CN107073361A - The device for the treatment of fluid mixture - Google Patents

The device for the treatment of fluid mixture Download PDF

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Publication number
CN107073361A
CN107073361A CN201580039221.2A CN201580039221A CN107073361A CN 107073361 A CN107073361 A CN 107073361A CN 201580039221 A CN201580039221 A CN 201580039221A CN 107073361 A CN107073361 A CN 107073361A
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China
Prior art keywords
liquid
filter
collecting chamber
listed
gas
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Granted
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CN201580039221.2A
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Chinese (zh)
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CN107073361B (en
Inventor
B·施利希特
S·施拉赫特尔
S·策勒
M·韦尔克
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Hydac Process Technology GmbH
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Hydac Process Technology GmbH
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D19/00Degasification of liquids
    • B01D19/0042Degasification of liquids modifying the liquid flow
    • B01D19/0052Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D45/00Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces
    • B01D45/12Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/0027Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with additional separating or treating functions
    • B01D46/003Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with additional separating or treating functions including coalescing means for the separation of liquid
    • B01D46/0031Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with additional separating or treating functions including coalescing means for the separation of liquid with collecting, draining means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/56Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition
    • B01D46/62Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition connected in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2267/00Multiple filter elements specially adapted for separating dispersed particles from gases or vapours
    • B01D2267/40Different types of filters

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Cyclones (AREA)
  • Separating Particles In Gases By Inertia (AREA)
  • Filtering Of Dispersed Particles In Gases (AREA)
  • Fuel Cell (AREA)

Abstract

The device for the treatment of fluid mixture.The device for the treatment of fluid mixture, the fluid mixture contains such as especially hydrogen (H2), air, nitrogen (N2) or natural gas gas, and such as especially liquid of ionic liquid, hydraulic oil or process liquid, the device has at least one first separation level (29), to the gas component the liquid component pollution that fluid mixture is separated into liquid component and is remained, the liquid component of residual is thus removed from the gas component at least another second separation level (67).

