CN106889239A - A kind of preparation method of the compound caffein of sleeping - Google Patents
A kind of preparation method of the compound caffein of sleeping Download PDFInfo
- Publication number
- CN106889239A CN106889239A CN201710030858.6A CN201710030858A CN106889239A CN 106889239 A CN106889239 A CN 106889239A CN 201710030858 A CN201710030858 A CN 201710030858A CN 106889239 A CN106889239 A CN 106889239A
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- Prior art keywords
- tea
- caffein
- sleeping
- lily
- powder
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/30—Further treatment of dried tea extract; Preparations produced thereby, e.g. instant tea
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/18—Extraction of water soluble tea constituents
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation method of the compound caffein of sleeping.It is the instant compound caffein being made up of steps such as raw material preparation → crushing → eliminating caffeine → tea powder preparation → millet paste decoction → concentration → freeze-dryings with gross tea, lily, corydalis tuber, cortex albiziae as raw material.The instant caffein of gained not only flavour mellowness, and the effects such as with improving the health care of sleep, calming the nerves Xie Yu, the health that clears away heart-fire, moisten the lung and relieve the cough.
Description
Technical field
The present invention relates to field of foodstuff beverage, and in particular to a kind of preparation method of the compound caffein of sleeping.
Background technology
With the quickening and the increase of operating pressure of social rhythm, crowd's quantity that there is sleep-disorder the country is gradually increasing
Plus, more than 300,000,000.People are on conducing to sleep simultaneously and do not influence healthy drink demand being continuously increased, and sleeping
The tea-drinking that the appearance layout of caffein is a kind of for people provide to be easy to brew, conveniently drunk is selected, even more to there is insomnia
Crowd bring Gospel.Therefore, a kind of compound caffein of sleeping is invented significant for improving the sleep quality of people.
The content of the invention
It is an object of the invention to provide a kind of novel form of organic resistance to leaf of making tea, the invention product sequence is simple, stabilization
Property is good, can discharge for a long time, and the invention preparation method operating time is short, low cost.The present invention is realized by following scheme:
A kind of preparation method of the compound caffein of sleeping, it is raw material to use lily, corydalis tuber, cortex albiziae and gross tea, and is passed through
Following steps are obtained:
(1) lily, corydalis tuber, cortex albiziae are crushed to 350-400 mesh with pulverizer respectively, respectively obtain lily ultra micro
Powder, corydalis tuber and cortex albiziae Ultramicro-powder;
(2) after first gross tea impurity elimination is cleaned, according to solid-to-liquid ratio 1:15 to 1:20, add gross tea and deionization frozen water compound
Into container, then extracted in vacuum drying chamber case, filter leaching liquor, filter residue is the tealeaves of caffein-free;
(3) by the drying tea leaves of eliminating caffeine to water content 15%-20%, 350-400 is first crushed in pulverizer
Mesh, obtains the super fine tea powder of eliminating caffeine;
(4) by lily root flour, tetrahydropalmatine, cortex albiziae powder and gross tea powder according to 2:1:1:6 ratio is mixed to get mixture,
According to solid-to-liquid ratio 1:5 add clear water, are placed on materials decoction device, repeat to decoct twice, and temperature is 75-80 DEG C, and the time is 10-
15min, merges decoction liquor;Temperature is reduced to 5 DEG C, is filtrated to get decoction liquor;
(5) decoction liquor is put into ultrasonic homogenizer, the homogeneous under conditions of frequency 20kHz, pressure 1.8MPa, true
Reciprocal of duty cycle is 75kPa, temperature is vacuum concentration in the environment of 50 DEG C, to relative density 1.9-2.0g/cm3Concentrate;
(6) decoction liquor is put into the environment of -25 to -20 DEG C, is freezed 3-4 hours, the mixed liquor after freezing is being loaded
Amount 8-9kg/cm2, operating pressure 55-65Pa, dried under conditions of parsing pressure 30-35Pa, 40-45 DEG C of temperature, sleeping is obtained
Compound tea powder;Recycling microwave heating equipment carries out expanding treatment to tea powder, and the time is 3-5min, obtains final product the compound caffein of sleeping.
Further, described lily, corydalis tuber and cortex albiziae soak 10- before crushing with 35-40 DEG C of clear water
15min, washes away debris;Dried to water content 15%-20% in the environment of 70-75 DEG C again.
Further, described lily, corydalis tuber, cortex albiziae be when crushing, and is first crushed to after 130-150 mesh again with super
350-400 mesh is crushed in pulverizer.
