CN107136139A - A kind of preparation method of Chinese herbal medicine pesticide - Google Patents
A kind of preparation method of Chinese herbal medicine pesticide Download PDFInfo
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- CN107136139A CN107136139A CN201710547955.2A CN201710547955A CN107136139A CN 107136139 A CN107136139 A CN 107136139A CN 201710547955 A CN201710547955 A CN 201710547955A CN 107136139 A CN107136139 A CN 107136139A
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Agronomy & Crop Science (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of preparation method of Chinese herbal medicine pesticide, using making steps such as crushing, purifications；Preparation method of the present invention is simple, with low cost, effectively can preserve and play the performance that raw material kills insect pest；The Chinese herbal medicine pesticide that the present invention is prepared has the effect for significantly killing insect, and insect is not likely to produce resistance, and energy natural degradation, and Environmental compatibility is good, so that the residues of pesticides of agricultural product are avoided, it is safe and pollution-free to natural ecological environment.
Description
Technical field
The present invention relates to a kind of method for producing insecticide, and in particular to a kind of preparation method of Chinese herbal medicine pesticide, category
In technical field of pesticide.
Background technology
The evil because worm of nature is had a famine, people can spraying insecticide in Planting Crops.The desinsection now used at present
Some in agent can turn into innocuous substance, and the organochlorine class desinsection including DDT by biodegradation within a short period of time
Agent is difficult to degrade, then is the strong insecticide of residual.According to the characteristic of residual, persistent insecticide can be divided into three kinds：Easily
The insecticide remained in plant part is referred to as plant residue insecticide；It is easy to the insecticide referred to as soil remained in soil
Persistent insecticide, and insecticide of the extended residual in water is referred to as residue in water insecticide.Persistent insecticide plant,
Remaining form in soil and water body has two kinds：It is a kind of to be to maintain original chemical constitution；It is another with its chemical conversion products
Or the form remaining of biodegradable product, remain in the insecticide in soil and entered by the root system of plant in plant, it is different
Insecticide residue in plant part depends on their absorbabilities to insecticide.It is residual although can kill off the insect pests
The insecticide stayed can carry out very big harm to zoology, into crops, cause food pollution, endanger the health of people, unfavorable
In the use of people, now current insecticide do not have can kill off the insect pests and noresidue, human body is not damaged it is excellent
Point.
The content of the invention
A kind of degradable in view of the deficiencies of the prior art, the present invention provides noresidue, safe and harmless Chinese herbal medicine pesticide
Preparation method.
The technical solution adopted by the present invention is as follows：
A kind of preparation method of Chinese herbal medicine pesticide, it is characterised in that：Comprise the following steps：
1st, vomiting nut, ginger, yellow wormwood artemisia, sage, kuh-seng, rhizoma arisaematis, mustard, capsicum, garlic, Chinese prickly ash, selfheal, lotus are chosen
Leaf, fennel, Chinese cassia tree, orange peel, cordate houttuynia and cape jasmine, go the removal of impurity, are put into inside agitating device and are mixed, mixing time
5-8min, is made mixed material；
2nd, mixed material made from step 1 is handled with micronizer, after 100-200 mesh sieves, powdered original is made
Material；
3rd, by dusty raw materials ethyl alcohol purification made from step 2, the ethanol of concentration 60% that 10 times of amounts of raw material are added for the first time is carried out
Extract, extraction time 1.5hrs, the ethanol of concentration 80% of second of addition 5 times of amount of raw material are extracted, extraction time 1.5hrs,
Filtered after extraction, extract solution is made；
4th, vinegar is added in extract solution made from step 3 and mixes stirring, mixing speed 200-300r/min, mixing time 15-
30min, carries out vacuum-concentrcted again after stirring and evenly mixing, thickening temperature is controlled at 20-30 DEG C, is concentrated to relative density 1.1-
1.2, produced after drying.
150 mesh sieves are most preferably crossed in the step 2.
Mixing speed is most preferably 220r/min in the step 4, and mixing time is most preferably 25min, and thickening temperature is most
Preferably 27 DEG C.
The present invention compared with prior art, specific following advantageous effects：
1st, the Chinese herbal medicine pesticide that the present invention is prepared has the effect for significantly killing insect, and insect is not likely to produce resistance, can
Extend the service life of insecticide, expand insecticidal spectrum, reduce unit area dosage, cost accounting is low.
2nd, preparation method of the present invention is easy and effective, with low cost, effectively can preserve and play the property that raw material kills insect pest
Energy.
3rd, the present invention has the advantages that good disinsection effect and environmental-protecting performance are superior, and long-term use will not destroy the ecological balance.
