CN106865658A - A kind of water quality cleansing agent and preparation method thereof - Google Patents
A kind of water quality cleansing agent and preparation method thereof Download PDFInfo
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- CN106865658A CN106865658A CN201710291124.3A CN201710291124A CN106865658A CN 106865658 A CN106865658 A CN 106865658A CN 201710291124 A CN201710291124 A CN 201710291124A CN 106865658 A CN106865658 A CN 106865658A
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- attapulgite
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
- C02F1/683—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water by addition of complex-forming compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/306—Pesticides
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/04—Disinfection
Abstract
The invention discloses a kind of water quality cleansing agent and preparation method thereof, it is related to cleanser technical field, including the raw material that following part is counted：200 ~ 250 parts of 65 ~ 75 parts of 80 ~ 90 part, nanometer haydite of attapulgite, 45 ~ 55 parts of bagasse, 30 ~ 40 parts of amino acid, 25 ~ 30 parts of shitosan, 25 ~ 30 parts of herbal component, 10 ~ 20 parts of organic matter, 15 ~ 20 parts of tourmaline particles, 15 ~ 20 parts of modifying agent, 2 ~ 6 parts of trace element and water.The present invention can effectively purifying water body, mitigate water pollution, improve water quality, safety non-toxic, low manufacture cost is applied widely.
Description
Technical field
The present invention relates to cleanser technical field, and in particular to a kind of water quality cleansing agent and preparation method thereof.
Background technology
The conventional method of Water warfare is by flocculation, precipitation, filtering and is chemically treated, typically can effectively remove most of
Dirt and kill most of microbe, but can not very effectively remove such as hormone, agricultural chemicals, virus, toxin and heavy metal from
The class material such as son.These harmful substances are remained in water source, give people to cause harm.And Concave-convex clay rod can use contact or filtering
Technical finesse water, can eliminate these harmful substances.If making the recessed soil regeneration of absorption pollutant, can heat or be subject to chemical agent
Treatment.Therefore, application of the recessed soil in sewage disposal is very important to preserving the ecological environment, ensureing the health of the mankind, and
Consumption is wide on a large scale, the need for meeting the raising of social development living standards of the people.
The content of the invention
It is an object of the invention to provide a kind of water quality cleansing agent and preparation method thereof, can effectively purifying water body, mitigate
Water pollution, improves water quality, and safety non-toxic, low manufacture cost is applied widely.
The invention provides following technical scheme：A kind of water quality cleansing agent, including the raw material that following part is counted：Attapulgite
80 ~ 90 65 ~ 75 parts of part, nanometer haydites, 45 ~ 55 parts of bagasse, 30 ~ 40 parts of amino acid, 25 ~ 30 parts of shitosan, herbal component
25 ~ 30 parts, 10 ~ 20 parts of organic matter, 15 ~ 20 parts of tourmaline particles, 15 ~ 20 parts of modifying agent, trace element 2 ~ 6 parts and water 200 ~
250 parts；
The herbal component includes the raw material of following part meter：It is 5 ~ 10 parts of Chinese gall, 2 ~ 8 parts of Chinese lobelia, 2 ~ 6 parts of chrysanthemum indicum, white
The palm 2 ~ 6 parts, 1 ~ 4 part of honeysuckle, 1 ~ 3 part of magnolia obovata；
The modifying agent includes the raw material of following part meter：10 ~ 12 parts of sodium carbonate, 1 ~ 2 part of sodium acid carbonate and NaOH 0.2 ~ 1.2
Part.
Preferably, including following part meter raw material：70 parts of 85 part, nanometer haydite of attapulgite, 50 parts of bagasse, amino acid
35 parts, 27 parts of shitosan, 27 parts of herbal component, 15 parts of organic matter, 17 parts of tourmaline particles, 17 parts of modifying agent, trace element 4
225 parts of part and water；
The herbal component includes the raw material of following part meter：7 parts of Chinese gall, 5 parts of Chinese lobelia, 4 parts of chrysanthemum indicum, white 4 parts of the palm, gold
2.5 parts of honeysuckle flower, 2 parts of magnolia obovata；
The modifying agent includes the raw material of following part meter：0.7 part of 11 parts of sodium carbonate, 1.5 parts of sodium acid carbonate and NaOH.
