CN107057876A - A kind of solidifying pearl of antibacterial laundry and preparation method thereof - Google Patents
A kind of solidifying pearl of antibacterial laundry and preparation method thereof Download PDFInfo
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- CN107057876A CN107057876A CN201710244688.1A CN201710244688A CN107057876A CN 107057876 A CN107057876 A CN 107057876A CN 201710244688 A CN201710244688 A CN 201710244688A CN 107057876 A CN107057876 A CN 107057876A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
- C11D3/323—Amides; Substituted amides urea or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses the solidifying pearl of the antibacterial laundry of one kind, it includes AEO, C10 isomeric alcohol polyethenoxy ethers, the AEOs of C12 14, the alkyl glucosides of C8 16, laureth sodium sulfovinate, acetic acid chlorhexidine, parachlorometaxylenol, glycerine, alkali protease, pigment, preservative, essence, cellulase.The invention also discloses a kind of preparation method of the antibacterial solidifying pearl of laundry.The solidifying pearl of antibacterial laundry of the present invention, is a kind of concentration liquid detergent of Low-foam and easily cleaning with stronger dirt-removing power and fungistatic effect.
Description
Technical field
The invention belongs to daily use chemicals technical field, and in particular to a kind of antibacterial solidifying pearl of laundry and preparation method thereof.
Background technology
Laundry clothes, the most flat thing in life.For in the product of clothes washing, washing powder, soap, liquid detergent
Main status is accounted for always.Traditional washing powder, soap uses anionic surfactant, is with sodium sulfonate and hard
It is relatively strong (washing powder PH is generally higher than 12) with the product alkalescence that this kind of raw material is produced based on resin acid sodium, carcinogen is remained, and then
Stimulation and injury when in use to skin is larger.
The solidifying pearl of laundry is a kind of water-soluble PVA water soluble films parcel Superconcentrated washing liquid, is designed exclusively for machine washing, operation
Simply, convenient not dirty hand, the solidifying pearl of a laundry can wash a clothes, and what sales volume was huge in the market is that Procter ＆ Gamble releases
The solidifying pearl of green wave laundry, as a main washing product for emphasizing detergency, its fungistatic effect need to be improved.
The content of the invention
In order to overcome the deficiencies in the prior art, it is an object of the invention to provide the solidifying pearl of the antibacterial laundry of one kind, with stronger
Dirt-removing power and fungistatic effect, be a kind of concentration liquid detergent of Low-foam and easily cleaning.
Another object of the present invention is to provide a kind of preparation method of the solidifying pearl of antibacterial laundry.
To solve the above problems, the technical solution adopted in the present invention is as follows：
A kind of solidifying pearl of antibacterial laundry, it includes the following components being calculated in mass percent：
AEO 22.0%-25.0%
C10- isomeric alcohol polyethenoxy ethers 35.0%-42.0%,
C12-14 AEOs 25.0%-28.0%,
C8-16 alkyl glucosides 3.0%-5.0%,
Laureth sodium sulfovinate 8.0%-10.0%,
Acetic acid chlorhexidine 0.2%-0.3%,
Parachlorometaxylenol 0.2%-0.3%,
Glycerine 1.0%-3.0%,
Alkali protease 0.1%-0.3%,
Cellulase 0.05%-0.2%,
Preservative 0.1%-0.2%,
Essence 1.0%-2.0%,
Pigment 0.01%-0.02%；
The mass percent sum of above component is 100%.
A kind of preparation method of the solidifying pearl of antibacterial laundry, the preparation method comprises the following steps：
1) in advance will emulsification pot, pipeline, storage tank, the sterilization of weighing vessel cleaning.
2) AEO, C8-16 alkyl glucosides, laureth sulfuric ester are weighed respectively according to formula ratio
Sodium, C12-14 AEOs add in emulsification pot moderate-speed mixer to transparency liquid；
3) C10- isomeric alcohol polyethenoxy ethers, acetic acid chlorhexidine, parachlorometaxylenol are weighed prewired according to formula ratio
It is well mixed in pot and is heated to transparency liquid, is pumped into emulsification pot moderate-speed mixer to transparency liquid；
4) weigh glycerine, alkali protease, cellulase respectively according to formula ratio to add in emulsification pot, stirring at low speed is to transparent
Liquid；
5) preservative, essence, pigment are weighed respectively according to formula ratio and adds in emulsification pot stirring at low speed to transparency liquid；
6) physical and chemical index examines qualified filtering and discharging；
7) it is filling after standing 24 hours.
