CN106675806A - Laundry liquid containing kiwifruit enzyme and plant extract and preparation method of laundry liquid - Google Patents
Laundry liquid containing kiwifruit enzyme and plant extract and preparation method of laundry liquid Download PDFInfo
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- CN106675806A CN106675806A CN201610980485.4A CN201610980485A CN106675806A CN 106675806 A CN106675806 A CN 106675806A CN 201610980485 A CN201610980485 A CN 201610980485A CN 106675806 A CN106675806 A CN 106675806A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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Abstract
The invention discloses a laundry liquid containing kiwifruit enzyme and plant extract and a preparation method of the laundry liquid. The laundry liquid comprises the following components by weight: 8-12% of kiwifruit enzyme, 16-22% of plant extract, 8-10% of alkyl glycoside, 0.5-1% of disodium ethylenediamine tetraacetate, 1-1.5% of hydroxyethyl cellulose, 0.2-0.3% of spice, 2-3% of sodium chloride, 1-2% of ginger juice, 0.5-1% of artemisia vulgaris liquid and the balance of purified water, wherein the plant extract is a mixture composed of sapindus mukorossi extract and gleditsia sinensis extract at a weight ratio of (5-6):(3-5). The laundry liquid containing kiwifruit enzyme and plant extract proposed by the invention is natural and free of phosphorus, fluorescent agent and bleaching agent, and has advantages of being efficient in decontamination, natural and antibacterial, safe, environmentally friendly, promoting skin wound healing, and being mild and non-irritating to skin and the like.
Description
Technical field
The present invention relates to detergent technical field, more particularly to the liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss and plant extraction liquid
And preparation method thereof.
Background technology
For the sustainable development of the mankind, must be resource, safety, to environment in the R＆D process of detergent
Impact, washing function considers.And presently commercially available liquid detergent is formed by chemical substance mixture, alkalescence is big, right
Human body skin zest is big, be finished rear skin has burning sensation, and some chemical substances meeting Jing pores are penetrated in body, may be to people
Body organ produces very serious healthy hidden danger.Poisoning in aqueous bio body can be caused if being discharged in water after being finished, river is made
Stream fish and shrimp have death risk, water plant also can be contaminated, and destroy ecological balance, have had a strong impact on the sustainable development of society
Exhibition.Secondly as to cleaning product functional requirement more and more higher, common with the addition of various efficient chemical surfactant things
Matter, can only remove the spots such as oil stain, bad to some stain removal effects, and its anti-microbial property for being publicized all be by
Chemical antibacterial composition, it is harmful, therefore in a large number consumer urgently wants to look for the safety of a high-effective cleansing, complete function
Green wash articles for use.
The content of the invention
Based on the technical problem that background technology is present, the present invention proposes a kind of ferment containing Fructus actinidiae chinensiss with plant extraction liquid
Liquid detergent and preparation method thereof, its have high-effective cleansing, natural antibacterial, safe green environmental protection, promote skin wound healing, to skin
The advantages of skin does not gently stimulate.
The liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid, its include by weight percentage with
Lower component：Fructus actinidiae chinensiss ferment 8-12%, plant extraction liquid 16-22%, alkyl polyglucoside 8-10%, disodiumedetate 0.5-
1%th, hydroxyethyl cellulose 1-1.5%, spice 0.2-0.3%, Sodium Chloride 2-3%, Rhizoma Zingiberis Recens juice 1-2%, wormwood liquid 0.5-1%,
Remaining is purified water；The plant extraction liquid is by weight for 5-6 by soapberry extract and Fructus Gleditsia extracting solution:3-5 is constituted
Mixture.
Preferably, the ferment containing Fructus actinidiae chinensiss includes by weight percentage following components with the liquid detergent of plant extraction liquid：
Fructus actinidiae chinensiss ferment 10-11%, plant extraction liquid 18-20%, alkyl polyglucoside 8.5-9.5%, disodiumedetate 0.6-
0.8%th, hydroxyethyl cellulose 1.2-1.3%, spice 0.24-0.26%, Sodium Chloride 2.5-2.7%, Rhizoma Zingiberis Recens juice 1.2-1.8%,
Wormwood liquid 0.6-0.9%, remaining be purified water；The plant extraction liquid be by soapberry extract and Fructus Gleditsia extracting solution by weight
Than for 5.2-5.6:3.5-4.5 the mixture of composition.
Preferably, the ferment containing Fructus actinidiae chinensiss includes by weight percentage following components with the liquid detergent of plant extraction liquid：
Fructus actinidiae chinensiss ferment 10.6%, plant extraction liquid 19%, alkyl polyglucoside 9.22%, disodiumedetate 0.68%, ethoxy
Cellulose 1.25%, spice 0.25%, Sodium Chloride 2.6%, Rhizoma Zingiberis Recens juice 1.6%, wormwood liquid 0.8%, remaining be purified water；It is described
Plant extraction liquid is by weight for 5.5 by soapberry extract and Fructus Gleditsia extracting solution:The mixture of 4 compositions.
