CN106929941A - The fabric that the preparation method and the fiber of stalactite Chinese medicine mineral fibres are prepared - Google Patents

The fabric that the preparation method and the fiber of stalactite Chinese medicine mineral fibres are prepared Download PDF

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Publication number
CN106929941A
CN106929941A CN201511031022.5A CN201511031022A CN106929941A CN 106929941 A CN106929941 A CN 106929941A CN 201511031022 A CN201511031022 A CN 201511031022A CN 106929941 A CN106929941 A CN 106929941A
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CN
China
Prior art keywords
stalactite
chinese medicine
mineral fibres
mentioned
medicine mineral
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201511031022.5A
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Chinese (zh)
Inventor
沈守兵
陈秀苗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Shuixing Home Textile Co Ltd
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Shanghai Shuixing Home Textile Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Shanghai Shuixing Home Textile Co Ltd filed Critical Shanghai Shuixing Home Textile Co Ltd
Priority to CN201511031022.5A priority Critical patent/CN106929941A/en
Publication of CN106929941A publication Critical patent/CN106929941A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/88Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/92Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/08Melt spinning methods
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/253Formation of filaments, threads, or the like with a non-circular cross section; Spinnerette packs therefor
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • D01F1/103Agents inhibiting growth of microorganisms
    • DTEXTILES; PAPER
    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • DTEXTILES; PAPER
    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D03D15/40Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads
    • D03D15/44Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads with specific cross-section or surface shape

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Artificial Filaments (AREA)

Abstract

Select stalactite as raw material the invention discloses the fabric that the preparation method and its fiber of a kind of stalactite Chinese medicine mineral fibres are prepared, including (1), stalactite is worn into fritter, then calcine 20min at 950 DEG C;(2) the stalactite fritter after above-mentioned calcining is ground into 300-600 nanometers of nano-particle;(3) snap frozen and drying are carried out using vacuum freeze drying mode to above-mentioned nano-particle;(4) nano-particle of the following states of moisture 10ppm and polyester resin are pressed 80%:20% is mixed and melt process;(5) mixture after above-mentioned melting is compressed and is cooled down;(6) mixture that will have been cooled down cuts into the granular synthetic resin masterbatch containing stalactite drug substance;(7) polyester granulate of above-mentioned synthetic resin masterbatch and below pellet moisture rate 30ppm is pressed 5%:95% ratio is mixed, and is dried again;(8) after mixture being melted and mixed into 270-290 DEG C by melting compressor, then extrude, stalactite Chinese medicine mineral fibres is obtained.The stalactite Chinese medicine mineral fibres that the present invention is produced has antibacterial, deodorization and far infrared medical health care function.