Be used as further scheme, step 2 of the present invention) described in moderate-speed mixer speed for 80-120 turn/min, stirring
Time is 25min.
Be used as further scheme, step 3 of the present invention) described in moderate-speed mixer speed for 80-120 turn/min, during stirring
Between be 30min.
It is used as further scheme, step 3 of the present invention) in, heating-up temperature is 70-80 DEG C.
Be used as further scheme, step 4 of the present invention) in stirring at low speed speed for 30-60 turn/min, stirring
Time is 30min.
Be used as further scheme, step 5 of the present invention) in stirring at low speed speed for 30-60 turn/min, stirring
Time is 15 minutes.
Compared with prior art, the beneficial effects of the present invention are：
1. the solidifying pearl of antibacterial laundry of the present invention has stronger dirt-removing power and fungistatic effect；
2. it with the addition of C10- isomeric alcohol polyethenoxy ethers in the formula of the solidifying pearl of antibacterial laundry of the present invention and C10- be different
Two kinds of alcohol ethers of structure alcohol APEO, are that pearl is coagulated in a kind of laundry of Low-foam and easily cleaning with good dispersion effect.
The present invention is described in further detail with reference to embodiment.
Embodiment
A kind of solidifying pearl of antibacterial laundry, it includes the following components being calculated in mass percent：
AEO 22.0%-25.0%
C10- isomeric alcohol polyethenoxy ethers 35.0%-42.0%,
C12-14 AEOs 25.0%-28.0%,
C8-16 alkyl glucosides 3.0%-5.0%,
Laureth sodium sulfovinate 8.0%-10.0%,
Acetic acid chlorhexidine 0.2%-0.3%,
Parachlorometaxylenol 0.2%-0.3%,
Glycerine 1.0%-3.0%,
Alkali protease 0.1%-0.3%,
Cellulase 0.05%-0.2%,
Preservative 0.1%-0.2%,
Essence 1.0%-2.0%,
Pigment 0.01%-0.02%；
The mass percent sum of above component is 100%.
In the solidifying pearl formula of laundry of the present invention, C10- isomeric alcohol polyethenoxy ethers and C12-14 AEOs
Two kinds of isomery alcohol ethers, have that pour point is low, dissolution velocity is fast due to isomery alcohol ether, good interval narrow, the low bubble property of gel, easy rinsing and
The advantages of strong detergency；By adding both isomery alcohol ethers, the obtained solidifying pearl of laundry has the advantages that Low-foam and easily cleaning.In addition
Then the peptide bond that protein can be first resolved into solubility by adding neutral proteinase is further decomposed into amino acid, so that albumen
Matter dirt and the other dirts being bonded at by protein on clothing are easy to be removed by surfactant, realize superstrong pollution-removing.
A kind of preparation method of the solidifying pearl of antibacterial laundry, the preparation method comprises the following steps：
1) in advance will emulsification pot, pipeline, storage tank, the sterilization of weighing vessel cleaning.
2) AEO, C8-16 alkyl glucosides, laureth sulfuric ester are weighed respectively according to formula ratio
Sodium, C12-14 AEOs add in emulsification pot moderate-speed mixer to transparency liquid；
3) C10- isomeric alcohol polyethenoxy ethers, acetic acid chlorhexidine, parachlorometaxylenol are weighed prewired according to formula ratio
It is well mixed in pot and is heated to transparency liquid, is pumped into emulsification pot moderate-speed mixer to transparency liquid；
4) weigh glycerine, alkali protease, cellulase respectively according to formula ratio to add in emulsification pot, stirring at low speed is to transparent
Liquid；
5) preservative, essence, pigment are weighed respectively according to formula ratio and adds in emulsification pot stirring at low speed to transparency liquid；
6) physical and chemical index examines qualified filtering and discharging；
7) it is filling after standing 24 hours.
Be used as further scheme, step 2 of the present invention) described in moderate-speed mixer speed for 80-120 turn/min, stirring
Time is 25min.
Be used as further scheme, step 3 of the present invention) described in moderate-speed mixer speed for 80-120 turn/min, during stirring
Between be 30min.
It is used as further scheme, step 3 of the present invention) in, heating-up temperature is 70-80 DEG C.
Be used as further scheme, step 4 of the present invention) in stirring at low speed speed for 30-60 turn/min, stirring
Time is 30min.
