CN107262725A - Blood bag process for making blade - Google Patents

Blood bag process for making blade Download PDF

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Publication number
CN107262725A
CN107262725A CN201710331972.2A CN201710331972A CN107262725A CN 107262725 A CN107262725 A CN 107262725A CN 201710331972 A CN201710331972 A CN 201710331972A CN 107262725 A CN107262725 A CN 107262725A
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CN
China
Prior art keywords
stage
blade
blade base
sintering
incubated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710331972.2A
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Chinese (zh)
Inventor
刁红文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kunshan Yu Li Electronics Polytron Technologies Inc
Original Assignee
Kunshan Yu Li Electronics Polytron Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kunshan Yu Li Electronics Polytron Technologies Inc filed Critical Kunshan Yu Li Electronics Polytron Technologies Inc
Priority to CN201710331972.2A priority Critical patent/CN107262725A/en
Publication of CN107262725A publication Critical patent/CN107262725A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F7/00Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
    • B22F7/06Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10Processes characterised by the sequence of their steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00Aspects linked to processes or compositions used in powder metallurgy

Abstract

Present invention is disclosed blood bag process for making blade, comprise the following steps:Using alumina material as base material, silica is added, silicon nitride and graphene are mixed and made into suspension;Continued drying out after suspension is poured into ball grinder, ball milling in vacuum drying chamber, dried mixed powder is sieved;Powder is poured into the mould for needing to be molded, using hot pressed sintering mode, blade base is obtained after sintering;The adding thermal resistance being connected with each other and electrode pin are printed by conductive material in the upper and lower part of blade base, the controller of heating blade base is used as;Zirconium oxide, aluminum oxide and the rare earth oxide containing titanium valve are prepared by mixing into slurry, slurry is coated on to the top overlay controller of blade base, exposes the knife-edge portion of the bottom of original blade base;Carry out sinter molding stage by stage;Grinding and buffing processing is carried out to knife-edge portion.The blade of the present invention has a Thermal conductivity, homogeneous heating and is easily controlled.