Description

The fabric that the preparation method and the fiber of stalactite Chinese medicine mineral fibres are prepared
Technical field
The present invention relates to a kind of preparation method of Chinese medicine mineral fibres, the fabric that the preparation method and the fiber of more particularly to a kind of stalactite Chinese medicine mineral fibres are prepared.
Background technology
Recently as people to the relation more and more higher of health, in fiber, clothes and whole field to the care of health and high functionality material also being continuously increased, and correlative study activity is also a lot;Stalactite, first recorded in《Sheng Nong's herbal classic》, also known as stalactite;This product is carbonate mineral calcite race calcite, and its is sweet warm in nature for main calcium carbonate, there is that warm lung is supporing yang, the effect of relieving haperacidity of relievining asthma;Cure mainly deficiency syndrome of the lung heap soil or fertilizer over and around the roots and breathe heavily the diseases such as urgency, waist and knee crymodynia, pantothenic acid of having a stomachache, alactation.
The content of the invention
The technical problem to be solved in the present invention is to provide the fabric that the preparation method and the fiber of a kind of stalactite Chinese medicine mineral fibres are prepared.
To reach above-mentioned purpose, technical scheme is as follows:
A kind of preparation method of stalactite Chinese medicine mineral fibres, it is characterised in that the preparation method includes:
(1) stalactite is worn into fritter as raw material from stalactite, then calcines 20min at 950 DEG C;
(2) the stalactite fritter after above-mentioned calcining is ground into the nano-particle less than 600 nanometers, wherein crushing process is ground with high-precision fine grinder and obtained;
(3) snap frozen and drying are carried out using vacuum freeze drying mode to above-mentioned nano-particle, cooling time is 30min, air drying 5-7 hours;
(4) nano-particle of the following states of moisture 10ppm and polyester resin are pressed 80%:20% carries out helical screw agitator mixing and melt process, and melt temperature is 270-290 DEG C;
(5) mixture after above-mentioned melting is compressed by extruder and horizontal quenching, horizontal blowing temperature is 20-30 DEG C;
(6) mixture that will have been cooled down cuts into graininess, and it is just the synthetic resin masterbatch containing stalactite drug substance;
(7) polyester resin of above-mentioned synthetic resin masterbatch and below pellet moisture rate 30ppm is pressed 5%:95% ratio is mixed, and is dried again;
(8) by melting compressor by after dried mixture is melted and mixed to 270-290 DEG C in step (7), then extrude, stalactite Chinese medicine mineral fibres is obtained.
Preferably, ordinary cross-sectional is changed to odd-shaped cross section by the stalactite Chinese medicine mineral fibres by profile spinneret.
The fabric that a kind of utilization stalactite Chinese medicine mineral fibres is prepared, by screw extruder spinning, the barrel zone temperature of screw extruder is 270-290 DEG C to the stalactite Chinese medicine mineral fibres, and temperature is 260-280 DEG C in heating compartment component;Weaved cotton cloth as organizine and tram from spun silk, required fabric is obtained.
By above-mentioned technical proposal, the beneficial effects of the invention are as follows:
The stalactite Chinese medicine mineral fibres that the present invention is produced has antibacterial, deodorization and far infrared medical health care function;There are the fabric prepared using mammary calculus Chinese medicine mineral fibres 24 hours persistently to suppress the antibacterial functions such as more than 98% pulmonitis strain, staphylococcus in itself;At normal temperatures, without external heat source, releasing far infrared in a natural way (0.82) and (3000/cm, anion3)。
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, the present invention is further elucidated below.
Embodiment 1
The invention discloses a kind of preparation method of stalactite Chinese medicine mineral fibres, the preparation method includes:
(1) stalactite is worn into fritter as raw material from stalactite, then calcines 20min at 950 DEG C;
(2) the stalactite fritter after above-mentioned calcining is ground into the nano-particle less than 600 nanometers, wherein crushing process is ground with high-precision fine grinder and obtained;The effect of drugs of the smaller stalactite of particle diameter is better, will not also block spinneret orifice;
(3) snap frozen and drying are carried out using vacuum freeze drying mode to above-mentioned nano-particle, cooling time is 30min, air drying 5 hours;Moisture in removal particle, in order to avoid the quality of influence spinning;
(4) nano-particle of the following states of moisture 10ppm and polyester resin are pressed 80%:20% carries out helical screw agitator mixing and melt process, and melt temperature is 270 DEG C;
(5) mixture after above-mentioned melting is compressed by extruder and horizontal quenching, horizontal blowing temperature is 20 DEG C;
(6) mixture that will have been cooled down cuts into graininess, and it is just the synthetic resin masterbatch containing stalactite drug substance;
(7) polyester resin of above-mentioned synthetic resin masterbatch and below pellet moisture rate 30ppm is pressed 5%:95% ratio is mixed, and is dried again;
(8) by melting compressor by after dried mixture is melted and mixed to 270 DEG C in step (7), then extrude, stalactite Chinese medicine mineral fibres is obtained.
Ordinary cross-sectional is changed to odd-shaped cross section by the stalactite Chinese medicine mineral fibres that the present invention will be prepared by profile spinneret, has done three-dimensional crimp treatment and organosilicon treatment, increases its bulkiness and feel.
The method that stalactite Chinese medicine mineral fibres of the present invention prepares fabric is as follows, and by stalactite Chinese medicine mineral fibres by screw extruder spinning, the barrel zone temperature of screw extruder is 270 DEG C, and temperature is 260 DEG C in heating compartment component;Weaved cotton cloth as organizine and tram from spun silk, required fabric is obtained.
Embodiment 2
The invention discloses a kind of preparation method of stalactite Chinese medicine mineral fibres, the preparation method includes:
(1) stalactite is worn into fritter as raw material from stalactite, then calcines 20min at 950 DEG C;
(2) the stalactite fritter after above-mentioned calcining is ground into the nano-particle less than 600 nanometers, wherein crushing process is ground with high-precision fine grinder and obtained;The effect of drugs of the smaller stalactite of particle diameter is better, will not also block spinneret orifice;
(3) snap frozen and drying are carried out using vacuum freeze drying mode to above-mentioned nano-particle, cooling time is 30min, air drying 7 hours;Moisture in removal particle, in order to avoid the quality of influence spinning;
(4) nano-particle of the following states of moisture 10ppm and polyester resin are pressed 80%:20% carries out helical screw agitator mixing and melt process, and melt temperature is 290 DEG C;
(5) mixture after above-mentioned melting is compressed by extruder and horizontal quenching, horizontal blowing temperature is 30 DEG C;
(6) mixture that will have been cooled down cuts into graininess, and it is just the synthetic resin masterbatch containing stalactite drug substance;
(7) polyester resin of above-mentioned synthetic resin masterbatch and below pellet moisture rate 30ppm is pressed 5%:95% ratio is mixed, and is dried again;
(8) by melting compressor by after dried mixture is melted and mixed to 290 DEG C in step (7), then extrude, stalactite Chinese medicine mineral fibres is obtained.
Ordinary cross-sectional is changed to odd-shaped cross section by the stalactite Chinese medicine mineral fibres that the present invention will be prepared by profile spinneret, has done three-dimensional crimp treatment and organosilicon treatment, increases its bulkiness and feel.
The method that stalactite Chinese medicine mineral fibres of the present invention prepares fabric is as follows, and by stalactite Chinese medicine mineral fibres by screw extruder spinning, the barrel zone temperature of screw extruder is 290 DEG C, and temperature is 280 DEG C in heating compartment component;Weaved cotton cloth as organizine and tram from spun silk, required fabric is obtained.
There are the above-mentioned fabric prepared 24 hours persistently to suppress the antibacterial functions such as more than 98% pulmonitis strain, staphylococcus;With the deodorization function such as formaldehyde, ammonia of removal more than 95% in 2 hours;At normal temperatures, without external heat source, releasing far infrared in a natural way (0.82) and (3000/cm, anion3)。
General principle of the invention and principal character and advantages of the present invention has been shown and described above.It should be understood by those skilled in the art that; the present invention is not limited to the above embodiments; merely illustrating the principles of the invention described in above-described embodiment and specification; without departing from the spirit and scope of the present invention; various changes and modifications of the present invention are possible, and these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appending claims and its equivalent thereof.

