CN106929194A - Liquid detergent and preparation method thereof - Google Patents
Liquid detergent and preparation method thereof Download PDFInfo
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- CN106929194A CN106929194A CN201710097507.7A CN201710097507A CN106929194A CN 106929194 A CN106929194 A CN 106929194A CN 201710097507 A CN201710097507 A CN 201710097507A CN 106929194 A CN106929194 A CN 106929194A
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- China
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- parts
- liquid detergent
- bacteriostatic agent
- factor
- quercetin
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- 239000003599 detergent Substances 0.000 title claims abstract description 34
- 239000007788 liquid Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000022 bacteriostatic agent Substances 0.000 claims abstract description 14
- -1 sodium olefin sulfonates Chemical class 0.000 claims abstract description 11
- 239000011734 sodium Substances 0.000 claims abstract description 9
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 9
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 8
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 8
- 235000011187 glycerol Nutrition 0.000 claims abstract description 8
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 8
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 claims description 29
- 150000001408 amides Chemical class 0.000 claims description 18
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 14
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 claims description 14
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 claims description 14
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 14
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 claims description 14
- 229960001285 quercetin Drugs 0.000 claims description 14
- 235000005875 quercetin Nutrition 0.000 claims description 14
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims description 14
- 229930182490 saponin Natural products 0.000 claims description 14
- 150000007949 saponins Chemical class 0.000 claims description 14
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 claims description 13
- 235000021360 Myristic acid Nutrition 0.000 claims description 13
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 13
- 239000004378 Glycyrrhizin Substances 0.000 claims description 12
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 claims description 12
- 229960004949 glycyrrhizic acid Drugs 0.000 claims description 12
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 claims description 12
- 235000019410 glycyrrhizin Nutrition 0.000 claims description 12
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 12
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 11
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 11
- 239000000194 fatty acid Substances 0.000 claims description 11
- 229930195729 fatty acid Natural products 0.000 claims description 11
- 150000004665 fatty acids Chemical class 0.000 claims description 11
- 244000060011 Cocos nucifera Species 0.000 claims description 10
- 235000017709 saponins Nutrition 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 5
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000004744 fabric Substances 0.000 abstract description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 2
- 150000002012 dioxanes Chemical class 0.000 abstract description 2
- 239000006081 fluorescent whitening agent Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- 239000011574 phosphorus Substances 0.000 abstract description 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 2
- 238000013329 compounding Methods 0.000 description 8
- 230000001408 fungistatic effect Effects 0.000 description 4
- 235000019864 coconut oil Nutrition 0.000 description 3
- 239000003240 coconut oil Substances 0.000 description 3
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000011895 specific detection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000737241 Cocos Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 239000002068 microbial inoculum Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2096—Heterocyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of liquid detergent and preparation method thereof, the liquid detergent is prepared from by following raw materials：5 15 parts of glycerine, stain is gone easily to float 15 25 parts of the factor, 15 parts of α sodium olefin sulfonates, 15 parts of hydroxyethyl cellulose, 0.02 0.2 parts of bacteriostatic agent, 0.2 2 parts of EDETATE SODIUM, 65 75 parts of water.Liquid detergent of the present invention, the primary raw material used in formula is degradable raw material, can be biodegradable, environmental protection；Without materials such as fluorescent whitening agent, phosphorus, dioxanes, nonyl/octyl phenol and nonyl/OPEOs；Bright property, smoothness, pliability and the elasticity of fabric can be improved, excitant is low, dirt-removing power is strong, easily rinsing.It is suitable for the washing of infantile clothes.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, and in particular to a kind of liquid detergent and preparation method thereof.
Background technology
Liquid detergent is that occur and develop a kind of rapid personal clothing cleaning product, compared with washing powder, liquid detergent in recent years
There is soluble, low energy consumption, high active content, be following developing direction of cloth-detergent.But it is usually spaced apart by making
With liquid detergent and softener, i.e., first washed with liquid detergent, then added softener in rinse stage, in-convenience in use, increase
People have been added to wash the triviality of shield fabric.
Liquid detergent is just increasingly liked as the new lover in articles for washing market by consumer.Washing in the market
Clothing liquid is formed by chemical substance allotment mostly, for a long time using that can produce injury to skin, is also unfavorable for environmental protection.
The content of the invention
For above shortcomings in the prior art, one of technical problems to be solved by the invention are to provide one kind and wash
Clothing liquid.
