CN107245884A - A kind of garment material antibiosis and sterilization agent and preparation method thereof - Google Patents

A kind of garment material antibiosis and sterilization agent and preparation method thereof Download PDF

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Publication number
CN107245884A
CN107245884A CN201710635765.6A CN201710635765A CN107245884A CN 107245884 A CN107245884 A CN 107245884A CN 201710635765 A CN201710635765 A CN 201710635765A CN 107245884 A CN107245884 A CN 107245884A
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parts
antibiosis
sterilization agent
garment material
agent
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龚利峰
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SUZHOU IMURA GARMENTS CO Ltd
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SUZHOU IMURA GARMENTS CO Ltd
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Priority to CN201710635765.6A priority Critical patent/CN107245884A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/507—Polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/35—Heterocyclic compounds
    • D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/392—Nitroso compounds; Nitro compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/05—Cellulose or derivatives thereof
    • D06M15/09—Cellulose ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M19/00—Treatment of feathers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D06M2101/12—Keratin fibres or silk
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of garment material antibiosis and sterilization agent and preparation method thereof, the antibiosis and sterilization agent includes the composition of following parts by weight：Nano-silver loaded SiO2Particle, PLA, sodium carboxymethylcellulose, Tebuconazole, Difenoconazole, Choline Chloride, chitosan propionic acid, bromogeramine, vermiculite power, nitroethane, coupling agent, antioxidant, dispersant, surfactant, isopropanol, deionized water.The antibiosis and sterilization agent is safe, with broad spectrum antibacterial and excellent washing fastness, the whiteness of fabric, coloured light, strength, feel and gas permeability are had no adverse effects, it is cheap, it is easy to use, suitable for the anti-bacterial purifying finish of the fabrics such as eider down, cotton, silk, hair, polyester-cotton blend, viscous fibre, the fluffy softness of feel, composition design is reasonable, production cost is low, good in economic efficiency.

Description

A kind of garment material antibiosis and sterilization agent and preparation method thereof
Technical field
The invention belongs to garment material auxiliary agent technical field, and in particular to a kind of garment material antibiosis and sterilization agent and its system Preparation Method.
Background technology
Fabric is exactly the material for making clothes.As one of clothes three elements, fabric can not only annotate clothes Style and characteristic, and directly left and right the color of clothes, the expression effect of moulding.
Clothes are made with fabric, and fabric is exactly the material for making clothes.It is used as one of clothes three elements, fabric Can not only annotate the style and characteristic of clothes, and directly left and right the color of clothes, the expression effect of moulding.Presentation is come from The noble quality of body is perfect, soft.
Modern times are produced on the clothes of formal social life institute wear, many blended yarn weaved fabrics from high-quality.And it is pure cotton, pure The natural fabric such as hair, pure silk, pure fiber crops has become general cloth because there is the easily natural fabric such as wrinkle, yielding, compared with It is few to be used as high-grade clothing materials.Blended yarn weaved fabric has natural fabric sweat-absorbing breathable, it is soft comfortable the characteristics of, chemical fibre face is absorbed again Material is solid to wear well, overhangs the advantages of well-pressed, good luster color is vivid, has substantial amounts of high-grade high-quality blended yarn weaved fabric to be developed every year Come.Sometimes, the clothes of the pure leatherwork of wear, are also allowed.
For the antibiotic and sterilizing of garment material, the current country is primarily present following patent document：
Publication No. 106916635A Chinese patent discloses a kind of fabric disinfection sanitizer containing green-tea extract, the sterilization Disinfectant contains following component in terms of mass parts：0.5~1.8 part of green-tea extract, 0.5~1.8 part of APES, 0.8~1.6 part of grape seed extract, 0.1~0.3 part of Uruguay's essential oil, 2.5~6.5 parts of ethanol, 5~8 parts of triglycerides, lemon 1~1.55 part of lemon hydrochlorate, 0.2~0.3 part of formaldehyde, 24~30.4 parts of water.A kind of face containing green-tea extract that the present invention is provided Expect disinfection sanitizer, add pure natural green-tea extract, not only environmental protection but also the fiber of fabric can have been protected not receive infringement, the sterilization disappears Toxic agent has good detergency, and it sterilizes good anti-bacterial effect, can be hiding killing bacteria in the fibre, and makes Fabric has the effect of antibacterial.However, the patent provides and contains green-tea extract in disinfectant, its scope of application is limited.
The content of the invention
To solve above-mentioned problem, it is an object of the invention to provide a kind of garment material antibiosis and sterilization agent and its Preparation method, the antibiosis and sterilization agent is safe, with broad spectrum antibacterial and excellent washing fastness, whiteness to fabric, Coloured light, strength, feel and gas permeability have no adverse effects, cheap, easy to use, it is adaptable to eider down, cotton, silk, hair, polyester-cotton blend, The anti-bacterial purifying finish of the fabrics such as viscous fibre, the fluffy softness of feel, rationally, production cost is low, good in economic efficiency for composition design.
To reach above-mentioned purpose, the technical scheme is that：
A kind of garment material antibiosis and sterilization agent, the antibiosis and sterilization agent includes the composition of following parts by weight：Nano-silver loaded SiO2Particle：15 ~ 20 parts, PLA：30 ~ 40 parts, sodium carboxymethylcellulose：10 ~ 15 parts, Tebuconazole：15 ~ 20 parts, phenylate first Ring azoles：10 ~ 15 parts, Choline Chloride：5 ~ 10 parts, chitosan propionic acid：10 ~ 15 parts, bromogeramine：20 ~ 25 parts, vermiculite power：5~10 Part, nitroethane：5 ~ 10 parts, coupling agent：1 ~ 5 part, antioxidant：1 ~ 5 part, dispersant：1 ~ 5 part, surfactant：5 ~ 10 parts, Isopropanol：20 ~ 30 parts, deionized water：40 ~ 50 parts.
Further, the antibiosis and sterilization agent includes the composition of following parts by weight：Nano-silver loaded SiO2Particle：15 ~ 18 parts, PLA：35 ~ 40 parts, sodium carboxymethylcellulose：10 ~ 13 parts, Tebuconazole：17 ~ 20 parts, Difenoconazole：12 ~ 15 parts, chlorination Choline：5 ~ 7 parts, chitosan propionic acid：10 ~ 12 parts, bromogeramine：23 ~ 25 parts, vermiculite power：7 ~ 10 parts, nitroethane：8 ~ 10 parts, Coupling agent：1 ~ 3 part, dispersant：3 ~ 5 parts, surfactant：5 ~ 6 parts, isopropanol：25 ~ 30 parts, deionized water：45 ~ 50 parts.
Preferably, the antibiosis and sterilization agent includes the composition of following parts by weight：Nano-silver loaded SiO2Particle：18 parts, gather Lactic acid：37 parts, sodium carboxymethylcellulose：12 parts, Tebuconazole：18 parts, Difenoconazole：13 parts, Choline Chloride：7 parts, chitosan Propionic acid：12 parts, bromogeramine：23 parts, vermiculite power：7 parts, nitroethane：8 parts, coupling agent：2 parts, dispersant：4 parts, surface is lived Property agent：5 parts, isopropanol：25 parts, deionized water：45 parts.
Preferably, the surfactant is neopelex.
Preferably, the dispersant is polyacrylate.
Preferably, the coupling agent is soluble silane coupling agent.
Preferably, the antioxidant is antioxidant 1010.Antioxidant effect is good.
Meanwhile, the present invention also provides a kind of preparation method of garment material antibiosis and sterilization agent, and the preparation method includes Following steps：1) by nano-silver loaded SiO2Particle, PLA and antioxidant are added in banbury, 150 ~ 200 DEG C of temperature, are turned 70 ~ 80 revs/min of speed, banburying 5 ~ 10 minutes obtains emulsion；2) take stirred tank, add step 1) gained emulsion, carboxymethyl cellulose Sodium, Tebuconazole, Difenoconazole, Choline Chloride, chitosan propionic acid and 40 ~ 50% deionized water, at 800 ~ 1000 revs/min Stirred 15 ~ 25 minutes under rotating speed, 30 ~ 40 DEG C of whipping temp；2) 50 ~ 60 DEG C are warming up to, bromogeramine, vermiculite power, nitro is added Ethane, coupling agent, dispersant, surfactant, isopropanol and remaining deionized water, are stirred under 1000 ~ 1200 revs/min of rotating speed Mix 15 ~ 20 minutes, stirring is cooled to room temperature after finishing, and produces the garment material antibiosis and sterilization agent.Preparation technology is simple, section Energy emission reduction, it is environmentally friendly.
The invention has the advantages that：
The antibiosis and sterilization agent is safe, with broad spectrum antibacterial and excellent washing fastness, to the whiteness of fabric, coloured light, Strongly, feel and gas permeability have no adverse effects, cheap, easy to use, it is adaptable to eider down, cotton, silk, hair, polyester-cotton blend, viscous fibre etc. The anti-bacterial purifying finish of fabric, the fluffy softness of feel, rationally, production cost is low, good in economic efficiency for composition design.
Embodiment
Below by specific embodiment, the present invention is described further, but embodiment is not intended to limit the protection of the present invention Scope.
A kind of garment material antibiosis and sterilization agent provided by the present invention, the antibiosis and sterilization agent includes following parts by weight Composition：Nano-silver loaded SiO2Particle：15 ~ 20 parts, PLA：30 ~ 40 parts, sodium carboxymethylcellulose：10 ~ 15 parts, Tebuconazole： 15 ~ 20 parts, Difenoconazole：10 ~ 15 parts, Choline Chloride：5 ~ 10 parts, chitosan propionic acid：10 ~ 15 parts, bromogeramine：20~25 Part, vermiculite power：5 ~ 10 parts, nitroethane：5 ~ 10 parts, coupling agent：1 ~ 5 part, antioxidant：1 ~ 5 part, dispersant：1 ~ 5 part, surface Activating agent：5 ~ 10 parts, isopropanol：20 ~ 30 parts, deionized water：40 ~ 50 parts.
Further, the antibiosis and sterilization agent includes the composition of following parts by weight：Nano-silver loaded SiO2Particle：15 ~ 18 parts, PLA：35 ~ 40 parts, sodium carboxymethylcellulose：10 ~ 13 parts, Tebuconazole：17 ~ 20 parts, Difenoconazole：12 ~ 15 parts, chlorination Choline：5 ~ 7 parts, chitosan propionic acid：10 ~ 12 parts, bromogeramine：23 ~ 25 parts, vermiculite power：7 ~ 10 parts, nitroethane：8 ~ 10 parts, Coupling agent：1 ~ 3 part, dispersant：3 ~ 5 parts, surfactant：5 ~ 6 parts, isopropanol：25 ~ 30 parts, deionized water：45 ~ 50 parts.
Preferably, the antibiosis and sterilization agent includes the composition of following parts by weight：Nano-silver loaded SiO2Particle：18 parts, gather Lactic acid：37 parts, sodium carboxymethylcellulose：12 parts, Tebuconazole：18 parts, Difenoconazole：13 parts, Choline Chloride：7 parts, chitosan Propionic acid：12 parts, bromogeramine：23 parts, vermiculite power：7 parts, nitroethane：8 parts, coupling agent：2 parts, dispersant：4 parts, surface is lived Property agent：5 parts, isopropanol：25 parts, deionized water：45 parts.
Preferably, the surfactant is neopelex.
Preferably, the dispersant is polyacrylate.
Preferably, the coupling agent is soluble silane coupling agent.
Preferably, the antioxidant is antioxidant 1010.Antioxidant effect is good.
Meanwhile, the present invention also provides a kind of preparation method of garment material antibiosis and sterilization agent, and the preparation method includes Following steps：1) by nano-silver loaded SiO2Particle, PLA and antioxidant are added in banbury, 150 ~ 200 DEG C of temperature, are turned 70 ~ 80 revs/min of speed, banburying 5 ~ 10 minutes obtains emulsion；2) take stirred tank, add step 1) gained emulsion, carboxymethyl cellulose Sodium, Tebuconazole, Difenoconazole, Choline Chloride, chitosan propionic acid and 40 ~ 50% deionized water, at 800 ~ 1000 revs/min Stirred 15 ~ 25 minutes under rotating speed, 30 ~ 40 DEG C of whipping temp；2) 50 ~ 60 DEG C are warming up to, bromogeramine, vermiculite power, nitro is added Ethane, coupling agent, dispersant, surfactant, isopropanol and remaining deionized water, are stirred under 1000 ~ 1200 revs/min of rotating speed Mix 15 ~ 20 minutes, stirring is cooled to room temperature after finishing, and produces the garment material antibiosis and sterilization agent.Preparation technology is simple, section Energy emission reduction, it is environmentally friendly.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted.Although with reference to compared with The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to the technology of invention Scheme is modified or equivalent substitution, and without departing from the scope of technical solution of the present invention, it all should cover the power in the present invention In sharp claimed range.

Claims (8)

1. a kind of garment material antibiosis and sterilization agent, it is characterised in that the antibiosis and sterilization agent includes the composition of following parts by weight： Nano-silver loaded SiO2Particle：15 ~ 20 parts, PLA：30 ~ 40 parts, sodium carboxymethylcellulose：10 ~ 15 parts, Tebuconazole：15~20 Part, Difenoconazole：10 ~ 15 parts, Choline Chloride：5 ~ 10 parts, chitosan propionic acid：10 ~ 15 parts, bromogeramine：20 ~ 25 parts, leech Stone flour：5 ~ 10 parts, nitroethane：5 ~ 10 parts, coupling agent：1 ~ 5 part, antioxidant：1 ~ 5 part, dispersant：1 ~ 5 part, surface-active Agent：5 ~ 10 parts, isopropanol：20 ~ 30 parts, deionized water：40 ~ 50 parts.
2. garment material antibiosis and sterilization agent according to claim 1, it is characterised in that the antibiosis and sterilization agent is included such as The composition of lower parts by weight：Nano-silver loaded SiO2Particle：15 ~ 18 parts, PLA：35 ~ 40 parts, sodium carboxymethylcellulose：10~13 Part, Tebuconazole：17 ~ 20 parts, Difenoconazole：12 ~ 15 parts, Choline Chloride：5 ~ 7 parts, chitosan propionic acid：10 ~ 12 parts, new clean that Go out：23 ~ 25 parts, vermiculite power：7 ~ 10 parts, nitroethane：8 ~ 10 parts, coupling agent：1 ~ 3 part, dispersant：3 ~ 5 parts, surface-active Agent：5 ~ 6 parts, isopropanol：25 ~ 30 parts, deionized water：45 ~ 50 parts.
3. garment material antibiosis and sterilization agent according to claim 1, it is characterised in that the antibiosis and sterilization agent is included such as The composition of lower parts by weight：Nano-silver loaded SiO2Particle：18 parts, PLA：37 parts, sodium carboxymethylcellulose：12 parts, penta azoles Alcohol：18 parts, Difenoconazole：13 parts, Choline Chloride：7 parts, chitosan propionic acid：12 parts, bromogeramine：23 parts, vermiculite power：7 Part, nitroethane：8 parts, coupling agent：2 parts, dispersant：4 parts, surfactant：5 parts, isopropanol：25 parts, deionized water：45 Part.
4. garment material antibiosis and sterilization agent according to claim 1, it is characterised in that the surfactant is 12 Sodium alkyl benzene sulfonate.
5. garment material antibiosis and sterilization agent according to claim 1, it is characterised in that the dispersant is polyacrylic acid Ester.
6. garment material antibiosis and sterilization agent according to claim 1, it is characterised in that the coupling agent is water-soluble silicon Alkane coupling agent.
7. garment material antibiosis and sterilization agent according to claim 1, it is characterised in that the antioxidant is antioxidant 1010。
8. a kind of preparation method of garment material antibiosis and sterilization agent as any one of claim 1 ~ 7, its feature exists In the preparation method comprises the following steps：1) by nano-silver loaded SiO2Particle, PLA and antioxidant add banbury In, 150 ~ 200 DEG C of temperature, 70 ~ 80 revs/min of rotating speed, banburying 5 ~ 10 minutes obtains emulsion；2) stirred tank is taken, step 1 is added) gained Emulsion, sodium carboxymethylcellulose, Tebuconazole, Difenoconazole, Choline Chloride, chitosan propionic acid and 40 ~ 50% deionized water, Stirred 15 ~ 25 minutes under 800 ~ 1000 revs/min of rotating speed, 30 ~ 40 DEG C of whipping temp；2) 50 ~ 60 DEG C are warming up to, is added new clean You go out, vermiculite power, nitroethane, coupling agent, dispersant, surfactant, isopropanol and remaining deionized water, 1000 ~ Stirred 15 ~ 20 minutes under 1200 revs/min of rotating speed, stirring is cooled to room temperature after finishing, and produces the garment material and is disappeared with antibacterial Toxic agent.
CN201710635765.6A 2017-07-31 2017-07-31 A kind of garment material antibiosis and sterilization agent and preparation method thereof Pending CN107245884A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109853249A (en) * 2018-11-28 2019-06-07 安徽尚尚家纺有限公司 A kind of natural feather care agent and preparation method thereof of the anti-mite of antibacterial

Citations (3)

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CN105088766A (en) * 2015-09-07 2015-11-25 王璐 Mould-proof antibacterial agent for fabric
CN105220469A (en) * 2015-10-20 2016-01-06 湖州申祥丝织有限责任公司 A kind of composite fabric antiseptic and application thereof
CN106120314A (en) * 2016-07-12 2016-11-16 苏州宇希新材料科技有限公司 A kind of fabric antimildew and antibacterial agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105088766A (en) * 2015-09-07 2015-11-25 王璐 Mould-proof antibacterial agent for fabric
CN105220469A (en) * 2015-10-20 2016-01-06 湖州申祥丝织有限责任公司 A kind of composite fabric antiseptic and application thereof
CN106120314A (en) * 2016-07-12 2016-11-16 苏州宇希新材料科技有限公司 A kind of fabric antimildew and antibacterial agent

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109853249A (en) * 2018-11-28 2019-06-07 安徽尚尚家纺有限公司 A kind of natural feather care agent and preparation method thereof of the anti-mite of antibacterial

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Application publication date: 20171013