CN107267673A - Cane sugar manufacture technique - Google Patents
Cane sugar manufacture technique Download PDFInfo
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- CN107267673A CN107267673A CN201710551059.3A CN201710551059A CN107267673A CN 107267673 A CN107267673 A CN 107267673A CN 201710551059 A CN201710551059 A CN 201710551059A CN 107267673 A CN107267673 A CN 107267673A
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- bagasse
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/02—Expressing juice from sugar cane or similar material, e.g. sorghum saccharatum
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/02—Purification of sugar juices using alkaline earth metal compounds
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/08—Purification of sugar juices by oxidation or reduction
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/16—Purification of sugar juices by physical means, e.g. osmosis or filtration
- C13B20/165—Purification of sugar juices by physical means, e.g. osmosis or filtration using membranes, e.g. osmosis, ultrafiltration
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/002—Evaporating or boiling sugar juice
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/02—Crystallisation; Crystallising apparatus
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of cane sugar manufacture technique, comprise the following steps:Step 1: sugarcane is obtained into bagasse and sugar-cane juice through over cleaning, chopping, squeezing, filtering;Step 2: bagasse is carried out into steam blasting, the bagasse after steam blasting is collected;Step 3: spraying composite enzyme solution to the bagasse surface after steam blasting, enzymolysis liquid is obtained;Step 4: enzymolysis liquid is heated, pre- ash, nitrogen is passed through, sedimentation separation obtains the first clear liquid;Step 5: the first clear liquid is heated, pre- ash is passed through ozone, and sedimentation separation obtains the second clear liquid;Step 6: the second clear liquid is heated into boiling, impurity is filtered out, room temperature is cooled to, ultrafiltration, evaporating, concentrating and crystallizing purging is produced.The sugar that the present invention is produced is free of SO2, the chromatic value and turbidity value of product are effectively reduced, purity and concentration is improved.
Description
Technical field
The present invention relates to refined sugar technical field.It is more particularly related to a kind of cane sugar manufacture technique.
Background technology
China's cane sugar manufacture production more than 95% is applicable sulfurous method clarification process, i.e., using SO2Make primary clarifying agent, with
The Ca of milk of lime2+CaSO of the reaction generation with strong adsorption capacity3Precipitation, will there is the non-sugar absorption such as colloid, pigment in sugarcane juice
Coprecipitation, while SO2Also there is good bleaching, suppress the effect of pigment production.But due in sulfurous method clarifying process, pH
Value control is in neutral range, and sugarcane juice is a complicated component system, and its contained colloidal substance can hinder SO2With Ca2+Generation
CaSO3The reaction of precipitation, therefore unavoidably have SO2Remain in juice, in follow-up boiling process, can be inhaled by sucrose crystal
Attached, parcel enters sugar crystals, causes sugar to contain SO2.SO contained by sugar2Human body can be damaged in storage and edible process
Respiratory tract, eyes, the digestive system of human body, hepatic tissue and lymphatic system etc., therefore sugar sugar containing influence safety.Therefore, mesh
Before need a kind of sugar refining technology with more securities badly.
The content of the invention
It is an object of the invention to solve at least the above, and provide the advantage that at least will be described later.
It is a still further object of the present invention to provide a kind of cane sugar manufacture technique, its sugar produced is free of SO2, effectively reduction production
The chromatic value and turbidity value of product, improve purity and concentration.