The two of the technical problem of solution of the invention are to provide a kind of preparation method of liquid detergent.
The present invention seeks to what is be achieved through the following technical solutions：
A kind of liquid detergent, is prepared from by the raw material of following weight parts：
Glycerine 5-15 parts, go stain easily float factor 15-25 parts, α-sodium olefin sulfonate 1-5 parts, hydroxyethyl cellulose 1-5 parts, suppression
Microbial inoculum 0.02-0.2 parts, EDETATE SODIUM 0.2-2 parts, water 65-75 parts.
Preferably, described stain of going easily floats the factor for Dodecyl Polyglucosides, myristic acid diglycollic amide, coconut grease
One or more of mixture in fat acid diglycollic amide.
It is highly preferred that described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, coconut oil
Fatty diglycollic amide is mixed, the Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two
The mass ratio of glycollic amide is (1-3)：(1-3)：(1-3).
Preferably, described bacteriostatic agent is one or more in Tea Saponin, glycyrrhizin, Quercetin of mixture.
It is highly preferred that described bacteriostatic agent is mixed by Tea Saponin, glycyrrhizin, Quercetin, the Tea Saponin, Radix Glycyrrhizae
Element, the mass ratio of Quercetin are (1-3)：(1-3)：(1-3).
Present invention also offers the preparation method of above-mentioned liquid detergent, comprise the following steps：
Heat water to and sequentially add glycerine under 65-85 DEG C, stirring condition, go stain easily to float the factor to be uniformly mixed, drop
Temperature sequentially adds bacteriostatic agent, α-sodium olefin sulfonate, hydroxyethyl cellulose, EDETATE SODIUM and is uniformly mixed i.e. to 45-55 DEG C
.
Specifically, in the present invention：
Tea Saponin, No. CAS：8047-15-2.
Glycyrrhizin, No. CAS：578-86-9.
Quercetin, No. CAS：117-39-5.
Dodecyl Polyglucosides, No. CAS：110615-47-9.
Myristic acid diglycollic amide, No. CAS：7545-23-5.
Cocoanut fatty acid diethanolamide, No. CAS：68603-42-9.
EDETATE SODIUM, i.e. disodium ethylene diamine tetraacetate, No. CAS：139-33-3.
Glycerine, No. CAS：56-81-5.
α-sodium olefin sulfonate, No. CAS：68439-57-6, the α-alkenyl sulphur provided using Sinolight Chemical Co., Ltd.
Sour sodium (powder).
Hydroxyethyl cellulose, No. CAS：9004-62-0, the specific food provided using Anhui Ju De bio tech ltd
Grade hydroxyethyl cellulose.
Liquid detergent of the present invention, the primary raw material used in formula is degradable raw material, can be biodegradable, environmental protection；
Without materials such as fluorescent whitening agent, phosphorus, dioxanes, nonyl/octyl phenol and nonyl/OPEOs；Fabric can be improved
Bright property, smoothness, pliability and elasticity, excitant are low, and dirt-removing power is strong, easily rinsing.It is suitable for infantile clothes
Washing.
Specific embodiment
With reference to embodiment, the present invention is described further, as described below, is only to preferable implementation of the invention
Example, not does the limitation of other forms to the present invention, and any those skilled in the art are possibly also with the disclosure above
Technology contents be changed to the Equivalent embodiments of equal change.It is every without departing from the present invention program content, according to the present invention
Technical spirit any simple modification that following examples are made or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Liquid detergent raw material (weight portion)：10 parts of glycerine, to go stain easily to float 18 parts of the factor, 3 parts of α-sodium olefin sulfonate, ethoxy fine
3 parts of dimension element, 0.03 part of bacteriostatic agent, 0.25 part of EDETATE SODIUM, 70 parts of water.
Described stain of going easily floats the factor by Dodecyl Polyglucosides, myristic acid diglycollic amide, coco-nut oil fatty acid two
Glycollic amide is 1 in mass ratio：1：1 is uniformly mixed and obtains.
Described bacteriostatic agent is 1 by Tea Saponin, glycyrrhizin, Quercetin in mass ratio：1：1 is uniformly mixed and obtains.
The preparation method of above-mentioned liquid detergent, comprises the following steps：
75 DEG C are heated water to, glycerine is sequentially added under 500 revs/min of stirring conditions, is gone stain easily to float factor stirring 10 minutes
It is well mixed, 48 DEG C are cooled to, sequentially add bacteriostatic agent, α-sodium olefin sulfonate, hydroxyethyl cellulose, EDETATE SODIUM and continue to stir
Mix 20 minutes and be well mixed.Obtain the liquid detergent of embodiment 1.
