CN106946634A - A kind of profit phase gas transporting material device and technique - Google Patents
A kind of profit phase gas transporting material device and technique Download PDFInfo
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- CN106946634A CN106946634A CN201710169986.9A CN201710169986A CN106946634A CN 106946634 A CN106946634 A CN 106946634A CN 201710169986 A CN201710169986 A CN 201710169986A CN 106946634 A CN106946634 A CN 106946634A
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- aqueous phase
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- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
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Abstract
The invention discloses a kind of profit phase gas transporting material device and technique, including aqueous phase sealed reactor, oil phase sealed reactor, air compressor machine, oil phase pans, aqueous phase pans, oil phase storage tank, aqueous phase storage tank, static emulsifying apparatus, static state sensitization disperser, filling apparatus and control terminal, the air compressor machine includes aqueous phase air compressor machine and oil phase air compressor machine, the inner cylinder of aqueous phase sealed reactor and oil phase sealed reactor is made using pressure-resistant material, static emulsifying apparatus, static state sensitization disperser, filling apparatus, oil phase storage tank, aqueous phase storage tank, aqueous phase sealed reactor, oil phase sealed reactor, aqueous phase air compressor machine and oil phase air compressor machine are connected with control terminal, flowing has 0.2 0.3MPa compressed air in circulating line.The device is simple to operate, is the working condition that can control each equipment by control terminal, high degree of automation, the good airproof performance of device, and almost without liquid residue in course of conveying, using effect is good.
Description
Technical field
The present invention relates to Emulsion Explosive Production field, specifically a kind of profit phase gas transporting material device and technique.
Background technology
Emulsion is the water base ammonium nitrate explosive that the class grown up the seventies in last century newly emerges, because its have it is excellent
Good detonation property and water repelling property, so since the advent of the world is just paid close attention to by various countries, the preparation method of emulsion is first
Aqueous phase solution is dissolved into the heating of the oxidants such as ammonium nitrate, emulsifying agent, fuel agent heating oil-phase solution is fused into, then at certain
Process conditions under, by strong stirring formation water-in-oil type gel, then by gel sensitization emulsion finished product is made.
In actual production, the aqueous phase solution and oil-phase solution prepared needs to use longer pipeline to be sent to the storage of each bar production line
Tank, pipeline probably has 50-100 meters.Existing mode of movement has two kinds, and a kind of is traditional pumping, and pumping has the drawback that
The raffinate in rear pipeline has been sent to be difficult to solve, processing not with great difficulty plugging, and also aqueous phase solution crystallization point is high, is less than 80 in temperature
It can be crystallized after DEG C；Oil-phase solution freezing point is high, can be solidified after temperature is less than 60 DEG C；Another is to use compressed air force feed, pressure
The shortcoming of contracting air force feed is that preparation tank needs to seal, the more difficult sealing of ammonium nitrate charge door of particularly aqueous phase preparation tank, and this is just
Inconvenience is brought for the production of people.
The content of the invention
It is an object of the invention to provide a kind of profit phase gas transporting material device, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical scheme：
A kind of profit phase gas transporting material device, including aqueous phase sealed reactor, oil phase sealed reactor, air compressor machine,
Oil phase pans, aqueous phase pans, oil phase storage tank, aqueous phase storage tank, static emulsifying apparatus, static sensitization disperser, filling apparatus and
Control terminal, the air compressor machine includes aqueous phase air compressor machine and oil phase air compressor machine, aqueous phase sealed reactor and oil phase sealed reactor
Inner cylinder using pressure-resistant material make and aqueous phase sealed reactor and oil phase sealed reactor on charge door on be respectively mounted
There is Pneumatic gate valve, the lower end of aqueous phase sealed reactor is provided with aqueous phase check valve, and the lower end of oil phase sealed reactor is provided with oil
Phase check valve, aqueous phase sealed reactor is connected by circulating line with aqueous phase pans and in aqueous phase sealed reactor and aqueous phase
Between be provided with aqueous phase air compressor machine between tank, aqueous phase pans are connected by circulating line with aqueous phase storage tank, aqueous phase storage tank and aqueous phase
Sealed reactor be connected, oil phase sealed reactor be connected by circulating line with oil phase pans and oil phase sealed reactor and
Oil phase air compressor machine is provided between oil phase pans, oil phase pans are connected by circulating line with oil phase storage tank, oil phase storage tank
It is connected with oil phase sealed reactor, oil phase storage tank and aqueous phase storage tank are connected with static emulsifying apparatus, and static emulsifying apparatus is quick with static state
Change disperser be connected, static state sensitization disperser be connected with filling apparatus, static emulsifying apparatus, static state be sensitized disperser, filling apparatus,
Oil phase storage tank, aqueous phase storage tank, aqueous phase sealed reactor, oil phase sealed reactor, aqueous phase air compressor machine and oil phase air compressor machine with control
Terminal processed is connected, and flowing has 0.2-0.3MPa compressed air in circulating line.