4th, effective active composition of the invention is fully present and from natural herbs and natural ecosystems, it
Maximum feature is easily to be decomposed by daylight, plant or various edaphons, is one kind come in naturally, being attributed to the normal thing of nature
Matter endless form, it is safe and pollution-free to natural ecological environment.
Embodiment
Embodiment 1
A kind of preparation method of Chinese herbal medicine pesticide, it is characterised in that：Comprise the following steps：
1st, vomiting nut, ginger, yellow wormwood artemisia, sage, kuh-seng, rhizoma arisaematis, mustard, capsicum, garlic, Chinese prickly ash, selfheal, lotus are chosen
Leaf, fennel, Chinese cassia tree, orange peel, cordate houttuynia and cape jasmine, go the removal of impurity, are put into inside agitating device and are mixed, mixing time
5min, is made mixed material；
2nd, mixed material made from step 1 is handled with micronizer, after 100 mesh sieves, dusty raw materials is made；
3rd, by dusty raw materials ethyl alcohol purification made from step 2, the ethanol of concentration 60% that 10 times of amounts of raw material are added for the first time is carried out
Extract, extraction time 1.5hrs, the ethanol of concentration 80% of second of addition 5 times of amount of raw material are extracted, extraction time 1.5hrs,
Filtered after extraction, extract solution is made；
4th, vinegar is added in extract solution made from step 3 and mixes stirring, mixing speed 200r/min, mixing time 15min, stirring
Vacuum-concentrcted is carried out after mixing again, thickening temperature is controlled at 20-30 DEG C, is concentrated to relative density 1.1, is produced after drying.
Embodiment 2
A kind of preparation method of Chinese herbal medicine pesticide, it is characterised in that：Comprise the following steps：
1st, vomiting nut, ginger, yellow wormwood artemisia, sage, kuh-seng, rhizoma arisaematis, mustard, capsicum, garlic, Chinese prickly ash, selfheal, lotus are chosen
Leaf, fennel, Chinese cassia tree, orange peel, cordate houttuynia and cape jasmine, go the removal of impurity, are put into inside agitating device and are mixed, mixing time
6min, is made mixed material；
2nd, mixed material made from step 1 is handled with micronizer, after 150 mesh sieves, dusty raw materials is made；
3rd, by dusty raw materials ethyl alcohol purification made from step 2, the ethanol of concentration 60% that 10 times of amounts of raw material are added for the first time is carried out
Extract, extraction time 1.5hrs, the ethanol of concentration 80% of second of addition 5 times of amount of raw material are extracted, extraction time 1.5hrs,
Filtered after extraction, extract solution is made；
4th, vinegar is added in extract solution made from step 3 and mixes stirring, mixing speed 220r/min, mixing time 25min, stirring
Vacuum-concentrcted is carried out after mixing again, thickening temperature is controlled at 27 DEG C, is concentrated to relative density 1.2, is produced after drying.
Embodiment 3
A kind of preparation method of Chinese herbal medicine pesticide, it is characterised in that：Comprise the following steps：
1st, vomiting nut, ginger, yellow wormwood artemisia, sage, kuh-seng, rhizoma arisaematis, mustard, capsicum, garlic, Chinese prickly ash, selfheal, lotus are chosen
Leaf, fennel, Chinese cassia tree, orange peel, cordate houttuynia and cape jasmine, go the removal of impurity, are put into inside agitating device and are mixed, mixing time
8min, is made mixed material；
2nd, mixed material made from step 1 is handled with micronizer, after 200 mesh sieves, dusty raw materials is made；
3rd, by dusty raw materials ethyl alcohol purification made from step 2, the ethanol of concentration 60% that 10 times of amounts of raw material are added for the first time is carried out
Extract, extraction time 1.5hrs, the ethanol of concentration 80% of second of addition 5 times of amount of raw material are extracted, extraction time 1.5hrs,
Filtered after extraction, extract solution is made；
4th, vinegar is added in extract solution made from step 3 and mixes stirring, mixing speed 300r/min, mixing time 30min, stirring
Vacuum-concentrcted is carried out after mixing again, thickening temperature is controlled at 30 DEG C, is concentrated to relative density 1.2, is produced after drying.
Embodiment 4
A kind of preparation method of Chinese herbal medicine pesticide, it is characterised in that：Comprise the following steps：
1st, vomiting nut, ginger, yellow wormwood artemisia, sage, kuh-seng, rhizoma arisaematis, mustard, capsicum, garlic, Chinese prickly ash, selfheal, lotus are chosen
Leaf, fennel, Chinese cassia tree, orange peel, cordate houttuynia and cape jasmine, go the removal of impurity, are put into inside agitating device and are mixed, mixing time
7min, is made mixed material；
2nd, mixed material made from step 1 is handled with micronizer, after 180 mesh sieves, dusty raw materials is made；
3rd, by dusty raw materials ethyl alcohol purification made from step 2, the ethanol of concentration 60% that 10 times of amounts of raw material are added for the first time is carried out
Extract, extraction time 1.5hrs, the ethanol of concentration 80% of second of addition 5 times of amount of raw material are extracted, extraction time 1.5hrs,
Filtered after extraction, extract solution is made；
4th, vinegar is added in extract solution made from step 3 and mixes stirring, mixing speed 220r/min, mixing time 18min, stirring
Vacuum-concentrcted is carried out after mixing again, thickening temperature is controlled at 22 DEG C, is concentrated to relative density 1.1, is produced after drying.