Preferably, the preparation method of the bagasse is：To streptococcus acidi lactici fermented solution is added in bagasse, in 50 ~ 65 DEG C of bars
Mixed fermentation 10 ~ 15 days under part.
Preferably, the organic matter is one or more in dregs of beans, rapeseed dregs and crop stalk.
Preferably, the tourmaline particles are that the particle diameter being prepared into after crude tourmaline mineral are crushed is 500 ~ 600 purposes
Particulate.
Preferably, the crude tourmaline mineral are dravite, iron tourmaline, elbaite, tsilaisite and calcium and magnesium
Any one in tourmaline mineral.
Preferably, the raw material of the trace element including following part meter：0.2 ~ 1.2 part of ferrous sulfate, manganese sulfate 0.2 ~ 0.8
Part, 0.2 ~ 0.6 part of copper sulphate, 0.2 ~ 0.4 part of zinc sulfate, 0.1 ~ 0.3 part of ammonium molybdate, 0.1 ~ 0.3 part of boric acid and borax 0.08 ~
0.1 part.
The present invention also provides a kind of preparation method of water quality cleansing agent, comprises the following steps：
（1）, attapulgite pretreatment
Take attapulgite and crushed, cross 100 ~ 120 mesh sieves, the attapulgite of the fine powdered that will be obtained is added to quality 10
In~15 times of clear water, stir, centrifugal treating and filtered after 20~24h of immersion, attapulgite just finished product is obtained after drying；
（2）, attapulgite modified treatment
Sodium carbonate is configured to the sodium carbonate liquor that concentration is 5 ~ 10%, by step（1）In the attapulgite that obtains just in finished product plus
Enter sodium carbonate liquor, stir and heat, sodium acid carbonate and NaOH are added in whipping process, the heat time is 2.5~3h,
Heating terminates and filters, and pulverizer crushing is put into after drying, and crosses 150 ~ 200 mesh sieves, obtains modified attapulgite；
（3）, high-temperature calcination
By step（2）In the modified attapulgite feeding calcining furnace that obtains, 1 ~ 2h is calcined at 500 ~ 650 DEG C, take out
It is attapulgite modified after to calcining, it is standby；
（4）, prepare Chinese herbal medicine fluid
Chinese gall, Chinese lobelia, chrysanthemum indicum, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, 100 ~ 120 mesh sieves are crushed and cross, obtained
To mixed-powder, ultrasonic assistant ethanol extraction is carried out to mixed-powder, to 10~15 times of weight portions of addition in mixed-powder
30 ~ 45% ethanol, under ultrasonic assistant effect, 10~30min of refluxing extraction under the conditions of 50~60 DEG C is extracted 3 times, will be extracted
Filtrate merge, refrigeration place 20~24h after, under the conditions of 55~85 DEG C be concentrated under reduced pressure reclaim ethanol, it is institute to obtain concentrate
Chinese herbal medicine fluid is stated, it is standby；
（5）, prepare finished product
By step（3）Attapulgite modified and step after the calcining for obtaining（4）Obtain Chinese herbal medicine fluid mixing, according to proportioning according to
Secondary addition surplus stock, heats and stirs, and obtains mixed material, is then spray-dried, and is finally putting into comminutor and makes
Grain, the finished product for obtaining is the water quality cleansing agent.