It is used as further scheme of the invention：Circulating line uses sleeve pipe, and sleeve pipe includes stainless steel tube and seamless steel pipe, nothing
Steel pipe socket is stitched in the outside of stainless steel tube.
It is used as further scheme of the invention：Control terminal includes touch display screen and computer.
It is used as further scheme of the invention：Oil phase flowmeter is installed between oil phase sealed reactor and oil phase storage tank,
Aqueous phase flowmeter is installed between aqueous phase sealed reactor and aqueous phase storage tank.
The workflow of the profit phase gas transporting material device, is comprised the following steps that：
Step one, control terminal is worked, and user is operated in control terminal, added Aqueous Phase Raw Material by feeder sleeve
Into aqueous phase sealed reactor, Aqueous Phase Raw Material heating is dissolved into aqueous phase solution by aqueous phase sealed reactor, by feeder sleeve by oil
Phase raw material is added into oil phase sealed reactor, and oil phase raw material reacts in oil phase sealed reactor, and oil-phase solution is made；
Step 2, opens aqueous phase check valve and aqueous phase air compressor machine, aqueous phase solution 0.2-0.3Mpa compressed air it is defeated
Send down and deliver to successively aqueous phase pans and aqueous phase storage tank, the aqueous phase solution of aqueous phase storage tank is delivered to static emulsifying apparatus, unnecessary water
Phase storage tank flows back to aqueous phase sealed reactor, and the flow liquid phase compatible with water of oil-phase solution is same, and aqueous phase solution and oil-phase solution are quiet
Emulsified in state emulsifier, product after emulsification enters static sensitization disperser and disperseed, filling apparatus is to the feed liquid that mixes
Carry out filling.
Compared with prior art, the beneficial effects of the invention are as follows：The device is reasonable in design, simple in construction, and fault rate is low, makes
With security and good operation stability；The device is simple to operate, is the work that can control each equipment by control terminal
100% without liquid residue in situation, high degree of automation, the good airproof performance of device, course of conveying, and using effect is good.And
The conveying device and technique do not have any influence on properties of product, and this is also a quantum jump.
Brief description of the drawings
Fig. 1 is the structural representation of profit phase gas transporting material device.
