CN107022907A - The method dyed using vegetable colour to cashmere ready-made clothes - Google Patents

The method dyed using vegetable colour to cashmere ready-made clothes Download PDF

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Publication number
CN107022907A
CN107022907A CN201611072079.4A CN201611072079A CN107022907A CN 107022907 A CN107022907 A CN 107022907A CN 201611072079 A CN201611072079 A CN 201611072079A CN 107022907 A CN107022907 A CN 107022907A
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CN
China
Prior art keywords
cashmere
ready
made clothes
dyed
dye solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611072079.4A
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Chinese (zh)
Inventor
李胜利
张朝清
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Dongguan Dongsheng Cashmere Products Co Ltd
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Dongguan Dongsheng Cashmere Products Co Ltd
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Publication date
Application filed by Dongguan Dongsheng Cashmere Products Co Ltd filed Critical Dongguan Dongsheng Cashmere Products Co Ltd
Priority to CN201611072079.4A priority Critical patent/CN107022907A/en
Publication of CN107022907A publication Critical patent/CN107022907A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02Material containing basic nitrogen
    • D06P3/04Material containing basic nitrogen containing amide groups
    • D06P3/14Wool
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02After-treatment

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention discloses the method dyed using vegetable colour to cashmere ready-made clothes, it includes:(i) cationization processing is carried out to cashmere ready-made clothes to be dyed;(ii) the treated cashmere ready-made clothes of step (i) is immersed in dye solution, then carries out temperature adjustment processing so that the cashmere ready-made clothes absorbs the dye solution and color is bonded to the cashmere ready-made clothes;Wherein, vegetable colour of the dye solution comprising 0.1 5%o.w.f. and 0.5 1.0%o.w.f. bleeding agent and pH value are 3.5 4.0, and the vegetable colour is tobacco leaf and stem extraction.Warming temperature twice is employed in the method for the present invention, ready-made clothes can be made to fully absorb dyestuff, it is to avoid dyeing flower phenomenon, and dyestuff is fully bonded to ready-made clothes surface, mordant need not be added in dyeing course simultaneously, dyeing is simplified, shortens dyeing time and reduce dyeing temperature.