Beneficial effects of the present invention：Can effectively purifying water body, mitigate water pollution, improve water quality, safety non-toxic, system
Make low cost, it is applied widely, it is specific as follows：
（1）, the present invention with attapulgite as primary raw material, modification is done to attapulgite, can effectively go the removal of impurity, carry
The activity of attapulgite high, dispersiveness and suspension, are provided with stirring and heating operation in modifying process, and in the process of stirring
In, sodium acid carbonate and NaOH are added while stirring, improve the modified active of attapulgite using the principle of chemical reaction
Degree so that attapulgite it is modified more thorough, modified attapulgite adhesion by force, not easy disintegrating；
（2）, modified attapulgite high-temperature calcination treatment in the present invention, increase its interfloor distance, specific surface area is big, outstanding
Buoyancy is good, suction-operated enhancing, can effectively adsorb the class things such as hormone in water, agricultural chemicals, virus, toxin and heavy metal ion
Matter, anti-water pollution, antirancidity, with excellent purifying water effect；In addition, high-temperature calcination treatment is attapulgite modified, its ratio
Heavy and light, sinking speed is slow, and water body sufficiently can be purified, and improves the overall utilization rate of cleanser；
（3）, add nanometer haydite in the present invention, after nanometer haydite input water body, make water negative ionization, produce Mg, Fe, F, Se,
The trace elements such as N, P, K, these can supply algal grown necessary to nutrient, prevent that algae is dead to produce microcystin
Element, influences Water quality, addition nanometer haydite to improve the survival rate of aquaculture organism in water indirectly, reduce aquaculture organism
Illness rate, makes water quality cleansing agent of the invention not only can also improve water body environment with purifying water body, increases water nutrition,
Suppress harmful levels of pathogens flourish, strengthen aquiculture animal immunity of organisms and disease resistance ability；
（4）, the present invention in add herbal component, add water body after, can be as anti pathologic immunity conditioning agent, so as to reach increasing
Strong aquatic animal constitution, improve the anti-stress ability of aquatic animal and the effect of immune disease-resistance power, improve aquatic animal into
Motility rate.
Specific embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
A kind of water quality cleansing agent, including the raw material that following part is counted：
80 parts of attapulgite；
65 parts of haydite of nanometer；
45 parts of bagasse；
30 parts of amino acid；
25 parts of shitosan；
25 parts of herbal component；
10 parts of organic matter；
15 parts of tourmaline particles；
15 parts of modifying agent；
2 parts of trace element；
200 parts of water；
The herbal component includes the raw material of following part meter：5 parts of Chinese gall, 2 parts of Chinese lobelia, 2 parts of chrysanthemum indicum, white 2 parts of the palm, gold
1 part of honeysuckle flower, 1 part of magnolia obovata；
The modifying agent includes the raw material of following part meter：0.2 part of 10 parts of sodium carbonate, 1 part of sodium acid carbonate and NaOH.
Wherein, the preparation method of the bagasse is：To streptococcus acidi lactici fermented solution is added in bagasse, mixed under the conditions of 50 DEG C
Close fermentation 10 days.
Wherein, the organic matter is dregs of beans.
Wherein, the tourmaline particles are the particulate that the particle diameter being prepared into after crude tourmaline mineral are crushed is 500 mesh.
Wherein, the crude tourmaline mineral are dravite.
Wherein, the raw material of the trace element including following part meter：0.2 part of ferrous sulfate, 0.2 part of manganese sulfate, copper sulphate
0.08 part of 0.2 part, 0.2 part of zinc sulfate, 0.1 part of ammonium molybdate, 0.1 part of boric acid and borax.