Embodiment 2
It is substantially the same manner as Example 1, differ only in：Described bacteriostatic agent is in mass ratio by glycyrrhizin, Quercetin
1：1 is uniformly mixed and obtains.Obtain the liquid detergent of embodiment 2.
Embodiment 3
It is substantially the same manner as Example 1, differ only in：Described bacteriostatic agent is in mass ratio by Tea Saponin, Quercetin
1：1 is uniformly mixed and obtains.Obtain the liquid detergent of embodiment 3.
Embodiment 4
It is substantially the same manner as Example 1, differ only in：Described bacteriostatic agent is in mass ratio by Tea Saponin, glycyrrhizin
1：1 is uniformly mixed and obtains.Obtain the liquid detergent of embodiment 4.
Embodiment 5
It is substantially the same manner as Example 1, differ only in：Described stain of going easily floats the factor by myristic acid diethanol acyl
Amine, cocoanut fatty acid diethanolamide are 1 in mass ratio：1 is uniformly mixed and obtains.Obtain the liquid detergent of embodiment 5.
Embodiment 6
It is substantially the same manner as Example 1, differ only in：Described stain of going easily floats the factor by Dodecyl Polyglucosides, coconut palm
Seed oil fatty diglycollic amide is 1 in mass ratio：1 is uniformly mixed and obtains.Obtain the liquid detergent of embodiment 6.
Embodiment 7
It is substantially the same manner as Example 1, differ only in：Described stain of going easily floats the factor by Dodecyl Polyglucosides, meat
Myristic acid diglycollic amide is 1 in mass ratio：1 is uniformly mixed and obtains.Obtain the liquid detergent of embodiment 7.
Test case 1
According to professional standard QB/T 2850-2007 antibacterial bacteriostatic type detergent, fungistatic effect test, activity are carried out
1wt% is, action time is 20 minutes, and specific detection data refers to table 1.
Table 1：Hand cleanser fungistatic effect tests table
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (Tea Saponin, glycyrrhizin, Quercetin compounding) fungistatic effect are obvious
Better than embodiment 2-4 (any the two compounding in Tea Saponin, glycyrrhizin, Quercetin)；Comparing embodiment 1 and embodiment 5-7, implement
Example 1 (Dodecyl Polyglucosides, myristic acid diglycollic amide, cocoanut fatty acid diethanolamide compounding) fungistatic effect is obvious
It is (any in Dodecyl Polyglucosides, myristic acid diglycollic amide, cocoanut fatty acid diethanolamide better than embodiment 5-7
The two compounding).
Test case 2
According to the method that QB/T 1224-2007 specify, the detergency of liquid detergent obtained in detection embodiment of the present invention 1-7.
Standard flour solution concentration is 0.2wt%, and liquid detergent solution concentration to be measured is 0.3wt%, hard with 250mg/kg respectively
Water is prepared, the method and soiled cotton specified using QB/T 13174-2008, and the decontamination of laundry fluid samples and standard flour is determined with machine
Power.
Specific detection data, refers to table 2.
Table 2：Detergency test result table
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (Tea Saponin, glycyrrhizin, Quercetin compounding) detergency are substantially excellent
In embodiment 2-4 (any the two compounding in Tea Saponin, glycyrrhizin, Quercetin)；Comparing embodiment 1 and embodiment 5-7, embodiment
1 (Dodecyl Polyglucosides, myristic acid diglycollic amide, cocoanut fatty acid diethanolamide compounding) detergency is substantially better than
Embodiment 5-7 is (both any in Dodecyl Polyglucosides, myristic acid diglycollic amide, cocoanut fatty acid diethanolamide
Compounding).
Claims (6)
1. a kind of liquid detergent, it is characterised in that be prepared from by the raw material of following weight parts：Glycerine 5-15 parts, go stain easily float because
Sub- 15-25 parts, α-sodium olefin sulfonate 1-5 parts, hydroxyethyl cellulose 1-5 parts, bacteriostatic agent 0.02-0.2 parts, EDETATE SODIUM 0.2-2
Part, water 65-75 parts.