In order to realize according to object of the present invention and further advantage there is provided a kind of cane sugar manufacture technique, including with
Lower step:
Step 1: sugarcane is obtained into bagasse and sugar-cane juice through over cleaning, chopping, squeezing, filtering;
Step 2: by bagasse be transferred to temperature be 100 DEG C, steam pressure be that to carry out steam under conditions of 1~2MPa quick-fried
Broken, the steam blasting time is less than 0.01s, and the dwell time is 1min, discharges pressure to normal pressure every 15s afterwards, is discharged into every time
The gross weight of the bagasse of normal pressure is 25%, collects the bagasse after steam blasting;
Step 3: spraying composite enzyme solution to the bagasse surface after steam blasting, surface is infiltrated to dripping, protect
10min is held, then sugar-cane juice is mixed, is squeezed, filtered, obtain enzymolysis liquid, wherein, the mass fraction of composite enzyme solution
0.8%, complex enzyme is glycosidase, trypsase, amylase, the mixture of pectase, often in mL complex enzymes, the vigor of glycosidase
For 6000IU/mL, the vigor of trypsase is 2000IU/mL, and the vigor of amylase is 800IU/mL, and the vigor of pectase is
800IU/mL;
Step 4: enzymolysis liquid is heated into 70~80 DEG C, it is 6.5 to add phosphoric acid and pre- ash is carried out with milk of lime to pH, is led to
Enter nitrogen to 9.0MPa, be warming up to 85 DEG C with 1 DEG C/s speed, be incubated 5min, 90 DEG C, guarantor are warming up to 0.5 DEG C/s speed
Warm 5min, boiling is warming up to 0.1 DEG C/s speed, is incubated 5min, is returned back to atmosphere at room temperature pressure, it is clear that sedimentation separation obtains first
Liquid;
Step 5: the first clear liquid is heated into 70~80 DEG C, add phosphoric acid and is carried out with milk of lime pre- ash to pH be 6.5,
Ozone is passed through to 1.0MPa, 85 DEG C is warming up to 1 DEG C/s speed, is incubated 5min, 90 DEG C are warming up to 0.5 DEG C/s speed,
5min is incubated, boiling is warming up to 0.1 DEG C/s speed, 5min is incubated, returns back to atmosphere at room temperature pressure, sedimentation separation obtains second
Clear liquid;
Step 6: the second clear liquid is heated into boiling, impurity is filtered out, room temperature, ultrafiltration, evaporating, concentrating and crystallizing purging is cooled to
Produce.
Preferably, the nitrogen in described cane sugar manufacture technique, step 4, the ozone in step 5 are by by air
Nitrogen and oxygen-enriched air are separated into, oxygen-enriched air is then prepared what ozone was obtained.
Preferably, the ultrafiltration in described cane sugar manufacture technique, step 6 is by tubular ultra-filtration membrane filter process
Obtain, the membrane flux of tubular ultra-filtration membrane filter is 30L/h/m2。
Preferably, the concentration of the milk of lime in described cane sugar manufacture technique, step 4 is 8~13 Baume degrees.
Preferably, in described cane sugar manufacture technique, step 3, spray compound to the bagasse surface after steam blasting
Before enzyme solutions, in addition to:Immersion, the bagasse after steam blasting is immersed in 6h in ethanol solution, then by squeezing and
Filtering, is repeated 3 times, and filter residue and filtrate are merged respectively, and the filter residue sprinkling composite enzyme solution of merging carries out next step process, merged
Filtrate mixed with the second clear liquid in step 6, carry out next step process.
Preferably, described cane sugar manufacture technique, the concentration of ethanol solution is 75wt.%, the addition of ethanol solution
For:Bagasse surface is not crossed.
The present invention at least includes following beneficial effect:
Firstth, the present invention is expanded by bagasse using steam blasting, makes cellulose, hemicellulose, lignin expanded loose,
It is easy to hydrolysis, repeatedly release pressure is easy to segmented softening fibre, more gently, softens using complex enzyme coordinated enzymatic hydrolysis
Bagasse, further hydrolysis obtains sugar, and suppresses bacterium purity, the concentration of subsequent handling are influenceed, HTHP indifferent gas
Atmosphere is handled enzymolysis liquid, destroys color source property material such as melanin, aldehydes matter, polyphenol oxidase etc., and high temperature higher pressure is smelly
Oxygen is handled the first clear liquid, and color source property material further is oxidized into small molecule colourless substance, reaches color in removal sugarcane juice
The effect of element;
Secondth, air is separated into nitrogen and oxygen-enriched air using usual manner, then oxygen-enriched air is supported into ozone, fully
Using resource, and the air pressure of forming step four, step 5, coordinate high temperature high pressure process;Tubular type ultrafiltration removes what is remained in juice
Colloid, starch polymer material, good decolorizing effect;Alcohol leaching squeezes bagasse, dissolution and Transformation of Sugarcane sugar after steam blasting, just
In shortening follow-up enzymolysis process duration, accelerate sugaring process.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
It should be noted that experimental method described in following embodiments, is conventional method unless otherwise specified, institute
Reagent and material are stated, unless otherwise specified, is commercially obtained.