A kind of preparation method of water quality cleansing agent is also provided in the present embodiment, is comprised the following steps：
（1）, attapulgite pretreatment
Take attapulgite and crushed, cross 100 mesh sieves, the attapulgite of the fine powdered that will be obtained is added to 10 times of quality
In clear water, stir, centrifugal treating and filtered after immersion 20h, attapulgite just finished product is obtained after drying；
（2）, attapulgite modified treatment
Sodium carbonate is configured to the sodium carbonate liquor that concentration is 5%, by step（1）In the attapulgite that obtains just add in finished product
Sodium carbonate liquor, is stirred and heats, and sodium acid carbonate and NaOH are added in whipping process, and the heat time is 2.5h, heating
Terminate and filter, pulverizer crushing is put into after drying, cross 150 mesh sieves, obtain modified attapulgite；
（3）, high-temperature calcination
By step（2）In the modified attapulgite feeding calcining furnace that obtains, 1h is calcined at 500 DEG C, taking-up is calcined
Afterwards attapulgite modified, it is standby；
（4）, prepare Chinese herbal medicine fluid
Chinese gall, Chinese lobelia, chrysanthemum indicum, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, 100 mesh sieves are crushed and cross, is mixed
Powder is closed, ultrasonic assistant ethanol extraction is carried out to mixed-powder, to 10 times of 30% ethanol of weight portion of addition in mixed-powder,
Under ultrasonic assistant effect, refluxing extraction 10min under the conditions of 50 DEG C is extracted 3 times, and the filtrate that will be extracted merges, and refrigeration is placed
After 20h, it is concentrated under reduced pressure under the conditions of 55 DEG C and reclaims ethanol, obtains concentrate for the Chinese herbal medicine fluid, it is standby；
（5）, prepare finished product
By step（3）Attapulgite modified and step after the calcining for obtaining（4）Obtain Chinese herbal medicine fluid mixing, according to proportioning according to
Secondary addition surplus stock, heats and stirs, and obtains mixed material, is then spray-dried, and is finally putting into comminutor and makes
Grain, the finished product for obtaining is the water quality cleansing agent.
Embodiment 2
A kind of water quality cleansing agent, including the raw material that following part is counted：
90 parts of attapulgite；
75 parts of haydite of nanometer；
55 parts of bagasse；
40 parts of amino acid；
30 parts of shitosan；
30 parts of herbal component；
20 parts of organic matter；
20 parts of tourmaline particles；
20 parts of modifying agent；
6 parts of trace element；
250 parts of water；
The herbal component includes the raw material of following part meter：10 parts of Chinese gall, 8 parts of Chinese lobelia, 6 parts of chrysanthemum indicum, white 6 parts of the palm,
4 parts of honeysuckle, 3 parts of magnolia obovata；
The modifying agent includes the raw material of following part meter：1.2 parts of 12 parts of sodium carbonate, 2 parts of sodium acid carbonate and NaOH.
Wherein, the preparation method of the bagasse is：To streptococcus acidi lactici fermented solution is added in bagasse, mixed under the conditions of 55 DEG C
Close fermentation 13 days.
Wherein, the organic matter is rapeseed dregs.
Wherein, the tourmaline particles are the particulate that the particle diameter being prepared into after crude tourmaline mineral are crushed is 600 mesh.
Wherein, the crude tourmaline mineral are iron tourmaline.
Wherein, the raw material of the trace element including following part meter：1.2 parts of ferrous sulfate, 0.8 part of manganese sulfate, copper sulphate
0.1 part of 0.6 part, 0.4 part of zinc sulfate, 0.3 part of ammonium molybdate, 0.3 part of boric acid and borax.
The present embodiment also provides a kind of preparation method of water quality cleansing agent, comprises the following steps：
（1）, attapulgite pretreatment
Take attapulgite and crushed, cross 120 mesh sieves, the attapulgite of the fine powdered that will be obtained is added to 15 times of quality
In clear water, stir, centrifugal treating and filtered after immersion 24h, attapulgite just finished product is obtained after drying；
（2）, attapulgite modified treatment
Sodium carbonate is configured to the sodium carbonate liquor that concentration is 10%, by step（1）In the attapulgite that obtains just add in finished product
Sodium carbonate liquor, is stirred and heats, and sodium acid carbonate and NaOH are added in whipping process, and the heat time is 3h, heating knot
Beam is simultaneously filtered, and pulverizer crushing is put into after drying, and crosses 200 mesh sieves, obtains modified attapulgite；
（3）, high-temperature calcination
By step（2）In the modified attapulgite feeding calcining furnace that obtains, 2h is calcined at 650 DEG C, taking-up is calcined
Afterwards attapulgite modified, it is standby；
（4）, prepare Chinese herbal medicine fluid
Chinese gall, Chinese lobelia, chrysanthemum indicum, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, 120 mesh sieves are crushed and cross, is mixed
Powder is closed, ultrasonic assistant ethanol extraction is carried out to mixed-powder, to 15 times of 45% ethanol of weight portion of addition in mixed-powder,
Under ultrasonic assistant effect, refluxing extraction 30min under the conditions of 60 DEG C is extracted 3 times, and the filtrate that will be extracted merges, and refrigeration is placed
After 24h, it is concentrated under reduced pressure under the conditions of 85 DEG C and reclaims ethanol, obtains concentrate for the Chinese herbal medicine fluid, it is standby；
（5）, prepare finished product
By step（3）Attapulgite modified and step after the calcining for obtaining（4）Obtain Chinese herbal medicine fluid mixing, according to proportioning according to
Secondary addition surplus stock, heats and stirs, and obtains mixed material, is then spray-dried, and is finally putting into comminutor and makes
Grain, the finished product for obtaining is the water quality cleansing agent.
