CN106723302B - Tobacco tar and preparation method thereof - Google Patents
Tobacco tar and preparation method thereof Download PDFInfo
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- CN106723302B CN106723302B CN201611195143.8A CN201611195143A CN106723302B CN 106723302 B CN106723302 B CN 106723302B CN 201611195143 A CN201611195143 A CN 201611195143A CN 106723302 B CN106723302 B CN 106723302B
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- perfume base
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A24F47/008—
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Abstract
The present invention provides a kind of tobacco tar, including tobacco perfume base, tobacco rectifying liquid and organic solvent, the tobacco perfume base include heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base, phenols perfume base and aldehydes perfume base.The tobacco tar of the present invention can simulate the suction mouthfeel of reduction cigarette.The present invention also provides the preparation methods of the tobacco tar.
Description
Technical field
The present invention relates to electronic cigarette technical field more particularly to the preparation methods of a kind of tobacco tar and the tobacco tar.
Background technology
Traditional cigarette generates a large amount of aroma components in combustion, and consumer generates it certain dependence.Electronic cigarette
By heating tobacco tar, its atomization is set to generate flue gas, to simulate the mouthfeel of traditional cigarette.However, existing tobacco tar is difficult to simulate
Go out the fragrance of traditional cigarette, can not restore traditional cigarette sucks impression.
Invention content
The main purpose of the present invention is to provide a kind of tobacco tar, it is desirable to provide can simulate the tobacco tar of traditional cigarette fragrance.
To achieve the above object, tobacco tar provided by the invention, including tobacco perfume base, tobacco rectifying liquid and organic solvent, institute
It includes heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base, phenols perfume base and aldehydes perfume base to state tobacco perfume base.
Preferably, the tobacco perfume base includes the heterocyclic perfume base, mass fraction that mass fraction is 0.116~0.323 part
For 0.166~0.769 part of alcohols perfume base, the acids perfume base that mass fraction is 0.08~0.375 part, mass fraction 0.021-
0.069 part of ketone perfume base, the phenols perfume base that mass fraction is 0.401~1.466 part and mass fraction are 0.111~0.253
The aldehydes perfume base of part.
Preferably, the heterocyclic perfume base contains 2- methylpyrazines, 2,3- dimethyl pyrazines, 2- acetyl group pyrazine, 2,3,
At least one of 5,6- Tetramethylpyrazines, pyridine, 2- acetyl pyrroles.
Preferably, the acids perfume base contains at least one of glacial acetic acid, propionic acid, butyric acid.
Preferably, the alcohols perfume base contains at least one of acetylmethyl carbinol, furfuryl alcohol and n-butanol.
Preferably, the ketone perfume base contains furanone and/or too white ketone.
Preferably, the phenols perfume base contains at least one in guaiacol, ethylmaltol and 4-ethyl guaiacol
Kind.
Preferably, the aldehydes perfume base contains vanillin propylene glycol acetal, anisic aldehyde, cinnamic aldehyde, diethanol acetal, ocean
At least one of jasminal propylene glycol acetal and furfural.
Preferably, the mass percent of the tobacco perfume base is 3~30%, and the mass percent of the tobacco rectifying liquid is
1~20%, the mass percent of the organic solvent is 50~96%.
The present invention also provides a kind of preparation methods of tobacco tar, include the following steps：
Heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base, phenols perfume base and aldehydes perfume base are dissolved in the third two
Tobacco perfume base is made in alcohol；
Cocoa tincture is coated on tobacco leaf, after being refined, toasting, offal is made in crushing, heats the offal, impregnates extraction
The offal obtains tobacco rectifying liquid；
The tobacco perfume base, the tobacco rectifying liquid are dissolved in organic solvent, and filtered, filtrate is obtained, it is as described
Tobacco tar.