Preferably, the spice is clove oil, Herba Lysimachiae foenum-graeci quintessence oil, sweet orange oil, Oleum Pelargonii Graveolentiss, Peppermint essential oil, lemon extract
One or more in oil.
Preferably, the soapberry extract is prepared according to following technique：It is put into after peel of Fructus Sapindi Mukouossi is cleaned pure
Change in water and soak three times, collect lixiviating solution after immersion every time, merge three lixiviating solution and obtain the soapberry extract；Wherein,
In each immersion process, the weight of purified water used is 4-6 times of peel of Fructus Sapindi Mukouossi weight, and each soak time is 20-
30h。
Preferably, the Fructus Gleditsia extracting solution is prepared according to following technique：It is put into after Fructus Gleditsia is cleaned in purified water and soaks
Bubble three times, collects lixiviating solution after immersion every time, merges three lixiviating solution and obtains the Fructus Gleditsia extracting solution；Wherein, soaking every time
During, the weight of purified water used is 2-4 times of Fructus Gleditsia weight, and each soak time is 20-30h.
Preferably, the Rhizoma Zingiberis Recens juice is prepared according to following technique：Cut into slices after Rhizoma Zingiberis Recenss are cleaned, with 85-95 DEG C of hot water
Immersion 1-3min, takes out chopping, adds and is beaten after purified water immersion 4-6h, filters, and collects serosity, stands 8-12h, centrifugation point
From, supernatant is collected, add the potassium sorbate of the 0.4-0.6wt% on the basis of supernatant weight and with supernatant weight as base
The Sal of quasi- 0.5-1.5wt%, obtains the Rhizoma Zingiberis Recens juice after mix homogeneously；Wherein, the weight of purified water is the 1-2 of Rhizoma Zingiberis Recenss weight
Times.
Preferably, the wormwood liquid is prepared according to following technique：Folium Artemisiae Argyi is cleaned, is dried, crushing obtains Folium Artemisiae Argyi powder
End, adds purified water, is heated to reflux extracting 2-4h at 90-98 DEG C, and cooled and filtered is collected filtrate and obtains the wormwood liquid；
Wherein, the weight of purified water is 3-5 times of Folium Artemisiae Argyi powder weight.
Preferably, the hydroxyethyl cellulose is modified hydroxyethylcellulosadsorbing；The modified hydroxyethylcellulosadsorbing is by following
Technique is prepared：20-30 parts hydroxyethyl cellulose is added in 50-60 part ethanol by weight, nitrogen is passed through after stirring
Gas, adds 15-20 part acrylamides, 0.5-1.5 parts Ammonium persulfate. and 0.8-1.5 part potassium peroxydisulfates, stirs anti-at 52-58 DEG C
2-3h is answered, Ammonium persulfate. and potassium peroxydisulfate is then removed, 8-12 parts epoxychloropropane and 4-7 part sodium hydroxide is added, in nitrogen
Stirring reaction 5-6h under the protection of gas, wherein, reaction temperature is 62-68 DEG C, is subsequently adding and is steamed by 1-3 parts sodium borate and 6-12 parts
Mixed solution, 12-20 part dodecyl dimethyl benzyl ammonium chloride obtained in distilled water, after stirring reaction 6-7h at 72-78 DEG C,
Regulation pH value is 7-8, and sucking filtration obtains modified hydroxyethylcellulosadsorbing after being dried.
In above-mentioned technical proposal, hydroxyethyl cellulose is modified, modified hydroxyethylcellulosadsorbing remains ethoxy
The advantages of thickening property, biodegradable of cellulose itself, while also giving hydroxyethyl cellulose other performances；Modifying process
In, sodium borate crosslinks reaction with hydroxyethyl cellulose, in improve the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid
The dispersibility of each material；Acrylamide is with hydroxyethyl cellulose by etherification reaction, epoxychloropropane, dodecyl dimethyl benzyl
Ammonium chloride is connected on the side chain of hydroxyethyl cellulose with hydroxyethyl cellulose by graft reaction, not only improves ethoxy fine
The side chain lengths of dimension element, due to the effect of electrostatic repulsion, make hydroxyethyl cellulose have good extensibility, improve its rheological characteristic
Can, and dodecyl dimethyl benzyl ammonium chloride makes hydroxyethyl cellulose have good disinfection effect, with sodium borate
Coordinate, have good adsorption effect to the water soluble contaminants in water body.Modified hydroxyethyl cellulose and Rhizoma Zingiberis Recens juice, Folium Artemisiae Argyi
Liquid, Sodium Chloride, plant extraction liquid, Fructus actinidiae chinensiss ferment coordinate, and with the good compatibility, further increase liquid detergent and efficiently go
Dirty, anti-inflammation ability.
Preferably, the Fructus actinidiae chinensiss ferment is prepared according to following technique：Fructus actinidiae chinensiss are rinsed well with water, then will
It is put into be soaked in the potassium permanganate solution that mass fraction is 0.01-0.03wt% and take out after 15-25min, is rinsed well with water
Its surface moisture is drained again, is added in the fermentation tank with pure water after section, add yeast, brown sugar and ferment ten months
To the Fructus actinidiae chinensiss ferment；Wherein, first month every other day opens fermentation tank deflation, and afterwards nine months sealing and standing fermentation tanks make
Its natural fermentation.
