CN106801217B - A kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode - Google Patents

A kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode Download PDF

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Publication number
CN106801217B
CN106801217B CN201710073591.9A CN201710073591A CN106801217B CN 106801217 B CN106801217 B CN 106801217B CN 201710073591 A CN201710073591 A CN 201710073591A CN 106801217 B CN106801217 B CN 106801217B
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Prior art keywords
washer
dewar
yoke
tetrafluoro
pedestal
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CN201710073591.9A
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CN106801217A (en
Inventor
邱清泉
汪天龙
屈飞
靖立伟
张国民
肖立业
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Institute of Electrical Engineering of CAS
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Institute of Electrical Engineering of CAS
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering
    • C23C14/35Sputtering by application of a magnetic field, e.g. magnetron sputtering
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/56Apparatus specially adapted for continuous coating; Arrangements for maintaining the vacuum, e.g. vacuum locks
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16JPISTONS; CYLINDERS; SEALINGS
    • F16J15/00Sealings
    • F16J15/02Sealings between relatively-stationary surfaces
    • F16J15/06Sealings between relatively-stationary surfaces with solid packing compressed between sealing surfaces
    • F16J15/10Sealings between relatively-stationary surfaces with solid packing compressed between sealing surfaces with non-metallic packing
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L59/00Thermal insulation in general
    • F16L59/06Arrangements using an air layer or vacuum
    • F16L59/065Arrangements using an air layer or vacuum using vacuum

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Containers, Films, And Cooling For Superconductive Devices (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

A kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode, including superconducting coil (1), yoke, glass steel plate washer (5,6), Dewar, glass reinforced plastic sleeve (10), big tetrafluoro washer (11), stainless steel washer (12), small tetrafluoro washer (13) and cathode bracket (14);It is supported and is insulated with glass steel plate washer (5,6) between superconducting coil (1) and Dewar end cap (7) and bottom yoke (4), Dewar pedestal (8) uses vacuum interlayer structure or filling-foam material to reduce thermal losses;It seals and insulate using big tetrafluoro washer (11) fitted seal circle between Dewar pedestal (8) and stainless steel washer (12), using fiberglass bolt or the fastening of the metal bolts with glass fibre reinforced plastic insulating casing between big tetrafluoro washer (11), stainless steel washer (12), small tetrafluoro washer (13) and Dewar pedestal (8);It is sealed using sealing ring between stainless steel washer (12) and cathode bracket (14) and common metal bolt is used to fasten.

