CN106726895A

CN106726895A - A kind of Huanghua Pear eyeshield frost and preparation method thereof

Info

Publication number: CN106726895A
Application number: CN201611107799.XA
Authority: CN
Inventors: 蔡日芬; 刘小峰
Original assignee: Individual
Current assignee: Individual
Priority date: 2016-12-06
Filing date: 2016-12-06
Publication date: 2017-05-31

Abstract

The invention discloses Huanghua Pear eyeshield frost and preparation method thereof, the eyeshield frost mainly includes following component：Huanghua Pear extract, glycerine, saualane, trehalose, cetostearyl alcohol, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, ring five dimethyl silicone polymer, Sodium Hyaluronate, cetostearyl alcohol olive oleate, the smooth olive oleate of sorb, the smooth palmitate of sorb, cetanol palmitate, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers, hyaluronic acid, peach girder phenol, citric acid, sodium citrate, yellow glue original, Carbomer, tocopherol, RNA sodium, nano gold sol, nanosizing collagen, Microemulsified Acid emulsion.The Huanghua Pear extract that the present invention is used has functions that significantly to moisten, highlights, Firm so that obtained eyeshield frost have to eye skin compact, bright color, the effect of reparation.

Description

A kind of Huanghua Pear eyeshield frost and preparation method thereof

Technical field

The invention belongs to cosmetic technical field, and in particular to a kind of Huanghua Pear eyeshield frost and preparation method thereof.

Background technology

The raising of the requirement with people to quality of life, the maintenance to skin becomes the problem of people's growing interest. The aging of skin senescence especially eye skin is increasingly paid close attention to by people, therefore with moistening, improve microgroove effect Eyeshield frost has more wide market.

The A of CN 103599062 disclose a kind of agent of addition poly- polysaccharide Firm, beta glucan, hyaluronic acid, resveratrol etc. The eye cream of active component, with good Firm moisture-keeping function, but it is not notable in anti-ageing next aspect effect；CN 105287340 A discloses a kind of skin whitening, moisturizing eye cream, good penetrability, easily absorbs, and with enhancing Yanzhou skin elastic and improves irritated, lax existing As, but extract essence used is more, and technique is cumbersome.

Huanghua Pear scientific name dalbergia odorifera, originates in China Hainan province.Huanghua Pear possesses effect of life moisturizing, repair cell. Had shown that through modern expert's research, the material that Huanghua Pear contains can stimulate cytothesis and metabolism, skin-nourishing, have excellent Crease-resistant function, can promote skin tissue regeneration and enhancing skin elasticity.

In addition, according to authoritative department to the analysis shows of Hainan chrysanthemum pears leaf, it contains various isoflavones type components, mainly Composition is genistein and Biochanin A, and its content is determined by HPLC (high performance liquid chromatography) and is respectively 6.8% He 3.6%.Genistein and Biochanin A are the representative composition of soybean isoflavone, and documents and materials show, genistein There is weak estrogenic activity and antioxidation activity with Biochanin A, the estrogen-like of isoflavones can make women Skin smooth, exquisiteness, tender, high resilience, radiate the vigour of youth elegance, and its antioxidation activity can desalinate microgroove, and antioxygen maintenance has Beauty, the effect of anti-aging.

The content of the invention

For these reasons, applicant is by years of researches, there is provided a kind of Huanghua Pear eyeshield frost and preparation method thereof, Be characterized in effectively moistening eye, help improve it is dark yellow, uniform highlight near the eyes, profit bullet is tight near the eyes to tighten up pouch, smooth fine lines, order The effects such as cause, sliding thoroughly white children, fundamentally improve effect of the white anti-aging of the eyeshield；And fill up on the market without Huanghua Pear The blank of eyeshield frost.