<Embodiment 1>
A kind of cane sugar manufacture technique, comprises the following steps:
Step 1: sugarcane is obtained into bagasse and sugar-cane juice through over cleaning, chopping, squeezing, filtering;
Step 2: by bagasse be transferred to temperature be 100 DEG C, steam pressure be that to carry out steam under conditions of 1~2MPa quick-fried
Broken, the steam blasting time is less than 0.01s, and the dwell time is 1min, discharges pressure to normal pressure every 15s afterwards, is discharged into every time
The gross weight of the bagasse of normal pressure is 25%, collects the bagasse after steam blasting;
Step 3: spraying composite enzyme solution to the bagasse surface after steam blasting, surface is infiltrated to dripping, protect
10min is held, then sugar-cane juice is mixed, is squeezed, filtered, obtain enzymolysis liquid, wherein, the mass fraction of composite enzyme solution
0.8%, complex enzyme is glycosidase, trypsase, amylase, the mixture of pectase, often in mL complex enzymes, the vigor of glycosidase
For 6000IU/mL, the vigor of trypsase is 2000IU/mL, and the vigor of amylase is 800IU/mL, and the vigor of pectase is
800IU/mL;
Step 4: enzymolysis liquid is heated into 70~80 DEG C, add phosphoric acid and is carried out with milk of lime pre- ash to pH be 6.5, stone
The concentration of grey breast is 8~13 Baume degrees, is passed through nitrogen to 9.0MPa, is warming up to 85 DEG C with 1 DEG C/s speed, is incubated 5min, with
0.5 DEG C/s speed is warming up to 90 DEG C, is incubated 5min, and boiling is warming up to 0.1 DEG C/s speed, is incubated 5min, returns back to room
Warm atmospheric pressure, sedimentation separation obtains the first clear liquid;
Step 5: the first clear liquid is heated into 70~80 DEG C, add phosphoric acid and is carried out with milk of lime pre- ash to pH be 6.5,
The concentration of milk of lime is 8~13 Baume degrees, is passed through ozone to 1.0MPa, is warming up to 85 DEG C with 1 DEG C/s speed, is incubated 5min,
90 DEG C are warming up to 0.5 DEG C/s speed, 5min is incubated, boiling is warming up to 0.1 DEG C/s speed, 5min is incubated, returns back to
Atmosphere at room temperature pressure, sedimentation separation obtains the second clear liquid;
Step 6: the second clear liquid is heated into boiling, impurity is filtered out, room temperature is cooled to, passes through tubular ultra-filtration membrane filter
Processing, the membrane flux of tubular ultra-filtration membrane filter is 30L/h/m2, evaporating, concentrating and crystallizing purging produces;
Wherein, the nitrogen in step 4, the ozone in step 5 are by being separated into by air liquefaction, using boiling point difference
Nitrogen and oxygen-enriched air, then prepare what ozone was obtained by oxygen-enriched air ionization.