Preferably, arginine content is 20-30mg/L in the Fructus actinidiae chinensiss ferment.
The invention allows for a kind of preparation method of the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, concrete steps
It is as follows：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water are added in plant extraction liquid, 20-45min is stirred；It is subsequently adding ethylenediamine
Tetraacethyl disodium, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice, treat that each material fully dissolves, and regulation pH value is 7-7.5, adds hydroxyl
Ethyl cellulose, after stirring 1.5-3h 20-30h is stood, and obtains the liquid detergent of the ferment containing Fructus actinidiae chinensiss and plant extraction liquid.
Preferably, it is sodium hydroxide solution to adjust pH value agents useful for same.
The present invention adopts Fructus actinidiae chinensiss ferment, and on the one hand it can decompose oils and fatss as natural biologic enzyme effective active matter
Into small-molecule substance so as to realize the purpose of deep layer cleaning, on the other hand because Fructus actinidiae chinensiss ferment contains polytype amino
Acid, wherein arginine have promotion wound healing effect, therefore addition Fructus actinidiae chinensiss ferment is carried as ferment containing Fructus actinidiae chinensiss with plant
After the composition of the liquid detergent for taking liquid, when having wound on hand when washing, it contributes to wound healing, is really achieved and does not hurt hands；Plant
, using Fructus Sapindi Mukouossi extractant and Fructus Gleditsia extractant, containing saponin, strong detergency, biological degradability is good, with life for thing extractant
Sucus Zingberis, wormwood liquid, Sodium Chloride, modified hydroxyethylcellulosadsorbing coordinate, the effect with anti-inflammation；Fructus actinidiae chinensiss ferment is carried with plant
Various stains such as agent cooperation, decomposable asymmetric choice net bloodstain are taken, light decontamination is realized, and product easily rinsing is not remained, wash time
It is short, while white fabrics can be made to keep whiteness and cleannes, colored fabric to keep the vividness of original color, wash in hard water
Best results during bafta, wash rear fabric and have soft sense, and dress is more comfortable, washes rear medicated clothing natural fragrance；Due to containing Fructus actinidiae chinensiss
Ferment is in neutrality with the liquid detergent entirety pH value of plant extraction liquid, good to human body skin affinity, non-stimulated, and is killed with natural
Bacterium composition, it is adaptable to the cleaning of infantile clothes and adult's underwear.Ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid
Natural without phosphorus, the unstressed configuration agent of liquid detergent, without bleach, with high-effective cleansing, natural antibacterial, safe green environmental protection, promote skin
Skin wound healing, the advantages of gently stimulation skin.
Description of the drawings
Fig. 1 speckles with the yarn of bloodstain in the clean effect for the ferment containing Fructus actinidiae chinensiss of embodiment 3 and the liquid detergent of plant extraction liquid
Butut.
Fig. 2 is after the ferment containing Fructus actinidiae chinensiss of embodiment 3 is cleaned with bloodstain in the clean effect of the liquid detergent of plant extraction liquid
Gauze figure.
Fig. 3 speckles with a large amount of oil stains in the clean effect for the ferment containing Fructus actinidiae chinensiss of embodiment 3 and the liquid detergent of plant extraction liquid
Gauze figure.
Fig. 4 is after the ferment containing Fructus actinidiae chinensiss of embodiment 3 is cleaned with oil stain in the clean effect of the liquid detergent of plant extraction liquid
Gauze figure.
Fig. 5 is the Bactericidal test design sketch of the ferment containing Fructus actinidiae chinensiss of embodiment 3 and the liquid detergent of plant extraction liquid.
Specific embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
The liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid, its include by weight percentage with
Lower component：Fructus actinidiae chinensiss ferment 8%, plant extraction liquid 22%, alkyl polyglucoside 8%, disodiumedetate 1%, ethoxy are fine
Dimension element 1%, spice 0.3%, Sodium Chloride 2%, Rhizoma Zingiberis Recens juice 1%, wormwood liquid 1%, remaining be purified water；The plant extraction liquid is
By weight it is 6 by soapberry extract and Fructus Gleditsia extracting solution:The mixture of 5 compositions.
The invention allows for a kind of preparation method of the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, concrete steps
It is as follows：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water are added in plant extraction liquid, 20min is stirred；It is subsequently adding ethylenediamine tetraacetic
Acetic acid disodium, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice, treat that each material fully dissolves, and it is 7 to adjust pH value, adds ethoxy fine
Dimension element, after stirring 1.5h 20h is stood, and obtains the liquid detergent of the ferment containing Fructus actinidiae chinensiss and plant extraction liquid.