Embodiment 3
A kind of water quality cleansing agent, including the raw material that following part is counted：
85 parts of attapulgite；
70 parts of haydite of nanometer；
50 parts of bagasse；
35 parts of amino acid；
27 parts of shitosan；
27 parts of herbal component；
15 parts of organic matter；
17 parts of tourmaline particles；
17 parts of modifying agent；
4 parts of trace element；
225 parts of water；
The herbal component includes the raw material of following part meter：7 parts of Chinese gall, 5 parts of Chinese lobelia, 4 parts of chrysanthemum indicum, white 4 parts of the palm, gold
2.5 parts of honeysuckle flower, 2 parts of magnolia obovata；
The modifying agent includes the raw material of following part meter：0.7 part of 11 parts of sodium carbonate, 1.5 parts of sodium acid carbonate and NaOH.
Wherein, the preparation method of the bagasse is：To streptococcus acidi lactici fermented solution is added in bagasse, mixed under the conditions of 58 DEG C
Close fermentation 11 days.
Wherein, the organic matter is crop stalk.
Wherein, the tourmaline particles are the particulate that the particle diameter being prepared into after crude tourmaline mineral are crushed is 550 mesh.
Wherein, the crude tourmaline mineral are tsilaisite.
Wherein, the raw material of the trace element including following part meter：0.7 part of ferrous sulfate, 0.6 part of manganese sulfate, copper sulphate
0.09 part of 0.4 part, 0.3 part of zinc sulfate, 0.2 part of ammonium molybdate, 0.2 part of boric acid and borax.
The present embodiment also provides a kind of preparation method of water quality cleansing agent, comprises the following steps：
（1）, attapulgite pretreatment
Take attapulgite and crushed, cross 110 mesh sieves, the attapulgite of the fine powdered that will be obtained is added to 12 times of quality
In clear water, stir, centrifugal treating and filtered after immersion 22h, attapulgite just finished product is obtained after drying；
（2）, attapulgite modified treatment
Sodium carbonate is configured to the sodium carbonate liquor that concentration is 7%, by step（1）In the attapulgite that obtains just add in finished product
Sodium carbonate liquor, is stirred and heats, and sodium acid carbonate and NaOH are added in whipping process, and the heat time is 2.5h, heating
Terminate and filter, pulverizer crushing is put into after drying, cross 150 mesh sieves, obtain modified attapulgite；
（3）, high-temperature calcination
By step（2）In the modified attapulgite feeding calcining furnace that obtains, 1.5h is calcined at 600 DEG C, taking-up is forged
It is attapulgite modified after burning, it is standby；
（4）, prepare Chinese herbal medicine fluid
Chinese gall, Chinese lobelia, chrysanthemum indicum, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, 110 mesh sieves are crushed and cross, is mixed
Powder is closed, ultrasonic assistant ethanol extraction is carried out to mixed-powder, to 12 times of 32% ethanol of weight portion of addition in mixed-powder,
Under ultrasonic assistant effect, refluxing extraction 20min under the conditions of 55 DEG C is extracted 3 times, and the filtrate that will be extracted merges, and refrigeration is placed
After 22h, it is concentrated under reduced pressure under the conditions of 70 DEG C and reclaims ethanol, obtains concentrate for the Chinese herbal medicine fluid, it is standby；
（5）, prepare finished product
By step（3）Attapulgite modified and step after the calcining for obtaining（4）Obtain Chinese herbal medicine fluid mixing, according to proportioning according to
Secondary addition surplus stock, heats and stirs, and obtains mixed material, is then spray-dried, and is finally putting into comminutor and makes
Grain, the finished product for obtaining is the water quality cleansing agent.