Make one pleasant comprising what is generated in a large amount of traditional cigarette combustion processes in the tobacco rectifying liquid of technical solution of the present invention
Aroma component, can be farthest in electronic cigarette aspiration procedure comprising a certain proportion of tobacco rectifying liquid in tobacco tar
Restore the fragrance of traditional cigarette；And the addition of tobacco perfume base can then modify the flue gas that tobacco tar atomization generates so that suck mouthfeel
It is more mellow and fuller, fine and smooth, submissive, wherein heterocyclic perfume base has strong burnt odor and baking fragrant, and alcohols perfume base has the pure and fresh fragrance of a flower
And fruity, fresh and sweet note can be brought, flue gas is made to have fine and smooth sense, acids perfume base that can neutralize the alkaline components in flue gas, subtract
Flue gas can be modified, augment and be coordinated to few stimulation, ketone perfume base, and phenols perfume base can generate burnt sweet tea, burnt odor breath, aldehydes perfume base
With the breath that plant is pure and fresh, improve pleasant impression.
Specific implementation mode
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is general
The every other embodiment that logical technical staff is obtained without creative efforts belongs to what the present invention protected
Range.
In addition, the technical solution between each embodiment can be combined with each other, but must be with ordinary skill
Personnel can be implemented as basis, will be understood that this technical side when the combination of technical solution appearance is conflicting or cannot achieve
The combination of case is not present, also not the present invention claims protection domain within.
The present invention provides a kind of tobacco tar, and the tobacco tar includes tobacco perfume base, tobacco rectifying liquid and organic solvent, the tobacco
Perfume base includes heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base, phenols perfume base and aldehydes perfume base.
Further, organic solvent includes propylene glycol and glycerine, and the mass ratio of the two is 4~7:6~3, wherein the third two
Alcohol is medicinal grade propylene glycol, and glycerine is pharmaceutical grade vegetable glycerides.Propylene glycol can effectively dissolve tobacco perfume base and tobacco rectifying liquid,
And glycerine can generate spray during tobacco tar heats, and increase the humidity of flue gas.
Make one pleasant comprising what is generated in a large amount of traditional cigarette combustion processes in the tobacco rectifying liquid of technical solution of the present invention
Aroma component, can be farthest in electronic cigarette aspiration procedure comprising a certain proportion of tobacco rectifying liquid in tobacco tar
Restore the fragrance of traditional cigarette；Tobacco perfume base by a certain proportion of heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base,
Phenols perfume base and aldehydes perfume base are allocated, and the addition of tobacco perfume base can modify the flue gas that tobacco tar atomization generates so that suck
Mouthfeel is more mellow and fuller, fine and smooth, submissive.Wherein, heterocyclic perfume base has strong burnt odor and baking fragrant, and alcohols perfume base has pure and fresh
The fragrance of a flower and fruity can bring fresh and sweet note, and flue gas is made to have a fine and smooth sense, acids perfume base can neutralize the alkalinity in flue gas at
Point, stimulation is reduced, flue gas can be modified, augment and be coordinated to ketone perfume base, and phenols perfume base can generate burnt sweet tea, burnt odor breath, aldehyde
The breath that class perfume base has plant pure and fresh improves pleasant impression.
The tobacco perfume base includes the heterocyclic perfume base that mass fraction is 0.116~0.323 part, mass fraction 0.166
~0.769 part of alcohols perfume base, the acids perfume base that mass fraction is 0.08~0.375 part, mass fraction are 0.021-0.069 parts
Ketone perfume base, the phenols perfume base that mass fraction is 0.401~1.466 part and aldehydes that mass fraction is 0.111~0.253 part
Perfume base.
Include a certain proportion of heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone in technical solution of the present invention tobacco perfume base
Class perfume base, phenols perfume base and aldehydes perfume base can preferably modify the fragrance of tobacco tar generation, keep its mouthfeel more mellow and fuller, submissive.Often
More natural, strong tobacco aroma can be generated when there is unique fragrance when a kind of perfume base exclusive use, and being applied in combination.
The heterocyclic perfume base contains 2- methylpyrazines, 2,3- dimethyl pyrazines, 2- acetyl group pyrazine, 2,3,5,6- tetramethyls
At least one of base pyrazine, pyridine, 2- acetyl pyrroles.