The present invention provides following technical scheme：A kind of Huanghua Pear eyeshield frost, is composed of the following components in parts by weight：Chrysanthemum Pears extract 4%~9%, glycerine 1%~6%, saualane 2%~6%, trehalose 1.5%~3.5%, cetostearyl alcohol 1% ~5%, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 1%~6%, ring five dimethyl silicone polymer 0.1%~0.6%, Sodium Hyaluronate 0.1%~0.6%, the smooth olive oleate 0.6%~1.5%, sorb of cetostearyl alcohol olive oleate 1%~4%, sorb is smooth Palmitate 0.6%~1.2%, cetanol palmitate 0.6%~1.2%, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers 0.2%~1.8%, hyaluronic acid 0.01%~0.08%, peach girder phenol 0.001%~0.006%, citric acid 0.01%~ 0.05%th, sodium citrate 0.2%~0.8%, yellow glue original 0.1%~0.4%, Carbomer 0.1%~0.6%, tocopherol 0.03%~0.12%, RNA sodium 0.01%~0.05%, nano gold sol 0.5%~4%, nanosizing collagen 0.1%~ 0.6%th, Microemulsified Acid emulsion 0.2%~2%, balance of water.

Specifically, the eyeshield frost is composed of the following components in parts by weight：Huanghua Pear extract 5%~8%, glycerine 1% ~5%, saualane 2%~4%, trehalose 1.5%~2.5%, cetostearyl alcohol 1%~3%, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 1%~5%, ring five dimethyl silicone polymer 0.1%~0.5%, Sodium Hyaluronate 0.1%~0.5%, cetostearyl alcohol olive The smooth palmitate 0.6%~1.0%, cetanol of the smooth olive oleate 0.6%~1.0%, sorb of oleate 1%~3%, sorb Palmitate 0.6%~1.0%, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers 0.2%~1.5%, hyaluronic acid 0.01% ~0.05%, peach girder phenol 0.001%~0.003%, citric acid 0.01%~0.03%, sodium citrate 0.2%~0.5%, Huang Collagen 0.1%~0.2%, Carbomer 0.1%~0.2%, tocopherol 0.05%~0.09%, RNA sodium 0.01%~0.03%, Nano gold sol 1%~3%, nanosizing collagen 0.1%~0.5%, Microemulsified Acid emulsion 0.2%~1%, balance of water.

A kind of preparation method of Huanghua Pear eyeshield frost, comprises the steps of：

A, Jiang Shui, hyaluronic acid, yellow glue original, Carbomer, RNA sodium, glycerine, add water phase pot to be stirred after being heated to 50~60 DEG C Mix uniform, be pumped into vacuum emulsifying machine, homogeneous 5 minutes, be incubated standby；

B, by saualane, tocopherol, cetostearyl alcohol, peach girder phenol, trehalose, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, spermaceti it is hard The smooth olive oleate of lipidol olive oleate, sorb, cetanol palmitate, the smooth palmitate of sorb, the poly dimethyl silicon of ring five Oxygen alkane, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers, add oil phase pot, are stirred after being heated to 50~60 DEG C, are pumped into true In empty mulser；

C, start are uniformly mixed, and homogeneous 8~10 minutes adds water, tocopherol, Sodium Hyaluronate, starts cooling；

D, it is cooled to 35 DEG C, adds water, Huanghua Pear extract, nano gold sol, nanosizing collagen, micro emulsion yogurt Liquid, continues to stir；

E, the citric acid that will have been dissolved in advance, sodium citrate are added, and adjust pH to 6.5~7, homogeneous 1 minute, insulated and stirred 5 minutes；

F, the Huanghua Pear eyeshield frost steam sterilizing 5~8 minutes that pH will be adjusted；

It is g, the Huanghua Pear eyeshield frost after sterilizing is filling, get product.

Specifically, described Huanghua Pear extract is to be crushed Huanghua Pear trunk, branches and leaves, then by the Huang after crushing Flower pear tree is dry, branches and leaves are put into steam engine carries out steam extraction, and the extract of gained is Huanghua Pear extract.

Preferably, Huanghua Pear trunk, branches and leaves are cleaned by ultrasonic during supersonic wave cleaning machine is put into before being crushed, after dehydration again It is put into supersonic wave cleaning machine, adjustment supersonic frequency carries out ultrasonication treatment for 25000-30000Hz, is then placed in crushing Machine, grinding particle size is 0.1~1mm.