Be used as further scheme, step 5 of the present invention) in stirring at low speed speed for 30-60 turn/min, stirring
Time is 15 minutes.
The following is specific embodiment of the present invention, the raw material used in the following embodiments, equipment can pass through purchase
Buyer's formula is obtained.
Embodiment 1
A kind of solidifying pearl of antibacterial laundry, it includes the following components being calculated in mass percent：
AEO 22.0%%
C10- isomeric alcohol polyethenoxy ethers 39.4%,
C12-14 AEOs 25.49%,
C8-16 alkyl glucosides 3.0%,
Laureth sodium sulfovinate 8.0%,
Acetic acid chlorhexidine 0.2%,
Parachlorometaxylenol 0.3%,
Glycerine 1.0%,
Alkali protease 0.1%,
Cellulase 0.2%,
Preservative 0.2%,
Essence 1.0%,
Pigment 0.01%；
The mass percent sum of above component is 100%.
The solidifying pearl of the laundry, which is prepared by the following method, to be formed：
1) in advance will emulsification pot, pipeline, storage tank, the sterilization of weighing vessel cleaning.
2) AEO, C8-16 alkyl glucosides, laureth sulfuric ester are weighed respectively according to formula ratio
Sodium, C12-14 AEOs add emulsification pot and stir 25min to transparency liquid with 80 turns/min rotating speed；
3) C10- isomeric alcohol polyethenoxy ethers, acetic acid chlorhexidine, parachlorometaxylenol are weighed prewired according to formula ratio
70-80 DEG C of heating is well mixed in pot to transparency liquid, is pumped into emulsification pot and 30min is stirred to transparent with 80 turns/min rotating speed
Liquid；
4) weigh glycerine, alkali protease, cellulase respectively according to formula ratio to add in emulsification pot, with turning for 30 turns/min
Speed stirs 30 minutes to transparency liquid；
5) preservative, essence, pigment is weighed respectively according to formula ratio to add in emulsification pot with 30 turns/min rotating speed stirring
15 minutes to transparency liquid；
6) physical and chemical index examines qualified filtering and discharging；
7) it is filling after standing 24 hours.
Embodiment 2
A kind of solidifying pearl of antibacterial laundry, it includes the following components being calculated in mass percent：
AEO 22.5%
C10- isomeric alcohol polyethenoxy ethers 35.33%,
C12-14 AEOs 25.0%,
C8-16 alkyl glucosides 3.0%,
Laureth sodium sulfovinate 8.0%,
Acetic acid chlorhexidine 0.3%,
Parachlorometaxylenol 0.2%,
Glycerine 3.0%,
Alkali protease 0.1%,
Cellulase 0.05%,
Preservative 0.1%,
Essence 2.0%,
Pigment 0.02%；
The mass percent sum of above component is 100%.
The solidifying pearl of the laundry, which is prepared by the following method, to be formed：
1) in advance will emulsification pot, pipeline, storage tank, the sterilization of weighing vessel cleaning.
2) AEO, C8-16 alkyl glucosides, laureth sulfuric ester are weighed respectively according to formula ratio
Sodium, C12-14 AEOs add emulsification pot and stir 25min to transparency liquid with 100 turns/min rotating speed；
3) C10- isomeric alcohol polyethenoxy ethers, acetic acid chlorhexidine, parachlorometaxylenol are weighed prewired according to formula ratio
75 DEG C of heating is well mixed in pot to transparency liquid, is pumped into emulsification pot and 30min is stirred to transparent liquid with 100 turns/min rotating speed
Body；
4) weigh glycerine, alkali protease, cellulase respectively according to formula ratio to add in emulsification pot, with turning for 45 turns/min
Speed stirs 30 minutes to transparency liquid；
5) preservative, essence, pigment is weighed respectively according to formula ratio to add in emulsification pot with 50 turns/min rotating speed stirring
15 minutes to transparency liquid；
6) physical and chemical index examines qualified filtering and discharging；
7) it is filling after standing 24 hours.
Embodiment 3
A kind of solidifying pearl of antibacterial laundry, it includes the following components being calculated in mass percent：
AEO 22.0%
C10- isomeric alcohol polyethenoxy ethers 36.78%,
C12-14 AEOs 25.5%,
C8-16 alkyl glucosides 3.0%,
Laureth sodium sulfovinate 10.0%,
Acetic acid chlorhexidine 0.2%,
Parachlorometaxylenol 0.3%,
Glycerine 1.0%,
Alkali protease 0.1%,
Cellulase 0.05%,
Preservative 0.1%,
Essence 1.0%,
Pigment 0.01%；
The mass percent sum of above component is 100%.
