CN107287263B - Preparation method for high-purity maltose and co-production of beta-limit dextrin - Google Patents
Preparation method for high-purity maltose and co-production of beta-limit dextrin Download PDFInfo
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- CN107287263B CN107287263B CN201710668516.7A CN201710668516A CN107287263B CN 107287263 B CN107287263 B CN 107287263B CN 201710668516 A CN201710668516 A CN 201710668516A CN 107287263 B CN107287263 B CN 107287263B
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- beta
- maltose
- prepare
- limit dextrin
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- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 title claims abstract description 68
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 title claims abstract description 68
- 229920001353 Dextrin Polymers 0.000 title claims abstract description 57
- 239000004375 Dextrin Substances 0.000 title claims abstract description 57
- 235000019425 dextrin Nutrition 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 229920002472 Starch Polymers 0.000 claims abstract description 30
- 235000019698 starch Nutrition 0.000 claims abstract description 30
- 239000008107 starch Substances 0.000 claims abstract description 30
- 238000005342 ion exchange Methods 0.000 claims abstract description 18
- 238000007670 refining Methods 0.000 claims abstract description 18
- 238000001035 drying Methods 0.000 claims abstract description 17
- 235000013336 milk Nutrition 0.000 claims abstract description 15
- 239000008267 milk Substances 0.000 claims abstract description 15
- 210000004080 milk Anatomy 0.000 claims abstract description 15
- 108010019077 beta-Amylase Proteins 0.000 claims abstract description 13
- 238000011033 desalting Methods 0.000 claims abstract description 12
- 238000006243 chemical reaction Methods 0.000 claims abstract description 9
- 108090000790 Enzymes Proteins 0.000 claims description 13
- 102000004190 Enzymes Human genes 0.000 claims description 13
- 238000001914 filtration Methods 0.000 claims description 13
- 230000003544 deproteinization Effects 0.000 claims description 12
- 229920002261 Corn starch Polymers 0.000 claims description 11
- 238000013375 chromatographic separation Methods 0.000 claims description 11
- 239000008120 corn starch Substances 0.000 claims description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 239000012535 impurity Substances 0.000 claims description 9
- 238000004042 decolorization Methods 0.000 claims description 8
- 238000005349 anion exchange Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 238000001223 reverse osmosis Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 4
- 230000002779 inactivation Effects 0.000 claims description 2
- 108090000623 proteins and genes Proteins 0.000 claims description 2
- 102000004169 proteins and genes Human genes 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- 238000000926 separation method Methods 0.000 abstract description 7
- 230000009286 beneficial effect Effects 0.000 abstract description 5
- 238000004587 chromatography analysis Methods 0.000 abstract 1
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 58
- 229960002160 maltose Drugs 0.000 description 58
- 239000000047 product Substances 0.000 description 35
- 229940088598 enzyme Drugs 0.000 description 11
- 239000006188 syrup Substances 0.000 description 10
- 235000020357 syrup Nutrition 0.000 description 10
- 229910052799 carbon Inorganic materials 0.000 description 6
- 238000003825 pressing Methods 0.000 description 6
- DBTMGCOVALSLOR-UHFFFAOYSA-N 32-alpha-galactosyl-3-alpha-galactosyl-galactose Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(OC2C(C(CO)OC(O)C2O)O)OC(CO)C1O DBTMGCOVALSLOR-UHFFFAOYSA-N 0.000 description 5
- RXVWSYJTUUKTEA-UHFFFAOYSA-N D-maltotriose Natural products OC1C(O)C(OC(C(O)CO)C(O)C(O)C=O)OC(CO)C1OC1C(O)C(O)C(O)C(CO)O1 RXVWSYJTUUKTEA-UHFFFAOYSA-N 0.000 description 5
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 5
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 5
- 238000005341 cation exchange Methods 0.000 description 5
- 150000001768 cations Chemical class 0.000 description 5
- 238000001514 detection method Methods 0.000 description 5
- 239000008103 glucose Substances 0.000 description 5
- 230000000415 inactivating effect Effects 0.000 description 5
- FYGDTMLNYKFZSV-UHFFFAOYSA-N mannotriose Natural products OC1C(O)C(O)C(CO)OC1OC1C(CO)OC(OC2C(OC(O)C(O)C2O)CO)C(O)C1O FYGDTMLNYKFZSV-UHFFFAOYSA-N 0.000 description 5
- 238000000746 purification Methods 0.000 description 5
- FYGDTMLNYKFZSV-BYLHFPJWSA-N β-1,4-galactotrioside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-BYLHFPJWSA-N 0.000 description 5
- LUEWUZLMQUOBSB-UHFFFAOYSA-N UNPD55895 Natural products OC1C(O)C(O)C(CO)OC1OC1C(CO)OC(OC2C(OC(OC3C(OC(O)C(O)C3O)CO)C(O)C2O)CO)C(O)C1O LUEWUZLMQUOBSB-UHFFFAOYSA-N 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- UYQJCPNSAVWAFU-UHFFFAOYSA-N malto-tetraose Natural products OC1C(O)C(OC(C(O)CO)C(O)C(O)C=O)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(O)C(CO)O2)O)C(CO)O1 UYQJCPNSAVWAFU-UHFFFAOYSA-N 0.000 description 4
- LUEWUZLMQUOBSB-OUBHKODOSA-N maltotetraose Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O[C@@H]3[C@@H](O[C@@H](O)[C@H](O)[C@H]3O)CO)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-OUBHKODOSA-N 0.000 description 4