Further, the tealeaves of described eliminating caffeine uses superfine flour again when crushing after being first crushed to 100-120 mesh
350-400 mesh is crushed in broken machine.
Preferably, the gross tea in raw material can be the gross tea of black tea or the gross tea of green tea, it is also possible to be replaced with tea fresh leaves.
Lily, corydalis tuber, cortex albiziae and the gross tea raw material that the present invention chooses are widely present, and reduce production cost;Technique
Upper easy to operate, advantage of lower cost, small investment, pollution is few, it is easy to industrialize;Lily, corydalis tuber after deep processing, cortex albiziae
Compound caffein, not only flavour mellowness, and the effects such as with improving the health care of sleep, calming the nerves Xie Yu, the health that clears away heart-fire, moisten the lung and relieve the cough, especially
It is to lose to support symptom for mind such as the sleep-disorder person of the depressed emotion symptoms such as gloomy not happy, dysphoria and dreaminess, hidrosis
Insomniac has preferable mitigation.
Specific embodiment
In order that those skilled in the art more fully understands technical scheme, further is made to the present invention below
Explanation:
Embodiment one:
A kind of preparation method of the compound caffein of sleeping, it is raw material to use lily, corydalis tuber, cortex albiziae and gross tea, and is passed through
Following steps are obtained:
(1) select good colour, without going mouldy, dry lily, corydalis tuber and cortex albiziae, soaked with 40 DEG C of clear water
12min, washes away debris;Dried to water content 15% in the environment of 75 DEG C again.
(2) lily, corydalis tuber, cortex albiziae are crushed to 350 mesh with pulverizer respectively, respectively obtain lily Ultramicro-powder, prolongs
Hu Suo and cortex albiziae Ultramicro-powder;
(3) after first gross tea impurity elimination is cleaned, according to solid-to-liquid ratio 1:15, add gross tea and deionization frozen water compound to container
In, then extracted in vacuum drying chamber case, leaching liquor is filtered, filter residue is the tealeaves of caffein-free;
(4) by the drying tea leaves of eliminating caffeine to water content 15%, 350 mesh are crushed in pulverizer, are sloughed
The super fine tea powder of caffeine;
(5) by lily root flour, tetrahydropalmatine, cortex albiziae powder and gross tea powder according to 2:1:1:6 ratio is mixed to get mixture,
According to solid-to-liquid ratio 1:5 add clear water, are placed on materials decoction device, repeat to decoct twice, and temperature is 75 DEG C, and the time is 15min, is closed
And decoction liquor;Temperature is reduced to 5 DEG C, is filtrated to get decoction liquor;
(6) decoction liquor is put into ultrasonic homogenizer, the homogeneous under conditions of frequency 20kHz, pressure 1.8MPa, true
Reciprocal of duty cycle is 75kPa, temperature is vacuum concentration in the environment of 50 DEG C, to relative density 1.9-2.0g/cm3Concentrate;
(7) decoction liquor is put into the environment of -25 DEG C, is freezed 4 hours, by the mixed liquor after freezing in useful load 8kg/
cm2, operating pressure 55Pa, dried under conditions of parsing pressure 30-Pa, 40 DEG C of temperature, the compound tea powder of sleeping is obtained;Recycle micro-
Wave heating equipment carries out expanding treatment to tea powder, and the time is 3min, obtains final product the compound caffein of sleeping.
Embodiment two:
A kind of preparation method of the compound caffein of sleeping, it is raw material to use lily, corydalis tuber, cortex albiziae and gross tea, and is passed through
Following steps are obtained:
(1) select good colour, without going mouldy, dry lily, corydalis tuber and cortex albiziae, soaked with 40 DEG C of clear water
12min, washes away debris;Dried to water content 20% in the environment of 75 DEG C again.