The solidifying pearl of the laundry, which is prepared by the following method, to be formed：
1) in advance will emulsification pot, pipeline, storage tank, the sterilization of weighing vessel cleaning.
2) AEO, C8-16 alkyl glucosides, laureth sulfuric ester are weighed respectively according to formula ratio
Sodium, C12-14 AEOs add emulsification pot and stir 25min to transparency liquid with 120 turns/min rotating speed；
3) C10- isomeric alcohol polyethenoxy ethers, acetic acid chlorhexidine, parachlorometaxylenol are weighed prewired according to formula ratio
80 DEG C of heating is well mixed in pot to transparency liquid, is pumped into emulsification pot and 30min is stirred to transparent liquid with 120 turns/min rotating speed
Body；
4) weigh glycerine, alkali protease, cellulase respectively according to formula ratio to add in emulsification pot, with turning for 60 turns/min
Speed stirs 30 minutes to transparency liquid；
5) preservative, essence, pigment is weighed respectively according to formula ratio to add in emulsification pot with 60 turns/min rotating speed stirring
15 minutes to transparency liquid；
6) physical and chemical index examines qualified filtering and discharging；
7) it is filling after standing 24 hours.
Performance detection and effect assessment
1. detergency test
According to GB/T 13174-2008, the solidifying pearl of antibacterial laundry described in embodiment 1-3 is prepared into quality with 250mg/kg hard water
The laundry liquor of fraction 0.25%, tests to carbon black soiled cotton and the detergency of sebum soiled cotton, is contrasted with standard liquid detergent,
Decontamination ratio is calculated, as a result referring to table 1.
Table 1：Detergency test result
2. foaming properties test
The solidifying pearl of antibacterial laundry described in embodiment 1-3 is prepared to the aqueous solution of 60mL mass fractions 0.1% with deionized water, added
In the test cylinder for adding to the dynamic foam instrument of Kr ü ss DFA 100, constant temperature sets air velocity 0.3L/min, air-blowing to 30 DEG C
Time 30s, record foam height and half-life period.Result is recorded referring to table 2.
Table 2：Foaming properties test result
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Foam height (mm) | 158 | 165 | 161 |
| Half foam life period (s) | 210 | 260 | 235 |
3. fungistatic effect is tested
According to the evaluation of the daily chemical products antibacterial bacteriostatic effect of QB/T 2738-2012 People's Republic of China (PRC) light industry standard
Antibacterial laundry of the method to embodiment 1-3 is coagulated pearl and tested, strain:Staphylococcus aureus (ATCC6538), Escherichia coli
(ATCC25922), purchased from China Preventive Medicial Science Institute, Candida albicans (ATCC10231) is purchased from Chinese military medicine science
Institute, aspergillus niger (ATCC16404) is purchased from China General Microbiological Culture Collection.
Test result indicates that：The antibacterial solidifying pearl of laundry of the present invention respectively to staphylococcus aureus, Escherichia coli with
And aspergillus niger has good inhibiting effect.
Above-mentioned embodiment is only the preferred embodiment of the present invention, it is impossible to limit the scope of protection of the invention with this,
The change and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention
Claimed scope.
Claims (7)
1. a kind of solidifying pearl of antibacterial laundry, it is characterised in that it includes the following components being calculated in mass percent：
AEO 22.0%-25.0%
C10- isomeric alcohol polyethenoxy ethers 35.0%-42.0%,
C12-14 AEOs 25.0%-28.0%,
C8-16 alkyl glucosides 3.0%-5.0%,
Laureth sodium sulfovinate 8.0%-10.0%,
Acetic acid chlorhexidine 0.2%-0.3%,
Parachlorometaxylenol 0.2%-0.3%,
Glycerine 1.0%-3.0%,
Alkali protease 0.1%-0.3%,
Cellulase 0.05%-0.2%,
Preservative 0.1%-0.2%,
Essence 1.0%-2.0%,
Pigment 0.01%-0.02%；
The mass percent sum of above component is 100%.
2. a kind of preparation method of the antibacterial solidifying pearl of laundry as claimed in claim 1, it is characterised in that the preparation method include with
Lower step：
1) in advance will emulsification pot, pipeline, storage tank, the sterilization of weighing vessel cleaning.