Description

The method dyed using vegetable colour to cashmere ready-made clothes
Technical field
Present invention relates in general to a kind of colouring method, specifically, the present invention relates to using vegetable colour to cashmere into The method that clothing is dyed.
Background technology
Vegetable colour is nontoxic, and health will not be caused any harm.The fabric color shape dyed by vegetable colour It is natural, prolonged not take off, and with insect prevention, the effect of antibacterial, it is also that modern clothing is chased after not available for chemical dye that this, which is, The quality asked.Existing market has had the commercial application that vegetable colour is dyed to cotton and chemical & blended fabric, but is Step section, and cost is too high, influences the expansion in its market.Wool product is of a relatively high with its added value, has larger exploitation empty Between, and vegetable colour more conforms to the consumption concept of natural fiber.
Existing vegetable colour dyeing mostly need to be by media material, the more difficult control of reappearance;And existing dyer Skill dyeing temperature is all more than 90 DEG C, and dyeing time is longer.
Chinese patent application CN105178067A discloses a kind of process of gamene vegetable dye dyeing wool bar, wherein The method of disclosed vegetable colour dyeing wool bar needs to carry out mordant dyeing as mordant by the aluminium ion contained in alum, belongs to Traditional dye for fabrics dyeing.
Chinese patent application CN105369654A, which discloses a kind of blueberry leaf vegetable colour, is used for the dye of black-and-blue silk Color technique, it primarily focuses on dyeing silk product, and the process time is longer.
Chinese patent application CN104711869A discloses a kind of method that use vegetable colour is dyed to cashmere, It is primarily directed to goat cashmere fabric, rather than cashmere ready-made clothes.
The content of the invention
For the deficiencies in the prior art, the present invention is provided one kind and cashmere ready-made clothes is dyed using vegetable colour Method, it includes:
(i) cationization processing is carried out to cashmere ready-made clothes to be dyed;
(ii) will step (i) it is treated cashmere ready-made clothes immersion dye solution in, then carry out temperature adjustment processing so that The cashmere ready-made clothes absorbs the dye solution and color is bonded to the cashmere ready-made clothes, wherein, using bath raio as 1:20 to 1: 25 immerse the cashmere ready-made clothes to be dyed in the dye solution.
Vegetable colour and 0.5-1.0% that the dye solution used in the method for the present invention includes 0.1-5%o.w.f. O.w.f. bleeding agent and pH value are 3.5-4.0, also, the dye solution by by the vegetable colour with 0.1-5% O.w.f. concentration is dissolved in the soft water that pH is 3.4-4.0, is subsequently added the bleeding agent that concentration is 0.5-1.0%o.w.f. and is matched somebody with somebody System is formed, wherein, the bleeding agent is SP-2 bleeding agents, and the vegetable colour is tobacco leaf and stem extraction.
Temperature adjustment processing in the method for the present invention includes:Dye solution is warming up to by 30- with 1 DEG C/min of speed 45 DEG C are incubated 10-15 minute, it is preferable that 38 DEG C of insulations 10 minutes are warming up to, then again with 0.5 DEG C/min of speed by dyestuff Solution is warming up to 65 DEG C -75 DEG C and is incubated 25-35 minutes, is preferably warming up to 70 DEG C -75 DEG C and is incubated 30 minutes.
The present invention method in cationization by by the cashmere ready-made clothes to be dyed using bath raio as 1:20-1:25 Ratio immerses the water by being prepared during bleeding agent using 0.5-1.0%o.w.f. concentration are dissolved in into pH as 3.5-4.0 soft water In solution, 70-80 DEG C of insulation is then warming up to 9 DEG C/min of speed and realized within 15-25 minutes, wherein, the bleeding agent is SP-2 bleeding agents.
The method of the present invention also includes the cashmere ready-made clothes after being dyed to step (ii) and post-processed, wherein, the rear place Reason includes:Remove the loose colour on the cashmere ready-made clothes surface after dyeing.
Terms used herein " cashmere ready-made clothes " includes cashmere clothes, scarf for being made etc., such as slubbing cashmere blouse, thick Wool cashmere scarf etc..
Terms used herein " bath raio " refers to the ratio that clothing and dye solution is made in the cashmere dyed to contaminate mode, specifically For, the part by weight of clothing and dye solution is made for the cashmere that need to dye.
The product that terms used herein " color fastness " refers to dyeing is subjected to external influence and can keep the property of its original color and luster Can, color fastness typically evaluates (totally 5 grades) with series, and series is higher, and color fastness is better.
Warming temperature twice is employed in the method that the use vegetable colour of the present invention is dyed to cashmere ready-made clothes, this phase Ready-made clothes can be made to fully absorb dyestuff for a warming temperature of the prior art, it is to avoid dyeing flower phenomenon, and enable dyestuff Fully it is bonded to ready-made clothes surface.The warming temperature twice used simultaneously in the colouring method of the present invention need not be warming up to high temperature Degree, and insulation ten minutes to 30 points is only needed after heating every time, mordant need not be added in dyeing course, dyeing is simplified Technique, shortens dyeing time and reduces dyeing temperature.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, it is illustrated with further below to this hair Bright to be described in detail but described below embodiments of the present invention are merely illustrative, not to present invention composition Any limitation.
Embodiment 1
The present embodiment is so that background color is this white slubbing cashmere jumper blouse as an example, using from Dimora Colours Inc. The tobacco leaf and stem extraction dyestuff FW16-11 of company's purchase are dyed in horizontal garment dyeing machine to the cashmere jumper blouse, Colouring method comprises the following steps:
(i) the pre-treatment aqueous solution is prepared:Bleeding agent using 0.5%o.w.f. concentration are dissolved to pH soft as 3.5-4.0 In water, the pre-treatment aqueous solution is obtained;
(ii) pre-treatment:Using bath raio as 1:20-1:25 ratio, the water-soluble of step (i) preparation is immersed by cashmere jumper blouse In liquid, it is warming up to 80 DEG C with 9 DEG C/min of speed and is incubated 20 minutes, be then cooled to room temperature;
(iii) dye solution is prepared:By dyestuff FW16-11 using 1.25%o.w.f. concentration be dissolved to pH as 3.8 it is soft In water, then bleeding agent is dissolved in wherein with 0.5%o.w.f. concentration;
(iv) dye:By the treated cashmere jumper blouse of step (ii) using bath raio as 1:25 ratio immersion step (iii) In the dye solution of preparation, 38 DEG C are warming up to 1 DEG C/min of speed, 10 minutes are incubated, so that cashmere jumper blouse is fully absorbed Vegetable colour, then 75 DEG C are warming up to 0.5 DEG C/min of speed, 30 minutes are incubated, so that vegetable colour is fully bonded to cashmere Jumper blouse, is then cooled to room temperature;
(v) post-process:Soap loose colour one time, obtain cashmere jumper blouse sample #1 of the dyeing for lightpink.
Embodiment 2
The present embodiment is so that background color is this white slubbing cashmere scarf as an example, using public from Dimora Colours Inc. The tobacco leaf and stem extraction dyestuff FW16-1 for taking charge of purchase are dyed in horizontal garment dyeing machine to the cashmere scarf, dyeing side Method comprises the following steps:
(i) the pre-treatment aqueous solution is prepared:Bleeding agent using 1%o.w.f. concentration are dissolved to pH as the soft of 3.5-4.0 In water, the pre-treatment aqueous solution is obtained;
(ii) pre-treatment:Using bath raio as 1:20-1:25 ratio, the aqueous solution that step (i) is prepared is immersed by cashmere scarf In, it is warming up to 80 DEG C with 9 DEG C/min of speed and is incubated 20 minutes, is then cooled to room temperature;
(iii) dye solution is prepared:Vegetable colour FW16-1 using 3.6%o.w.f. concentration are dissolved to pH as 3.6 In soft water, then bleeding agent is dissolved in wherein with 1%o.w.f. concentration;
(iv) dye:By the treated cashmere scarf of step (ii) using bath raio as 1:20 ratio immersion step (iii) is matched somebody with somebody In the dye solution of system, 38 DEG C are warming up to 1 DEG C/min of speed, 10 minutes are incubated, so that slubbing cashmere scarf is fully absorbed Vegetable colour, then 75 DEG C are warming up to 0.5 DEG C/min of speed, 30 minutes are incubated, so that vegetable colour is fully bonded to slubbing Cashmere scarf, is then cooled to room temperature;
(v) post-process:Soap twice of loose colour, obtain cashmere scarf sample #2 of the dyeing for middle grey.
Embodiment 3
The present embodiment is so that background color is the male blouse of this white slubbing cashmere as an example, using from Dimora Colours Inc. The tobacco leaf and stem extraction dyestuff FW16-7 of company's purchase are dyed in horizontal garment dyeing machine to the male blouse of the cashmere, are contaminated Color method comprises the following steps:
(i) the pre-treatment aqueous solution is prepared:Bleeding agent using 1%o.w.f. concentration are dissolved to pH as the soft of 3.5-4.0 In water, the pre-treatment aqueous solution is obtained;
(ii) pre-treatment:Using bath raio as 1:20-1:25 ratio, the water-soluble of step (i) preparation is immersed by the male blouse of cashmere In liquid, it is warming up to 80 DEG C with 9 DEG C/min of speed and is incubated 20 minutes, be then cooled to room temperature;
(iii) dye solution is prepared:By vegetable colour FW16-7 and FW16-11 respectively with 1%o.w.f. concentration and 4% O.w.f. concentration is dissolved in the soft water that pH is 3.5, is then dissolved in bleeding agent wherein with 1%o.w.f. concentration;
(iv) dye:By the male blouse of the treated cashmere of step (ii) using bath raio as 1:20 ratio immersion step (iii) In the dye solution of preparation, 38 DEG C are warming up to 1 DEG C/min of speed, 10 minutes are incubated, so that cashmere man's blouse is fully absorbed Vegetable colour, then 75 DEG C are warming up to 0.5 DEG C/min of speed, 30 minutes are incubated, so that vegetable colour is fully bonded to cashmere Male blouse, is then cooled to room temperature;
(v) post-process:Soap twice of loose colour, obtain cashmere male blouse sample #3 of the dyeing for crocus.
According to GB/T3922-2013, GB/T3920-2008, GB/T3921-2008, GB/T5713-2013, to above-mentioned reality Sample #1 to the #3 progress dyeing color fastness tests that example 1 to 3 is obtained are applied, test result is listed in table 1 below.According to GB/ T8427-2005 was using 500 light fastness test instrument Exposure to Sunlight of Meccah rope 20 hours, the sample #1 obtained to above-described embodiment 1 to 3 Weathering color fastness test is carried out to #3, test result is listed in table 2 below.
The sample #1 to #3 of table 1. dyeing color fastness test result
The sample #1 to #3 of table 2. weathering color fastness test result
From the test result of upper Tables 1 and 2 can be seen that using the present invention method dyed obtained by cashmere into Every color fastness of clothing meets or exceeds 4 grades, and some also reach 5 grades, this show by the method for the present invention using tobacco leaf and Stem extraction dyestuff, which carries out dyeing, can make dyestuff fully be bonded to cashmere ready-made clothes.
Above in association with embodiment, the present invention is described, and these embodiments are merely exemplary , it is impossible to protection scope of the present invention is limited with this, those skilled in the art can be with the premise of essence of the present invention is not departed from Carry out various modifications, change or replacement.Therefore, the various equivalent variations made according to the present invention, still fall within the present invention and are covered Scope.