The invention has the advantages that：

Invention is cleaned using supersonic wave cleaning machine to chrysanthemum pears leaf, in can effectively removing blade Impurity, ultrasound makes liquid flow and produce ten hundreds of micro-bubbles, and the micro-bubble (cavitation nucleus) being present in liquid exists Vibrated in the presence of sound field, when acoustic pressure reaches certain value, bubble is increased rapidly, then closed suddenly, produced when bubble is closed Raw shock wave, produces thousands of atmospheric pressures around it, destroys insoluble dirt and them is scattered in cleaning fluid, can be with Remains of pesticide on part removal blade.Adjustment supersonic frequency, the acoustic streaming and shock wave produced using ultrasonic cavitation can cause Fuel factor and mechanism, so as to reach the effect of destruction cell membrane, without the other compositions contained in destruction cell, so that most Limits ground utilizes vitamin therein and other nutrients, is more easy to beneficial to absorption of human body.

The present invention is extracted using steam extraction technology to Huanghua Pear trunk, branches and leaves, because isoflavones is soluble in In weak polar solvent, in water solubility, the isoflavones of sequestered is substantially insoluble in water, by steam extraction technology using high Huanghua Pear trunk, branches and leaves that the steam of warm high pressure is constantly washed away after crushing, fully extract nutriment therein, obtained from Isoflavones of the Huanghua Pear extract rich in sequestered, is conducive to absorption of human body.

Using Huanghua Pear extract, the extract can stimulate cytothesis and metabolism to the technical scheme that the present invention is provided, Eye skin blood circulation can be promoted, Skin Cell regeneration and enhancing skin elasticity are promoted while nourishing eyes skin, there is excellent Different crease-resistant function.Adding the eyeshield frost after the extract can effectively moisten eye, help improve it is dark yellow, tighten up pouch, flat Sliding microgroove, order near the eyes profit bullet compact, children it is sliding thoroughly white, the effect with beauty, anti-aging, can make women skin smooth, exquisiteness, Tender, high resilience, radiate the vigour of youth elegance.The tocopherol and RNA sodium for incorporating can reach reduction eye with the extract components matching Portion's wrinkle generation, keeps skin pattern careful flexible, prevents the effect of skin ageing.

The present invention constitutes a kind of very unique emulsified body using vegetable oil and modified vegetable oil plus cetostearyl alcohol System, belongs to natural environmental-protective quasi-grease emulsification system.The cetostearyl alcohol olive olein of use have height moisture retention and into Film, can effective slow-release, make eyeshield frost permanent effectively, skin is preferably absorbed；Cetostearyl alcohol can To suppress greasy feeling, raw material stickiness is reduced, make that skin is submissive, smooth, moistening is without glutinous greasy.

The peach girder phenol that the present invention is used is natural antiseptic agent, not only assists in antibacterial, moreover it is possible to improve acne small pox, can be kept Eye skin is smooth, fine and smooth, tender.

The present invention not only facilitates the stabilization of the nm of gold for improving generation using the strong flavones synthesis nm of gold of inoxidizability Property, additionally it is possible to the nm of gold of Surface coating flavones biomembrane and regular arrangement is generated, has very strong to Huanghua Pear extract Suction-operated, while the property of adsorbed material will not be changed；Nano gold sol has high surface energy, easily reunites, and quiet Free settling during putting, adds nano-collagen that the absorption protective layer of similar chelate can be formed in gold surface wherein, Due to the steric effect of protective layer, the internuclear mutual collision of Jin Jing can be suppressed and produce coagulation, so that nano gold sol stabilization, protects The stabilization of the obtained eyeshield frost emulsion of card；Microemulsified Acid emulsion can adjust skin acid balance and keep skin moisture, soften epidermis Cuticula, can be such that nano gold sol, nanosizing collagen and Huanghua Pear extract is absorbed through skin；Nm of gold itself With promoting cell propagation, the function of enhancing metabolism effectively to reduce microgroove into eye, skin-tightening is kept to have Elasticity.