Wherein：1- aqueous phase sealed reactors, 2- aqueous phase check valves, 3- aqueous phase air compressor machines, 4- aqueous phase pans, the storage of 5- aqueous phases
Tank, 6- control terminals, 7- oil phase sealed reactors, 8- oil phase check valves, 9- oil phase air compressor machines, 10- oil phase pans, 11- oil
Phase storage tank, 12- static emulsifying apparatus, 13- static state sensitization dispersers, 14- filling apparatus, 15- circulating lines.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Referring to Fig. 1, a kind of profit phase gas transporting material device, including the sealing reaction of aqueous phase sealed reactor 1, oil phase
7 kettles, air compressor machine, oil phase pans 10, aqueous phase pans 4, oil phase storage tank 11, aqueous phase storage tank 5, static emulsifying apparatus 12, static state are quick
Change disperser 13, filling apparatus 14 and control terminal 6, the air compressor machine includes aqueous phase air compressor machine 3 and oil phase air compressor machine 9, aqueous phase
The inner cylinder of sealed reactor 1 and oil phase sealed reactor 7 is made and aqueous phase sealed reactor 1 and oil phase using pressure-resistant material
Pneumatic gate valve is mounted on charge door on sealed reactor 7, the lower end of aqueous phase sealed reactor 1 is provided with aqueous phase check valve
2, the lower end of oil phase sealed reactor 7 is provided with oil phase check valve 8, and aqueous phase sealed reactor 1 passes through circulating line 15 and aqueous phase
Pans 4 are connected and aqueous phase air compressor machine 3, aqueous phase pans 4 are provided between aqueous phase sealed reactor 1 and aqueous phase pans 4
It is connected by circulating line 15 with aqueous phase storage tank 5, aqueous phase storage tank 5 is connected with aqueous phase sealed reactor 1, oil phase sealed reactor 7
It is connected by circulating line 15 with oil phase pans 10 and is provided with oil between oil phase sealed reactor 7 and oil phase pans 10
Phase air compressor machine 9, oil phase pans 10 are connected by circulating line 15 with oil phase storage tank 11, and oil phase storage tank 11 is sealed with oil phase to react
Kettle 7 is connected, and oil phase storage tank 11 and aqueous phase storage tank 5 are connected with static emulsifying apparatus 12, and static emulsifying apparatus 12 and static sensitization are scattered
Device 13 is connected, and static state sensitization disperser 13 is connected with filling apparatus 14, and static emulsifying apparatus 12, static state are sensitized disperser 13, filling
Equipment 14, oil phase storage tank 11, aqueous phase storage tank 5, aqueous phase sealed reactor 1, oil phase sealed reactor 7, aqueous phase air compressor machine 3 and oil phase
Air compressor machine 9 is connected with control terminal 6, and flowing has 0.2-0.3MPa compressed air in circulating line 15.Circulating line 15 is adopted
With sleeve pipe, sleeve pipe includes stainless steel tube and seamless steel pipe, and seamless steel pipe is enclosed within the outside of stainless steel tube.Control terminal 6 includes touching
Touch display screen and computer.Oil phase flowmeter, aqueous phase sealing reaction are installed between oil phase sealed reactor 7 and oil phase storage tank 11
Aqueous phase flowmeter is installed between kettle 1 and aqueous phase storage tank 5.
Profit phase gas transporting material technique, is comprised the following steps that：
Step one, disintegrating machine crushes oxidant, and the oxidant after crushing is delivered to aqueous phase by conveying worm and sealed
In reactor, oxidant heating is dissolved into aqueous phase solution by aqueous phase sealed reactor；
Step 2, solid material is melted through changing wax pan, and emulsifying agent is heated through carburetion groove, after the solid material of fusing and heating
Emulsifying agent feeding oil phase sealed reactor in react, be made oil-phase solution, be stored in oil phase storage tank；
Step 3, air compressor machine is by the air compression conveying in gas tank and compressed air passes through oil expeller oil removing, opens
Aqueous phase check valve and aqueous phase air compressor machine, aqueous phase solution are delivered in the middle of aqueous phase successively under the conveying of 0.2-0.3Mpa compressed air
Tank and aqueous phase storage tank, the aqueous phase solution of aqueous phase storage tank are delivered to static emulsifying apparatus, and it is anti-that unnecessary aqueous phase storage tank flows back to aqueous phase sealing
Kettle is answered, the flow liquid phase compatible with water of oil-phase solution is same, and aqueous phase solution and oil-phase solution are emulsified in static emulsifying apparatus, after emulsification
Product enter static sensitization disperser and disperseed, filling apparatus is filling to the feed liquid progress mixed.
Sealed reactor inner cylinder is pressure-resistant 0.3MPa, sealed reactor is controlled using Pneumatic gate valve, solves the close of charge door
Envelope problem.
The pipeline that the technique is used uses the work high in the middle and low on both ends laid by certain slope, further function as preventing materials accumulation
With.Because oil-phase solution density is less than aqueous phase solution density, the pressure of force feed oil-phase solution is less than force feed aqueous phase solution, added
The characteristic of conveying device and technique of the present invention, present invention conveying material device and technique maximum delivery are highly about 20m.