Description

The device for the treatment of fluid mixture
Technical field
The present invention relates to a kind of device for the treatment of fluid mixture, fluid mixture contains gas such as especially hydrogen (H2), air, nitrogen (N2) or natural gas, and liquid such as especially ionic liquid, hydraulic oil or process liquid.
The invention particularly relates to the processing of fluid mixture under high pressure, the mixture contains gas such as hydrogen and small Partially liq such as ionic liquid.
Background technology
The accurate understanding of so-called ionic liquid, as an example, in professional paper " Ionische Fl ü ssigkeiten: Einzigartige Materialien mit(ionic liquid:With various each Pointed out in the unique material of sample possibility ", can be in internet site " CHE Manager-online.com " downloads, 2014 7 The data that the moon 15 was announced.
Hydrogen is prepared with about 700bar to 1000bar high pressure in the gas station for driving automobile in hydrogen recently.Advantageously adopt Be compressed with so-called " ion compression machine ", as example the publication of mutual communication network thing ", lonenverdichtertech Nologie, Wie funktioniert ein lonenverdichter(how ion compression machine technique, ion compression machine rises Effect) " company illustrate disclosed in material " Flowserve ", can be fromwww.dbi-gti.deDownload, on July 15th, 2014 Disclosed data (FCS-Praesentation 170909deutsch-DBI) are downloaded.Here, being the pressure of similar piston compressor Contracting machine, it replaces piston using ion fluid column.Play the liquid of extrusion compared with extrusion piston, with can preferably band The advantage of heat produced by walking, because it is conveyed with gas compressed from compressor in certain proportion.Ionic liquid is Know the organic salt that the temperature below 100 DEG C is in a liquid state, and be not dissolved in this salt in solvent such as water.In the high pressure When ion compression machine is run, liquid component enters in gas under power level.It is this to enter the also known as entrainment on technical term (Verschleppung), this makes treatment fluid mixture necessitate.
The content of the invention
In view of this problem, task of the invention is to provide a kind of device, make more reliably separate mixture components turn into May.
According to the present invention, the task with patent right by more asking the device of 1 whole features to solve.
Accordingly, the present invention set at least one first separation level, for fluid mixture be separated into liquid portion and by The gas part of residual liquid component pollution, thus removes the liquid component of the residual at least another separation level.Thus, According to the present invention, separation process occurs in multistage, with this after the first separation process is performed, and is carried out in the second separation level Fine separation, to make relevant liquid portion such as ionic liquid with available again for the necessary purity of application, And the gas component obtained does not contain this liquid.
Whizzer can be particularly advantageously set as first and separate level, the wherein big liquid of density ratio gas, due to The centrifugal action of produced eddy flow, is moved to cyclone cylinder enclosure wall section, to be dripped at this.Because playing separation process Centrifugal force by inflow cyclone cylinder shell and flow through the device fluid mixture speed produce, so according to the present invention dress Effec-tive Function can also be carried out by putting.
In order to effectively carry out the fine separation of residual liquid part, coalescing filter can be particularly advantageously set as Two separation levels.The second separation level can be directly connected to the first separation level, or preferably be connected indirectly by intermediary interface 3rd separation level.
In particularly advantageous embodiment of the present invention, all separation levels are all disposed within a common shell, the shell Entrance with fluid mixture, the outlet of the gas part separated with liquid, and at least one isolates to draw The liquid come unloads Air Export.Therefore, one compact structure unit of whole device formation, without external pipe connection (Verrohrungen) good, it is contemplated that very high stress level, this is particularly advantageous.
The shell can have a cavity extended along vertical axis, and wherein whizzer is set at thereon Between the collecting chamber of coalescing filter and the liquid of the receiving deposition under it.Under this arrangement liquid can directly from Whizzer instills collecting chamber.
Here, the arrangement can be advantageously designed to, the inwall of whizzer cyclone cylinder cylinder is in itself in itself and receipts Collect the lower end of chamber adjoining, circular openings are limited between the concentric pipeline section of axle, the latter forms cyclone cylinder cylinder axial distal end Connection between region and collecting chamber.Therefore, the droplet being attached on cyclone cylinder outer casing inner wall can instill receipts to no transition Collect chamber.
Cyclone cylinder cylinder axis proximally region and collecting chamber upper area can be formed by limiting the pipeline section of the circular openings Between coupling part, to be used as the less component of mixture of density in the gas in cyclone cylinder shell axial proximal region Directly reach the upper area of collecting chamber.
It is absolutely empty in internal ramp that the coalescing filter can have the usual manner in such filter to surround Between filtering material, wherein collecting chamber and the cyclone cylinder cylinder axis upper area that proximally region is connected by pipeline section and coalescence Interface channel is set between the filter hollow space of filter.Should be by the pipeline section from containing that cyclone separator comes out with this The gas of the liquid portion reduced reaches the second separation level that this is finely separated.