The inventors discovered that Huanghua Pear extract, nano-Au solution, nanosizing collagen and Microemulsified Acid emulsion it Between there is synergy well, interact each other, mutually encourage, and be with cosmetic base between several components Compatible, can reach makes women skin smooth, exquisiteness, tender, high resilience, and radiate the vigour of youth elegance, can desalinate microgroove, finally reaches To beauty, the effect of anti-aging.

Specific embodiment,

With reference to specific embodiment, claim of the invention is further described in detail, but not structure Into any limitation of the invention, the limited number of time modification that anyone is made within the scope of the invention as claimed, still in the present invention Claims.

Embodiment 1：Eyeshield of the present invention frost is by as follows into being grouped into：Huanghua Pear extract 6.0g, glycerine 3.0g, spiny dogfish Alkane 2.0g, trehalose 1.5g, cetostearyl alcohol 1.0g, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 2.5g, ring five dimethyl silicone polymer 0.2g, Sodium Hyaluronate 0.2g, cetostearyl alcohol olive oleate 1.6g, the smooth olive oleate 0.6g of sorb, the smooth palm of sorb Acid esters 0.6g, cetanol palmitate 0.6g, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers 0.5g, hyaluronic acid 0.02g, Peach girder phenol 0.001g, citric acid 0.01g, sodium citrate 0.3g, yellow glue original 0.15g, Carbomer 0.1g, tocopherol 0.06g, RNA Sodium 0.01g, nano gold sol 1.0g, nanosizing collagen 0.1g, Microemulsified Acid emulsion 0.4g, balance of water.

The preparation method of eyeshield frost is：

A, by water 17.0g, hyaluronic acid 0.02g, yellow glue original 0.15g, Carbomer 0.1g, RNA sodium 0.01g, glycerine 3.0g, Add water phase pot to be stirred after being heated to 50~60 DEG C, be pumped into vacuum emulsifying machine, homogeneous 5 minutes, be incubated standby；

B, by saualane 2.0g, tocopherol 0.04g, cetostearyl alcohol 1.0g, peach girder phenol 0.001g, trehalose 1.5g, pungent Acid/certain herbaceous plants with big flowers acid glycerol three ester 2.5g, cetostearyl alcohol olive oleate 1.6g, the smooth olive oleate 0.6g of sorb, the smooth palm of sorb Acid esters 0.6g, cetanol palmitate 0.6g, ring five dimethyl silicone polymer 0.2g, acryloyldimethyl ox naphthenic acid ammonium/VP are common Polymers 0.5g, adds oil phase pot, is stirred after being heated to 50~60 DEG C, is pumped into vacuum emulsifying machine；

C, start are uniformly mixed, and homogeneous 8~10 minutes adds water 6.5, tocopherol 0.02g, Sodium Hyaluronate 0.2g, starts cooling；

D, it is cooled to 35 DEG C, adds water 6.5g, Huanghua Pear extract 6.0g, nano gold sol 1g, nanosizing collagen 0.1g, Microemulsified Acid emulsion 0.4g, continue to stir；

E, citric acid 0.01g, the sodium citrate 0.3g that will dissolve in advance are added, and adjust PH to 6.5~7,1 point of homogeneous Clock, insulated and stirred 5 minutes；

Embodiment 2：Eyeshield of the present invention frost is by as follows into being grouped into：Huanghua Pear extract 7.0g, glycerine 4.0g, spiny dogfish Alkane 3.0g, trehalose 2.0g, cetostearyl alcohol 2.0g, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 3.0g, ring five dimethyl silicone polymer 0.3g, Sodium Hyaluronate 0.3g, cetostearyl alcohol olive oleate 2.0g, the smooth olive oleate 0.8g of sorb, the smooth palm of sorb Acid esters 0.8g, cetanol palmitate 0.8g, acryloyldimethyl ox naphthenic acid ammonium/VP copolymer 1s .0g, hyaluronic acid 0.03g, Peach girder phenol 0.001g, citric acid 0.02g, sodium citrate 0.4g, yellow glue original 0.15g, Carbomer 0.1g, tocopherol 0.07g, RNA Sodium 0.02g, nano gold sol 2g, nanosizing collagen 0.3g, Microemulsified Acid emulsion 0.6g, balance of water.