Description

Blood bag process for making blade
Technical field
The invention belongs to blade manufacturing technology field, more particularly to a kind of blood bag process for making blade.
Background technology
Blood bag product application amount in medical device industry is very big, and blood bag is when carrying out sealing outward flange usually using high frequency Solder up mould, presses upper die and lower die at blood bag opening when high-frequency welding sealing die is sealed, will by high frequency electric The heat that upper die and lower die are produced makes the thawing at blood bag mouthful and is bonded together, and completes sealing.Meanwhile, knife is provided with mould The heat transfer of mould to the position of otch is needed, is formed hanging hole, the reinforcement of hanging hole heating rear projection formation melting by tool, cutter Muscle, effectively prevents hanging hole from tearing.Prior art needs to use current control, and cost is higher, cuts the wearability that metal cuts and needs Improve, need to change cutter often.
The content of the invention
The invention aims to solve above-mentioned technical problem, and a kind of blood bag process for making blade is provided, so that Realize Thermal conductivity, homogeneous heating and be easily controlled.In order to achieve the above object, technical solution of the present invention is as follows:
Blood bag process for making blade, comprises the following steps:
S1, using alumina material as base material, adds silica, silicon nitride and graphene, is situated between using absolute ethyl alcohol as scattered Matter, is mixed and made into suspension;
S2, suspension is poured into and continues drying out 36-45h after ball grinder, ball milling in vacuum drying chamber, keeping temperature 120- 140 DEG C, dried mixed powder is sieved;
S3, powder is poured into the mould for needing to be molded, and using hot pressed sintering mode, 1600-1700 DEG C of sintering temperature is burnt Knot pressure power 50-55MPa, blade base is obtained after being incubated 40-50min, sintering;
S4, prints the adding thermal resistance being connected with each other by conductive material in the upper and lower part of blade base and electrode draws Pin, is used as the controller of heating blade base;
S5, is prepared by mixing into slurry by zirconium oxide, aluminum oxide and the rare earth oxide containing titanium valve, slurry is coated on The top overlay controller of blade base, exposes the knife-edge portion of the bottom of original blade base;
S6, by the way of high temperature co-firing, in high temperature furnace under the protection of nitrogen, carries out sinter molding stage by stage;
S7, grinding and buffing processing is carried out to knife-edge portion.
Specifically, the sintering stage by stage includes first stage sintering, 950-970 DEG C is warming up to, 2-2.2h is incubated;Second Stage is sintered, and 1600-1640 DEG C is warming up to again, is incubated 4-5.5h;Phase III sinters, and temperature drop is to 1000 DEG C, insulation 30-45min;Fourth stage is sintered, and temperature drop is incubated 1-2h to 880-900 DEG C.
Compared with prior art, blood bag of the present invention is mainly reflected in the beneficial effect of process for making blade:Blade base Preferable self-lubricating effect is made it have comprising graphene, the edge of a knife is highly polished, be easy to cutting;Set on the top of blade base Heating controller, in order to reach good hot melt effect, the specially treated suitable for blood bag hanging hole position in knife-edge positions;On blade Portion and the common sintering processes of bottom, make it is integral sintered coupling part is even closer together, no mark of break, do not influence cutting imitate Really;The edge of a knife carries out grinding and buffing, makes its sharper gloss, and overall structure has good thermal shock resistance, and the strength of materials is high, Thermal conductivity is good, and thermal coefficient of expansion is low, homogeneous heating and is easily controlled.
Embodiment
Clear, complete description will be carried out to the technical scheme in the embodiment of the present invention below, it is clear that described implementation Example only a part of embodiment of the invention, rather than whole embodiments.
Embodiment 1:
The present embodiment is blood bag process for making blade, is comprised the following steps:
S1, using alumina material as base material, add silica, silicon nitride, graphene, using absolute ethyl alcohol be used as it is scattered be situated between Matter, is mixed and made into suspension.
S2, suspension is poured into and continues drying out 36-45h after ball grinder, ball milling in vacuum drying chamber, keeping temperature 120- 140 DEG C, dried mixed powder is sieved.
S3, powder is poured into the mould for needing to be molded, and using hot pressed sintering mode, 1600-1700 DEG C of sintering temperature is burnt Knot pressure power 50-55MPa, is incubated 40-50min.Obtain including the blade base of graphene after sintering, blade has preferable lubrication Effect, not sizing, so as to reduce the friction and wear of tool surface.
S4, prints the adding thermal resistance being connected with each other by conductive material in the upper and lower part of blade base and electrode draws Pin, is used as the controller of heating blade base.
S5, is prepared by mixing into slurry by zirconium oxide, aluminum oxide and the rare earth oxide containing titanium valve, slurry is coated on The top overlay controller of blade base, exposes the knife-edge portion of the bottom of original blade base.
S6, by the way of high temperature co-firing, in high temperature furnace, under the protection of nitrogen, carries out sinter molding stage by stage, bag First stage sintering is included, 950 DEG C are warming up to, 2h is incubated;Second stage is sintered, and 1600 DEG C are warming up to again, is incubated 4h;3rd rank Section sintering, temperature drop is incubated 30min to 1000 DEG C;Fourth stage is sintered, and temperature drop is incubated 1h to 880 DEG C.On blade Portion and bottom are sintered jointly, make it have heating effect, and integrally reduce the coefficient of friction of blade after sintering stage by stage, make blade Surface is more smooth, and cutting effect is good.
S7, grinding and buffing processing is carried out to knife-edge portion.
Embodiment 2:
It is with the distinguishing characteristics part of embodiment 1:S6, by the way of high temperature co-firing, in high temperature furnace, in the guarantor of nitrogen Under shield, sinter molding stage by stage, including first stage sintering are carried out, 960 DEG C is warming up to, is incubated 2.1h;Second stage is sintered, then It is secondary to be warming up to 1620 DEG C, it is incubated 5h;Phase III sinters, and temperature drop is incubated 40min to 1000 DEG C;Fourth stage is sintered, temperature Degree drops to 890 DEG C, is incubated 1.5h.Further feature is identical, is not repeating.
Embodiment 3:
It is with the distinguishing characteristics part of embodiment 1:S6, by the way of high temperature co-firing, in high temperature furnace, in the guarantor of nitrogen Under shield, sinter molding stage by stage, including first stage sintering are carried out, 970 DEG C is warming up to, is incubated 2.2h;Second stage is sintered, then It is secondary to be warming up to 1640 DEG C, it is incubated 5.5h;Phase III sinters, and temperature drop is incubated 45min to 1000 DEG C;Fourth stage is sintered, Temperature drop is incubated 2h to 900 DEG C.Further feature is identical, is not repeating.
During using above the present embodiment, blade base makes it have preferable self-lubricating effect, edge of a knife light comprising graphene Cleanliness is high, is easy to cutting;Heating controller is set on the top of blade base, in order to reach good hot melt effect in knife-edge positions Really, the specially treated suitable for blood bag hanging hole position;The common sintering processes of blade upper and lower part, make it is integral sintered together, Coupling part is even closer, no mark of break, does not influence cutting effect;The edge of a knife carries out grinding and buffing, makes its sharper gloss, whole Body structure has a good thermal shock resistance, and the strength of materials is high, and thermal conductivity is good, and thermal coefficient of expansion is low, homogeneous heating and is easily controlled.
Above-described is only some embodiments of the present invention.For the person of ordinary skill of the art, not On the premise of departing from the invention design, various modifications and improvements can be made, these belong to the protection model of the present invention Enclose.