Claims (3)
1. a kind of preparation method of Chinese herbal medicine pesticide, it is characterised in that：Comprise the following steps：
（1）, choose vomiting nut, ginger, yellow wormwood artemisia, sage, kuh-seng, rhizoma arisaematis, mustard, capsicum, garlic, Chinese prickly ash, selfheal, lotus
Leaf, fennel, Chinese cassia tree, orange peel, cordate houttuynia and cape jasmine, go the removal of impurity, are put into inside agitating device and are mixed, mixing time
5-8min, is made mixed material；
（2）, mixed material made from step 1 handled with micronizer, after 100-200 mesh sieves, be made powdered
Raw material；
（3）, by dusty raw materials ethyl alcohol purification made from step 2, the ethanol of concentration 60% that 10 times of amounts of raw material are added for the first time enter
Row is extracted, extraction time 1.5hrs, and the ethanol of concentration 80% of second of addition 5 times of amount of raw material are extracted, extraction time
1.5hrs, is filtered after extraction, and extract solution is made；
（4）, in extract solution made from step 3 add vinegar mix stirring, mixing speed 200-300r/min, mixing time 15-
30min, carries out vacuum-concentrcted again after stirring and evenly mixing, thickening temperature is controlled at 20-30 DEG C, is concentrated to relative density 1.1-
1.2, produced after drying.
2. a kind of preparation method of Chinese herbal medicine pesticide according to claim 1, it is characterised in that：Step（2）In it is optimal
Selected 150 mesh sieves.
3. a kind of preparation method of Chinese herbal medicine insect control pesticide according to claim 1, it is characterised in that：Step（4）In
Mixing speed is most preferably 220r/min, and mixing time is most preferably 25min, and thickening temperature is most preferably 27 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710547955.2A CN107136139A (en) | 2017-07-06 | 2017-07-06 | A kind of preparation method of Chinese herbal medicine pesticide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710547955.2A CN107136139A (en) | 2017-07-06 | 2017-07-06 | A kind of preparation method of Chinese herbal medicine pesticide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107136139A true CN107136139A (en) | 2017-09-08 |
Family
ID=59785995
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710547955.2A Pending CN107136139A (en) | 2017-07-06 | 2017-07-06 | A kind of preparation method of Chinese herbal medicine pesticide |
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| Country | Link |
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| CN (1) | CN107136139A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107771623A (en) * | 2017-11-24 | 2018-03-09 | 恭城福茂生油茶文化产业发展有限公司 | A kind of high-yield planting method of bamboo shoots |
| CN109601276A (en) * | 2019-01-28 | 2019-04-12 | 四川师范大学 | A kind of implantation methods of green vegetables (bean sprout raw material) |
| CN109892347A (en) * | 2019-03-29 | 2019-06-18 | 江西樟树成方中药饮片有限公司 | A kind of Chinese herbal medicine plantation environmental-pollution insecticide and preparation method thereof |
| CN113498795A (en) * | 2021-08-17 | 2021-10-15 | 北京中农绿安有机农业科技有限公司 | Preparation method of pure natural plant acaricide |
-
2017
- 2017-07-06 CN CN201710547955.2A patent/CN107136139A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107771623A (en) * | 2017-11-24 | 2018-03-09 | 恭城福茂生油茶文化产业发展有限公司 | A kind of high-yield planting method of bamboo shoots |
| CN109601276A (en) * | 2019-01-28 | 2019-04-12 | 四川师范大学 | A kind of implantation methods of green vegetables (bean sprout raw material) |
| CN109892347A (en) * | 2019-03-29 | 2019-06-18 | 江西樟树成方中药饮片有限公司 | A kind of Chinese herbal medicine plantation environmental-pollution insecticide and preparation method thereof |
| CN113498795A (en) * | 2021-08-17 | 2021-10-15 | 北京中农绿安有机农业科技有限公司 | Preparation method of pure natural plant acaricide |
| CN113498795B (en) * | 2021-08-17 | 2022-08-26 | 北京中农绿安有机农业科技有限公司 | Preparation method of pure natural plant acaricide |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170908 |
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| WD01 | Invention patent application deemed withdrawn after publication |