2. liquid detergent as claimed in claim 1, it is characterised in that：It is described go stain easily float the factor for Dodecyl Polyglucosides,
One or more of mixture in myristic acid diglycollic amide, cocoanut fatty acid diethanolamide.
3. liquid detergent as claimed in claim 2, it is characterised in that：It is described go stain easily float the factor by Dodecyl Polyglucosides,
Myristic acid diglycollic amide, cocoanut fatty acid diethanolamide are mixed, the Dodecyl Polyglucosides, myristic acid
Diglycollic amide, the mass ratio of cocoanut fatty acid diethanolamide are (1-3)：(1-3)：(1-3).
4. the liquid detergent as any one of claim 1-3, it is characterised in that：Described bacteriostatic agent is Tea Saponin, Radix Glycyrrhizae
One or more of mixture in element, Quercetin.
5. liquid detergent as claimed in claim 4, it is characterised in that：Described bacteriostatic agent is mixed by Tea Saponin, glycyrrhizin, Quercetin
Conjunction is formed, and the Tea Saponin, glycyrrhizin, the mass ratio of Quercetin are (1-3)：(1-3)：(1-3).
6. the preparation method of the liquid detergent as any one of claim 1-5, it is characterised in that comprise the following steps：
Heat water to and sequentially add glycerine under 65-85 DEG C, stirring condition, go stain easily to float the factor to be uniformly mixed, be cooled to
45-55 DEG C, sequentially add bacteriostatic agent, α-sodium olefin sulfonate, hydroxyethyl cellulose, EDETATE SODIUM and be uniformly mixed and obtain final product.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710097507.7A CN106929194A (en) | 2017-02-22 | 2017-02-22 | Liquid detergent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710097507.7A CN106929194A (en) | 2017-02-22 | 2017-02-22 | Liquid detergent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN106929194A true CN106929194A (en) | 2017-07-07 |
Family
ID=59423734
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710097507.7A Withdrawn CN106929194A (en) | 2017-02-22 | 2017-02-22 | Liquid detergent and preparation method thereof |
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| Country | Link |
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| CN (1) | CN106929194A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108070461A (en) * | 2018-01-25 | 2018-05-25 | 陈昭 | Highly effective plaque-removing washing powder and preparation method thereof |
| CN112080354A (en) * | 2020-09-26 | 2020-12-15 | 福建省梦娇兰日用化学品有限公司 | Baby laundry detergent containing silver ion bacteriostatic agent and preparation method thereof |
| CN114410392A (en) * | 2022-02-14 | 2022-04-29 | 福建省梦娇兰日用化学品有限公司 | Antibacterial laundry detergent and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104419543A (en) * | 2013-08-21 | 2015-03-18 | 左华炜 | Laundry detergent |
| CN105623903A (en) * | 2016-01-20 | 2016-06-01 | 惠州市明荃化妆品有限公司 | High-dirt-removing-power antibacterial protective laundry detergent and preparation method thereof |
| CN106244352A (en) * | 2016-08-11 | 2016-12-21 | 李金新 | Antibacterial low foam laundry liquid and preparation method thereof |
-
2017
- 2017-02-22 CN CN201710097507.7A patent/CN106929194A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104419543A (en) * | 2013-08-21 | 2015-03-18 | 左华炜 | Laundry detergent |
| CN105623903A (en) * | 2016-01-20 | 2016-06-01 | 惠州市明荃化妆品有限公司 | High-dirt-removing-power antibacterial protective laundry detergent and preparation method thereof |
| CN106244352A (en) * | 2016-08-11 | 2016-12-21 | 李金新 | Antibacterial low foam laundry liquid and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 梁月荣: "《茶资源综合利用》", 30 November 2013, 浙江大学出版社 * |
| 梅全喜: "《香药 沉香》", 31 July 2016, 中国中医药出版社 * |
| 陈长勋等: "《中药药理学 第2版》", 31 January 2015, 上海科学技术出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108070461A (en) * | 2018-01-25 | 2018-05-25 | 陈昭 | Highly effective plaque-removing washing powder and preparation method thereof |
| CN112080354A (en) * | 2020-09-26 | 2020-12-15 | 福建省梦娇兰日用化学品有限公司 | Baby laundry detergent containing silver ion bacteriostatic agent and preparation method thereof |
| CN114410392A (en) * | 2022-02-14 | 2022-04-29 | 福建省梦娇兰日用化学品有限公司 | Antibacterial laundry detergent and preparation method thereof |
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Application publication date: 20170707 |