The preparation method of eyeshield frost is：

A, by water 20.0g, hyaluronic acid 0.03g, yellow glue original 0.15g, Carbomer 0.1g, RNA sodium 0.02g, glycerine 4.0g, Add water phase pot to be stirred after being heated to 50~60 DEG C, be pumped into vacuum emulsifying machine, homogeneous 5 minutes, be incubated standby；

B, by saualane 3g, tocopherol 0.04g, cetostearyl alcohol 2.0g, peach girder phenol 0.001g, trehalose 2.0g, octanoic acid/ Certain herbaceous plants with big flowers acid glycerol three ester 3.0g, cetostearyl alcohol olive oleate 2.0g, the smooth olive oleate 0.8g of sorb, the smooth palmitate of sorb 0.8g, cetanol palmitate 0.8g, ring five dimethyl silicone polymer 0.3g, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers 1.0g, adds oil phase pot, is stirred after being heated to 50~60 DEG C, is pumped into vacuum emulsifying machine；

C, start are uniformly mixed, and homogeneous 8~10 minutes adds water 8.0g, tocopherol 0.03g, Sodium Hyaluronate 0.03g, starts cooling；

D, it is cooled to 35 DEG C, adds water 8.0g, Huanghua Pear extract 7.0g, nano gold sol 2g, nanosizing collagen 0.3g, Microemulsified Acid emulsion 0.6g, continue to stir；

E, citric acid 0.02g, the sodium citrate 0.4g that will dissolve in advance are added, and adjust PH to 6.5~7,1 point of homogeneous Clock, insulated and stirred 5 minutes；

Comparative example 1：Lack nano gold sol, nanosizing collagen, Microemulsified Acid emulsion components relative to embodiment 1.

Comparative example 2：Lack nano gold sol, Microemulsified Acid emulsion components relative to embodiment 1.

Comparative example 3：Lack nanosizing collagen, Microemulsified Acid emulsion components relative to embodiment 1.

Comparative example 4：Lack nano gold sol, nanosizing collagen component relative to embodiment 1.

Comparative example 5:Lack nano gold sol component relative to embodiment 1.

Comparative example 6:Lack nanosizing collagen component relative to embodiment 1.

Comparative example 7:Lack Microemulsified Acid emulsion components relative to embodiment 1.

Test method：Healthy women volunteer 100, at 25~45 years old age, informs that volunteer cleans face sooner or later daily Afterwards eyeshield frost is smeared according to correct method.

Volunteer is satisfied with number and see the table below for experiment effect：

After on probation, excitant and allergic phenomena are not found.

As can be known from the table data, obtained in embodiment 1,2 eyeshield frost its Firm anti-wrinkle effect apparently higher than comparative example 1,2, 3.It follows that add obtained in Huanghua Pear extract, nano gold sol, nanosizing collagen and Microemulsified Acid emulsion simultaneously Eyeshield frost can improve eye skin circulation with the crease-resistant effect of good Firm, improve eye skin vigor, make to moisten near the eyes Bullet compacts, at the same improve it is dark yellow, uniformly highlight near the eyes, eye skin is effectively moistened.

It should be noted last that, above specific embodiment is merely to illustrate technical scheme and unrestricted, Although being described in detail to the present invention with reference to case study on implementation, it will be understood by those within the art that, can be to this The technical scheme of invention is modified or equivalent, and without deviating from the spirit and scope of technical solution of the present invention, it all should Cover in the middle of scope of the presently claimed invention.