Embodiment 2
The liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid, its include by weight percentage with
Lower component：Fructus actinidiae chinensiss ferment 12%, plant extraction liquid 16%, alkyl polyglucoside 10%, disodiumedetate 0.5%, hydroxyl second
Base cellulose 1.5%, spice 0.2%, Sodium Chloride 3%, Rhizoma Zingiberis Recens juice 2%, wormwood liquid 0.5%, remaining be purified water；The plant
Extracting solution is by weight for 5 by soapberry extract and Fructus Gleditsia extracting solution:The mixture of 3 compositions.
The invention allows for a kind of preparation method of the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, concrete steps
It is as follows：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water are added in plant extraction liquid, 45min is stirred；It is subsequently adding ethylenediamine tetraacetic
Acetic acid disodium, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice, treat that each material fully dissolves, and it is 7.5 to adjust pH value, adds ethoxy
Cellulose, after stirring 3h 30h is stood, and obtains the liquid detergent of the ferment containing Fructus actinidiae chinensiss and plant extraction liquid.
Embodiment 3
The liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid, its include by weight percentage with
Lower component：Fructus actinidiae chinensiss ferment 10.6%, plant extraction liquid 19%, alkyl polyglucoside 9.22%, disodiumedetate 0.68%,
Hydroxyethyl cellulose 1.25%, spice 0.25%, Sodium Chloride 2.6%, Rhizoma Zingiberis Recens juice 1.6%, wormwood liquid 0.8%, remaining be purification
Water；The plant extraction liquid is by weight for 5.5 by soapberry extract and Fructus Gleditsia extracting solution:The mixture of 4 compositions.
Wherein, the spice is 2 for clove oil, Peppermint essential oil and Fructus Citri Limoniae quintessence oil by weight:1:The mixing of 1 composition
Thing；
The Fructus actinidiae chinensiss ferment is prepared according to following technique：Fresh Fructus actinidiae chinensiss are rinsed well with water, then by it
It is put into is soaked in the potassium permanganate solution that mass fraction is 0.01wt% and take out after 20min, is rinsed well with water and drain again its table
Face moisture, adds in the fermentation tank with pure water after section, adds yeast, brown sugar fermentation and obtains within ten months the macaque
Fructus Persicae ferment；Wherein, first month every other day opens fermentation tank deflation, and afterwards nine months sealing and standing fermentation tanks make it send out naturally
Ferment.
The soapberry extract is prepared according to following technique：It is put into after peel of Fructus Sapindi Mukouossi is cleaned in purified water and soaks
Bubble three times, collects lixiviating solution after immersion every time, merges three lixiviating solution and obtains the soapberry extract；Wherein, soaking every time
During bubble, the weight of purified water used is 5 times of peel of Fructus Sapindi Mukouossi weight, and each soak time is 24h.
The Fructus Gleditsia extracting solution is prepared according to following technique：It is put into after Fructus Gleditsia is cleaned in purified water and soaks three times,
Every time lixiviating solution is collected after immersion, merge three lixiviating solution and obtain the Fructus Gleditsia extracting solution；Wherein, in each immersion process,
The weight of purified water used is 3 times of Fructus Gleditsia weight, and each soak time is 24h.
The Rhizoma Zingiberis Recens juice is prepared according to following technique：Cut into slices after Rhizoma Zingiberis Recenss are cleaned, with 90 DEG C of hot-water soak 2min, take
Go out chopping, add and be beaten after purified water immersion 5h, filter, collect serosity, stand 10h, supernatant is collected in centrifugation, then is added
Enter the potassium sorbate of the 0.5wt% on the basis of supernatant weight and the Sal of the 1wt% on the basis of supernatant weight, mix homogeneously
After obtain the Rhizoma Zingiberis Recens juice；Wherein, the weight for adding purified water is 1.5 times of Rhizoma Zingiberis Recenss weight.
The wormwood liquid is prepared according to following technique：Folium Artemisiae Argyi is cleaned, is dried, crushing obtains Folium Artemisiae Argyi powder, add
Purified water, is heated to reflux extracting 3h at 95 DEG C, and cooled and filtered is collected filtrate and obtains the wormwood liquid；Wherein, purified water
Weight is 4 times of Folium Artemisiae Argyi powder weight.
The hydroxyethyl cellulose is modified hydroxyethylcellulosadsorbing；The modified hydroxyethylcellulosadsorbing is carried out by following technique
Prepare：25 parts of hydroxyethyl celluloses are added in 55 parts of ethanol by weight, nitrogen is passed through after stirring, add 17 parts of propylene
Then amide, 1 part of Ammonium persulfate. and 1.1 parts of potassium peroxydisulfates, stirring reaction 2.5h at 55 DEG C removes Ammonium persulfate. and persulfuric acid
Potassium, adds 10 parts of epoxychloropropane and 5.5 parts of sodium hydroxide, stirring reaction 5.5h under the protection of nitrogen, wherein, reaction temperature
Spend for 64 DEG C, be subsequently adding mixed solution, 16 parts of dodecyl dimethyl benzyls by obtained in 2 parts of sodium borate and 10 parts of distilled water
Ammonium chloride, after stirring reaction 6.5h at 75 DEG C, it is 7 to adjust pH value, and sucking filtration obtains modified hydroxyethylcellulosadsorbing after being dried.