The present invention has been described in detail with reference to the foregoing embodiments, for a person skilled in the art, its according to
The technical scheme described in foregoing embodiments can so be modified, or which part technical characteristic is equally replaced
Change.All any modification, equivalent substitution and improvements within the spirit and principles in the present invention, made etc., should be included in the present invention
Protection domain within.
Claims (8)
1. a kind of water quality cleansing agent, it is characterised in that the raw material including following part meter：Part, nanometer haydite 65 of attapulgite 80 ~ 90
~ 75 parts, 45 ~ 55 parts of bagasse, 30 ~ 40 parts of amino acid, 25 ~ 30 parts of shitosan, 25 ~ 30 parts of herbal component, organic matter 10 ~ 20
200 ~ 250 parts of part, 15 ~ 20 parts of tourmaline particles, 15 ~ 20 parts of modifying agent, 2 ~ 6 parts of trace element and water；
The herbal component includes the raw material of following part meter：It is 5 ~ 10 parts of Chinese gall, 2 ~ 8 parts of Chinese lobelia, 2 ~ 6 parts of chrysanthemum indicum, white
The palm 2 ~ 6 parts, 1 ~ 4 part of honeysuckle, 1 ~ 3 part of magnolia obovata；
The modifying agent includes the raw material of following part meter：10 ~ 12 parts of sodium carbonate, 1 ~ 2 part of sodium acid carbonate and NaOH 0.2 ~ 1.2
Part.
2. water quality cleansing agent according to claim 1, it is characterised in that the raw material including following part meter：Attapulgite 85
Part, 70 parts of nanometer haydite, 50 parts of bagasse, 35 parts of amino acid, 27 parts of shitosan, 27 parts of herbal component, 15 parts of organic matter, electricity
17 parts of gas stone particulate, 17 parts of modifying agent, micro- 4 parts and 225 parts of water；
The herbal component includes the raw material of following part meter：7 parts of Chinese gall, 5 parts of Chinese lobelia, 4 parts of chrysanthemum indicum, white 4 parts of the palm, gold
2.5 parts of honeysuckle flower, 2 parts of magnolia obovata；
The modifying agent includes the raw material of following part meter：0.7 part of 11 parts of sodium carbonate, 1.5 parts of sodium acid carbonate and NaOH.
3. water quality cleansing agent according to claim 1, it is characterised in that the preparation method of the bagasse is：To sugarcane
Streptococcus acidi lactici fermented solution is added in slag, mixed fermentation 10 ~ 15 days under the conditions of 50 ~ 65 DEG C.
4. water quality cleansing agent according to claim 1, it is characterised in that the organic matter is dregs of beans, rapeseed dregs and farming
One or more in thing straw.
5. water quality cleansing agent according to claim 1, it is characterised in that the tourmaline particles are crude tourmaline mineral
The particle diameter being prepared into after broken is the particulate of 500 ~ 600 mesh.
6. water quality cleansing agent according to claim 5, it is characterised in that the crude tourmaline mineral be dravite,
Any one in iron tourmaline, elbaite, tsilaisite and uvite mineral.
7. water quality cleansing agent according to claim 1, it is characterised in that the original of the trace element including following part meter
Material：0.2 ~ 1.2 part of ferrous sulfate, 0.2 ~ 0.8 part of manganese sulfate, 0.2 ~ 0.6 part of copper sulphate, 0.2 ~ 0.4 part of zinc sulfate, ammonium molybdate
0.08 ~ 0.1 part of 0.1 ~ 0.3 part, 0.1 ~ 0.3 part of boric acid and borax.