Claims (2)

1. blood bag process for making blade, it is characterised in that comprise the following steps:
S1, using alumina material as base material, adds silica, silicon nitride and graphene, using absolute ethyl alcohol as decentralized medium, mixes Suspension is made in conjunction;
S2, suspension is poured into and continues drying out 36-45h after ball grinder, ball milling in vacuum drying chamber, keeping temperature 120-140 DEG C, dried mixed powder is sieved;
S3, powder is poured into the mould for needing to be molded, using hot pressed sintering mode, 1600-1700 DEG C of sintering temperature, sintering pressure Power 50-55MPa, blade base is obtained after being incubated 40-50min, sintering;
S4, prints the adding thermal resistance being connected with each other and electrode pin by conductive material in the upper and lower part of blade base, makees To heat the controller of blade base;
S5, is prepared by mixing into slurry by zirconium oxide, aluminum oxide and the rare earth oxide containing titanium valve, slurry is coated on into blade The top overlay controller of matrix, exposes the knife-edge portion of the bottom of original blade base;
S6, by the way of high temperature co-firing, in high temperature furnace under the protection of nitrogen, carries out sinter molding stage by stage;
S7, grinding and buffing processing is carried out to knife-edge portion.
2. blood bag process for making blade according to claim 1, it is characterised in that:The sintering stage by stage includes first Stage sinters, and is warming up to 950-970 DEG C, is incubated 2-2.2h;Second stage is sintered, and 1600-1640 DEG C is warming up to again, is incubated 4- 5.5h;Phase III sinters, and temperature drop is incubated 30-45min to 1000 DEG C;Fourth stage is sintered, temperature drop to 880- 900 DEG C, it is incubated 1-2h.
CN201710331972.2A 2017-05-11 2017-05-11 Blood bag process for making blade Pending CN107262725A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710331972.2A CN107262725A (en) 2017-05-11 2017-05-11 Blood bag process for making blade

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710331972.2A CN107262725A (en) 2017-05-11 2017-05-11 Blood bag process for making blade

Publications (1)

Publication Number Publication Date
CN107262725A true CN107262725A (en) 2017-10-20

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Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040238795A1 (en) * 2003-06-02 2004-12-02 The Regents Of The University Of California, A California Corporation Electrically conductive Si-Ti-C-N ceramics
CN1649449A (en) * 2004-01-20 2005-08-03 珠海粤科清华电子陶瓷有限公司 High temperature coburning heating element and its producing method
CN101001486A (en) * 2006-12-25 2007-07-18 杨世养 Preparation method of ceramic heating core for sensor
CN101000320A (en) * 2006-12-25 2007-07-18 杨世养 Chip oxygen sensor and its preparation method
CN103044014A (en) * 2013-01-17 2013-04-17 山东大学 Preparation method of graphene-nanosheet-reinforced alumina ceramic
CN204184629U (en) * 2014-09-03 2015-03-04 山东中保康医疗器具有限公司 Blood bag solder up mould
CN104876611A (en) * 2015-04-09 2015-09-02 浙江泰索科技有限公司 Graphene-reinforced ceramic and preparation method thereof
CN205272173U (en) * 2015-10-20 2016-06-01 北京拓威能效技术有限公司 Rubber cutter utensil is shelled in heatable
CN106431361A (en) * 2016-10-31 2017-02-22 东南大学 Self-lubricated ceramic cutter material added with alumina coated graphene

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040238795A1 (en) * 2003-06-02 2004-12-02 The Regents Of The University Of California, A California Corporation Electrically conductive Si-Ti-C-N ceramics
CN1649449A (en) * 2004-01-20 2005-08-03 珠海粤科清华电子陶瓷有限公司 High temperature coburning heating element and its producing method
CN101001486A (en) * 2006-12-25 2007-07-18 杨世养 Preparation method of ceramic heating core for sensor
CN101000320A (en) * 2006-12-25 2007-07-18 杨世养 Chip oxygen sensor and its preparation method
CN103044014A (en) * 2013-01-17 2013-04-17 山东大学 Preparation method of graphene-nanosheet-reinforced alumina ceramic
CN204184629U (en) * 2014-09-03 2015-03-04 山东中保康医疗器具有限公司 Blood bag solder up mould
CN104876611A (en) * 2015-04-09 2015-09-02 浙江泰索科技有限公司 Graphene-reinforced ceramic and preparation method thereof
CN205272173U (en) * 2015-10-20 2016-06-01 北京拓威能效技术有限公司 Rubber cutter utensil is shelled in heatable
CN106431361A (en) * 2016-10-31 2017-02-22 东南大学 Self-lubricated ceramic cutter material added with alumina coated graphene

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Application publication date: 20171020