Description

A kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode
Technical field
The present invention relates to a kind of magnetic control sputtering cathode, more particularly to a kind of insulation and thermal insulation of superconduction high field magnetic control sputtering cathode And sealing structure.
Background technology
Magnetron sputtering is widely used in material film plating field, in order to explore optimal coating process, in Past 30 Years, and exploitation Various magnetic control sputtering devices.High-intensity magnetic field magnetic control sputtering device is integrated in High-quality transparent conductive film and submicron order There is apparent advantage compared to conventional magnetron sputter equipment in the manufacturing process of circuit.
Ishibashi has studied permanent magnetic strong magnetic field magnetic control sputtering device in nineteen ninety first, which can be lower It discharges under cathode voltage, to obtain low-resistivity tin indium oxide (ITO) film.The reason of film resiativity reduces under high-intensity magnetic field Being considered as high-intensity magnetic field can inhibit anion to bombard the high energy of deposition film.2003, Japan Nagoya university Mizutani first proposed using the excitatory high-intensity magnetic field magnetic control sputtering device of superconduction block material, in low pressure, high voltage and long target In the case of substrate spacing, magnetic charging is realized.2004, Hazama was had studied with the excitatory magnetron sputtering apparatus of superconducting block The Cu thin film preparation processes of 200nm ranks are found in low air pressure, the target base spacing plasma heat radiation of length to the shadow of substrate Very little is rung, the film for preparing high quality is conducive to.2007, Yamaguchi was prepared for the magnetic control sputtering device that superconducting block swashs Optical mirror slip of the reflectivity up to 70%.2008, Ikuta heated in the case of system using superconduction magnetic control sputtering device in no substrate ZnO transparent electrode thin films are adulterated for Ga, film resiativity is 4.7 × 10-4Ω cm, approached can practical application resistivity water It is flat.2009, Chinese patent 200910093159.1 disclosed a kind of based on round and excitatory track type superconducting coil strong magnetic Field planar megnetron sputtering device, 2014, Chinese patent 201410766299.1 disclosed superconducting intense magnetic field magnetic control sputtering cathode Low-temperature cooling system.Above-mentioned patent proposes master-plan and the low-temperature cooling system of superconduction high field magnetic control sputtering cathode, to the greatest extent Pipe in this way, due to superconduction magnetic control sputtering cathode particularity, the sealing problem under low-temperature insulation, thermal insulation and low temperature, relatively often The magnetic control sputtering cathode for advising permanent magnetism and electromagnetic type is increasingly complex.Since cooled cryostat is directly connected to cathode power, voltage is usual For minus hundreds of to negative upper kilovolt, but cathode bracket needs to be grounded, voltage zero, and superconducting magnet needs to connect power supply for magnet coils, electricity Pressure is 0-10V, needs to carry out low temperature electric insulation and sealing, while low temperature between superconducting magnet, current feed and cooled cryostat Also need to carry out low-temperature insulation and sealing between Dewar and cathode bracket, at the same realize low-temperature insulation and low temperature seal be one very Complicated problem.In addition, since cooled cryostat temperature is very low, and cathode bracket is mounted on vacuum chamber, temperature is room temperature, is Reduction heat loss by exhaust, it is also desirable to solve the problems, such as the adiabatic of cooled cryostat and cathode bracket.
Invention content
Present invention aim to address the superconducting magnet of superconduction high field magnetic control sputtering cathode, cooled cryostat and cathode bracket it Between insulate, adiabatic and sealing problem, it is proposed that the insulating of a kind of superconduction magnetic control sputtering cathode, adiabatic and sealing structure.This hair The bright superconducting intense magnetic field magnetic control sputtering device that can be used for circular flat and rectangle plane.
The technical solution adopted by the present invention is as follows:
A kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode, by superconducting coil, inner yoke, outer magnetic Yoke, bottom yoke, glass steel plate washer, Dewar end cap, Dewar pedestal, electrical conductor, glass reinforced plastic sleeve, big tetrafluoro washer, stainless steel Washer, small tetrafluoro washer, cathode bracket are constituted.Outer yoke is located at the outside of inner yoke, and bottom yoke is located at the bottom of interior outer yoke, Superconducting coil is installed between interior magnet yoke, outer yoke and bottom yoke;Dewar pedestal is located at the lower section of Dewar end cap, superconducting coil, Inner yoke, outer yoke and bottom yoke are mounted in the space that Dewar end cap and Dewar pedestal surround;Big tetrafluoro washer is located at Dewar The lower section of pedestal, stainless steel washer are located at the lower section of big tetrafluoro washer, and small tetrafluoro washer is mounted on the lower section of stainless steel washer, cloudy Pole bracket is used to support magnetic control sputtering cathode mounted on the lower section of stainless steel washer, the outside of small tetrafluoro washer.
