in that the NMF is selected from glycerine, butanediol, first
Base propane diols, panthenol, one or more mixtures of trehalose.
6. collagen protein face according to claim 1, it is characterised in that described skin conditioning agent is carried selected from purslane
Take one or more mixtures of thing, hyaluronic acid, niacinamide.
7. collagen protein face according to claim 1, it is characterised in that the preservative is selected from methyl hydroxybenzoate, oxybenzene
Propyl ester, Chlorphenesin, one or more mixtures of decoyl hydroximic acid.
8. collagen protein face according to claim 1, it is characterised in that the pH value of the facial mask is 4.0-5.5.
9. collagen according to claim 1, it is characterised in that the solvent is water.
10. a kind of preparation method of collagen protein face liquid, it is characterised in that including step：S1, by part water, hydrochloric acid solution,
Sodium hydroxide solution is mixed, and pH is between 4.0-5.5 for regulation, obtains mixed solution；S2, that collagen is added into above-mentioned mixing is molten
Liquid, stirs to being uniformly dissolved, obtains collagen solution；S3, the water for weighing remaining part, NMF, skin conditioning agent, preservative
It is uniformly dissolved to obtain collagen protein face liquid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710624677.6A CN107320355A (en) | 2017-07-27 | 2017-07-27 | A kind of collagen protein face and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710624677.6A CN107320355A (en) | 2017-07-27 | 2017-07-27 | A kind of collagen protein face and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110840765A (en) * | 2019-12-12 | 2020-02-28 | 陕西省石油化工研究设计院 | Antiseptic and bactericidal composition and preparation method thereof |
| US10959933B1 (en) | 2020-06-01 | 2021-03-30 | The Procter & Gamble Company | Low pH skin care composition and methods of using the same |
| US11110049B2 (en) | 2017-06-23 | 2021-09-07 | The Procter & Gamble Company | Composition and method for improving the appearance of skin |
| CN114009794A (en) * | 2021-11-05 | 2022-02-08 | 上海极迦生物科技有限公司 | Composition with function of delaying skin aging and application thereof |
| CN115531241A (en) * | 2022-10-10 | 2022-12-30 | 深圳市诗婷泰格生物科技有限公司 | Collagen mask and production method thereof |
| US11583488B2 (en) | 2020-06-01 | 2023-02-21 | The Procter & Gamble Company | Method of improving penetration of a vitamin B3 compound into skin |
| US11622963B2 (en) | 2018-07-03 | 2023-04-11 | The Procter & Gamble Company | Method of treating a skin condition |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11110049B2 (en) | 2017-06-23 | 2021-09-07 | The Procter & Gamble Company | Composition and method for improving the appearance of skin |
| US11622963B2 (en) | 2018-07-03 | 2023-04-11 | The Procter & Gamble Company | Method of treating a skin condition |
| CN110840765A (en) * | 2019-12-12 | 2020-02-28 | 陕西省石油化工研究设计院 | Antiseptic and bactericidal composition and preparation method thereof |
| US10959933B1 (en) | 2020-06-01 | 2021-03-30 | The Procter & Gamble Company | Low pH skin care composition and methods of using the same |
| US11583488B2 (en) | 2020-06-01 | 2023-02-21 | The Procter & Gamble Company | Method of improving penetration of a vitamin B3 compound into skin |
| US11911498B2 (en) | 2020-06-01 | 2024-02-27 | The Procter & Gamble Company | Low pH skin care composition and methods of using the same |
| CN114009794A (en) * | 2021-11-05 | 2022-02-08 | 上海极迦生物科技有限公司 | Composition with function of delaying skin aging and application thereof |
| CN114009794B (en) * | 2021-11-05 | 2024-01-16 | 上海极迦生物科技有限公司 | Composition with skin aging delaying function and application thereof |
| CN115531241A (en) * | 2022-10-10 | 2022-12-30 | 深圳市诗婷泰格生物科技有限公司 | Collagen mask and production method thereof |
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Application publication date: 20171107 |