Claims (3)

1. the preparation method of stalactite Chinese medicine mineral fibres, it is characterised in that the preparation method includes:
(1) stalactite is worn into fritter as raw material from stalactite, then calcines 20min at 950 DEG C;
(2) the stalactite fritter after above-mentioned calcining is ground into the nano-particle less than 600 nanometers, wherein Crushing process is ground with high-precision fine grinder and obtained;
(3) snap frozen and drying are carried out using vacuum freeze drying mode to above-mentioned nano-particle, is freezed Time is 30min, air drying 5-7 hours;
(4) nano-particle of the following states of moisture 10ppm and polyester resin are pressed 80%:20% carries out screw rod Stirring mixing and melt process, melt temperature are 270-290 DEG C;
(5) mixture after above-mentioned melting is compressed by extruder and horizontal quenching, horizontal blowing Temperature is 20-30 DEG C;
(6) mixture that will have been cooled down cuts into graininess, and it is just the conjunction containing stalactite drug substance Resin masterbatch;
(7) polyester resin of above-mentioned synthetic resin masterbatch and below pellet moisture rate 30ppm is pressed 5%:95% Ratio is mixed, and is dried again;
(8) dried mixture in step (7) is melted and mixed to 270-290 DEG C by melting compressor Afterwards, then extrude, stalactite Chinese medicine mineral fibres is obtained.
2. the preparation method of stalactite Chinese medicine mineral fibres according to claim 1, it is characterised in that Ordinary cross-sectional is changed to odd-shaped cross section by the stalactite Chinese medicine mineral fibres by profile spinneret.
3. the fabric that the stalactite Chinese medicine mineral fibres in a kind of utilization claim 1 is prepared, its feature It is that the stalactite Chinese medicine mineral fibres is by screw extruder spinning, the barrel zone temperature of screw extruder It it is 270-290 DEG C, temperature is 260-280 DEG C in heating compartment component;From spun silk as organizine and Tram is weaved cotton cloth, and required fabric is obtained.
CN201511031022.5A 2015-12-31 2015-12-31 The fabric that the preparation method and the fiber of stalactite Chinese medicine mineral fibres are prepared Pending CN106929941A (en)

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Application Number Priority Date Filing Date Title
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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1197857A (en) * 1997-04-02 1998-11-04 石美秀 Loess-containing fiber and its manufacturing method
CN1537652A (en) * 2003-10-14 2004-10-20 李元亮 Health-care stomach pocket with gold and Chinese medicine and its manufacturing method
CN101896539A (en) * 2007-12-13 2010-11-24 埃西勒国际通用光学公司 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles
CN102406244A (en) * 2011-09-02 2012-04-11 成钢 Weight-reducing body-scenting wrinkle-preventing whitening multifunctional body-building nano element fabric underwear for females
CN102433598A (en) * 2011-09-01 2012-05-02 成钢 Nano-element life prolonging fiber fabric garment able to prolong cell gene breeding cycle
CN103451973A (en) * 2013-09-03 2013-12-18 上海波顺服饰有限公司 Far infrared fabric and preparation method thereof as well as healthcare shoulder pad made of far infrared fabric

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1197857A (en) * 1997-04-02 1998-11-04 石美秀 Loess-containing fiber and its manufacturing method
CN1537652A (en) * 2003-10-14 2004-10-20 李元亮 Health-care stomach pocket with gold and Chinese medicine and its manufacturing method
CN101896539A (en) * 2007-12-13 2010-11-24 埃西勒国际通用光学公司 Method of preparing a transparent polymer material comprising a thermoplastic polycarbonate and mineral nanoparticles
CN102433598A (en) * 2011-09-01 2012-05-02 成钢 Nano-element life prolonging fiber fabric garment able to prolong cell gene breeding cycle
CN102406244A (en) * 2011-09-02 2012-04-11 成钢 Weight-reducing body-scenting wrinkle-preventing whitening multifunctional body-building nano element fabric underwear for females
CN103451973A (en) * 2013-09-03 2013-12-18 上海波顺服饰有限公司 Far infrared fabric and preparation method thereof as well as healthcare shoulder pad made of far infrared fabric

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
叶静: "PET/纳米矿物粒子纤维的结构与性能", 《纺织学报》 *
陈革 等: "《纺织机械概论》", 31 May 2011 *
高天爱 等: "《矿物药真伪图鉴及应用》", 28 February 2014 *

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Application publication date: 20170707