8. the preparation method of water quality cleansing agent of the one kind according to any one of claim 1 ~ 7, it is characterised in that including following
Step：
（1）, attapulgite pretreatment
Take attapulgite and crushed, cross 100 ~ 120 mesh sieves, the attapulgite of the fine powdered that will be obtained is added to quality 10
In~15 times of clear water, stir, centrifugal treating and filtered after 20~24h of immersion, attapulgite just finished product is obtained after drying；
（2）, attapulgite modified treatment
Sodium carbonate is configured to the sodium carbonate liquor that concentration is 5 ~ 10%, by step（1）In the attapulgite that obtains just in finished product plus
Enter sodium carbonate liquor, stir and heat, sodium acid carbonate and NaOH are added in whipping process, the heat time is 2.5~3h,
Heating terminates and filters, and pulverizer crushing is put into after drying, and crosses 150 ~ 200 mesh sieves, obtains modified attapulgite；
（3）, high-temperature calcination
By step（2）In the modified attapulgite feeding calcining furnace that obtains, 1 ~ 2h is calcined at 500 ~ 650 DEG C, take out
It is attapulgite modified after to calcining, it is standby；
（4）, prepare Chinese herbal medicine fluid
Chinese gall, Chinese lobelia, chrysanthemum indicum, the white palm, honeysuckle magnolia obovata are weighed according to proportioning, 100 ~ 120 mesh sieves are crushed and cross, obtained
To mixed-powder, ultrasonic assistant ethanol extraction is carried out to mixed-powder, to 10~15 times of weight portions of addition in mixed-powder
30 ~ 45% ethanol, under ultrasonic assistant effect, 10~30min of refluxing extraction under the conditions of 50~60 DEG C is extracted 3 times, will be extracted
Filtrate merge, refrigeration place 20~24h after, under the conditions of 55~85 DEG C be concentrated under reduced pressure reclaim ethanol, it is institute to obtain concentrate
Chinese herbal medicine fluid is stated, it is standby；
（5）, prepare finished product
By step（3）Attapulgite modified and step after the calcining for obtaining（4）Obtain Chinese herbal medicine fluid mixing, according to proportioning according to
Secondary addition surplus stock, heats and stirs, and obtains mixed material, is then spray-dried, and is finally putting into comminutor and makes
Grain, the finished product for obtaining is the water quality cleansing agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710291124.3A CN106865658A (en) | 2017-04-28 | 2017-04-28 | A kind of water quality cleansing agent and preparation method thereof |
Applications Claiming Priority (1)
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| CN108383196A (en) * | 2018-04-02 | 2018-08-10 | 合肥卓畅农业科技有限公司 | Antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and preparation method thereof |
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| CN107253768A (en) * | 2017-08-11 | 2017-10-17 | 王婧宁 | Water treatment agent based on plant extracts |
| CN107555611A (en) * | 2017-09-22 | 2018-01-09 | 河南科技大学 | A kind of efficiently fishing improver of water quality and its preparation method and application |
| CN107537448A (en) * | 2017-10-17 | 2018-01-05 | 诸暨马谷亲科技有限公司 | Medicament of heavy metal and preparation method thereof in a kind of removal trade effluent |
| CN108037122A (en) * | 2017-12-07 | 2018-05-15 | 鲁忠华 | A kind of reagent for water quality detection and preparation method thereof |
| CN108383196A (en) * | 2018-04-02 | 2018-08-10 | 合肥卓畅农业科技有限公司 | Antibacterial decontamination environment-friendly high-efficiency water purification agent of one kind and preparation method thereof |
| CN108607529A (en) * | 2018-05-08 | 2018-10-02 | 中国科学院烟台海岸带研究所 | A kind of purification filtrate of Organic-inorganic composite contaminant water and its preparation method and application |
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| CN109126733A (en) * | 2018-09-29 | 2019-01-04 | 哈尔滨工业大学（深圳） | It is a kind of for adsorbing the preparation method of the modification haydite composite filling of pollutant |
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| CN111389348A (en) * | 2020-04-16 | 2020-07-10 | 南京信息工程大学 | Attapulgite water pollution treatment agent and preparation method thereof |
| CN113006195A (en) * | 2021-03-05 | 2021-06-22 | 广州隆盛景观建设有限公司 | Environment-friendly garden landscape rainwater treatment and reuse method |
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