- 239000004382 Amylase Substances 0.000 description 3
- 108010065511 Amylases Proteins 0.000 description 3
- 102000013142 Amylases Human genes 0.000 description 3
- 235000019418 amylase Nutrition 0.000 description 3
- 150000001720 carbohydrates Chemical class 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 2
- 229920000945 Amylopectin Polymers 0.000 description 1
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000011097 chromatography purification Methods 0.000 description 1
- 235000020965 cold beverage Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 235000013365 dairy product Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 229940079919 digestives enzyme preparation Drugs 0.000 description 1
- 150000002016 disaccharides Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/22—Preparation of compounds containing saccharide radicals produced by the action of a beta-amylase, e.g. maltose
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/12—Disaccharides
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- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710668516.7A CN107287263B (en) | 2017-08-08 | 2017-08-08 | Preparation method for high-purity maltose and co-production of beta-limit dextrin |
Applications Claiming Priority (1)
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CN201710668516.7A CN107287263B (en) | 2017-08-08 | 2017-08-08 | Preparation method for high-purity maltose and co-production of beta-limit dextrin |
Publications (2)
Publication Number | Publication Date |
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CN107287263A CN107287263A (en) | 2017-10-24 |
CN107287263B true CN107287263B (en) | 2021-10-15 |
Family
ID=60105366
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201710668516.7A Active CN107287263B (en) | 2017-08-08 | 2017-08-08 | Preparation method for high-purity maltose and co-production of beta-limit dextrin |
Country Status (1)
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CN (1) | CN107287263B (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109234329A (en) * | 2018-09-25 | 2019-01-18 | 山东百龙创园生物科技股份有限公司 | A kind of preparation method of high-purity maltotetraose coproduction limit dextrin |
CN112111542B (en) * | 2020-09-01 | 2022-11-15 | 山东百龙创园生物科技股份有限公司 | Preparation method of high-purity isomaltooligosaccharide co-produced resistant dextrin |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5562937A (en) * | 1994-12-19 | 1996-10-08 | National Starch And Chemical Investment Holding Corporation | Amylase-treated waxy starch in foods and process of making |
CN103194509A (en) * | 2013-04-24 | 2013-07-10 | 山东百龙创园生物科技有限公司 | Method for preparing high-purity beta-limit dextrin |
CN106636257A (en) * | 2017-01-24 | 2017-05-10 | 邵阳学院 | Low-foam high-sugaring-temperature starch syrup and production technology thereof |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5482560A (en) * | 1994-07-27 | 1996-01-09 | American Maize Technology, Inc. | Beta-limit dextrin from dull waxy starch |
-
2017
- 2017-08-08 CN CN201710668516.7A patent/CN107287263B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5562937A (en) * | 1994-12-19 | 1996-10-08 | National Starch And Chemical Investment Holding Corporation | Amylase-treated waxy starch in foods and process of making |
CN103194509A (en) * | 2013-04-24 | 2013-07-10 | 山东百龙创园生物科技有限公司 | Method for preparing high-purity beta-limit dextrin |
CN106636257A (en) * | 2017-01-24 | 2017-05-10 | 邵阳学院 | Low-foam high-sugaring-temperature starch syrup and production technology thereof |
Non-Patent Citations (4)
Title |
---|
β-limit dextrin-Properties and applications;Richard F. Tester等;《Food Hydrocolloids》;20111231;第1899-1903页 * |
β-淀粉酶对蜡质玉米淀粉的酶解规律及其产物性质研究;陈旭 等;《食品工业科技》;20130731;第100页"1.2.1淀粉酶解物的制备及其产物分离纯化",第101页右栏第1段 * |
用β-淀粉酶制备蜡质大米糊精及其性质研究;雷俊华 等;《食品与发酵工业》;20141031;第22-26页 * |
酶法制备的蜡质玉米淀粉β-限制糊精的性质;邵兰兰 等;《食品科学》;20111031;第28-32页 * |
Also Published As
Publication number | Publication date |
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CN107287263A (en) | 2017-10-24 |
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB02 | Change of applicant information |
Address after: 251200 Dexin Street, Dezhou (Yucheng) National High-tech Industrial Development Zone, Shandong Province Applicant after: SHANDONG BAILONG CHUANGYUAN BIO-TECH Co.,Ltd. Address before: 251200 Dexin Street, Yucheng High-tech Development Zone, Dezhou City, Shandong Province Applicant before: SHANDONG BAILONG CHUANGYUAN BIO-TECH Co.,Ltd. |
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CB02 | Change of applicant information | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: High purity maltose co production b- Preparation of Limit Dextrin Effective date of registration: 20221202 Granted publication date: 20211015 Pledgee: China Construction Bank Corporation Yucheng Sub branch Pledgor: SHANDONG BAILONG CHUANGYUAN BIO-TECH Co.,Ltd. Registration number: Y2022980024523 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20211015 Pledgee: China Construction Bank Corporation Yucheng Sub branch Pledgor: SHANDONG BAILONG CHUANGYUAN BIO-TECH Co.,Ltd. Registration number: Y2022980024523 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |