CN107141100A - It is a kind of with liquid organic fertilizer processed containing amino-acid liquid and preparation method thereof - Google Patents
It is a kind of with liquid organic fertilizer processed containing amino-acid liquid and preparation method thereof Download PDFInfo
- Publication number
- CN107141100A CN107141100A CN201710407311.3A CN201710407311A CN107141100A CN 107141100 A CN107141100 A CN 107141100A CN 201710407311 A CN201710407311 A CN 201710407311A CN 107141100 A CN107141100 A CN 107141100A
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- Prior art keywords
- acid
- liquid
- organic fertilizer
- containing amino
- bacillus
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Biotechnology (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Health & Medical Sciences (AREA)
- Fertilizers (AREA)
Abstract
The present invention relates to a kind of with liquid organic fertilizer processed containing amino-acid liquid and preparation method thereof and performance.Belong to crop special novel organic fertilizer and its preparing technical field.Its main component is amino acid, organic acid, nucleic acid, EPS, LPS, alkaloid, and the bacterium such as bacillus subtilis, wax Bacillus, thermophilic salt Bacillus, amino-acid liquid regulation will be contained and arrive aimed concn, after pretreatment, mixed with appropriate mentioned microorganism and other food ingredients, liquid organic fertilizer is made after composition fermentation.Suitable zingiberaceous plant dedicated liquid organic fertilizer prepared by the present invention, it can not only consume and largely contain amino acid waste liquid produced by amino acids production industry, it is combination of the organic waste using technology and microbial biotechnology and the organic fertilizer produced is adapted to growing for zingiberaceous plant.
Description
Technical field
The present invention relates to a kind of using the method that liquid organic fertilizer is prepared containing amino-acid liquid, more particularly to one kind utilizes amino
Sour industrial wastewater and functional microorganism produce the method to the particularly effective liquid organic fertilizer of Zingiber crop, and belonging to new has
The technical field of machine/biologic compound fertilizer.
This hair is more particularly to a kind of to be produced to the particularly effective liquid of Zingiber crop using amino acids industry waste water and functional microorganism
The method of body organic fertilizer, falls within industrial wastewater recycle utilization technology field.
Background technology
Now, demand of the society to amino acid in terms of bio-pharmaceuticals, Animal nutrition is increasing, particularly to Lys, Met,
The demand of the necessary amino acid of the mankind such as Ser, Ile is bigger, and amino acids industry has very big development space.Therefore, amino acid work
The generation scale of industry waste water also will be increasing.
The waste water fraction of current amino acid fermentation industry is used for the exploitation of liquid fertilizer, and also very little part is used for SOLID ORGANIC
The slurry-spraying pelletizing technique of fertilizer.But, slurry-spraying pelletizing needs liquid measure few, it is impossible to consume substantial amounts of amino acids industry waste liquid.Simultaneously
Due to the fundamental characteristics of liquid, it there is such as acid, amino acid waste liquid composition heavier compared with strong, foul smell compared with strong, corrosivity and be difficult to
Optimize, field efficacy is bad, negative factor even harmful to some crops etc., makes profit of the amino acid waste liquid in terms of organic fertilizer
Be constantly subjected to limitation, the fertilizer produced, either solid waste or liquid fertilizer, are all difficult to promote.These all suppress
Recycling for amino acids industry waste water.With the development of amino acids industry, the amount of produced amino acid wastewater is also more next
It is more.Belong to water resource together more and more in short supply, environmental protection pressure is increasing, the processing of amino acids industry waste water also increasingly into
For a great problem of puzzlement amino acids industry development.
The characteristics of amino acids industry waste water has itself.Either amino acid fermentation industrial wastewater or hydrolysis amino acid extract useless
Water, is still remained containing substantial amounts of amino acid residues and organic matter.This aspect make it that amino acid wastewater BOD is very high, processing
Get up very difficult, on the other hand possess the potentiality utilized in terms of planting industry aquaculture again.
Microbial biotechnology can realize the conversion for having feature, shape using the metabolic function of microorganism to the organic principle in material
Into the secondary metabolites for having feature, and change the physical chemistry characteristic and biochemical characteristics of material.Certain micro-organisms again can be right simultaneously
The growth of crops produces facilitation, and soil is played a part of to lift respiration capability, soil improvement and vegetable fertilizer is brought
Effect, is the main force of microbial manure.
Physicochemical method and biological method are combined, can weaken amino acids industry waste water is unfavorable for the negative of agricultural production
Factor, or even improved soil, the contributing factors for promoting plant growth, promoting agricultural sustainable development are translated into, this is this
The background science background of invention.
The present inventor develops a kind of waste water of livestock poultry harmless treatment side using microbial biotechnology accumulation so far
Method (CN102211838) and a kind of waste water of livestock poultry isolate comprehensive utilization technique (CN102701807) are comprehensive in agriculture wastes
Close in utilizing and fully used microbial biotechnology, realize predetermined effect.According to literature search, microorganism biological is utilized
Technology will contain amino-acid liquid and be processed as zingiberaceous plant organic fertilizer special has no correlative study and report at present.
The content of the invention
In view of the shortcomings of the prior art, it is an object of the invention to provide a kind of organic with the liquid processed containing amino-acid liquid
Fertilizer and preparation method thereof.The organic fertilizer has high amino acid content, content of organic matter height, living microorganism content high, raw
The characteristics of thing activity height, fertilizer effect height, utilization rate of fertilizer height etc. " six is high ", be a kind of novel organic fertilizer material.
It is a further object to provide the method for liquid organic fertilizer being prepared into containing amino-acid liquid.
This method includes the key technologies such as deodorization, the regulation of physical chemistry characteristic, microorganism regulation；With production cost it is low,
The low feature of environmental protection pressure, this is also a kind of liquid debris environmental protection pressure for dissolving amino acids industry, controls foul smell to produce
New method.
The present invention provides a class I liquid I organic fertilizer, and its composition is following (being percetage by weight)：Amino acids industry waste water
75-85；Acidity-basicity regulator 3-8；Microbe additive 0.01-2；Microbial nutrition additive 4-8 (has aqueous vapor, carbon dioxide
With the escape of other gases, and resulting Mass lost)
The foul smell of material is controlled using biological method：
(1) biological deodorizing microbial inoculum (CN102851231) W58 invented before this using the present inventor, carries out biological deodorizing.
(2) W58 pulvis boiling water is dissolved, shaken up after placing 10-24 hours, added by institute's certainty ratio in material, stirring.
(3) by streams closed 2-3 days, or in surface of material plastics, it is made 2-11 days with air exclusion.
The acid-base value of material is adjusted using KH2PO4 or K2HPO4.Added concentration according to being formulated surely
As needed, material can be heated with appropriate volume method, outlet temperature is between 80-95 degrees Celsius
Can.
According to production purpose and corresponding factory formula, it is selected produce in advance deployed phosphorous material, material containing potassium, with
And the mineral such as calcic, iron, magnesium, zinc, sulphur, selenium, appropriate to add, stirring.
Add above-mentioned phosphorous material, material containing potassium and containing micro element mineral after, be fully stirred.After mixing thoroughly,
Add the supplies such as vitamin, boric acid.Mix thoroughly.
According to production purpose and corresponding factory formula, selected a kind to 28 kinds or more of the microorganism produced in advance
The pulvis and/or liquor of bacterial strain configuration, are made into the bacterium solution of defined density in formula, are added in fixed ratio is formulated
Liquid material.
Strain density is added up in mixed material after being sufficiently mixed for 103-106cfu/ml.At a temperature of 12-37 DEG C, fill
Divide after mixing, shading is capped at a temperature of 12-37 DEG C or is cultivated 3-25 days under light illumination.
According to production purpose and corresponding factory formula, 2 kinds to 15 kinds of material after above-mentioned culture is selected, is determined by formula
Ratio mixing, after being sufficiently mixed, at a temperature of 12-37 DEG C be capped shading or under light illumination cultivate 3-25 days.
Divide and take said mixture 20-2000ml, carry out preliminary quality analysis.Preliminary quality analysis includes physical property, preliminary peace
Total quality and component content etc..
According to preliminary quality analysis result, continue to adjust the content of various elements until reaching set target zone.
Operation during adjustment repeats the step of above-mentioned [0017] arrives [0024].
According to the characteristics of fertilizer and object crop, appropriate crop is selected to carry out security test and the fertilizer efficiency of fertilizer.Peace
Full property test and fertilizer efficiency test are carried out indoors.
The security test and manure trial of intelligence development special fertilizer utilize the potted plant of intelligence development or its kindred plant indoors
Or experimental plot is carried out.
The security test and manure trial of the special fertilizer of other crops utilize the crop or the potted plant plant of its kindred plant
Strain is indoors or experimental plot is carried out.
The security test and manure trial of wide usage fertilizer utilize pakchoi, tomato or capsicum, the potted plant of cucumber
Indoors or experimental plot carry out.
According to the result of experiment, security and fertilizer efficiency are adjusted, until reaching set target zone.During adjustment
Operation repeat above-mentioned [0017] arrive [0024] the step of.
Pass through safety testing and manure trial, qualified material, you can carry out packaging distribution.Underproof material is returned
To above-mentioned [0025], content detection and analysis are re-started.Until security test and manure trial are qualified.
With reference to embodiment, the present invention is further elaborated, but institute's protection domain of the present invention is not limited only to this.
Potassium dihydrogen phosphate, dipotassium hydrogen phosphate, boric acid, vitamin, microbial bacterial agent etc. are common commercially available production in this example
Product.
Brief description of the drawings
Fig. 1 is a kind of preparation method schematic diagram with the liquid organic fertilizer processed containing amino-acid liquid of the invention.
Embodiment
Embodiment 1：One once produce 100 tons of fertilizer flowline.
Material needed for the 100 tons of intelligence development plant dedicated liquid organic fertilizers prepared is as follows：
70 tons of zymotic fluid containing amino acid；8 tons of W58 pulvis, 5 tons of potassium dihydrogen phosphate, 5 tons of dipotassium hydrogen phosphate, zinc sulfate 1
Ton, 1 ton of potassium fulvate, 2 tons of calcium magnesium phosphate, 0.5 ton of B B-complex, 0.8 ton of boric acid, 2 tons of microbial bacterial agent, microculture
5 tons of base；0.02 ton of trace plant growth regulator
Preparation method is as follows：
(1) amino acid zymotic fluid stoste is injected into fermentation vat, while the standing 16h injected after boiling water dissolving W58 solution,
Mix, sealing and standing is discharged into reaction tank after 2 days through Filter Press, forms mixed material 1；Filter plant is filter press,
Canvas press cloth aperture is 50 mesh, and pressure limit is 0.5-2MPa；
(2) dipotassium hydrogen phosphate is added in mixed material 1, stirred, the pH value of mixed liquor is adjusted to 6.5, form mixing
Material 2, and suction filtration is discharged into next pond；
(3) addition microbiological culture media and microbial bacterial agent in the fermentation vat of mixed material 2, are sealed, at 28 DEG C
At a temperature of be sufficiently mixed, stir 15 days, form mixed material 3；
The fluid nutrient medium that mentioned microorganism culture medium is prepared by potato and glucose, microbial bacterial agent is withered grass bud
Spore bacterium (Bacillus substilis) and a small amount of yeast；
(4) mixed material 3 is heated, outlet temperature control is allowed at 85 DEG C, suction filtration is into next reaction tank；Add sulfur-bearing
Sour zinc, potassium fulvate, calcium magnesium phosphate stirring, form mixed material 4；
(5) potassium dihydrogen phosphate is added in mixed material 4, the pH value of regulation mixture is in faintly acid, and adds boric acid, answers
Close vitamin and plant growth regulator regulation viable bacteria state；After being sufficiently mixed, lucifuge is stored 15 days at 28 DEG C, forms mixing
Material 5；
(6) by the filtering mesh screen suction filtration of the 50-100 mesh of mixed material 5, sampling chemical examination；
(7) it is divided to and takes mixture 1000ml two, first quality analysis is carried out after mixing.First quality analysis include physical property,
Preliminary safety quality and component content etc..
(8) according to preliminary quality analysis result, the content of various elements is adjusted.Operation during adjustment repeats above-mentioned [0038]
The step of to [0044].
(9) security test and manure trial of intelligence development plant special fertilizer utilize the potted plant of intelligence development indoors or experiment
Field is carried out；
(10) by safety testing and manure trial, qualified material, you can carry out packaging distribution.Underproof material
Above-mentioned [0044] is returned to, content detection and analysis is re-started.Until security test and manure trial are qualified.
Claims (9)
1. it is a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：9- containing amino acid in dry
15%, organic matter 8-20%, other organic acid 0.1-4%, EPS polysaccharide 0.1-4%, LPS polysaccharide 0.04-1%, nucleic acid 0.01-
1%, live body function bacterium 106-109cfu/ml, alkaloid is a small amount of and a small amount of additive.
2. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
Crop growth can be effectively facilitated, increases agricultural output, and improves agricultural product quality, the especially effect on Zingiber crop is outstanding
To be notable.
3. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
Described live body function bacterium be bacillus subtilis (Bacillus substilis), wax Bacillus (Bacillus cereus),
Bacterium and a small amount of yeast such as thermophilic salt Bacillus (Bacillus halodurans).
4. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
Described can be animal/vegetable protein hydrolyzate, amino acid zymotic fluid, protein hydrolytic amino acid industrial wastes etc. containing amino-acid liquid,
Its acid-base value is near neutral or faintly acid.
5. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
EPS and LPS is bacillus subtilis (Bacillus substilis), wax Bacillus (Bacillus cereus), thermophilic salt gemma
Product synthesized by the bacteriums such as bacterium (Bacillus halodurans) and a small amount of yeast, rather than commercial synthesis composition.
6. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
Organic acid is contained non-volatile low molecular organic acid in amino acids industry waste liquid, rather than commercial synthesis composition.
7. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
Organic matter is contained natural organic matter in the biological raw material in acid hydrolysis or amino acids industry, rather than commercial synthesis
Composition.
8. it is according to claim 1 a kind of with the liquid organic fertilizer processed containing amino-acid liquid, it is characterised in that：
A small amount of additive can be the acid-base value buffering component that regulation acid-base value is added in order to improve and enhance product performance, with
And improving field efficacy and the material that is a small amount of, having certain effect to agricultural production that adds, its addition does not constitute organic fertilizer
The change of property.
9. a kind of preparation method with the liquid organic fertilizer processed containing amino-acid liquid is as follows：
(1) by material (liquid charging stock) by the pretreatment such as filtering, deodorization, contained solid content is allowed in 50 mesh or smaller, stink
Intensity is below the intensity of plant technology code defined；
(2) acid-base value of material is adjusted to neutral or faintly acid with appropriate KH2PO4, K2HPO4 or water, by viscosity
Adjust with product standard to the difficulty scope that matches；
(3) material is sufficiently mixed with determining microbiological culture media at a temperature of 12-37 DEG C；Wherein：
A) strain density is added up in mixture for 103-106cfu/ml；
B) seal and be sufficiently stirred for after mixing, mixing speed is 50-200rpm；
C) adjusted with minimal amount of KH2PO4 or K2HPO4 to fixed acid-base value (generally faintly acid)；
D) needs of mixed liquor state Han viable bacteria are regarded, appropriate supplies are added.Supplies can comprising vitamin, boric acid,
Magnesia and other miberal powders etc.；
E) it is sufficiently mixed；
(4) resulting material under the illumination of lucifuge or institute's wavelength range, is stored more than 10 days at a temperature of 12-37 DEG C；
(5) by the filtering screen filtration of resulting material 20-100 mesh, impurity, and chemical examination of sampling are removed；
Qualified material will be chemically examined to dispense according to fixed component, be put in storage after capping.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710407311.3A CN107141100A (en) | 2017-06-02 | 2017-06-02 | It is a kind of with liquid organic fertilizer processed containing amino-acid liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710407311.3A CN107141100A (en) | 2017-06-02 | 2017-06-02 | It is a kind of with liquid organic fertilizer processed containing amino-acid liquid and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107141100A true CN107141100A (en) | 2017-09-08 |
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ID=59780900
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710407311.3A Pending CN107141100A (en) | 2017-06-02 | 2017-06-02 | It is a kind of with liquid organic fertilizer processed containing amino-acid liquid and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108254509A (en) * | 2018-03-06 | 2018-07-06 | 余金龙 | A kind of experimental method with Exo-biopolymer embedding slow-release phosphate fertilizer |
| CN112194538A (en) * | 2020-10-10 | 2021-01-08 | 四川龙蟒福生科技有限责任公司 | Gibberellin bacterial residue treatment method and liquid fertilizer containing gibberellin bacterial residue treatment product |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1129683A (en) * | 1995-04-14 | 1996-08-28 | 北京兆元技术发展公司 | Multiple component organic composite liquid fertilizer and preparation thereof |
| CN101088968A (en) * | 2006-06-13 | 2007-12-19 | 王荣辉 | Organic phosphate fertilizer and its production process |
-
2017
- 2017-06-02 CN CN201710407311.3A patent/CN107141100A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1129683A (en) * | 1995-04-14 | 1996-08-28 | 北京兆元技术发展公司 | Multiple component organic composite liquid fertilizer and preparation thereof |
| CN101088968A (en) * | 2006-06-13 | 2007-12-19 | 王荣辉 | Organic phosphate fertilizer and its production process |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108254509A (en) * | 2018-03-06 | 2018-07-06 | 余金龙 | A kind of experimental method with Exo-biopolymer embedding slow-release phosphate fertilizer |
| CN112194538A (en) * | 2020-10-10 | 2021-01-08 | 四川龙蟒福生科技有限责任公司 | Gibberellin bacterial residue treatment method and liquid fertilizer containing gibberellin bacterial residue treatment product |
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