<Embodiment 2>
A kind of cane sugar manufacture technique, comprises the following steps:
Step 1: sugarcane is obtained into bagasse and sugar-cane juice through over cleaning, chopping, squeezing, filtering;
Step 2: by bagasse be transferred to temperature be 100 DEG C, steam pressure be that to carry out steam under conditions of 1~2MPa quick-fried
Broken, the steam blasting time is less than 0.01s, and the dwell time is 1min, discharges pressure to normal pressure every 15s afterwards, is discharged into every time
The gross weight of the bagasse of normal pressure is 25%, collects the bagasse after steam blasting;
Step 3: the bagasse after steam blasting is immersed in into 6h in ethanol solution, the concentration of ethanol solution is
75wt.%, the addition of ethanol solution, then by squeezing and filtering, is repeated 3 times not have bagasse surface, respectively
Merge filter residue and filtrate, filtrate is stand-by, composite enzyme solution sprayed to the filter residue surface of merging, surface is infiltrated to dripping,
10min is kept, then sugar-cane juice is mixed, is squeezed, filtered, obtain enzymolysis liquid, wherein, the mass fraction of composite enzyme solution
0.8%, complex enzyme is glycosidase, trypsase, amylase, the mixture of pectase, often in mL complex enzymes, the vigor of glycosidase
For 6000IU/mL, the vigor of trypsase is 2000IU/mL, and the vigor of amylase is 800IU/mL, and the vigor of pectase is
800IU/mL;
Step 4: enzymolysis liquid is heated into 70~80 DEG C, add phosphoric acid and is carried out with milk of lime pre- ash to pH be 6.5, stone
The concentration of grey breast is 8~13 Baume degrees, is passed through nitrogen to 9.0MPa, is warming up to 85 DEG C with 1 DEG C/s speed, is incubated 5min, with
0.5 DEG C/s speed is warming up to 90 DEG C, is incubated 5min, and boiling is warming up to 0.1 DEG C/s speed, is incubated 5min, returns back to room
Warm atmospheric pressure, sedimentation separation obtains the first clear liquid;
Step 5: the first clear liquid is heated into 70~80 DEG C, add phosphoric acid and is carried out with milk of lime pre- ash to pH be 6.5,
The concentration of milk of lime is 8~13 Baume degrees, is passed through ozone to 1.0MPa, is warming up to 85 DEG C with 1 DEG C/s speed, is incubated 5min,
90 DEG C are warming up to 0.5 DEG C/s speed, 5min is incubated, boiling is warming up to 0.1 DEG C/s speed, 5min is incubated, returns back to
Atmosphere at room temperature pressure, sedimentation separation obtains the second clear liquid;
Step 6: the filtrate that step 4 is obtained mixes with the second clear liquid, boiling is heated to, impurity is filtered out, is cooled to room temperature,
By tubular ultra-filtration membrane filter process, the membrane flux of tubular ultra-filtration membrane filter is 30L/h/m2, evaporating, concentrating and crystallizing purging
Produce;
Wherein, the nitrogen in step 4, the ozone in step 5 are by being separated into by air liquefaction, using boiling point difference
Nitrogen and oxygen-enriched air, then prepare what ozone was obtained by oxygen-enriched air ionization.
<Comparative example>
Handled using conventional sulfurous method.Sugar-cane juice is 6.5 through pre- ash to pH, 60~70 DEG C is once heated to, using SO2
In intensity it is that 8~12mL, pH are that stove drying is neutralized under the conditions of 7 with milk of lime, then reheating enters settler to 100 DEG C, separates
Go out purified juice and mud juice, mud juice mixes again heated, multiple-effect evaporation into syrup through filtering to obtain filtered juice, then with purified juice, then passes through
Syrup stove drying obtains clear syrup and makees crystallization raw material.
Performance detection is carried out to sugar product prepared by embodiment 1,2 and comparative example, as a result as shown in table 1.
Number of devices and treatment scale described herein are the explanations for simplifying the present invention.To the present invention application,
Modifications and variations will be readily apparent to persons skilled in the art.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, the present invention is not limited
In specific details and shown here as the details with description.