Claims (9)

1. the method dyed using vegetable colour to cashmere ready-made clothes, it includes:
(i) cationization processing is carried out to cashmere ready-made clothes to be dyed;
(ii) the treated cashmere ready-made clothes of step (i) is immersed in dye solution, then carries out temperature adjustment processing so that described Cashmere ready-made clothes absorbs the dye solution and color is bonded to the cashmere ready-made clothes;
Wherein, vegetable colour of the dye solution comprising 0.1-5%o.w.f. and 0.5-1.0%o.w.f. bleeding agent and pH It is worth for 3.5-4.0, the vegetable colour is tobacco leaf and stem extraction.
2. the method for claim 1, wherein the temperature adjustment processing includes:With 1 DEG C/min of speed by dyestuff Solution be warming up to 30-45 DEG C be incubated 10-15 minutes, then again with 0.5 DEG C/min of speed by dye solution be warming up to 65 DEG C- 75 DEG C are incubated 25-35 minutes.
3. method as claimed in claim 2, wherein, the temperature adjustment processing includes:With 1 DEG C/min of speed by dyestuff Solution is warming up to 38 DEG C and is incubated 10 minutes, and dye solution then is warming up into 70 DEG C of -75 DEG C of guarantors with 0.5 DEG C/min of speed again Temperature 30 minutes.
4. the method for claim 1, wherein the dye solution by by the vegetable colour with 0.1-5% O.w.f. concentration is dissolved in the soft water that pH is 3.4-4.0, is subsequently added the bleeding agent that concentration is 0.5-1.0%o.w.f. and is matched somebody with somebody System is formed.
5. the method for claim 1, wherein using bath raio as 1:20 to 1:25 immerse the cashmere ready-made clothes to be dyed In the dye solution.
6. the method as described in claim 1, the cationization will by the way that the cashmere ready-made clothes immersion to be dyed is passed through In the aqueous solution that bleeding agent using 0.5-1.0%o.w.f. concentration are prepared in being dissolved in pH as 3.5-4.0 soft water, then with 9 DEG C/min speed be warming up to 70-80 DEG C of insulation and 15-25 minutes realize.
7. method as claimed in claim 6, wherein, the cashmere ready-made clothes to be dyed is using bath raio as 1:20-1:25 ratio Immerse in the aqueous solution.
8. the method as described in claim 1, methods described also includes locating after the cashmere ready-made clothes after dyeing step (ii) is carried out Reason, wherein, the post processing includes:Remove the loose colour on the cashmere ready-made clothes surface after dyeing.
9. the method as described in claim 1 or 4, wherein, the bleeding agent is:SP-2 bleeding agents.
CN201611072079.4A 2016-11-29 2016-11-29 The method dyed using vegetable colour to cashmere ready-made clothes Pending CN107022907A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109183465A (en) * 2018-10-18 2019-01-11 上海嘉麟杰纺织科技有限公司 A kind of plant dyeing method improving wool ready-made clothes coloured light depth
CN110387755A (en) * 2018-04-17 2019-10-29 广东印象派服装有限公司 The uvioresistant cashmere product of plant dyeing

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101003951A (en) * 2006-12-19 2007-07-25 江苏华恒科技发展有限公司 Tie-dyeing method for cashmere textile
CN102704281A (en) * 2012-06-13 2012-10-03 福建七匹狼实业股份有限公司 Preparation method for garments
CN104711869A (en) * 2015-02-11 2015-06-17 广东印象草原实业发展有限公司 Method for dyeing original ecological cashmere by using plant dye
CN105178067A (en) * 2015-09-28 2015-12-23 江苏丹毛纺织股份有限公司 Technology method for wool tops dyed with madder plant dye

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101003951A (en) * 2006-12-19 2007-07-25 江苏华恒科技发展有限公司 Tie-dyeing method for cashmere textile
CN102704281A (en) * 2012-06-13 2012-10-03 福建七匹狼实业股份有限公司 Preparation method for garments
CN104711869A (en) * 2015-02-11 2015-06-17 广东印象草原实业发展有限公司 Method for dyeing original ecological cashmere by using plant dye
CN105178067A (en) * 2015-09-28 2015-12-23 江苏丹毛纺织股份有限公司 Technology method for wool tops dyed with madder plant dye

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110387755A (en) * 2018-04-17 2019-10-29 广东印象派服装有限公司 The uvioresistant cashmere product of plant dyeing
CN109183465A (en) * 2018-10-18 2019-01-11 上海嘉麟杰纺织科技有限公司 A kind of plant dyeing method improving wool ready-made clothes coloured light depth

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Application publication date: 20170808