Technical solution of the present invention pyrazine compounds, as 2- methylpyrazines, 2,3- dimethyl pyrazines, 2- acetyl group pyrazine,
Tetramethylpyradine is the important flavor component of burley tobaccos, the substance is added in tobacco tar, being capable of more preferable simulation
The fragrance of cigarette.Wherein 2- acetyl group pyrazine has strong cream puffed rice fragrance, Tetramethylpyradine to have white rib
There is flue-cured tobacco body note, 2- acetyl pyrroles to have aromatic aldehydes like fragrance for the fragrance of cigarette, pyridine.
The acids perfume base contains at least one of glacial acetic acid, propionic acid, butyric acid.
Technical solution of the present invention glacial acetic acid, propionic acid, butyric acid can neutralize the alkaline components in flue gas, reduce stimulation so that
The mouthfeel milder of tobacco tar.
The alcohols perfume base contains at least one of acetylmethyl carbinol, furfuryl alcohol and n-butanol.
Technical solution of the present invention acetylmethyl carbinol, furfuryl alcohol and n-butanol have the pure and fresh fragrance of a flower and fruity, being capable of band
Carry out fresh and sweet note, the flue gas that tobacco tar atomization generates is made to have fine and smooth sense.
The ketone perfume base contains furanone and/or too white ketone.
Flue gas can be modified, augment and be coordinated to technical solution of the present invention furanone and Tai Bai ketone.
The phenols perfume base contains at least one of guaiacol, ethylmaltol and 4-ethyl guaiacol.
The ethylmaltol of technical solution of the present invention can generate burnt sweet tea, and ethylmaltol can generate burnt odor, sootiness perfume.
The aldehydes perfume base contains vanillin propylene glycol acetal, anisic aldehyde, cinnamic aldehyde, diethanol acetal, heliotropin
At least one of propylene glycol acetal and furfural.
Vanillin propylene glycol acetal, anisic aldehyde, cinnamic aldehyde, diethanol acetal, the heliotropin of technical solution of the present invention
The breath that propylene glycol acetal and furfural have plant pure and fresh, improves pleasant impression.
The mass percent of the tobacco perfume base is 3~30%, the mass percent of the tobacco rectifying liquid is 1~
20%, the mass percent of the organic solvent is 50~96%.
Technical solution of the present invention tobacco tar is formulated in appropriate proportions by tobacco perfume base, tobacco rectifying liquid and organic solvent,
Keep its concentration suitable, can obtain and preferably suck mouthfeel.
The present invention also provides a kind of preparation methods of tobacco tar, include the following steps：
Heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base, phenols perfume base and aldehydes perfume base are dissolved in the third two
Tobacco perfume base is made in alcohol；
Cocoa tincture is coated on tobacco leaf, after being refined, toasting, offal is made in crushing, heats the offal, impregnates extraction
The offal obtains tobacco rectifying liquid；
The tobacco perfume base, the tobacco rectifying liquid are dissolved in the organic solvent, and filtered, obtains filtrate, as
The tobacco tar.
Further, each component mass fraction is as follows in tobacco perfume base：Heterocyclic perfume base is 0.116~0.323 part, alcohols
Perfume base is 0.166~0.769 part, acids perfume base is 0.08~0.375 part, ketone perfume base is 0.021-0.069 parts, phenols perfume base
Be 0.111~0.253 part for 0.401~1.466 part, aldehydes perfume base, in addition, further include as solvent propylene glycol be 75~98
Part；Turkish tobaccos, burley tobaccos, flue-cured tobacco, Dark sun-cured, Sun cured tobacco one of which are chosen, is with the mass ratio with cocoa tincture by its tobacco leaf
1:0.5~4, after being coated with cocoa tincture on tobacco leaf by tobacco leaf in constant temperature and humidity under the conditions of carry out alcoholization 1~3 hour, and be placed on
It is 12.5% to be dried to its moisture under the conditions of 60~100 DEG C in baking oven；Tobacco leaf is ground into offal with pulverizer again, is claimed
Several offals are taken, are placed in the container for being connected with condensation reflux unit, are heated to 200~450 DEG C, and continue 45~
90min is cooled to room temperature, and obtains tobacco rectifying object；Ethyl alcohol with a concentration of 70~95% and gained tobacco rectifying amount of substance ratio
It is 1~3:Mixture is made in 1 ratio, and after extraction 12~for 24 hours is impregnated to it, suction filtration obtains tobacco rectifying liquid.