(2) lily, corydalis tuber, cortex albiziae are crushed to 150 mesh with pulverizer respectively, then are crushed to super pulverizer
400 mesh, respectively obtain lily Ultramicro-powder, corydalis tuber and cortex albiziae Ultramicro-powder;
(3) after first gross tea impurity elimination is cleaned, according to solid-to-liquid ratio 1:20, add gross tea and deionization frozen water compound to container
In, then extracted in vacuum drying chamber case, leaching liquor is filtered, filter residue is the tealeaves of caffein-free;
(4) 120 mesh are crushed to by the drying tea leaves of eliminating caffeine to water content 20%, in pulverizer, then with super
Pulverizer is crushed to 400 mesh, obtains the super fine tea powder of eliminating caffeine;
(5) by lily root flour, tetrahydropalmatine, cortex albiziae powder and gross tea powder according to 2:1:1:6 ratio is mixed to get mixture,
According to solid-to-liquid ratio 1:5 add clear water, are placed on materials decoction device, repeat to decoct twice, and temperature is 80 DEG C, and the time is 15min, is closed
And decoction liquor;Temperature is reduced to 5 DEG C, is filtrated to get decoction liquor;
(6) decoction liquor is put into ultrasonic homogenizer, the homogeneous under conditions of frequency 20kHz, pressure 1.8MPa, true
Reciprocal of duty cycle is 75kPa, temperature is vacuum concentration in the environment of 50 DEG C, to relative density 1.9-2.0g/cm3Concentrate;
(7) decoction liquor is put into the environment of -20 DEG C, is freezed 4 hours, by the mixed liquor after freezing in useful load 9kg/
cm2, operating pressure 65Pa, dried under conditions of parsing pressure 35Pa, temperature 45 C, the compound tea powder of sleeping is obtained;Recycle micro-
Wave heating equipment carries out expanding treatment to tea powder, and the time is 5min, obtains final product the compound caffein of sleeping.
Embodiment three:
A kind of preparation method of the compound caffein of sleeping, it is raw material to use lily, corydalis tuber, cortex albiziae and gross tea, and is passed through
Following steps are obtained:
(1) select good colour, without going mouldy, dry lily, corydalis tuber and cortex albiziae, soaked with 35 DEG C of clear water
15min, washes away debris;Dried to water content 20% in the environment of 75 DEG C again.
(2) lily, corydalis tuber, cortex albiziae are crushed to 140 mesh with pulverizer respectively, then are crushed to super pulverizer
400 mesh, respectively obtain lily Ultramicro-powder, corydalis tuber and cortex albiziae Ultramicro-powder;
(3) after first gross tea impurity elimination is cleaned, according to solid-to-liquid ratio 1:18, add gross tea and deionization frozen water compound to container
In, then extracted in vacuum drying chamber case, leaching liquor is filtered, filter residue is the tealeaves of caffein-free;
(4) 110 mesh are crushed to by the drying tea leaves of eliminating caffeine to water content 20%, in pulverizer, then with super
Pulverizer is crushed to 400 mesh, obtains the super fine tea powder of eliminating caffeine;
(5) by lily root flour, tetrahydropalmatine, cortex albiziae powder and gross tea powder according to 2:1:1:6 ratio is mixed to get mixture,
According to solid-to-liquid ratio 1:5 add clear water, are placed on materials decoction device, repeat to decoct twice, and temperature is 80 DEG C, and the time is 15min, is closed
And decoction liquor;Temperature is reduced to 5 DEG C, is filtrated to get decoction liquor;
(6) decoction liquor is put into ultrasonic homogenizer, the homogeneous under conditions of frequency 20kHz, pressure 1.8MPa, true
Reciprocal of duty cycle is 75kPa, temperature is vacuum concentration in the environment of 50 DEG C, to relative density 1.9-2.0g/cm3Concentrate;
(7) decoction liquor is put into the environment of -20 DEG C, is freezed 4 hours, by the mixed liquor after freezing in useful load 9kg/
cm2, operating pressure 65Pa, dried under conditions of parsing pressure 35Pa, temperature 45 C, the compound tea powder of sleeping is obtained;Recycle micro-
Wave heating equipment carries out expanding treatment to tea powder, and the time is 5min, obtains final product the compound caffein of sleeping.
Gross tea in above example can be the gross tea of black tea or the gross tea of green tea, it is also possible to be replaced with tea fresh leaves.
Deionization frozen water compound is that at normal atmospheric pressure, temperature is the ion under conditions of 0 DEG C in above example
Frozen water compound.
Some one exemplary embodiments of the invention only are described by way of explanation above, undoubtedly, for ability
The those of ordinary skill in domain, without departing from the spirit and scope of the present invention, can be with a variety of modes to institute
The embodiment of description is modified.Therefore, foregoing description is inherently illustrative, and should not be construed as will to right of the present invention
Ask the limitation of protection domain.