Claims (6)
1. a kind of cane sugar manufacture technique, it is characterised in that comprise the following steps:
Step 1: sugarcane is obtained into bagasse and sugar-cane juice through over cleaning, chopping, squeezing, filtering;
Step 2: by bagasse be transferred to temperature be 100 DEG C, steam pressure be to carry out steam blasting under conditions of 1~2MPa, steam
Vapour blasting time is less than 0.01s, and the dwell time is 1min, discharges pressure to normal pressure every 15s afterwards, normal pressure is discharged into every time
The gross weight of bagasse is 25%, collects the bagasse after steam blasting;
Step 3: spraying composite enzyme solution to the bagasse surface after steam blasting, surface is infiltrated to dripping, keep
10min, then mixes sugar-cane juice, is squeezed, filtered, obtains enzymolysis liquid, wherein, the mass fraction of composite enzyme solution
0.8%, complex enzyme is glycosidase, trypsase, amylase, the mixture of pectase, often in mL complex enzymes, the vigor of glycosidase
For 6000IU/mL, the vigor of trypsase is 2000IU/mL, and the vigor of amylase is 800IU/mL, and the vigor of pectase is
800IU/mL;
Step 4: enzymolysis liquid is heated into 70~80 DEG C, it is 6.5 to add phosphoric acid and pre- ash is carried out with milk of lime to pH, is passed through nitrogen
Gas is warming up to 85 DEG C to 9.0MPa with 1 DEG C/s speed, is incubated 5min, and 90 DEG C, insulation are warming up to 0.5 DEG C/s speed
5min, boiling is warming up to 0.1 DEG C/s speed, is incubated 5min, is returned back to atmosphere at room temperature pressure, it is clear that sedimentation separation obtains first
Liquid;
Step 5: the first clear liquid is heated into 70~80 DEG C, it is 6.5 to add phosphoric acid and pre- ash is carried out with milk of lime to pH, is passed through
Ozone is warming up to 85 DEG C to 1.0MPa with 1 DEG C/s speed, is incubated 5min, and 90 DEG C, insulation are warming up to 0.5 DEG C/s speed
5min, boiling is warming up to 0.1 DEG C/s speed, is incubated 5min, is returned back to atmosphere at room temperature pressure, it is clear that sedimentation separation obtains second
Liquid;
Step 6: the second clear liquid is heated into boiling, impurity is filtered out, room temperature, ultrafiltration is cooled to, evaporating, concentrating and crystallizing purging is
.
2. cane sugar manufacture technique as claimed in claim 1, it is characterised in that the ozone in nitrogen, step 5 in step 4
It is, by dividing air into nitrogen and oxygen-enriched air, oxygen-enriched air then to be prepared what ozone was obtained.
3. cane sugar manufacture technique as claimed in claim 1, it is characterised in that the ultrafiltration in step 6 is by tubular ultra-filtration membrane
What filter process was obtained, the membrane flux of tubular ultra-filtration membrane filter is 30L/h/m2。
4. cane sugar manufacture technique as claimed in claim 1, it is characterised in that the concentration of the milk of lime in step 4 is 8~13
Baume degrees.
5. cane sugar manufacture technique as claimed in claim 1, it is characterised in that in step 3, to the bagasse after steam blasting
Before surface sprinkling composite enzyme solution, in addition to:Immersion, is immersed in 6h in ethanol solution, so by the bagasse after steam blasting
Afterwards by squeezing and filtering, it is repeated 3 times, filter residue and filtrate is merged respectively, the filter residue sprinkling composite enzyme solution of merging is carried out next
Process is walked, the filtrate of merging mixes with the second clear liquid in step 6, carry out next step process.
6. cane sugar manufacture technique as claimed in claim 5, it is characterised in that the concentration of ethanol solution is 75wt.%, ethanol is molten
The addition of liquid is:Bagasse surface is not crossed.
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CN201710551059.3A CN107267673A (en) | 2017-07-07 | 2017-07-07 | Cane sugar manufacture technique |
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CN201710551059.3A CN107267673A (en) | 2017-07-07 | 2017-07-07 | Cane sugar manufacture technique |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109338019A (en) * | 2018-11-30 | 2019-02-15 | 合浦县工业和信息化局 | Sugarcane cleans automatically and the method for cane sugar manufacture |
CN109468418A (en) * | 2018-11-30 | 2019-03-15 | 合浦县工业和信息化局 | The cane sugar manufacture method of sucrose recovery rate can be improved |
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JP2011130680A (en) * | 2009-12-22 | 2011-07-07 | Ajinomoto Co Inc | Method for producing sugar solution from residue of sugarcane-squeezed juice |
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JP2011130680A (en) * | 2009-12-22 | 2011-07-07 | Ajinomoto Co Inc | Method for producing sugar solution from residue of sugarcane-squeezed juice |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109338019A (en) * | 2018-11-30 | 2019-02-15 | 合浦县工业和信息化局 | Sugarcane cleans automatically and the method for cane sugar manufacture |
CN109468418A (en) * | 2018-11-30 | 2019-03-15 | 合浦县工业和信息化局 | The cane sugar manufacture method of sucrose recovery rate can be improved |
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Application publication date: 20171020 |