Since Dewar end cap is negative high potential, superconducting coil is low potential, therefore between superconducting coil and Dewar end cap, And fiberglass pad support and insulation are respectively adopted between superconducting coil and bottom yoke, electrical conductor is drawn by Dewar pedestal, Glass reinforced plastic sleeve is sleeved on outside electrical conductor, is insulated using glass reinforced plastic sleeve between electrical conductor and Dewar pedestal.Du Watt pedestal uses vacuum interlayer structure or the structure of filling-foam material to reduce thermal losses, in order to use room temperature sealing structure Carry out vacuum sealing.Since Dewar pedestal is negative high potential, stainless steel washer is zero potential, and big tetrafluoro washer is installed on Du Watt between pedestal and stainless steel washer, big tetrafluoro washer upper and lower surface is provided with seal groove, and fitted seal circle is sealed and insulate, Big tetrafluoro washer, stainless steel washer, the stacking of small tetrafluoro gasket layer put, and are provided with screw hole, big tetrafluoro washer, stainless steel washer, small It is fastened using fiberglass bolt or the metal bolts with glass fibre reinforced plastic insulating casing between tetrafluoro washer and Dewar pedestal.Due to Stainless steel washer and the same current potential of cathode bracket are sealed and common gold between stainless steel washer and cathode bracket using sealing ring Belong to bolt fastening.
The insulation and thermal insulation and sealing structure for the superconduction high field magnetic control sputtering cathode that the present invention designs, can effectively solve superconduction The sealing problem under low-temperature insulation, thermal insulation and low temperature between magnet, cooled cryostat and cathode bracket, to solve superconduction high field magnetic The assembly of control sputter cathode and vacuum cavity provides key technology support.
Description of the drawings
Fig. 1 is the schematic diagram of superconduction high field magnetic control sputtering cathode;
Attachment structure schematic diagrams of the Fig. 2 between superconduction high field magnetic control sputtering cathode and cathode bracket.
Specific implementation mode
Below in conjunction with the drawings and specific embodiments, the invention will be further described.
Fig. 1 is superconduction high field magnetic control sputtering cathode schematic diagram of the present invention.As shown in Figure 1, superconduction high field magnetic control sputtering cathode By superconducting coil 1, inner yoke 2, outer yoke 3, bottom yoke 4, the first glass steel plate washer 5, the second glass steel plate washer 6, Dewar end cap 7, Dewar pedestal 8, electrical conductor 9, glass reinforced plastic sleeve 10, big tetrafluoro washer 11, stainless steel washer 12, small tetrafluoro washer 13 and the moon Pole bracket 14 is constituted.Outer yoke 3 is located at the outside of inner yoke 2, and bottom yoke 4 is located at the bottom of inner yoke 2 and outer yoke 3, superconduction Coil 1 is installed between interior magnet yoke 2, outer yoke 3 and bottom yoke 4;Superconducting coil 1, inner yoke 2, outer yoke 3 and the bottom magnetic Yoke 4 is mounted in the space that Dewar end cap 7 and Dewar pedestal 8 surround.
Attachment structure schematic diagrams of the Fig. 2 between superconduction high field magnetic control sputtering cathode and cathode bracket.As shown in Fig. 2, big Tetrafluoro washer 11 is located at the lower section of Dewar pedestal 8, and stainless steel washer 12 is located at the lower section of big tetrafluoro washer 11, small tetrafluoro washer 13 Mounted on the lower section of stainless steel washer 12, cathode bracket 14 be mounted on the lower section of stainless steel washer 12, small tetrafluoro washer 13 it is outer Portion is used to support magnetic control sputtering cathode.
Since Dewar end cap 7 is negative high potential, superconducting coil 1 is low potential, therefore superconducting coil 1 and Dewar end cap 7 Between using the first glass steel plate washer 5 support and insulate, between superconducting coil 1 and bottom yoke 4 use the second glass steel plate washer 6 Support and insulation.Electrical conductor 9 is drawn by Dewar pedestal 8, and glass reinforced plastic sleeve 10 is sleeved on the outside of electrical conductor 9, electrical conductor 9 It is insulated using glass reinforced plastic sleeve 10 between Dewar pedestal 8.Dewar pedestal 8 uses vacuum interlayer structure or filling-foam material The structure of material is to reduce thermal losses, to carry out vacuum sealing using room temperature sealing structure.Since Dewar pedestal 8 is negative height electricity Position, stainless steel washer 12 are zero potential, and big tetrafluoro washer 11 is mounted between Dewar pedestal 8 and stainless steel washer 12, big by four 11 upper and lower surface of fluorine washer is provided with seal groove, and fitted seal circle is sealed and insulate.Big tetrafluoro washer 11, stainless steel washer 12, small tetrafluoro washer 13 stacks layer by layer, and is provided with screw hole, big tetrafluoro washer 11, stainless steel washer 12, small tetrafluoro washer 13 and Du It is fastened using fiberglass bolt or the metal bolts with glass fibre reinforced plastic insulating casing between watt pedestal 8.Due to stainless steel washer 12 with 14 same current potential of cathode bracket, be sealed using sealing ring and use general between stainless steel washer 12 and cathode bracket 14 Logical metal bolts fastening.
The insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode of the present invention are suitable for circular flat magnetron sputtering Cathode and rectangle plane magnetron sputtering cathode.