The invention allows for a kind of preparation method of the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, concrete steps
It is as follows：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water are added in plant extraction liquid, 30min is stirred；It is subsequently adding ethylenediamine tetraacetic
Acetic acid disodium, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice, treat that each material fully dissolves, and adjust pH value with sodium hydroxide solution and are
7, hydroxyethyl cellulose is added, 24h is stood after stirring 2h, obtain the liquid detergent of the ferment containing Fructus actinidiae chinensiss and plant extraction liquid.
Embodiment 4
The liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid, its include by weight percentage with
Lower component：Fructus actinidiae chinensiss ferment 9.5%, plant extraction liquid 17.8%, alkyl polyglucoside 9.2%, disodiumedetate 0.65%,
Hydroxyethyl cellulose 1.16%, spice 0.22%, Sodium Chloride 2.35%, Rhizoma Zingiberis Recens juice 1.8%, wormwood liquid 0.6%, remaining be purification
Water；The plant extraction liquid is by weight for 5.8 by soapberry extract and Fructus Gleditsia extracting solution:The mixture of 3.1 compositions.
Wherein, the spice is Fructus Citri Limoniae quintessence oil；
The Fructus actinidiae chinensiss ferment is prepared according to following technique：Fructus actinidiae chinensiss are rinsed well with water, is then put it into
Mass fraction takes out to soak in the potassium permanganate solution of 0.03wt% after 15min, is rinsed well with water and drain again its surface water
Point, add in the fermentation tank with pure water after section, add yeast, brown sugar fermentation and obtain within ten months the Fructus actinidiae chinensiss ferment
Element；Wherein, first month every other day opens fermentation tank deflation, and afterwards nine months sealing and standing fermentation tanks make its natural fermentation.
Arginine content is 30mg/L in the Fructus actinidiae chinensiss ferment；
The soapberry extract is prepared according to following technique：It is put into after peel of Fructus Sapindi Mukouossi is cleaned in purified water and soaks
Bubble three times, collects lixiviating solution after immersion every time, merges three lixiviating solution and obtains the soapberry extract；Wherein, soaking every time
During bubble, the weight of purified water used is 4 times of peel of Fructus Sapindi Mukouossi weight, and each soak time is 20h.
The Fructus Gleditsia extracting solution is prepared according to following technique：It is put into after Fructus Gleditsia is cleaned in purified water and soaks three times,
Every time lixiviating solution is collected after immersion, merge three lixiviating solution and obtain the Fructus Gleditsia extracting solution；Wherein, in each immersion process,
The weight of purified water used is 4 times of Fructus Gleditsia weight, and each soak time is 30h.
The Rhizoma Zingiberis Recens juice is prepared according to following technique：Cut into slices after Rhizoma Zingiberis Recenss are cleaned, with 90 DEG C of hot-water soak 2min, take
Go out chopping, add and be beaten after purified water immersion 4h, filter, collect serosity, stand 8h, centrifugation is collected supernatant, added
The Sal of the potassium sorbate of the 0.5wt% on the basis of supernatant weight and the 1wt% on the basis of supernatant weight, after mix homogeneously
Obtain the Rhizoma Zingiberis Recens juice；Wherein, the weight of purified water is 1 times of Rhizoma Zingiberis Recenss weight.
The wormwood liquid is prepared according to following technique：Folium Artemisiae Argyi is cleaned, is dried, crushing obtains Folium Artemisiae Argyi powder, add
Purified water, is heated to reflux extracting 4h at 95 DEG C, and cooled and filtered is collected filtrate and obtains the wormwood liquid；Wherein, purified water
Weight is 5 times of Folium Artemisiae Argyi powder weight.
The hydroxyethyl cellulose is modified hydroxyethylcellulosadsorbing；The modified hydroxyethylcellulosadsorbing is carried out by following technique
Prepare：20 parts of hydroxyethyl celluloses are added in 50 parts of ethanol by weight, nitrogen is passed through after stirring, add 15 parts of propylene
Then amide, 0.5 part of Ammonium persulfate. and 0.8 part of potassium peroxydisulfate, stirring reaction 2h at 52 DEG C removes Ammonium persulfate. and persulfuric acid
Potassium, adds 8 parts of epoxychloropropane and 4 parts of sodium hydroxide, stirring reaction 5h under the protection of nitrogen, wherein, reaction temperature is
62 DEG C, it is subsequently adding mixed solution, 12 parts of dodecyl dimethyl Benzylmagnesium chlorides by obtained in 1 part of sodium borate and 6 parts of distilled water
Ammonium, after stirring reaction 7h at 72 DEG C, it is 7.5 to adjust pH value, and sucking filtration obtains modified hydroxyethylcellulosadsorbing after being dried.