Technical solution of the present invention is coated with cocoa tincture in tobacco leaf, and cocoa tincture can play as a kind of fragrance and increase tobacco leaf gas
The effect of the concentration of taste and thick and solid degree, abundant fragrance further crushes tobacco leaf, Titian, extraction, makes in subsequent processes
It obtains the intrinsic aroma component of tobacco to release, and is mixed with cocoa tincture, substantially have class after the tobacco rectifying liquid mist of preparation
Like the breath of cigarette；And tobacco perfume base is added in tobacco rectifying liquid, the fragrance of tobacco tar can be modified.
Embodiment one：
Tobacco rectifying liquid is prepared to include the following steps：
The tobacco leaf for choosing Turkish tobaccos, weighs tobacco leaf and cocoa tincture respectively, and it is 1 to make its mass ratio:0.5, on tobacco leaf uniformly
It is coated with cocoa tincture, tobacco leaf is then carried out to alcoholization 1 hour under the conditions of constant temperature and humidity, and is placed in baking oven under the conditions of 60 DEG C
It is 12.5% to be dried to its moisture；
The tobacco leaf obtained through above-mentioned processing is ground into offal with pulverizer, weighs several offals, is placed in and is connected with condensation
In the round-bottomed flask of reflux, 200 DEG C are heated to, and continue 45min, be cooled to room temperature, obtains tobacco rectifying object；
It is 1 with a concentration of 70% ethyl alcohol and gained tobacco rectifying amount of substance ratio:Mixture is made in 1 ratio, is soaked to it
After bubble extraction 12h, suction filtration obtains tobacco rectifying liquid.
Tobacco tar is prepared to include the following steps：
It is as follows to weigh each component mass fraction：Heterocyclic perfume base is 0.116 part, alcohols perfume base is 0.166 part, acids perfume base is
0.08 part, ketone perfume base be 0.021 part, phenols perfume base is 0.401 part, aldehydes perfume base is 0.111 part, concrete component is as shown in the table：
Each component is dissolved in propylene glycol, tobacco perfume base is obtained；
By medicinal grade propylene glycol, pharmaceutical grade vegetable glycerides with 7:Organic solvent is made in 3 mass ratio；
With mass fraction will be respectively 3% by tobacco rectifying liquid, tobacco perfume base, organic solvent made from above-mentioned steps,
96%, 1% mixing, and with the strainer filtering of 250 mesh, filtrate is obtained, tobacco tar as obtained.
Embodiment two：
Tobacco rectifying liquid is prepared to include the following steps：
The tobacco leaf for choosing Turkish tobaccos, weighs tobacco leaf and cocoa tincture respectively, and it is 1 to make its mass ratio:4, it is uniformly applied on tobacco leaf
Tobacco leaf is then carried out alcoholization 3 hours by cloth cocoa tincture under the conditions of constant temperature and humidity, and is placed in baking oven under the conditions of 100 DEG C
It is 12.5% to be dried to its moisture；
The tobacco leaf obtained through above-mentioned processing is ground into offal with pulverizer, weighs several offals, is placed in and is connected with condensation
In the round-bottomed flask of reflux, 450 DEG C are heated to, and continue 45min, be cooled to room temperature, obtains tobacco rectifying object；
It is 3 with a concentration of 95% ethyl alcohol and gained tobacco rectifying amount of substance ratio:Mixture is made in 1 ratio, is soaked to it
After bubble extraction for 24 hours, suction filtration obtains tobacco rectifying liquid.