In a particularly advantageous embodiment, the coalescing filter has coaxial inner tube, and the inner tube imports outer in its upper end The space abutted with filter head housings outer side surface of shell, and guide the housing outlet of gas part into its lower end.It is particularly advantageous , gas is made from the filter chamber containing coalescing filter with this, without being drawn from the space for surrounding filter housing surface, And drawn by axial inner tube, to maintain optimal flow state in the filter chamber, and following risk is occurred without with this, The coalesced liquid deposited in filter housing outer side surface is taken away together.According to this construction of coalescing filter with inner pipe Another advantage of structure is easy to disassemble when changing filtering material.So the filtering material can be with inner tube together as peace Unit is filled to take out from the device after shell is removed, and the installation unit more renewed.At this moment, the housing outlet of gas part With the interface channel towards filter chamber, it can be arranged in the device part do not dismantled together with shell.
In order to particularly effectively finely be separated, here it is particularly advantageous that collecting chamber upper end and guiding coalescing filter into Filter hollow space inside interface channel between, set demister be used as the 3rd separation level.Therefore, the 3rd separation level It is arranged between the first separation level and the second separation level.
In collecting chamber bottom section and unload particulate filter can be set between Air Export, so that ionic liquid is in receipts of unstowing Maintenance filtering (Pflegefiltration) is carried out when collecting chamber.The collecting chamber can design to store liquid volume, wherein can be with Level sensing is set, to carry out unloading null process according to the ratio of liquid level.
According to the device of the present invention in the case where the pipeline size for connection that shell closely is implemented and needed is minimum, Particularly effective liquid is set to be separated into possibility, wherein the frame mode of pressure stability can be set with stainless steel parts technology.
Now with reference to embodiment shown in the accompanying drawings, the present invention is set forth in.
Brief description of the drawings
In accompanying drawing:
Fig. 1 is the simplification vertical section of one embodiment of the device according to the present invention;
Fig. 2 is the vertical section of an expression whizzer and the interruption in coalescing filter region thereon, wherein should Section have rotated 90 ° relative to Fig. 1;
Fig. 3 corresponds to 1 hatching I11-I11 of figure horizontal profile;
Fig. 4 is the partial longitudinal section of the amplification display of the longitudinal sections comprising whizzer, and it has cuts with Fig. 1 identicals Face;And
Fig. 5 is the partial longitudinal section that whizzer and coalescing filter longitudinal region equally amplify, with identical with Fig. 2 Section.
Embodiment
The present invention is illustrated by taking device as an example now with reference to accompanying drawing, the device, which is set, to be come from 700bar to 1000bar pressures The liquid flow separation liquid component of fluid mixture under power.Originally the fluid mixture has the hydrogen with some ionic liquid Gas.It is present in the solid particle in fluid mixture and is equally possible and is separately come out from gas by means of the device.Obviously, institute The device of description can contain liquid portion to be separated and solid to be separated in some cases for handling in gas Other medium mixtures of particle.
Embodiment shown in the device, with longitudinally extending shell 1, it in huge entirety there is circular hollow to justify The shape of cylinder, its axle 3 capwise on the device embedded position.Shell 1 has upper outer casing member 5, and it is with the end of its rounding Section 7 defines coalescer-filter chamber 9.Upper 5 times open ends of outer casing member are spirally connected with the sealing of middleware 11, form lower casing part 13 The cylindrical shape of outer casing member 5 in transition, continuation, and define in internal collecting chamber 15, seal what is be screwed into its lower end Bottom parts 17 are closed.Have in bottom parts 17 and unload Air Export 19, the particulate filter 21 connect before having, in collecting chamber 15 Liquid can be drawn by it from the bottom section of collecting chamber 15.
Middleware 11 has the shape of rotary body, and it is connected on the thread segment 23 that it is spirally connected with upper outer casing member 5, is formed radially The flange 25 of stretching, is again coupled to lower thread segment 27 thereon, forms the sealing with lower casing part 13 thereon and is spirally connected.At this moment, flange 25 form the corresponding bearing-surface of the end edge of outer casing member 5 or the end edge of lower casing part 13 in the upper side and lower side. Have in middleware 11 to be formed the first separation level whizzer 29, the cyclone cylinder shell 31 with the cylinder concentric with axle 3, Ostium 33 is passed through in its upper end.The fluid intake 35 that fluid mixture is formed by it from flange 25 is flowed into along tangent line Cyclone cylinder shell 31, to be conventionally formed eddy flow or rotation in the case of cyclone separator 29 in cyclone cylinder shell 31 Air duct.In addition, have outlet 37 in middleware 11, to draw the gas part separated from fluid mixture, relative Entrance 35 and outlet 37 stagger 90 ° of fluid issuings set 39 (referring to Fig. 2 and 5) and formed liquid connection passage.
As Fig. 4 is most evident that, the sleeve pipe 41 of insertion middleware 11 is formed, it exists axially through the lower end of middleware 11 The side of collecting chamber 15 extends up to the latter end of 31 inwall of cyclone cylinder shell 43.Inwall 43 is limited in the lower end of sleeve pipe 41 between pipeline section 47 Circular openings 45, it and axle 3 are concentric to be extended in sleeve pipe 41, and extends into collecting chamber 15 by its lower end.In this set Under, the connection between the axial distal end lower area of the formation cyclone cylinder of circular openings 45 shell 31 and collecting chamber 15, that is, outlet Hole, collecting chamber 15 can be directly instilled by its drop, and it is centrifuged as the larger component of mixture of fluid mixture density Power effect is accumulated on inwall 43.