Claims

1. a kind of Huanghua Pear eyeshield is white, it is characterised in that the eyeshield frost is composed of the following components in parts by weight：Huanghua Pear is extracted Liquid 4%~9%, glycerine 1%~6%, saualane 2%~6%, trehalose 1.5%~3.5%, cetostearyl alcohol 1%~5%, Octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 1%~6%, ring five dimethyl silicone polymer 0.1%~0.6%, Sodium Hyaluronate 0.1%~ 0.6%th, the smooth smooth palmitic acid of olive oleate 0.6%~1.5%, sorb of cetostearyl alcohol olive oleate 1%~4%, sorb Ester 0.6%~1.2%, cetanol palmitate 0.6%~1.2%, acryloyldimethyl ox naphthenic acid ammonium/VP copolymers 0.2% ~1.8%, hyaluronic acid 0.01%~0.08%, peach girder phenol 0.001%~0.006%, citric acid 0.01%~0.05%, lemon Lemon acid sodium 0.2%~0.8%, yellow glue original 0.1%~0.4%, Carbomer 0.1%~0.6%, tocopherol 0.03%~ 0.12%th, RNA sodium 0.01%~0.05%, nano gold sol 0.5%~4%, nanosizing collagen 0.1%~0.6%, micro- Lactic acid emulsion 0.2%~2%, balance of water.

2. a kind of Huanghua Pear eyeshield according to claim 1 is white, it is characterised in that the eyeshield frost is by following weight portion Into being grouped into：Huanghua Pear extract 5%~8%, glycerine 1%~5%, saualane 2%~4%, trehalose 1.5%~2.5%, Cetostearyl alcohol 1%~3%, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 1%~5%, ring five dimethyl silicone polymer 0.1%~0.5%, The smooth olive oleate 0.6% of Sodium Hyaluronate 0.1%~0.5%, cetostearyl alcohol olive oleate 1%~3%, sorb~ 1.0%th, the smooth palmitate 0.6%~1.0% of sorb, cetanol palmitate 0.6%~1.0%, acryloyldimethyl Niu Huan Sour ammonium/VP copolymers 0.2%~1.5%, hyaluronic acid 0.01%~0.05%, peach girder phenol 0.001%~0.003%, lemon Acid 0.01%~0.03%, sodium citrate 0.2%~0.5%, yellow glue original 0.1%~0.2%, Carbomer 0.1%~0.2%, Tocopherol 0.05%~0.09%, RNA sodium 0.01%~0.03%, nano gold sol 1%~3%, nanosizing collagen 0.1%~0.5%, Microemulsified Acid emulsion 0.2%~1%, balance of water.

3. the preparation method of a kind of Huanghua Pear eyeshield frost, it is characterised in that comprise the steps of：

A, Jiang Shui, hyaluronic acid, yellow glue original, Carbomer, RNA sodium, glycerine, stirring is equal after adding water phase pot to be heated to 50~60 DEG C It is even, it is pumped into vacuum emulsifying machine, homogeneous 5 minutes, it is incubated standby；

B, by saualane, tocopherol, cetostearyl alcohol, peach girder phenol, trehalose, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, cetostearyl alcohol The smooth olive oleate of olive oleate, sorb, cetanol palmitate, the smooth palmitate of sorb, ring five dimethyl silicone polymer, Acryloyldimethyl ox naphthenic acid ammonium/VP copolymers, adds oil phase pot, is stirred after being heated to 50~60 DEG C, is pumped into vacuum breast In change machine；

D, it is cooled to 35 DEG C, adds water, Huanghua Pear extract, nano gold sol, nanosizing collagen, Microemulsified Acid emulsion, after It is continuous to stir；

E, the citric acid that will have been dissolved in advance, sodium citrate are added, and adjust pH to 6.5~7, homogeneous 1 minute, 5 points of insulated and stirred Clock；

4. a kind of preparation method of Huanghua Pear eyeshield frost according to claim 3, it is characterised in that described Huanghua Pear extraction It is to be crushed Huanghua Pear trunk, branches and leaves to take liquid, and then the Huanghua Pear trunk after crushing, branches and leaves are put into steam engine and are steamed Vapour is extracted, and the extract of gained is Huanghua Pear extract.

5. the preparation method of a kind of Huanghua Pear eyeshield frost according to claim 4, it is characterised in that Huanghua Pear trunk, branch Leaf is cleaned by ultrasonic during supersonic wave cleaning machine is put into before being crushed, and is placed again into supersonic wave cleaning machine after dehydration, adjustment ultrasound Frequency carries out ultrasonication treatment for 25000-30000Hz, is then placed in disintegrating machine, and grinding particle size is 0.1~1mm.