Tobacco tar is prepared to include the following steps：
It is as follows to weigh each component mass fraction：Heterocyclic perfume base is 0.323 part, alcohols perfume base is 0.769 part, acids perfume base
For 0.375 part, ketone perfume base be 0.069 part, phenols perfume base is 1.466 parts, aldehydes perfume base is 0.253 part, and concrete component is as follows
Shown in table：
Each component is dissolved in propylene glycol, tobacco perfume base is obtained；
By medicinal grade propylene glycol, pharmaceutical grade vegetable glycerides with 4:Organic solvent is made in 3 mass ratio；
With mass fraction will be respectively 30% by tobacco rectifying liquid, tobacco perfume base, organic solvent made from above-mentioned steps,
50%, 20% mixing, and with the strainer filtering of 250 mesh, filtrate is obtained, tobacco tar as obtained obtains tobacco tar.
Embodiment three：
Tobacco rectifying liquid is prepared to include the following steps：
The tobacco leaf for choosing Turkish tobaccos, weighs tobacco leaf and cocoa tincture respectively, and it is 1 to make its mass ratio:2, it is uniformly applied on tobacco leaf
Tobacco leaf is then carried out alcoholization 2 hours by cloth cocoa tincture under the conditions of constant temperature and humidity, and is placed in baking oven and is dried under the conditions of 80 DEG C
It is 12.5% to do to its moisture；
The tobacco leaf obtained through above-mentioned processing is ground into offal with pulverizer, weighs several offals, is placed in and is connected with condensation
In the round-bottomed flask of reflux, 300 DEG C are heated to, and continue 60min, be cooled to room temperature, obtains tobacco rectifying object；
It is 2 with a concentration of 80% ethyl alcohol and gained tobacco rectifying amount of substance ratio:Mixture is made in 1 ratio, is soaked to it
After bubble extraction 16h, suction filtration obtains tobacco rectifying liquid.
Tobacco tar is prepared to include the following steps：
It is as follows to weigh each component mass fraction：Heterocyclic perfume base is 0.243 part, alcohols perfume base is 0.510 part, acids perfume base
For 0.270 part, ketone perfume base be 0.550 part, phenols perfume base is 1.005 parts, aldehydes perfume base is 0.151 part, and concrete component is as follows
Shown in table：
Each component is dissolved in propylene glycol, tobacco perfume base is obtained；
By medicinal grade propylene glycol, pharmaceutical grade vegetable glycerides with 7:Organic solvent is made in 3 mass ratio；
With mass fraction will be respectively 3% by tobacco rectifying liquid, tobacco perfume base, organic solvent made from above-mentioned steps,
50%, 1% mixing, and with the strainer filtering of 250 mesh, filtrate is obtained, tobacco tar as obtained.
It these are only the preferred embodiment of the present invention, be not intended to limit the scope of the invention, it is every to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (8)
1. a kind of preparation method of tobacco tar, which is characterized in that include the following steps：
Heterocyclic perfume base, alcohols perfume base, acids perfume base, ketone perfume base, phenols perfume base and aldehydes perfume base are dissolved in propylene glycol, made
Tobacco perfume base is obtained, the ketone perfume base contains furanone and/or too white ketone；
Cocoa tincture is coated on tobacco leaf, after being refined, toasting, offal is made in crushing, heats the offal, is heated to
200~450 DEG C, and continue 45~90min, it is cooled to room temperature, impregnates and extract the offal, obtain tobacco rectifying liquid；
The tobacco perfume base, the tobacco rectifying liquid are dissolved in organic solvent, and filtered, filtrate is obtained, the as described tobacco tar.
2. the preparation method of tobacco tar as described in claim 1, which is characterized in that the tobacco perfume base includes that mass fraction is
0.116~0.323 part of heterocyclic perfume base, the alcohols perfume base that mass fraction is 0.166~0.769 part, mass fraction 0.08
~0.375 part of acids perfume base, the ketone perfume base that mass fraction is 0.021-0.069 parts, mass fraction are 0.401~1.466
The aldehydes perfume base that the phenols perfume base and mass fraction of part are 0.111~0.253 part.