In the upper end of cyclone cylinder shell 31, in middleware 11, the support bar 49 of grappling is coaxially passed through outside cyclone cylinder at 48 Shell 31 extends, and is extended out via the lower end of pipeline section 47.By means of the plug 51 positioned at the lower end 50 of support bar 49, in support bar 49 On cap portion 52 is installed, then the lower end of pipeline section 47 is spirally connected with this, so as to support bar 49 formation pipeline section 47 support member, it Surround the segment distance of support bar 49 1.The inner space 53 of pipeline section 47 forms the axial proximal region of cyclone cylinder shell 31 and gas with this Connection between outlet connection 55, the inside of cap portion 52 is imported in the inner space 53 of pipeline section 47.Therefore, outside cyclone cylinder Gas part in the axial proximal region of shell 31 enters the upper area of collecting chamber 15 by discharge coupling 55.
In middleware 11 towards on the transverse plane of collecting chamber 15, there are funnel-shaped recesses 59 inside its end edge 57.By This sets out, as preferably from Fig. 5 it is readily apparent that interface channel 61 extends to the upper transverse plane of middleware 11.In end edge Demister 65 is set with frame mode known per se between edge 57 and the inner wall section 63 of lower casing part 13, it surround sleeve pipe 41 from The end that groove 59 stretches out.Therefore, the gas part that is come out from pipe joint 55 and liquid is mixed with least in part and cylindrical The week side of boss surrounds other gas parts of pipeline section 47, and demister 65 is passed through before groove 59 is entered, in corresponding gas part from liquid Body further before release, flows through interface channel 61 in ascending motion on the flow path, flows to the upside of middleware 11.
In the upside of middleware 11 for forming the lower end of coalescing filter chamber 9, set and form the second coalescence filtration for separating level Device 67.It has the base portion 69 of the seat for the formation bottom 71 for abutting against the upside of middleware 11, and filtering material 73 is under End extends to the upper end 75 of coalescing filter 67.In the inside of the filter hollow space 77 surrounded by filtering material 63, Inner tube 79 extends coaxially through whole coalescing filter 67, and wherein the end 81 of the fastening end 75 of inner tube 79 at an upper portion thereof is opened Open, and therefore the space with filter chamber 9 is connected.Another lower end of the inner tube 79 extended in middleware 11, as Figures 1 and 4 It is shown, it is connected by access ramp 83 with the outlet 37 of gas part.
As shown in Fig. 5 flow arrows, the gas flowed out in the upper area of collecting chamber 15 from pipe joint 55, through centrifugation point There is the liquid component reduced from after device 29, by demister 65, by interface channel 61, subsequent base portion 69 After perforate 87 in path 85, and the bottom 71 of coalescing filter 67, reach inside the hollow space 77 of filter 67, from The filtering material 73 to form the second separation level is flowed through from inside to outside.Here, the liquid component of residual remains in the outside of filtering material 73, From here in the inner downlink of filter chamber 9, and liquid outlet 39 is reached from the bottom of filter chamber 9 by vertical channel 89.
The gas for the filter chamber 9 that encirclement is reached after filtering material 73, warp are flowed through inside filter hollow space 77 Cross after cyclone separator 29, by not liquid containing component after demister 65 and coalescing filter 67.By means of cyclonic separation Device 29, not only liquid but also solid particle are because density ratio hydrogen is big and can be separated with hydrogen.Access in the middle of in separation process Demister 65 makes it possible drop more than 5 μm from the flow deposition of fluid mixture, so as to followed by coalescing filter 67 Only it is used for handling the drop less than 5 μm.Therefore it is used for spy as the 3rd separation level before demister 65 is located at coalescing filter 67 Not effective fine separation.As shown in figure 5, from filter chamber 9, the gas represented with arrow 91 reaches inner tube 79 by upper end 81 It is interior, and reach side outlet 37 from there through access ramp 83.Following danger is avoided when flowing through axial inner tube 79, Drop i.e. in the outside of filtering material in filter chamber 9 73 is brought to gas vent 37.
In an illustrated embodiment, collecting chamber 15 is formed, is instilled to receive by the circular openings 45 of cyclone cylinder shell 31 The storage of the separation liquid of collecting chamber, for example, can wherein receive 5 liter capacities in collecting chamber 15 in lower casing part 13.Such as Fig. 1 It is shown, in order to control to unload null process by what outlet 19 was carried out, the control device by means of fluid level indicator can be set.Working as In preceding example, the floating body 93 guided in guide device 95 is arranged in this respect, forms the measurement of stroke measurment system 97 Section.Here, can be noncontacting pickup device, for example, magnetostriction method, wherein being tensioned waveguide inside guide device 95 Pipe.
All in all, it may be determined that the embodiment according to the device of the present invention is used for handling only somewhat carrying Liquid, the high pressure draught of the ionic liquid of such as at most contaminated 5% order of magnitude, for example, hydrogen.
For following separation, there are three different separation levels according to the solution of the device of the present invention, not only use To separate liquid form and be used for separating particulate pollutant.By the order of processing procedure, this is:
1. whizzer, make it possible partition density higher particle and liquid,
2. demister, makes separation larger, the drop for being greater than 5 μm is possibly realized, and prevents coalescing filter member with this The liquid of part is penetrated, and
3. coalescence filtration part, for depositing most thin aerosol, the preferred aerosol with 5 μm of drop size <.
Gas after filtering from collecting chamber 9 by the export of delivery line 79 that is coaxially disposed for device except providing Liquid entrainment minimize beyond, also have other advantages, you can with the filter housing of pressure vessel or coalescing filter with two Partly (component 5 and 11) is implemented, wherein all introducings and ejector can be placed in the fixed part 11 of the device.This is different It is easy to part exchanging ordinaryly, because pipeline need not be dismantled, the shell tank allows " easily " to touch, so as to renewal part. Otherwise must be the Shell structure into three parts, this brings the more inconvenient and higher cost of maintenance.