2) weighed respectively according to formula ratio AEO, C8-16 alkyl glucosides, laureth sodium sulfovinate,
C12-14 AEOs add in emulsification pot moderate-speed mixer to transparency liquid；
3) C10- isomeric alcohol polyethenoxy ethers, acetic acid chlorhexidine, parachlorometaxylenol are weighed in prewired pot according to formula ratio
It is well mixed to be heated to transparency liquid, moderate-speed mixer is pumped into emulsification pot to transparency liquid；
4) weigh glycerine, alkali protease, cellulase respectively according to formula ratio to add in emulsification pot, stirring at low speed to transparent liquid
Body；
5) preservative, essence, pigment are weighed respectively according to formula ratio and adds in emulsification pot stirring at low speed to transparency liquid；
6) physical and chemical index examines qualified filtering and discharging；
7) it is filling after standing 24 hours.
3. preparation method according to claim 1, it is characterised in that step 2) described in the speed of moderate-speed mixer be 80-
120 turns/min, mixing time is 25min.
4. preparation method according to claim 2, it is characterised in that step 3) described in moderate-speed mixer speed be 80-120
Turn/min, mixing time is 30min.
5. preparation method according to claim 3, it is characterised in that step 3) in, heating-up temperature is 70-80 DEG C.
6. preparation method according to claim 4, it is characterised in that step 4) in stirring at low speed speed turn for 30-60/
Min, mixing time is 30min.
7. preparation method according to claim 1, it is characterised in that step 5) in stirring at low speed speed turn for 30-60/
Min, mixing time is 15 minutes.
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| CN201710244688.1A CN107057876A (en) | 2017-04-14 | 2017-04-14 | A kind of solidifying pearl of antibacterial laundry and preparation method thereof |
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| CN201710244688.1A CN107057876A (en) | 2017-04-14 | 2017-04-14 | A kind of solidifying pearl of antibacterial laundry and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107711870A (en) * | 2017-09-30 | 2018-02-23 | 珠海国佳凝胶研究院有限公司 | The solidifying pearl of one kind sterilization and its application method |
| CN108219993A (en) * | 2018-01-09 | 2018-06-29 | 广州市加茜亚化妆品有限公司 | A kind of micro-perfume capsule liquid detergent and preparation method thereof |
| CN108865485A (en) * | 2018-06-22 | 2018-11-23 | 西安开米股份有限公司 | A kind of solvent type efficient concentration liquid detergent and preparation method thereof |
| CN109112003A (en) * | 2018-09-28 | 2019-01-01 | 广州市加茜亚化妆品有限公司 | A kind of use in dishwasher washs solidifying pearl and preparation method |
| CN112753708A (en) * | 2020-12-25 | 2021-05-07 | 宁波子沐新材料科技有限公司 | Long-acting antibacterial composition and application thereof in laundry detergent |
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| CN1273032A (en) * | 1999-05-11 | 2000-11-15 | 高占奎 | Water-soluble aromatic xibitane iodine |
| CN105779159A (en) * | 2016-04-09 | 2016-07-20 | 福建省金鹿日化股份有限公司 | Softening clothes washing condensate ball and preparation method thereof |
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| CN107711870A (en) * | 2017-09-30 | 2018-02-23 | 珠海国佳凝胶研究院有限公司 | The solidifying pearl of one kind sterilization and its application method |
| CN108219993A (en) * | 2018-01-09 | 2018-06-29 | 广州市加茜亚化妆品有限公司 | A kind of micro-perfume capsule liquid detergent and preparation method thereof |
| CN108865485A (en) * | 2018-06-22 | 2018-11-23 | 西安开米股份有限公司 | A kind of solvent type efficient concentration liquid detergent and preparation method thereof |
| CN109112003A (en) * | 2018-09-28 | 2019-01-01 | 广州市加茜亚化妆品有限公司 | A kind of use in dishwasher washs solidifying pearl and preparation method |
| CN109112003B (en) * | 2018-09-28 | 2021-08-06 | 广州市加茜亚化妆品有限公司 | Washing gel bead for dish-washing machine and preparation method |
| CN112753708A (en) * | 2020-12-25 | 2021-05-07 | 宁波子沐新材料科技有限公司 | Long-acting antibacterial composition and application thereof in laundry detergent |
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