3. the preparation method of tobacco tar as described in claim 1, which is characterized in that the heterocyclic perfume base contains 2- methyl pyrroles
In piperazine, 2,3- dimethyl pyrazines, 2- acetyl group pyrazine, Tetramethylpyradine, pyridine and 2- acetyl pyrroles at least
It is a kind of.
4. the preparation method of tobacco tar as described in claim 1, which is characterized in that the acids perfume base contain glacial acetic acid, propionic acid,
And at least one of butyric acid.
5. the preparation method of tobacco tar as described in claim 1, which is characterized in that the alcohols perfume base contains acetylmethyl original
At least one of alcohol, furfuryl alcohol and n-butanol.
6. the preparation method of tobacco tar as described in claim 1, which is characterized in that the phenols perfume base contains guaiacol, second
At least one of base maltol and 4-ethyl guaiacol.
7. the preparation method of tobacco tar as described in claim 1, which is characterized in that the aldehydes perfume base contains vanillic aldehyde propylene glycol
At least one of acetal, anisic aldehyde, cinnamic aldehyde, diethanol acetal, heliotropin propylene glycol acetal and furfural.
8. the preparation method of tobacco tar as described in claim 1, which is characterized in that the mass percent of the tobacco perfume base is 3
~30%, the mass percent of the tobacco rectifying liquid is 1~20%, the mass percent of the organic solvent is 50~
96%.
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| CN108813742B (en) * | 2018-09-07 | 2020-09-22 | 云南中烟工业有限责任公司 | Electronic cigarette oil with cocoa baking fragrance and preparation method thereof |
| CN109007981A (en) * | 2018-09-10 | 2018-12-18 | 深圳市新宜康科技股份有限公司 | A kind of liquid nicotine salt and preparation method thereof |
| CN109363255A (en) * | 2018-12-19 | 2019-02-22 | 深圳昱朋科技有限公司 | Method, electronic cigarette oil additive and the electronics tobacco tar of electronic cigarette oil additive are prepared using waste tobacco leaf |
| CN111449270B (en) * | 2020-03-12 | 2022-04-26 | 深圳瀚星翔科技有限公司 | Smoke softener, electronic cigarette tobacco tar and preparation method thereof |
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| US6863074B2 (en) * | 2002-08-30 | 2005-03-08 | Philip Morris Usa Inc. | Cigarette filters comprising unfunctionalized porous polyaromatic resins for removing gas phase constituents from mainstream tobacco smoke |
| CN1201682C (en) * | 2002-12-20 | 2005-05-18 | 罗智渊 | Composite tobacco processing method and composite additive |
| WO2014005614A1 (en) * | 2012-07-02 | 2014-01-09 | Symrise Ag | A method of flavouring a smoking product |
| CN104172464B (en) * | 2013-05-28 | 2017-10-20 | 贵州中烟工业有限责任公司 | A kind of method of nicotine content in reduction tobacco leaf |
| CN103849465B (en) * | 2014-02-27 | 2015-05-27 | 恩施市锦华生物工程有限责任公司 | Preparation method of essence for electronic cigarette with strawberry flavor |
| CN104382224A (en) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | Solid state cartridge for electronic cigarettes and preparation method thereof |
| KR20160086118A (en) * | 2015-01-09 | 2016-07-19 | 오재호 | Electronic cigarette having one button |
| CN104770863B (en) * | 2015-02-11 | 2020-05-22 | 贵州中烟工业有限责任公司 | Electronic cigarette liquid with herbal tea flavor and application thereof |
| CN105341990A (en) * | 2015-12-16 | 2016-02-24 | 浙江中烟工业有限责任公司 | Electronic cigarette tobacco juice capable of improving physiological satisfaction of electronic cigarettes |
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