The temperature of the oil phase storage tank is 80-90 DEG C, and the temperature of aqueous phase storage tank is 90-100 DEG C, and static emulsifying apparatus X-axis is shaken
Dynamic frequency 0.9-1.0mm/s, static emulsifying apparatus Y axis vibration frequency 1.4-1.5mm/s, static emulsifying apparatus Z axis vibration frequency 0.1-
0.2mm/s.Device and technique operationally 100% safety are ensure that in theory.
The static emulsifying apparatus carries out X axis vibration alarm, Y axis vibration alarm, Z axis vibration alarm, electric current by sensor
The comprehensive alarm that too high, temperature is too high, cut off the water supply；Oil phase storage tank carries out that flow is too low, too high alarm by sensor, and aqueous phase is stored up
Tank carries out that flow is too low, too high alarm by sensor.Which further increases security.
The present invention operation principle be：The inner cylinder of aqueous phase sealed reactor 1 and oil phase sealed reactor 7 is adopted in the device
Made of pressure-resistant material, Pneumatic gate valve is installed at the charge door of aqueous phase sealed reactor 1 and oil phase sealed reactor 7, can be with
Solve sealing problem；Aqueous phase air compressor machine 3 and oil phase air compressor machine 9 prepare 0.2-0.3MPa compressed air, utilize 0.2-0.3MPa
Compressed air carry out force feed, had no effect without any raffinate, and to properties of product in circulating line 15.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as to the claim involved by limitation.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It may be appreciated other embodiment.
Claims (9)
1. a kind of profit phase gas transporting material device, it is characterised in that including aqueous phase sealed reactor, oil phase sealing reaction
Kettle, air compressor machine, oil phase pans, aqueous phase pans, oil phase storage tank, aqueous phase storage tank, static emulsifying apparatus, static sensitization disperser,
Filling apparatus and control terminal, the air compressor machine include aqueous phase air compressor machine and oil phase air compressor machine, aqueous phase sealed reactor and oil phase
The inner cylinder of sealed reactor is made and the charging on aqueous phase sealed reactor and oil phase sealed reactor using pressure-resistant material
Pneumatic gate valve is mounted on mouthful, the lower end of aqueous phase sealed reactor is provided with aqueous phase check valve, oil phase sealed reactor
End is provided with oil phase check valve, and aqueous phase sealed reactor is connected and aqueous phase sealing reaction by circulating line with aqueous phase pans
Aqueous phase air compressor machine is provided between kettle and aqueous phase pans, aqueous phase pans are connected by circulating line with aqueous phase storage tank, aqueous phase
Storage tank is connected with aqueous phase sealed reactor, and oil phase sealed reactor is connected by circulating line with oil phase pans and oil phase is close
Oil phase air compressor machine is provided between envelope reactor and oil phase pans, oil phase pans pass through circulating line and oil phase storage tank phase
Even, oil phase storage tank is connected with oil phase sealed reactor, and oil phase storage tank and aqueous phase storage tank are connected with static emulsifying apparatus, static emulsion
Device is connected with static state sensitization disperser, and static state sensitization disperser is connected with filling apparatus, and static emulsifying apparatus, static sensitization are scattered
Device, filling apparatus, oil phase storage tank, aqueous phase storage tank, aqueous phase sealed reactor, oil phase sealed reactor, aqueous phase air compressor machine and oil phase
Air compressor machine is connected with control terminal, and flowing has 0.2-0.3MPa compressed air in circulating line.
2. profit phase gas transporting material device according to claim 1, it is characterised in that the circulating line is using set
Pipe, sleeve pipe includes stainless steel tube and seamless steel pipe, and seamless steel pipe is enclosed within the outside of stainless steel tube.
3. profit phase gas transporting material device according to claim 1 or 2, it is characterised in that the control terminal bag
Include touch display screen and computer.
4. profit phase gas transporting material device according to claim 1, it is characterised in that the oil phase sealed reactor
Oil phase flowmeter is installed between oil phase storage tank, aqueous phase flowmeter is installed between aqueous phase sealed reactor and aqueous phase storage tank.