Claims (2)

1. a kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode, it is characterised in that:The superconduction high field The insulation and thermal insulation of magnetic control sputtering cathode and sealing structure by superconducting coil (1), inner yoke (2), outer yoke (3), bottom yoke (4), First glass steel plate washer (5), the second glass steel plate washer (6), Dewar end cap (7), Dewar pedestal (8), electrical conductor (9), glass Steel sleeve (10), big tetrafluoro washer (11), stainless steel washer (12), small tetrafluoro washer (13) and cathode bracket (14) are constituted; Outer yoke (3) is located at the outside of inner yoke (2), and bottom yoke (4) is located at the bottom of inner yoke (2) and outer yoke (3), superconducting coil (1) between installation interior magnet yoke (2), outer yoke (3) and bottom yoke (4);The superconducting coil (1), inner yoke (2), outer magnetic Yoke (3) and bottom yoke (4) are mounted in the space that Dewar end cap (7) and Dewar pedestal (8) surround;Big tetrafluoro washer (11) is located at The lower section of Dewar pedestal (8), stainless steel washer (12) are located at the lower section of big tetrafluoro washer (11), and small tetrafluoro washer (13) is mounted on The lower section of Dewar pedestal (8);Cathode bracket (14) be mounted on the lower section of stainless steel washer (12), small tetrafluoro washer (13) it is outer Portion is used to support magnetic control sputtering cathode;It is supported using the first glass steel plate washer (5) between superconducting coil (1) and Dewar end cap (7) And insulation, superconducting coil (1) and between bottom yoke (4) using the second glass steel plate washer (6) support and insulate, electrical conductor (9) it is insulated using glass reinforced plastic sleeve (10) between Dewar pedestal (8);Dewar pedestal (8) using vacuum interlayer structure or Filling-foam material, to reduce thermal losses, convenient for carrying out vacuum sealing using room temperature sealing structure.
2. the insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode as described in claim 1, it is characterised in that:Institute It is sealed and absolutely using big tetrafluoro washer (11) fitted seal circle between the Dewar pedestal (8) stated and stainless steel washer (12) Edge uses fiberglass spiral shell between big tetrafluoro washer (11), stainless steel washer (12), small tetrafluoro washer (13) and Dewar pedestal (8) Bolt or metal bolts with glass fibre reinforced plastic insulating casing are fastened;Using close between stainless steel washer (12) and cathode bracket (14) Seal is sealed and common metal bolt is used to fasten.
CN201710073591.9A 2017-02-10 2017-02-10 A kind of insulation and thermal insulation and sealing structure of superconduction high field magnetic control sputtering cathode Expired - Fee Related CN106801217B (en)

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CN108149209B (en) * 2017-12-26 2019-12-20 中国科学院电工研究所 Combined type magnetron sputtering cathode

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CA1184880A (en) * 1982-11-18 1985-04-02 Kovilvila Ramachandran Sputtering apparatus and method
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CN1245534C (en) * 2002-04-16 2006-03-15 北京科技大学 Non-magentic shielding type ferromagnetic target as sputter cathode
CN101719457B (en) * 2009-09-25 2012-05-30 中国科学院电工研究所 Superconducting coil-based high-intensity magnetic field magnetic control sputtering cathode
CN102420091B (en) * 2011-11-24 2014-07-30 中国科学院电工研究所 Composite magnetic control sputtering cathode

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Granted publication date: 20181113