The invention allows for a kind of preparation method of the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, concrete steps
It is as follows：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water are added in plant extraction liquid, 40min is stirred；It is subsequently adding ethylenediamine tetraacetic
Acetic acid disodium, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice, treat that each material fully dissolves, and it is 7.2 to adjust pH value, adds ethoxy
Cellulose, after stirring 2.5h 28h is stood, and obtains the liquid detergent of the ferment containing Fructus actinidiae chinensiss and plant extraction liquid.
Embodiment 5
The liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss proposed by the present invention and plant extraction liquid, its include by weight percentage with
Lower component：Fructus actinidiae chinensiss ferment 11.2%, plant extraction liquid 20.4%, alkyl polyglucoside 9.6%, disodiumedetate
0.85%th, hydroxyethyl cellulose 1.36%, spice 0.27%, Sodium Chloride 2.7%, Rhizoma Zingiberis Recens juice 1.2%, wormwood liquid 0.9%, remaining
For purified water；The plant extraction liquid is by weight for 5.2 by soapberry extract and Fructus Gleditsia extracting solution:The mixing of 5 compositions
Thing.
Wherein, the spice be Herba Lysimachiae foenum-graeci quintessence oil, sweet orange oil, Oleum Pelargonii Graveolentiss, Peppermint essential oil by weight be 1.5:1:2:3
The mixture of composition；
The Fructus actinidiae chinensiss ferment is prepared according to following technique：Fresh Fructus actinidiae chinensiss are rinsed well with water, then by it
It is put into is soaked in the potassium permanganate solution that mass fraction is 0.02wt% and take out after 25min, is rinsed well with water and drain again its table
Face moisture, adds in the fermentation tank with pure water after section, adds yeast, brown sugar fermentation and obtains within ten months the macaque
Fructus Persicae ferment；Wherein, first month every other day opens fermentation tank deflation, and afterwards nine months sealing and standing fermentation tanks make it send out naturally
Ferment.
Arginine content is 20mg/L in the Fructus actinidiae chinensiss ferment；
The soapberry extract is prepared according to following technique：It is put into after peel of Fructus Sapindi Mukouossi is cleaned in purified water and soaks
Bubble three times, collects lixiviating solution after immersion every time, merges three lixiviating solution and obtains the soapberry extract；Wherein, soaking every time
During bubble, the weight of purified water used is 6 times of peel of Fructus Sapindi Mukouossi weight, and each soak time is 30h.
The Fructus Gleditsia extracting solution is prepared according to following technique：It is put into after Fructus Gleditsia is cleaned in purified water and soaks three times,
Every time lixiviating solution is collected after immersion, merge three lixiviating solution and obtain the Fructus Gleditsia extracting solution；Wherein, in each immersion process,
The weight of purified water used is 2 times of Fructus Gleditsia weight, and each soak time is 20h.
The Rhizoma Zingiberis Recens juice is prepared according to following technique：Cut into slices after Rhizoma Zingiberis Recenss are cleaned, with 90 DEG C of hot-water soak 2min, take
Go out chopping, add and be beaten after purified water immersion 6h, filter, collect serosity, stand 12h, supernatant is collected in centrifugation, then is added
Enter the potassium sorbate of the 0.5wt% on the basis of supernatant weight and the Sal of the 1wt% on the basis of supernatant weight, mix homogeneously
After obtain the Rhizoma Zingiberis Recens juice；Wherein, the weight of purified water is 2 times of Rhizoma Zingiberis Recenss weight.
The wormwood liquid is prepared according to following technique：Folium Artemisiae Argyi is cleaned, is dried, crushing obtains Folium Artemisiae Argyi powder, add
Purified water, is heated to reflux extracting 2h at 95 DEG C, and cooled and filtered is collected filtrate and obtains the wormwood liquid；Wherein, purified water
Weight is 3 times of Folium Artemisiae Argyi powder weight.
The hydroxyethyl cellulose is modified hydroxyethylcellulosadsorbing；The modified hydroxyethylcellulosadsorbing is carried out by following technique
Prepare：30 parts of hydroxyethyl celluloses are added in 60 parts of ethanol by weight, nitrogen is passed through after stirring, add 20 parts of propylene
Then amide, 1.5 parts of Ammonium persulfate .s and 1.5 parts of potassium peroxydisulfates, stirring reaction 3h at 58 DEG C removes Ammonium persulfate. and persulfuric acid
Potassium, adds 12 parts of epoxychloropropane and 7 parts of sodium hydroxide, stirring reaction 6h under the protection of nitrogen, wherein, reaction temperature is
68 DEG C, it is subsequently adding mixed solution, 20 parts of dodecyl dimethyl Benzylmagnesium chlorides by obtained in 3 parts of sodium borate and 12 parts of distilled water
Ammonium, after stirring reaction 7h at 78 DEG C, it is 8 to adjust pH value, and sucking filtration obtains modified hydroxyethylcellulosadsorbing after being dried.
The invention allows for a kind of preparation method of the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, concrete steps
It is as follows：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water are added in plant extraction liquid, 25min is stirred；It is subsequently adding ethylenediamine tetraacetic
Acetic acid disodium, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice, treat that each material fully dissolves, and it is 7.5 to adjust pH value, adds ethoxy
Cellulose, after stirring 2.4h 26h is stood, and obtains the liquid detergent of the ferment containing Fructus actinidiae chinensiss and plant extraction liquid.