5. profit phase gas transporting material technique, it is characterised in that comprise the following steps that：
Step one, disintegrating machine crushes oxidant, and the oxidant after crushing is delivered to aqueous phase sealing reaction by conveying worm
In kettle, oxidant heating is dissolved into aqueous phase solution by aqueous phase sealed reactor；
Step 2, solid material is melted through changing wax pan, and emulsifying agent is heated through carburetion groove, the breast after the solid material of fusing and heating
Reacted in agent feeding oil phase sealed reactor, oil-phase solution is made, oil phase storage tank is stored in；
Step 3, air compressor machine is by the air compression conveying in gas tank and compressed air passes through oil expeller oil removing, opens aqueous phase
Check valve and aqueous phase air compressor machine, aqueous phase solution delivered to successively under the conveying of 0.2-0.3Mpa compressed air aqueous phase pans and
Aqueous phase storage tank, the aqueous phase solution of aqueous phase storage tank is delivered to static emulsifying apparatus, and unnecessary aqueous phase storage tank flows back to aqueous phase sealed reactor,
The flow liquid phase compatible with water of oil-phase solution is same, and aqueous phase solution and oil-phase solution are emulsified in static emulsifying apparatus, the production after emulsification
Thing enters static sensitization disperser and disperseed, and filling apparatus carries out filling to the feed liquid mixed.
6. profit phase gas transporting material technique according to claim 5, it is characterised in that the sealed reactor inner cylinder
Pressure-resistant 0.3MPa, sealed reactor is controlled using Pneumatic gate valve.
7. profit phase gas transporting material technique according to claim 5, it is characterised in that the pipeline that the technique is used
Using high in the middle and low on both ends by certain slope laying.
8. profit phase gas transporting material technique according to claim 5, it is characterised in that the temperature of the oil phase storage tank
For 80-90 DEG C, the temperature of aqueous phase storage tank is 90-100 DEG C, static emulsifying apparatus X axis vibration frequency 0.9-1.0mm/s, static emulsion
Device Y axis vibration frequency 1.4-1.5mm/s, static emulsifying apparatus Z axis vibration frequency 0.1-0.2mm/s.
9. profit phase gas transporting material technique according to claim 5, it is characterised in that the static emulsifying apparatus passes through
Sensor carry out X axis vibration alarm, Y axis vibration alarm, Z axis vibration alarm, electric current is too high, temperature is too high, cut off the water supply it is comprehensive
Alarm；Oil phase storage tank carries out that flow is too low, too high alarm by sensor, aqueous phase storage tank by sensor progress flow it is too low,
Too high alarm.
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| CN201710169986.9A CN106946634B (en) | 2017-03-21 | 2017-03-21 | A kind of grease phase gas transporting material device and technique |
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| CN106946634B CN106946634B (en) | 2018-11-13 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110681309A (en) * | 2019-09-30 | 2020-01-14 | 浙江工业大学 | Method for preparing emulsion by gas-driven emulsification |
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| CN105566018A (en) * | 2016-03-07 | 2016-05-11 | 湖北帅力化工有限公司 | Environmental-friendly powder emulsion explosive and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US3610088A (en) * | 1968-05-31 | 1971-10-05 | Intermountain Res & Eng | Apparatus and method for mixing and pumping fluid explosive compositions |
| CN1562916A (en) * | 2004-03-22 | 2005-01-12 | 煤炭科学研究总院***技术研究所 | Technical method and equipment for producing emulsion explosive |
| CN101423447A (en) * | 2008-11-15 | 2009-05-06 | 安徽江南化工股份有限公司 | Production process for primary continuous emulsification of powdery emulsifying explosive |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110681309A (en) * | 2019-09-30 | 2020-01-14 | 浙江工业大学 | Method for preparing emulsion by gas-driven emulsification |
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Address after: 323300 Zhuangshan, Suichang County, Lishui City, Zhejiang Province Patentee after: Zhejiang Lihua civil explosive Co.,Ltd. Address before: 323300 Zhuangshan, Suichang County, Lishui City, Zhejiang Province Patentee before: ZHEJIANG LIMIN CHEMICAL INDUSTRY CO.,LTD. |
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Denomination of invention: A material conveying device and process for oil water phase gas Effective date of registration: 20230914 Granted publication date: 20181113 Pledgee: Industrial Commercial Bank of China Ltd. Suichang branch Pledgor: Zhejiang Lihua civil explosive Co.,Ltd. Registration number: Y2023330002034 |