Claims (11)

1. processing contains gas such as especially hydrogen (H2), air, nitrogen (N2) or natural gas, and liquid such as especially from The device of the fluid mixture of sub- liquid, hydraulic oil or process liquid, it has at least one first separation level (29), is used to The gas component that fluid mixture is separated into liquid component and polluted by residual liquid component, thus at least another separation The remaining liquid component is removed in level (67).
2. according to the device of claim 1, it is characterised in that set whizzer (29) as the first separation level.
3. according to the device of claim 1 or 2, it is characterised in that set coalescing filter (67) as the second separation level.
4. according to the device of any one of above-listed claim, it is characterised in that all separation levels (29,67) are all disposed within one In common shell (1), there is the shell entrance (35) of fluid mixture, the gas part separated from liquid to use Outlet (37), and at least one liquid cleared out to draw unloads Air Export (19,39).
5. according to the device of any one of above-listed claim, it is characterised in that the shell (1) has to be prolonged along vertical axis (3) The cavity stretched, wherein whizzer (29) be set at coalescing filter (67) thereon and under it to receive Between the collecting chamber (15) for the liquid isolated.
6. according to the device of any one of above-listed claim, it is characterised in that the cyclone cylinder shell of whizzer (29) (31) inwall (43) defines ring in its lower end for abutting collecting chamber (15) between a pipeline section (47) concentric with axle (3) Shape perforate (45), the connection between its axial distal end region for forming cyclone cylinder cylinder (31) and collecting chamber (15).
7. according to the device of any one of above-listed claim, it is characterised in that the inner space (53) of pipeline section (47) forms rotation A part for connection between air duct cylinder (31) axial proximal region and collecting chamber (15) upper area.
8. according to the device of any one of above-listed claim, it is characterised in that coalescing filter (67), which has, surrounds filter The filtering material (73) of inner hollow space (77), and in collecting chamber (15) upper area and the filter of coalescing filter (67) Interface channel (61) is set between hollow space (77).
9. according to the device of any one of above-listed claim, it is characterised in that coalescing filter (67) has coaxial inner tube (79) space (9) with adjoining on the outside of filtering material (73) of shell (1), is imported in its upper end (81), and is introduced in its lower end The housing outlet (37) of gas part.
10. according to the device of any one of above-listed claim, it is characterised in that coalesced in collecting chamber (15) upper end and guiding into Between the interface channel (61) of the filter interior hollow space (77) of filter (67), demister (65) is set as the 3rd separation Level.
11. according to the device of any one of above-listed claim, it is characterised in that vacated in collecting chamber (15) bottom section and unloading Particulate filter (21) is set between mouth (19).
CN201580039221.2A 2014-08-13 2015-07-18 Device for treating fluid mixtures Active CN107073361B (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102014012094.5A DE102014012094A1 (en) 2014-08-13 2014-08-13 Device for the treatment of fluid mixtures
DE102014012094.5 2014-08-13
PCT/EP2015/001485 WO2016023610A1 (en) 2014-08-13 2015-07-18 Device for treating fluid mixtures

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CN107073361B CN107073361B (en) 2019-12-17

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US (1) US10561966B2 (en)
EP (1) EP3180131B1 (en)
JP (1) JP6412249B2 (en)
KR (1) KR102383209B1 (en)
CN (1) CN107073361B (en)
DE (1) DE102014012094A1 (en)
WO (1) WO2016023610A1 (en)

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JP2017524521A (en) 2017-08-31
JP6412249B2 (en) 2018-10-24
WO2016023610A1 (en) 2016-02-18
EP3180131B1 (en) 2020-09-09
CN107073361B (en) 2019-12-17
DE102014012094A1 (en) 2016-02-18
EP3180131A1 (en) 2017-06-21
KR20170043515A (en) 2017-04-21
US10561966B2 (en) 2020-02-18
KR102383209B1 (en) 2022-04-07
US20170225101A1 (en) 2017-08-10

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