Claims (5)
1. a kind of sleeping is combined the preparation method of caffein, it is characterised in that it is former to use lily, corydalis tuber, cortex albiziae and gross tea
Material, and be obtained as follows:
(1) lily, corydalis tuber, cortex albiziae are crushed to 350-400 mesh with pulverizer respectively, respectively obtain lily Ultramicro-powder, prolongs
Hu Suo and cortex albiziae Ultramicro-powder;
(2) after first gross tea impurity elimination is cleaned, according to solid-to-liquid ratio 1:15 to 1:20, add gross tea and deionization frozen water compound to appearance
In device, then extracted in vacuum drying chamber case, filter leaching liquor, filter residue is the tealeaves of caffein-free;
(3) by the drying tea leaves of eliminating caffeine to water content 15%-20%, 350-400 mesh is crushed in pulverizer, is obtained
The super fine tea powder of eliminating caffeine;
(4) by lily root flour, tetrahydropalmatine, cortex albiziae powder and gross tea powder according to 2:1:1:6 ratio is mixed to get mixture, according to
Solid-to-liquid ratio 1:5 add clear water, are placed on materials decoction device, repeat to decoct twice, and temperature is 75-80 DEG C, and the time is 10-15min,
Merge decoction liquor;Temperature is reduced to 5 DEG C, is filtrated to get decoction liquor;
(5) decoction liquor is put into ultrasonic homogenizer, the homogeneous under conditions of frequency 20kHz, pressure 1.8MPa, in vacuum
Be 75kPa, temperature be 50 DEG C in the environment of be concentrated in vacuo, to relative density 1.9-2.0g/cm3Concentrate;
(6) decoction liquor is put into the environment of -25 to -20 DEG C, is freezed 3-4 hours, by the mixed liquor after freezing in useful load 8-
9kg/cm2, operating pressure 55-65Pa, dried under conditions of parsing pressure 30-35Pa, 40-45 DEG C of temperature, sleeping is obtained and is combined
Tea powder;Recycling microwave heating equipment carries out expanding treatment to tea powder, and the time is 3-5min, obtains final product the compound caffein of sleeping.
2. the preparation method of the compound caffein of a kind of sleeping according to claim 1, it is characterised in that described lily, prolong
Hu Suo and cortex albiziae soak 10-15min before crushing with 35-40 DEG C of clear water, wash away debris;Again in the environment of 70-75 DEG C
Dry to water content 15%-20%.
3. the preparation method of the compound caffein of a kind of sleeping according to claim 1, it is characterised in that described lily, prolong
Hu Suo, cortex albiziae are first crushed to after 130-150 mesh again with being crushed to 350-400 mesh in super pulverizer when crushing.
4. a kind of sleeping according to claim 1 is combined the preparation method of caffein, it is characterised in that described sloughs coffee
The tealeaves of alkali is first crushed to after 100-120 mesh again with being crushed to 350-400 mesh in super pulverizer when crushing.
5. a kind of sleeping according to claim 1 is combined the preparation method of caffein, it is characterised in that the gross tea in raw material can
Being the gross tea of black tea or the gross tea of green tea, it is also possible to replaced with tea fresh leaves.
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CN201710030858.6A CN106889239A (en) | 2017-01-16 | 2017-01-16 | A kind of preparation method of the compound caffein of sleeping |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1843144A (en) * | 2006-05-08 | 2006-10-11 | 浙江经贸职业技术学院 | Method for eliminating caffeine from tea leaf |
CN103960410A (en) * | 2014-04-04 | 2014-08-06 | 马洪兵 | Tea with functions of calming nerves and aiding sleep and preparation method of tea |
CN105613889A (en) * | 2016-03-20 | 2016-06-01 | 柴华 | Preparation method of persimmon calyx and pueraria flower healthcare caffeine |
-
2017
- 2017-01-16 CN CN201710030858.6A patent/CN106889239A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1843144A (en) * | 2006-05-08 | 2006-10-11 | 浙江经贸职业技术学院 | Method for eliminating caffeine from tea leaf |
CN103960410A (en) * | 2014-04-04 | 2014-08-06 | 马洪兵 | Tea with functions of calming nerves and aiding sleep and preparation method of tea |
CN105613889A (en) * | 2016-03-20 | 2016-06-01 | 柴华 | Preparation method of persimmon calyx and pueraria flower healthcare caffeine |
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TA01 | Transfer of patent application right |
Effective date of registration: 20180424 Address after: 230000 350/352 2-1, three floor, Huaxia pocheng, 100 Baohe Road, Baohe District, Hefei, Anhui Applicant after: Hefei Furun Tea Technology Co. Ltd. Address before: 230000 Zhonghua University SA2011 214 to 216, 96 Jinzhai Road, Baohe District, Hefei, Anhui Applicant before: Ge Zhangzhi |
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Application publication date: 20170627 |
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