Ferment containing Fructus actinidiae chinensiss obtained by the present embodiment 3 is tried with the clean effect of the liquid detergent of plant extraction liquid below
Test：
As shown in figure 1, one piece of gauze for speckling with bloodstain is taken, with the gained ferment containing Fructus actinidiae chinensiss of the embodiment of the present invention 3 and plant
The liquid detergent of extracting solution is washed, and Fig. 2 is picture after bloodstain cleaning.Take one piece of gauze for speckling with a large amount of oil stains and see Fig. 3, with this
The gained ferment containing Fructus actinidiae chinensiss of inventive embodiments 3 is washed with the liquid detergent of plant extraction liquid, and 4 is to scheme after oil stain cleaning in figure
Piece.Bloodstain, oil stain are can be seen that from Fig. 1 to Fig. 4 can be washed off, and gauze is clean as before.It is possible thereby to prove, the present invention is specially
The ferment containing Fructus actinidiae chinensiss of the gained of sharp embodiment 3 can reach high-effective cleansing effect, and the present invention with the liquid detergent of plant extraction liquid
Natural without phosphorus, the unstressed configuration agent of liquid detergent of the ferment containing Fructus actinidiae chinensiss and the plant extraction liquid that propose, without bleach, environmental protection.
Ferment containing Fructus actinidiae chinensiss obtained by the present embodiment 3 is tried with the liquid detergent antibacterial effect of plant extraction liquid below
Test：
For trying strain：The escherichia coli that Nanjing Bian Zhen bio tech ltd provides
Culture medium：Beef-protein medium
Escherichia coli are seeded in Carnis Bovis seu Bubali cream culture fluid in aseptic processing room, are cultivated one day at 37 DEG C, repeated biography and connect 2
In generation, obtain kind of a bacterium solution.
A diameter of 25mm is taken, 5min in 20min circular sterilizations filter paper immersion liquid detergent will be incubated at a temperature of 121 DEG C of Jing,
Taking-up is dried standby.
The culture medium after sterilizing is poured in sterile petri dish on superclean bench, after solidification to be cooled, uses aseptic shifting
Liquid pipe is drawn 0.1mL kind bacterium solutions and is added on culture dish, is smoothened bacterium solution with spreading rod, then grips immersion treatment mistake with aseptic nipper
Filter paper be attached to surface containing bacterium culture medium, cultivate 24h at being placed in 37 DEG C, observation whether there is the formation of inhibition zone and inhibition zone
Size.As a result show there is the formation of inhibition zone in Fig. 5, illustrate that this sample has biocidal property to escherichia coli, its inhibition zone
Diameter is 36mm.It is possible thereby to prove, the liquid detergent of the gained of patent Example of the present invention 3 has the performance of natural antibacterial.
The Fructus actinidiae chinensiss ferment arginine content used by the implementation case 3 is detected below, it is as a result as follows：
Arginic content in Fructus actinidiae chinensiss ferment is detected using L-8900 type automatic amino acid analyzers, chromatograph inspection
Survey condition is：4.6mm × 60mm ion-exchange chromatographies；Flow velocity：The flow velocity of a number pump be 0.40mL/min, the flow velocity of No. two pumps
For 0.35mL/min；Detection wavelength：570nm；Column temperature：135℃；Sampling volume：20μL.It is with arginine standard sample preparation one
The titer of row variable concentrations, filter pressing examination with computer, obtains standard curve.5mL testing samples are taken, addition 15mL concentration is
The HCl solution of 6mol/L, hydrolyzes 22h in 110 DEG C of calorstats, and then whole hydrolyzed solutions are transferred in 50mL volumetric flasks, uses
One-level water constant volume, takes after the above-mentioned solution decompressions of 1mL are evaporated, and with the HCl solution dissolving that 2mL concentration is 0.02mol/L, crosses water system filter
Film loads upper engine room test, finally calculates arginine content 26mg/L in Fructus actinidiae chinensiss ferment.Promote wound because arginine has
Mouth Healing, therefore after Fructus actinidiae chinensiss ferment is as liquid detergent main component, when having wound on hand when washing, it contributes to wound
Mouth healing.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto,
Any those familiar with the art the invention discloses technical scope in, technology according to the present invention scheme and its
Inventive concept equivalent or change in addition, all should be included within the scope of the present invention.
Claims (10)
1. the liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss and plant extraction liquid, it is characterised in that it includes by weight percentage following
Component：Fructus actinidiae chinensiss ferment 8-12%, plant extraction liquid 16-22%, alkyl polyglucoside 8-10%, disodiumedetate 0.5-
1%th, hydroxyethyl cellulose 1-1.5%, spice 0.2-0.3%, Sodium Chloride 2-3%, Rhizoma Zingiberis Recens juice 1-2%, wormwood liquid 0.5-1%,
Remaining is purified water；The plant extraction liquid is by weight for 5-6 by soapberry extract and Fructus Gleditsia extracting solution:3-5 is constituted
Mixture.
2. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the spice is
One or more in clove oil, Herba Lysimachiae foenum-graeci quintessence oil, sweet orange oil, Oleum Pelargonii Graveolentiss, Peppermint essential oil, Fructus Citri Limoniae quintessence oil.
3. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the Fructus Sapindi Mukouossi
Extracting solution is prepared according to following technique：It is put into after peel of Fructus Sapindi Mukouossi is cleaned in purified water and soaks three times, every time after immersion
Lixiviating solution is collected, is merged three lixiviating solution and is obtained the soapberry extract；Wherein, in each immersion process, purification used
The weight of water is 4-6 times of peel of Fructus Sapindi Mukouossi weight, and each soak time is 20-30h.
4. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the Fructus Gleditsia is carried
Take liquid to be prepared according to following technique：It is put into after Fructus Gleditsia is cleaned in purified water and soaks three times, collects extraction after immersion every time
Liquid, merges three lixiviating solution and obtains the Fructus Gleditsia extracting solution；Wherein, in each immersion process, the weight of purified water used is
2-4 times of Fructus Gleditsia weight, each soak time is 20-30h.
5. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the Rhizoma Zingiberis Recens juice
It is prepared according to following technique：Cut into slices after Rhizoma Zingiberis Recenss are cleaned, with 85-95 DEG C of hot-water soak 1-3min, take out chopping, add pure
Change and be beaten after water immersion 4-6h, filter, collect serosity, stand 8-12h, centrifugation is collected supernatant, added with supernatant
The Sal of the potassium sorbate of 0.4-0.6wt% and the 0.5-1.5wt% on the basis of supernatant weight, mix homogeneously on the basis of weight
After obtain the Rhizoma Zingiberis Recens juice；Wherein, the weight of purified water is 1-2 times of Rhizoma Zingiberis Recenss weight.
6. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the wormwood liquid
It is prepared according to following technique：Folium Artemisiae Argyi is cleaned, is dried, crushing obtains Folium Artemisiae Argyi powder, purified water is added, at 90-98 DEG C
It is heated to reflux extracting 2-4h, cooled and filtered is collected filtrate and obtains the wormwood liquid；Wherein, the weight of purified water is Folium Artemisiae Argyi powder
3-5 times of last weight.
7. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the ethoxy
Cellulose is modified hydroxyethylcellulosadsorbing；The modified hydroxyethylcellulosadsorbing is prepared by following technique：By weight by 20-
30 parts of hydroxyethyl celluloses are added in 50-60 part ethanol, and nitrogen is passed through after stirring, and add 15-20 part acrylamides, 0.5-
Then 1.5 parts of Ammonium persulfate .s and 0.8-1.5 part potassium peroxydisulfates, stirring reaction 2-3h at 52-58 DEG C removes Ammonium persulfate. and mistake
Potassium sulfate, adds 8-12 parts epoxychloropropane and 4-7 part sodium hydroxide, stirring reaction 5-6h under the protection of nitrogen, wherein,
Reaction temperature is 62-68 DEG C, is subsequently adding mixed solution, 12-20 part ten by obtained in 1-3 parts sodium borate and 6-12 part distilled water
Dialkyl dimethyl benzyl ammonium chloride, after stirring reaction 6-7h at 72-78 DEG C, regulation pH value is 7-8, and sucking filtration is obtained after being dried
To modified hydroxyethylcellulosadsorbing.
8. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 1, it is characterised in that the Fructus actinidiae chinensiss
Ferment is prepared according to following technique：Fructus actinidiae chinensiss are rinsed well with water, mass fraction is then put it into for 0.01-
Soak in the potassium permanganate solution of 0.03wt% after 15-25min and take out, rinsed well with water and drain again its surface moisture, cut into slices
Add in the fermentation tank with pure water afterwards, add yeast, brown sugar fermentation and obtain within ten months the Fructus actinidiae chinensiss ferment；Its
In, first month every other day opens fermentation tank deflation, and afterwards nine months sealing and standing fermentation tanks make its natural fermentation.
9. the liquid detergent of ferment containing Fructus actinidiae chinensiss and plant extraction liquid according to claim 8, it is characterised in that the Fructus actinidiae chinensiss
Arginic content is 20-30mg/L in ferment.
10. the preparation side of the liquid detergent of a kind of ferment containing Fructus actinidiae chinensiss as any one of claim 1-9 and plant extraction liquid
Method, it is characterised in that comprise the following steps that：Alkyl polyglucoside, Fructus actinidiae chinensiss ferment, purified water, stirring are added in plant extraction liquid
20-45min；Disodiumedetate, Rhizoma Zingiberis Recens juice, wormwood liquid, Sodium Chloride, spice are subsequently adding, treat that each material fully dissolves,
Regulation pH value is 7-7.5, adds hydroxyethyl cellulose, and after stirring 1.5-3h 20-30h is stood, and obtains the ferment containing Fructus actinidiae chinensiss
With the liquid detergent of plant extraction liquid.
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